CN108434017A - A kind of tooth whitening liquid and preparation method thereof - Google Patents
A kind of tooth whitening liquid and preparation method thereof Download PDFInfo
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- CN108434017A CN108434017A CN201810604429.XA CN201810604429A CN108434017A CN 108434017 A CN108434017 A CN 108434017A CN 201810604429 A CN201810604429 A CN 201810604429A CN 108434017 A CN108434017 A CN 108434017A
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- tooth whitening
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- whitening liquid
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- oligosaccharide
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
Abstract
The invention discloses a kind of tooth whitening liquid and preparation method thereof, belong to field of oral care.The tooth whitening liquid, including following raw material：Sodium benzoate, phytic acid, glycerine, tween, surfactant, chondroitin sulfate, ellagic acid, xylo-oligosaccharide, water；The tooth whitening liquid is obtained by ultrasonic, mixing.The present invention is reinforcement system by using chondroitin sulfate, ellagic acid, xylo-oligosaccharide, improves the whitening effect of tooth whitening liquid.
Description
Technical field
The invention belongs to field of oral care, and in particular to a kind of tooth whitening liquid and preparation method thereof.
Background technology
With making constant progress for human society, people increasingly focus on personal image, and the whitening of tooth is also increasingly
It attracts attention, personal image can not only be improved by possessing the pure white tooth of a bite, moreover it is possible to greatly improve individual in social interaction
Self-confidence, however inevitably, cigarette stain, tea stain, coffee stain, betel nut stain can make dental surface jaundice or blackening, then various
The method of tooth-whitening is just come into being.Currently, there are three types of the pollution layer that method is used for removing dental surface, make tooth whitening：
First method, need to dentist, odontologist clinic it is one or many go to a doctor, and allow doctor with professional method clean tooth
Tooth, curative effect is than more significant, however, this kind of method needs are one or many medical to dentist's office, going to a doctor need not arrange every time
It is also required to expend the time of half an hour a to hour in the case of team, and a considerable expense need to be paid.
Second method, using house whitening set group, this suit is that the carboxylic acid amides peroxide of dependence percentage floats
White agent, is placed in mouth guard.Bleachability solution is likely to stimulation gum and generates side effect, is contacted for a long time with tooth, tooth meeting
Become easier to allergy.
The third method with the increase of use time, makes teeth whiter at leisure using whitening toothpaste.Expense is low, but
Effect is bad.All toothpaste all can pass through the pollutant of the effect removal dental surface of mild corrosive agent and rubbing agent.But it should
Kind method needs adhere to using sooner or later daily within the quite a long time, and effect is nor highly desirable.
A kind of Chinese patent literature " teeth whitening and preparation method thereof (patent No.：CN101040828B one) " is disclosed
0.01-0.1% sodium benzoates are added in clean container kind teeth whitening and preparation method thereof, and addition purifies water-soluble on a small quantity
Solution is complete, phytic acid 20-50%, glycerine 20-60%, tween 0.1-1.0% mixings is then added, then purified water is added to be settled to
Preparation is made in 100ml.The invention teeth whitening, product have no toxic side effect, to the cigarette stain of dental surface, tea stain, coffee stain,
The elimination effect of betel nut stain is good, and speed is fast, but not sufficiently effective problem.
Invention content
The object of the present invention is to provide a kind of tooth whitening liquid and preparation method thereof, to solve in a kind of patent document " tooth
The tooth whitening agent and preparation method thereof (patent No.：CN101040828B a kind of teeth whitening disclosed in) " and preparation method thereof
On the basis of, how to optimize component, dosage, method etc., improves the not sufficiently effective problem of tooth whitening liquid.
In order to solve the above technical problems, the present invention uses following technical scheme：
A kind of tooth whitening liquid, including following raw material：Sodium benzoate, phytic acid, glycerine, tween, surfactant, sulfuric acid are soft
Ossein, ellagic acid, xylo-oligosaccharide, water；
The chondroitin sulfate, ellagic acid, xylo-oligosaccharide weight ratio be (1-3)：(2-6)：(2-4).
Further, the chondroitin sulfate, ellagic acid, xylo-oligosaccharide weight ratio be 2:4:3.
Further, the tooth whitening liquid is as unit of parts by weight, including following raw material：Sodium benzoate 0.05-0.1
Part, 20-50 parts of phytic acid, 20-60 parts of glycerine, 0.5-1 parts of tween, 0.5-1 parts of surfactant, 1-3 parts of chondroitin sulfate, tan flower
It is 2-6 parts sour, 2-4 parts of xylo-oligosaccharide, 20-50 parts of water.
Further, the surfactant is selected from nonylphenol polyoxyethylene ether, N- acylsarcosines, isethionic acid ester sodium salt
At least one of.
Further, the surfactant is mass ratio 1:1 nonylphenol polyoxyethylene ether, isethionic acid ester sodium salt
Mixed solution.
Further, a concentration of 50%-70% of the phytic acid.
Further, the tooth whitening liquid is administered to dental surface by way of spraying or being coated with.
A kind of preparation method of above-mentioned tooth whitening liquid, includes the following steps：
(1) sodium benzoate will be added in clean container, a small amount of purifying water dissolution of addition is complete, and phytic acid is then added, sweet
Oil, tween, chondroitin sulfate, ellagic acid, xylo-oligosaccharide, water mixing fully dissolve；
(2) ultrasonic disperse 10-20min, power 250W, it is filling.
The invention has the advantages that：
(1) by the data of embodiment 1-3 and comparative example 5 as it can be seen that the whitening effect of tooth whitening liquid made from embodiment 1-3
It is significantly higher than the whitening effect of tooth whitening liquid made from comparative example 5；Simultaneously by the data of embodiment 1-3 as it can be seen that embodiment 1 is
Optimum embodiment.
(2) by embodiment 1 and the data of comparative example 1-4 as it can be seen that chondroitin sulfate, ellagic acid, xylo-oligosaccharide are preparing tooth
Synergistic effect is played in tooth whitening lotion, collaboration improves the whitening effect of tooth whitening liquid；This is：
The present invention forms teeth whitening by the raw materials such as phytic acid and surfactant, plays increase-volume, dissolving altogether, disperses and kill
The effect of bacterium anti-inflammatory, surfactant is with the multiple functions such as blistering, absorption, dissolving, dispersion, neutralization and bactericidal antiphlogistic, tooth
The spot on surface is dissolved dispersion under the assistance of surfactant, enhances the effect of teeth whitening, at the same can also bactericidal antiphlogistic,
It protects the health of one's mouth.Product has no toxic side effect, good to the elimination effect of the cigarette stain of dental surface, tea stain, coffee stain, betel nut stain,
Speed is fast, simple for process, easily operated, is suitable for industrial production.
Chondroitin sulfate is acid mucopolysaccharides, and polyanion has stronger affinity to gum epidermis, can
Whitening lotion is protected not cause to damage to it, while its gelling characteristics can be used as conveyance conduit in dental surface, promote tan flower
Sour isoreactivity substance reaches teeth crevice higher depth, promotes whitening effect；Ellagic acid is a kind of polyphenol dilactone, is gallic acid
Dimerization derivative, have bioactivity, the alkaline matters such as dental surface cigarette stain can be dissolved, while it can assist phytic acid to press down
Whitening effect is strengthened in the generation of pigment processed, has strong scavenging effect to oxygen radical, improves oral environment；Xylo-oligosaccharide is again
Claim wood oligose, be the functional polymerization sugar being combined into β-Isosorbide-5-Nitrae glycosidic bond by 2-7 xylose molecule, has steady well
It is qualitative, it can keep not decomposing for a long time in saliva of buccal cavity, and the hydroxyl on its molecular structure is by Hydrogenbond ellagic acid,
It reduces it to be dissolved into saliva, increases it in the residence time of dental surface, promote whitening effect.
(3) by the data of comparative example 6-8 as it can be seen that chondroitin sulfate, ellagic acid, xylo-oligosaccharide weight ratio not at (1-3)：
(2-6)：When in (2-4) range, the whitening effect numerical value and the numerical value of embodiment 1-3 of tooth whitening liquid obtained are very different,
It is suitable with the numerical value of the prior art (comparative example 5) much smaller than the numerical value of embodiment 1-3.Chondroitin sulfate of the present invention, ellagic acid,
Xylo-oligosaccharide as reinforcement system, when embodiment 1-3 controls prepare tooth whitening liquid by add chondroitin sulfate, ellagic acid,
The weight ratio of xylo-oligosaccharide is (1-3)：(2-6)：(2-4) realizes that in reinforcement system include gum using chondroitin sulfate, promotees
Reach teeth crevice higher depth into ellagic acid isoreactivity substance；Ellagic acid assists the generation of phytic acid inhibition pigment, to oxygen radical
With strong scavenging effect；Xylo-oligosaccharide stablizes ellagic acid, increases its residence time in dental surface；So that chondroitin sulfate,
The reinforcement system that ellagic acid, xylo-oligosaccharide are constituted improves the whitening effect of tooth whitening liquid in the tooth whitening liquid of the present invention.
Specific implementation mode
For ease of more fully understanding the present invention, it is illustrated by the following examples, these examples belong to the protection of the present invention
Range, but do not limit the scope of the invention.
Tooth whitening liquid is as unit of parts by weight, including following raw material：0.05-0.1 parts of sodium benzoate, 20-50 parts of phytic acid,
20-60 parts of glycerine, 0.5-1 parts of tween, 0.5-1 parts of surfactant, 1-3 parts of chondroitin sulfate, 2-6 parts of ellagic acid, oligomeric wood
It is 2-4 parts sugared, 20-50 parts of water.Tooth whitening liquid is administered to dental surface by way of spraying or being coated with.
The surfactant in nonylphenol polyoxyethylene ether, N- acylsarcosines, isethionic acid ester sodium salt at least
It is a kind of.
The surfactant is mass ratio 1:1 nonylphenol polyoxyethylene ether, the mixed solution of isethionic acid ester sodium salt.
A concentration of 50%-70% of the phytic acid.
A kind of preparation method of above-mentioned tooth whitening liquid, includes the following steps：
(1) sodium benzoate will be added in clean container, a small amount of purifying water dissolution of addition is complete, and phytic acid is then added, sweet
Oil, tween, chondroitin sulfate, ellagic acid, xylo-oligosaccharide, water mixing fully dissolve；
(2) ultrasonic disperse 10-20min, power 250W, it is filling.
Embodiment 1
Tooth whitening liquid is as unit of parts by weight, including following raw material：0.075 part of sodium benzoate, 35 parts of phytic acid, glycerine 40
Part, 0.75 part of tween, 0.75 part of surfactant, 2 parts of chondroitin sulfate, 4 parts of ellagic acid, 3 parts of xylo-oligosaccharide, 35 parts of water.Tooth
Tooth whitening lotion is administered to dental surface by way of spraying or being coated with.
The surfactant is mass ratio 1:1 nonylphenol polyoxyethylene ether, the mixed solution of isethionic acid ester sodium salt.
A concentration of the 60% of the phytic acid.
A kind of preparation method of above-mentioned tooth whitening liquid, includes the following steps：
(1) sodium benzoate will be added in clean container, a small amount of purifying water dissolution of addition is complete, and phytic acid is then added, sweet
Oil, tween, chondroitin sulfate, ellagic acid, xylo-oligosaccharide, water mixing fully dissolve；
(2) ultrasonic disperse 15min, power 250W, it is filling.
Embodiment 2
Tooth whitening liquid is as unit of parts by weight, including following raw material：0.05 part of sodium benzoate, 50 parts of phytic acid, glycerine 20
Part, 1 part of tween, 0.5 part of surfactant, 3 parts of chondroitin sulfate, 2 parts of ellagic acid, 4 parts of xylo-oligosaccharide, 20 parts of water.Tooth is beautiful
White liquor is administered to dental surface by way of spraying or being coated with.
The surfactant is mass ratio 1:1 nonylphenol polyoxyethylene ether, the mixed solution of isethionic acid ester sodium salt.
A concentration of the 50% of the phytic acid.
A kind of preparation method of above-mentioned tooth whitening liquid, includes the following steps：
(1) sodium benzoate will be added in clean container, a small amount of purifying water dissolution of addition is complete, and phytic acid is then added, sweet
Oil, tween, chondroitin sulfate, ellagic acid, xylo-oligosaccharide, water mixing fully dissolve；
(2) ultrasonic disperse 20min, power 250W, it is filling.
Embodiment 3
Tooth whitening liquid is as unit of parts by weight, including following raw material：0.1 part of sodium benzoate, 20 parts of phytic acid, glycerine 60
Part, 0.5 part of tween, 1 part of surfactant, 1 part of chondroitin sulfate, 6 parts of ellagic acid, 2 parts of xylo-oligosaccharide, 50 parts of water.Tooth is beautiful
White liquor is administered to dental surface by way of spraying or being coated with.
The surfactant is mass ratio 1:1 nonylphenol polyoxyethylene ether, the mixed solution of isethionic acid ester sodium salt.
A concentration of the 70% of the phytic acid.
A kind of preparation method of above-mentioned tooth whitening liquid, includes the following steps：
(1) sodium benzoate will be added in clean container, a small amount of purifying water dissolution of addition is complete, and phytic acid is then added, sweet
Oil, tween, chondroitin sulfate, ellagic acid, xylo-oligosaccharide, water mixing fully dissolve；
(2) ultrasonic disperse 10min, power 250W, it is filling.
Comparative example 1
It is essentially identical with the preparation process of embodiment 1, have only unlike prepare in the raw material of tooth whitening liquid and lack sulphur
Aching and limp ossein, ellagic acid, xylo-oligosaccharide.
Comparative example 2
It is essentially identical with the preparation process of embodiment 1, have only unlike prepare in the raw material of tooth whitening liquid and lack sulphur
Aching and limp ossein.
Comparative example 3
It is essentially identical with the preparation process of embodiment 1, have only unlike prepare in the raw material of tooth whitening liquid and lack tan
Spend acid.
Comparative example 4
It is essentially identical with the preparation process of embodiment 1, have only unlike prepare lack in the raw material of tooth whitening liquid it is low
Xylan.
Comparative example 5
Using a kind of Chinese patent literature " teeth whitening and preparation method thereof (patent No.：CN101040828B tool in) "
Body method described in embodiment 1 prepares a kind of teeth whitening and preparation method thereof.
Comparative example 6
It is essentially identical with the preparation process of embodiment 1, have only unlike to prepare sulfuric acid in the raw material of tooth whitening liquid soft
Ossein is 5 parts, ellagic acid is 1 part, xylo-oligosaccharide is 1 part.
Comparative example 7
It is essentially identical with the preparation process of embodiment 1, have only unlike to prepare sulfuric acid in the raw material of tooth whitening liquid soft
Ossein is 0.5 part, ellagic acid is 8 parts, xylo-oligosaccharide is 6 parts.
Comparative example 8
It is essentially identical with the preparation process of embodiment 1, have only unlike to prepare sulfuric acid in the raw material of tooth whitening liquid soft
Ossein is 5 parts, ellagic acid is 9 parts, xylo-oligosaccharide is 1 part.
Using effect evaluation is carried out to product made from embodiment 1-3 and comparative example 1-8.Choosing has cigarette stain tooth patient totally 110
Example, is divided into 10 groups of personnel, this 10 groups of personnel use product 14 days made from embodiment 1-3 and comparative example 1-8 respectively, sooner or later daily
Each 1 time, observation indicate that, it is divided into 5 grades and is evaluated, 5 is significantly improves, and 3 is have certain improvement, and 1 is no improvement, meter
Calculate average value.
| Experimental project | Whitening effect is evaluated |
| Embodiment 1 | 4.0 |
| Embodiment 2 | 3.9 |
| Embodiment 3 | 3.8 |
| Comparative example 1 | 2.8 |
| Comparative example 2 | 3.7 |
| Comparative example 3 | 3.6 |
| Comparative example 4 | 3.7 |
| Comparative example 5 | 3.0 |
| Comparative example 6 | 3.2 |
| Comparative example 7 | 3.3 |
| Comparative example 8 | 3.2 |
As seen from the above table：(1) by the data of embodiment 1-3 and comparative example 5 as it can be seen that tooth whitening made from embodiment 1-3
The whitening effect of liquid is significantly higher than the whitening effect of tooth whitening liquid made from comparative example 5；It simultaneously can by the data of embodiment 1-3
See, embodiment 1 is optimum embodiment.
(2) by embodiment 1 and the data of comparative example 1-4 as it can be seen that chondroitin sulfate, ellagic acid, xylo-oligosaccharide are preparing tooth
Synergistic effect is played in tooth whitening lotion, collaboration improves the whitening effect of tooth whitening liquid；This is：
The present invention forms teeth whitening by the raw materials such as phytic acid and surfactant, plays increase-volume, dissolving altogether, disperses and kill
The effect of bacterium anti-inflammatory, surfactant is with the multiple functions such as blistering, absorption, dissolving, dispersion, neutralization and bactericidal antiphlogistic, tooth
The spot on surface is dissolved dispersion under the assistance of surfactant, enhances the effect of teeth whitening, at the same can also bactericidal antiphlogistic,
It protects the health of one's mouth.Product has no toxic side effect, good to the elimination effect of the cigarette stain of dental surface, tea stain, coffee stain, betel nut stain,
Speed is fast, simple for process, easily operated, is suitable for industrial production.
Chondroitin sulfate is acid mucopolysaccharides, and polyanion has stronger affinity to gum epidermis, can
Whitening lotion is protected not cause to damage to it, while its gelling characteristics can be used as conveyance conduit in dental surface, promote tan flower
Sour isoreactivity substance reaches teeth crevice higher depth, promotes whitening effect；Ellagic acid is a kind of polyphenol dilactone, is gallic acid
Dimerization derivative, have bioactivity, the alkaline matters such as dental surface cigarette stain can be dissolved, while it can assist phytic acid to press down
Whitening effect is strengthened in the generation of pigment processed, has strong scavenging effect to oxygen radical, improves oral environment；Xylo-oligosaccharide is again
Claim wood oligose, be the functional polymerization sugar being combined into β-Isosorbide-5-Nitrae glycosidic bond by 2-7 xylose molecule, has steady well
It is qualitative, it can keep not decomposing for a long time in saliva of buccal cavity, and the hydroxyl on its molecular structure is by Hydrogenbond ellagic acid,
It reduces it to be dissolved into saliva, increases it in the residence time of dental surface, promote whitening effect.
(3) by the data of comparative example 6-8 as it can be seen that chondroitin sulfate, ellagic acid, xylo-oligosaccharide weight ratio not at (1-3)：
(2-6)：When in (2-4) range, the whitening effect numerical value and the numerical value of embodiment 1-3 of tooth whitening liquid obtained are very different,
It is suitable with the numerical value of the prior art (comparative example 5) much smaller than the numerical value of embodiment 1-3.Chondroitin sulfate of the present invention, ellagic acid,
Xylo-oligosaccharide as reinforcement system, when embodiment 1-3 controls prepare tooth whitening liquid by add chondroitin sulfate, ellagic acid,
The weight ratio of xylo-oligosaccharide is (1-3)：(2-6)：(2-4) realizes that in reinforcement system include gum using chondroitin sulfate, promotees
Reach teeth crevice higher depth into ellagic acid isoreactivity substance；Ellagic acid assists the generation of phytic acid inhibition pigment, to oxygen radical
With strong scavenging effect；Xylo-oligosaccharide stablizes ellagic acid, increases its residence time in dental surface；So that chondroitin sulfate,
The reinforcement system that ellagic acid, xylo-oligosaccharide are constituted improves the whitening effect of tooth whitening liquid in the tooth whitening liquid of the present invention.
The above content is it cannot be assumed that present invention specific implementation is confined to these explanations, for the technical field of the invention
Those of ordinary skill for, under the premise of not departing from present inventive concept, a number of simple deductions or replacements can also be made, all answers
When being considered as belonging to present invention scope of patent protection determined by the appended claims.
Claims (8)
1. a kind of tooth whitening liquid, which is characterized in that including following raw material：Sodium benzoate, phytic acid, glycerine, tween, surface-active
Agent, chondroitin sulfate, ellagic acid, xylo-oligosaccharide, water；
The chondroitin sulfate, ellagic acid, xylo-oligosaccharide weight ratio be (1-3)：(2-6)：(2-4).
2. tooth whitening liquid according to claim 1, which is characterized in that the chondroitin sulfate, ellagic acid, xylo-oligosaccharide
Weight ratio be 2:4:3.
3. tooth whitening liquid according to claim 1, which is characterized in that the tooth whitening liquid as unit of parts by weight,
Including following raw material：0.05-0.1 parts of sodium benzoate, 20-50 parts of phytic acid, 20-60 parts of glycerine, 0.5-1 parts of tween, surface-active
0.5-1 parts of agent, 1-3 parts of chondroitin sulfate, 2-6 parts of ellagic acid, 2-4 parts of xylo-oligosaccharide, 20-50 parts of water.
4. tooth whitening liquid according to claim 1, which is characterized in that the surfactant is selected from polyoxyethylene nonyl phenyl second
At least one of alkene ether, N- acylsarcosines, isethionic acid ester sodium salt.
5. tooth whitening liquid according to claim 4, which is characterized in that the surfactant is mass ratio 1:1 nonyl
The mixed solution of base phenol polyethenoxy ether, isethionic acid ester sodium salt.
6. tooth whitening liquid according to claim 1, which is characterized in that a concentration of 50%-70% of the phytic acid.
7. tooth whitening liquid according to claim 1, which is characterized in that the tooth whitening liquid is by spraying or being coated with
Mode is administered to dental surface.
8. a kind of preparation method according to claim 1-7 any one of them tooth whitening liquid, which is characterized in that including following
Step：
(1) sodium benzoate will be added in clean container, a small amount of purifying water dissolution of addition is complete, phytic acid is then added, glycerine is spat
Temperature, chondroitin sulfate, ellagic acid, xylo-oligosaccharide, water mixing fully dissolve；
(2) ultrasonic disperse 10-20min, power 250W, it is filling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810604429.XA CN108434017A (en) | 2018-06-13 | 2018-06-13 | A kind of tooth whitening liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810604429.XA CN108434017A (en) | 2018-06-13 | 2018-06-13 | A kind of tooth whitening liquid and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108434017A true CN108434017A (en) | 2018-08-24 |
Family
ID=63206297
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810604429.XA Withdrawn CN108434017A (en) | 2018-06-13 | 2018-06-13 | A kind of tooth whitening liquid and preparation method thereof |
Country Status (1)
| Country | Link |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1630521A (en) * | 2001-11-06 | 2005-06-22 | 奎格利公司 | Oral compositions and methods for prevention, reduction and treatment of radiation injury |
| CN1736388A (en) * | 2001-02-28 | 2006-02-22 | 江崎格力高株式会社 | Compositions having anti-dental caries function |
| JP2009046449A (en) * | 2007-08-22 | 2009-03-05 | Lion Corp | Liquid composition for oral cavity |
| CN101040828B (en) * | 2007-04-28 | 2010-05-19 | 长春迈灵生物工程有限公司 | Tooth whitening agent and the method for preparing the same |
-
2018
- 2018-06-13 CN CN201810604429.XA patent/CN108434017A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1736388A (en) * | 2001-02-28 | 2006-02-22 | 江崎格力高株式会社 | Compositions having anti-dental caries function |
| CN1630521A (en) * | 2001-11-06 | 2005-06-22 | 奎格利公司 | Oral compositions and methods for prevention, reduction and treatment of radiation injury |
| CN101040828B (en) * | 2007-04-28 | 2010-05-19 | 长春迈灵生物工程有限公司 | Tooth whitening agent and the method for preparing the same |
| JP2009046449A (en) * | 2007-08-22 | 2009-03-05 | Lion Corp | Liquid composition for oral cavity |
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Application publication date: 20180824 |