CN1861039A - Chewing bubble-producing type solid tooth-paste - Google Patents

Chewing bubble-producing type solid tooth-paste Download PDF

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Publication number
CN1861039A
CN1861039A CN 200610046311 CN200610046311A CN1861039A CN 1861039 A CN1861039 A CN 1861039A CN 200610046311 CN200610046311 CN 200610046311 CN 200610046311 A CN200610046311 A CN 200610046311A CN 1861039 A CN1861039 A CN 1861039A
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paste
solid tooth
type solid
tooth
producing type
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张少辉
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Abstract

A solid tooth-paste able to generate foams by chewing it for cleaning teeth without brushing is proportionally prepared from the foaming agent containing acidic substance chosen from citric acid, tartaric acid and malic acid and alkaline substance chosen from sodium bicarbonate, the cleaning agent chosen from sodium (potassium) laurylsulfonate, polyoxamer 407, steareth 30 and polysorbate 20, the rubbing agent chosen from calcium carbonate, calcium phosphate, SiO2, aluminum hydroxide and bentonite, and the filler chosen from xylitol, mannitol and lactose.

Description

Chewing bubble-producing type solid tooth-paste
(1) technical field
The present invention relates to a kind of toothpaste, specifically relate to a kind ofly clean one's teeth effectively, and the oral cavity chewing bubble-producing type solid tooth-paste of prevention oral disease function is arranged.
(2) background technology
Cleaning of teeth and oral health care are promoted healthy significant for the prevention oral disease.Brushing teeth and can remove food debris storage, reduce oral cavity bacterium and grow breeding, reduce in the oral cavity paathogenic factor and enhancing and organize resistance against diseases, is to keep oral cavity, cleaning of teeth in the daily life, takes care of one's teeth and the effective measures of periodontal tissue.Toothpaste is semi-liquid-like now, and solid powdery dentifrice is also arranged.Present toothpaste, when brushing teeth, dentifrice to use toothbrush.But faulty toothbrushing can produce odontopathy, as gingival atrophy, root of the tooth exposure, neck portion wedge shaped defect etc., and special population, the crowd who is not easy to brush teeth with toothbrush as child, patient, traveller, special environment personnel etc. usually is difficult to realize the purpose that cleans the teeth.In addition, the action of brushing teeth itself is loaded down with trivial details, causes a kind of burden sensation to life.
Chew gum and to play the effect in cleaning teeth and oral cavity to a certain extent.Its cleaning action mainly by the adhesive attraction of rubber, has certain cleaning action to the tooth projection, and recesses such as teeth space is not reached cleaning effect, uses oral cavity, back clean feel relatively poor, and importantly depleted colloid has tangible pollution to environment.
The collutory that can see on the market, oral cavity are mainly used in sterilization, taste removal, antiinflammatory and fresh breath with spray.Its kind is a lot, but most consumers is just liked using it to keep breath freshening.Main outstanding is medicinal function, and with after easily obey in the body, unavoidably produce some side effect.The function of its cleaning teeth relatively a little less than.
(3) summary of the invention
The objective of the invention is provides a kind of prevention oral disease that has at the problems referred to above, and it is effective to clean one's teeth, easy to use, helps the solid tooth-paste of the chewing bubble-producing type of environmental conservation.
The technical scheme that adopts is in order to achieve the above object:
Chewing bubble-producing type solid tooth-paste is the solid sheet type structure, mainly is formulated by foaming agent 25-80%, abrasivus 1-25%, cleaning agent 0.01-20%, filler 1-30%.Above-mentioned percentage ratio is weight percentage.Above-mentioned foaming agent is made up of acidic materials 10-40% and alkaline matter 10-40%.
Acid is got at least a in citric acid, tartaric acid, the malic acid, accounts for 10-40%.
The preferred sodium bicarbonate of basic species accounts for 10-40%.
Dodecyl sodium sulfate (potassium), Poltyo * amer407 are chosen in above-mentioned cleaning agent, stearetn30, at least a in the polysorbate 20.
At least a in the preferred calcium carbonate of above-mentioned abrasivus, calcium phosphate, silicon dioxide, aluminium hydroxide, the Bentonite.
At least a in the preferred xylitol of above-mentioned filler, mannitol, the lactose.
Chewing bubble-producing type solid tooth-paste of the present invention can add (pressing down) microbial inoculum 0.01-10%, desensitizer 0.01-5%, brightening agent 0.1-20%, caries preventive agent 0.01-2% and anti-tartar (stone) agent 0.1-8% extremely according to actual needs.
Above-mentioned (pressing down) microbial inoculum that kills is preferred:
Herba Menthae, Flos Caryophylli, green tea (tea polyphenols, catechin), Herba Pileae Scriptae, Radix Notoginseng, Radix Zanthoxyli extract, YUNNAN BAIYAO, watermelon crystal, Fructus Momordicae charantiae cremor, papain, polypeptide calcium, biological antibacterial peptide, lysozyme, Margarita powder, Borax, potassium sorbate, sodium benzoate.
Above-mentioned desensitizer: preferred strontium chloride, citric acid.
Above-mentioned brightening agent is preferably Dexol, sodium carbonate peroxide, peroxidating amine carbonate, calper calcium peroxide.
Above-mentioned caries preventive agent: preferred fluorinated sodium, potassium fluoride, prodan, ammonium fluosilicate and stannic fluoride.
Above-mentioned anticalculus agents is preferably pyrophosphate, polyphosphate, PC.
The present invention can add an amount of correctives according to actual needs.The optional Oleum Menthae Rotundifoliae of correctives, protein sugar, Oleum menthae, Oleum Caryophylli, wintergreen oil, Eucalyptus oil, Fructus Citri Limoniae oil, grapefruit and the various oiliness compounds of Citrus wet goods, and Mentholum, anethole and other green tea, lemon flavouring etc. are a kind of or the combination of some kinds of spice, except that having the flavoring function, wherein part also has the effect of deodorization and sterilization.In addition, also to add extender CMC-Na.
The preparation method of chewing bubble-producing type solid tooth-paste, with acids such as tartaric acid, citric acids as group 1, with basic species such as sodium bicarbonate, calcium carbonate as group 2, with cleaning agent, filler, function thing, correctives etc. as organizing 3.After will organizing the abundant respectively mixing of 1-3, get 50% ± 10% of every group of mixture respectively, granulate respectively with dehydrated alcohol, oven dry obtains granule 1,2,3.The remainder of three groups of mixture is put together, fully mix, granulate with dehydrated alcohol, oven dry obtains granule 4.Granule 1-4 is mixed, add magnesium stearate, tabletting, promptly.
The granule chance water afterreaction of making after the mixing of group 1-3 remainder is very fast, can improve expansion rate; Remix part after group 1-3 granulates is respectively met the water afterreaction relatively slowly, can prolong foamed time.
Chewing bubble-producing type solid tooth-paste of the present invention is the solid mixture of similar drug sheet, and is close with existing toothpaste composition.Foam by chewing, make cleaning agent with respect to teeth training, thus the effect of bringing into play cleaning oral cavity, taking care of one's teeth.In the oral cavity, chew in the process and mix, chemical reaction takes place, produce carbon dioxide and foam with saliva.This section is chewed, foaming process is as brushing teeth with toothpaste, has the effect of grinding tooth, touch gingiva, cleaning oral cavity, gargles afterwards that oral cavity and tooth have at least as the cleaning of brushing teeth with toothpaste, tasty and refreshing sense, but more more convenient than brushing teeth, comfortable.It is made with nontoxic pharmaceutic adjuvant or food additive, and is safe in utilization; Gargle the gurry non-environmental-pollution with the back water.
The present invention can make multiple packing specification as required, is convenient to preserve, transport, sell, carry and use.Can also make difformity, color, taste, make us pleasing, be applicable to various crowds.Can add difference and have the composition of health care, as brighten, effect such as sterilization, deodorization, hemostasis, preventing decayed tooth, to adapt to different needs: also can play the important function that prevents that illness finds its way in by the mouth.Its production, packing cost are low, and price is suitable, and is easy-to-use, comfortable, civilized, safe, pollution-free, harmless to tooth, the masses' that are easy to get approval.It is applicable to that small lots granting units such as hotel, hospital, passenger traffic, army, prison use: also be applicable to more to be applicable to the general population who needs oral cavity cleaning by special populations such as clerk, travel personnel, student, soldier, athlete, particular job environment personnel, handicapped person.It can partly substitute the method for brushing teeth of traditional toothpaste, toothbrush, hygienic article such as alternative chewing gum, collutory or as its important additional articles for use.
Function and function combinations
The effect that this product has cleaning oral cavity and tooth has teeth whitening, antiscale again concurrently, counteract oral malodour, the effect of prevention or treatment oral disease.According to different application targets, as clean, brighten, tooth protection, taste removal, preventing decayed tooth, sterilization, antiinflammatory, hemostasis, wound healing etc., and different crowd as child, adult, old man etc., carries out different function combinations.
Calcium carbonate, calcium phosphate, silicon dioxide, aluminium hydroxide, Bentonite etc. are toothpaste abrasivuss commonly used, bring into play friction effect in the foam motion, play cleaning effect.Dodecyl sodium sulfate (potassium), Polyoxamer407, Steareth30, polysorbate 20 etc. are the surfactants that toothpaste generally uses, and can play emulsifying, de-sludging, foaming, effect such as moistening, are used for the cleaning of oral cavity and tooth.Its toxicity is low, and cleaning effect is good, stimulates little to oral mucosa.Surfactant has wettability to insoluble material simultaneously, helps sterilization, anti-inflammatory drug better to bring into play effect.
In the practical application,, add scale preventative, brightening agent, desensitizer, kill a kind of or some kinds of function combinations things in (pressing down) microbial inoculum according to the function needs.
Pyrophosphate, polyphosphate, PC are commonly usedly in the toothpaste to prevent tartar (stone) agent.Dexol, sodium carbonate peroxide, peroxide phosphoamide, calper calcium peroxide etc. are the bonded brightening agents of hydrogen peroxide and corresponding compounds, have been widely used in home bleaching and the dental bleaching.Its bleaching principle is can discharge oxygen atom in aqueous solution, and oxidative degradation reaches the purpose of oxidation bleaching by the pigment in food and the medicine generation tartar.This oxidative degradation (oxidation bleaching) is considered to take place by following mechanism: hydrogen peroxide degraded, and the two keys in formation free radical (HO-) the attack colourant molecule, and the result makes two bond fissions, and carbon is oxidized to corresponding carbonic acyl radical.After carbonic acyl radical forms, occupy π (Pi) electronics though they resemble in C.dbd.C, they absorb ultraviolet spectra, can not decolour.Compare with the hydrogen peroxide of liquid state, perborate chemical compound etc. are to more gentle, the safety of effect of gums on every side.Simultaneously these peroxide also are antibacterial preferably, can reduce dental plaque, periodontal and dental caries, can make the dental enamel hardening, and dental caries is produced very strong inhibitory action.
The green tea extract Main Ingredients and Appearance is tea polyphenols, catechin etc., has effects such as strong tooth, control periodontitis, preventing decayed tooth, the smelly detoxifcation that disappears; YUNNAN BAIYAO has effects such as good hemostasis, pain relieving, removing toxic substances and promoting subsidence of swelling.Herba Pileae Scriptae extract contains Fumaric acid (fumaric acid), succinic acid (succinic acid), lignum-vitae base lignan (guaiacyl lignin), flavonoid glycoside, coumarin, lactone, tannin, isofraxidin and a small amount of volatilization wet goods, and thing boil on the nape opposite the mouth, periodontitis etc. have better therapeutic effect.Radix Notoginseng has another name called Radix Notoginseng, and its extract is mainly triterpene and Saponin class material, has activating blood circulation to dissipate blood stasis, and the hemostasis eliminating stagnation, restrains wound, prevents effect such as dentin hypersensitiveness promoting the circulation of QI to relieve pain.Flos Caryophylli extract Main Ingredients and Appearance eugenol or Oleum Caryophylli have effects such as sterilization, antiinflammatory, pain relieving, and Ancient Chinese is for just beginning to be applied to remove halitosis.The Herba Menthae active ingredient is Mentholum or oil, has the effect of sterilization, analgesia, antipruritic, aromatic refrigerant, is to be usually used in food, oral-cavity article.The Radix Zanthoxyli extract Main Ingredients and Appearance is nitidine, crystallization-8 etc., has antiinflammatory, analgesic effect.These functional mass all can be buied from market.
Watermelon crystal, Fructus Momordicae charantiae cremor have the sore-throat relieving of relieving inflammation or internal heat, the effect of anti-inflammatory analgetic.Papain has antiinflammatory, function of gallbladder promoting, pain relieving, digestant effect, but cleaning oral cavity removes denude and dental calculus.The medicinal function of Margarita powder, all on the books on 19 kinds of successive dynasties medicine ancient books and modern drug encyclopedia, can be summarized as: relieving cough and resolving phlegm, tranquillizing the mind by relieving convulsion, heat-clearing and toxic substances removing, sterilizing (to golden Fructus Vitis viniferae ball killing power maximum), hemostasia and promoting granulation, removing nebula etc. makes eye bright, by participating in the metabolism of cell DNA, can promote wound healing.Polypeptide calcium can promote the remineralization of tooth, reinforces and repair teeth.Biological antibacterial peptide, lysozyme etc. are that antibiotic substance is used in safe oral cavity clearly.All there is sale in these function thing markets.Borax is the inorganic salts cleaning agent for mouth cavity of using always, is widely used in and controls laryngopharynx swelling and pain, aphtha of the mouth and tongue.Potassium sorbate, sodium benzoate are the food preservatives of using always.Strontium chloride can make tooth desensitizers.
Xylitol, mannitol, lactose can not caused the dental caries microbial fermentation and be produced acidic materials, so can prevent to corrode tooth as filler.
Sodium fluoride, potassium fluoride, prodan, ammonium fluosilicate, stannic fluoride are the fluorides commonly used of preventing decayed teeth and tooth, are widely used in the toothpaste.
Using method:
Get this product, put into mouth, chew fast, it is mixed with saliva as far as possible; Stir broken powder and foam while chewing with tongue, contact with tooth.Treat that powder is molten substantially and stir, agitate intraoral foam after diffusing, wash away tooth and foreign body in mouth as far as possible.After half a minute, gargle with clear water, promptly approximately.
If gargle with a small amount of clear water earlier, make mouth-moistening, use this product then, effect is better.
To the people who gets used to brushing teeth with toothbrush, this product can substitute traditional toothpaste as required, in its foaming back with the toothbrush tooth of gently brushing teeth.
(4) specific embodiment
Embodiment one
Chewing bubble-producing type solid tooth-paste is to be mixed with by tartaric acid 20%, citric acid 8%, sodium bicarbonate 30%, calcium carbonate 10%, mannitol 20%, CMC-Na 5%, protein sugar 2%, tea polyphenols 2%, dodecyl sodium sulfate 1.5%, Mentholum 0.5%, magnesium stearate 1%.
Embodiment two
Chewing bubble-producing type solid tooth-paste is to be mixed with by tartaric acid 20%, citric acid 8%, sodium bicarbonate 25%, calcium carbonate 11.5%, mannitol 20%, CMC-Na 5%, Margarita powder 5%, protein sugar 2%, tea polyphenols 1%, dodecyl sodium sulfate 1%, Mentholum 0.5%, magnesium stearate 1%.
Embodiment three
Chewing bubble-producing type solid tooth-paste is by tartaric acid 20%, citric acid 5%, sodium bicarbonate 25%, calcium carbonate 10.5%, mannitol 20%, CMC-Na 5%, Margarita powder 5%, protein sugar 2%, dodecyl sodium sulfate 1%, Mentholum 0.5%, Na 2CO 3H 2O 25%, magnesium stearate 1% is mixed with.
Production technology is: with tartaric acid, citric acid as group 1, with sodium bicarbonate, calcium carbonate as group 2, mannitol, CMC-Na Na 2CO 3.H 2O 2, Margarita powder, protein sugar, tea polyphenols, dodecyl sodium sulfate, Mentholum be as group 3.To organize 1-3 fully mixes respectively; Get 50% ± 10% of every group of mixture respectively, granulate respectively with dehydrated alcohol, oven dry obtains granule 1,2,3.The remainder of three groups of mixture is put together, after fully mixing, granulate with dehydrated alcohol, oven dry obtains granule 4.Granule 1-4 is mixed, add magnesium stearate, tabletting, promptly.
Expansion rate and gas release are measured: get 2 in 100ml graduated cylinder, each adds 10ml water, loads onto the slice, thin piece of stating three prescriptions respectively and puts into graduated cylinder, measures the relation of investigation time and gas release.The result shows that prescription diacid sex ratio is slightly high, and expansion rate is fast, but persistency is not as other two prescriptions.
Table 1, foamed time and gas release measurement result
Time (second) Prescription one Prescription two Prescription three
0.5 6 8 7
1 11 13 10
1.5 16 17 13
2.0 18 21 17
2.5 21 23 19
3.0 23 25 22
4.0 25 29 26
5.0 27 35 28
6.0 29 35 30
7.0 31 35 31
8.0 32 35 32
9.0 33 35 34
10.0 34 35 34

Claims (7)

1, chewing bubble-producing type solid tooth-paste mainly is formulated by foaming agent 25-80%, abrasivus 1-25%, cleaning agent 0.01-20%, filler 1-30%; Foaming agent middle acid substance 10-40%, alkaline matter 10-40%, wherein:
At least a in foaming agent acidic materials optimization citric acid, tartaric acid, the malic acid; The preferred sodium bicarbonate of foaming agent alkaline matter;
The preferred dodecyl sodium sulfate of cleaning agent (potassium), Polyo * amer407, Steareth30, at least a in the polysorbate 20;
At least a in the preferred calcium carbonate of abrasivus, calcium phosphate, silicon dioxide, aluminium hydroxide, the Bentonite;
At least a in the preferred xylitol of filler, mannitol, the lactose.
2, chewing bubble-producing type solid tooth-paste according to claim 1 is characterized in that adding the anticalculus agents that accounts for toothpaste gross weight 0.1-8% in the solid tooth-paste, and anticalculus agents is preferably in pyrophosphate, polyphosphate, the PC at least a.
3, chewing bubble-producing type solid tooth-paste according to claim 1 is characterized in that adding sterilization, the antibacterial that accounts for toothpaste gross weight 0.01-10% in the solid paste, and sterilization, antibacterial are preferably Herba Menthae, Flos Caryophylli, green tea, Herba Pileae Scriptae, Radix Notoginseng, Radix Zanthoxyli extract, YUNNAN BAIYAO, watermelon crystal, Fructus Momordicae charantiae cremor, papain, polypeptide calcium, biological antibacterial peptide, lysozyme, Margarita powder, Borax, potassium sorbate, sodium benzoate at least a.
4, chewing bubble-producing type solid tooth-paste according to claim 1, it is characterized in that in the solid tooth-paste adding the caries preventive agent that accounts for toothpaste total amount 0.01-2%, caries preventive agent is preferably at least a in sodium fluoride, potassium fluoride, prodan, ammonium fluosilicate, the stannic fluoride.
5, chewing bubble-producing type solid tooth-paste according to claim 1 is characterized in that adding the desensitizer that accounts for toothpaste total amount 0.01-5% in the solid tooth-paste, and desensitizer is preferably strontium chloride.
6, chewing bubble-producing type solid tooth-paste according to claim 1 is characterized in that adding the brightening agent that accounts for toothpaste total amount 0.1-20% in the solid tooth-paste, is preferably sodium borate, sodium carbonate peroxide, peroxide phosphoamide, calper calcium peroxide.
7, chewing bubble-producing type solid tooth-paste according to claim 1, its production technology is: with acids such as tartaric acid, citric acids as group 1, with basic species such as sodium bicarbonate, calcium carbonate as group 2, with cleaning agent, filler, function thing etc. as organizing 3.After will organizing the abundant respectively mixing of 1-3, get 50% ± 10% of every group of mixture respectively, granulate respectively with dehydrated alcohol, oven dry obtains granule 1,2,3.The remainder of three groups of mixture is put together, fully mix, granulate with dehydrated alcohol, oven dry obtains granule 4.Granule 1-4 is mixed, add magnesium stearate, tabletting, promptly.
CN 200610046311 2006-04-14 2006-04-14 Chewing bubble-producing type solid tooth-paste Pending CN1861039A (en)

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Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013072932A3 (en) * 2011-09-30 2013-08-08 Rubicon Research Private Limited Oral care compositions
CN103432044A (en) * 2013-09-05 2013-12-11 桂林三金西瓜霜生态制品有限责任公司 Watermelon emulsum toothpaste and preparation method thereof
CN103767990A (en) * 2014-01-13 2014-05-07 赵君友 Oral cleaning grain and preparation method thereof
CN103830145A (en) * 2014-03-18 2014-06-04 林彤 Toothpaste containing biological peptides and traditional Chinese medicines
WO2015158638A1 (en) * 2014-04-17 2015-10-22 Unilever Plc Solid oral care compositions
CN104997660A (en) * 2015-07-21 2015-10-28 重庆登康口腔护理用品股份有限公司 Oral cavity composition, preparation method and oral cavity preparation and application thereof
CN105748369A (en) * 2016-04-11 2016-07-13 马鞍山中粮生物化学有限公司 Mouth wash for diminishing inflammation and removing halitosis
CN105997605A (en) * 2016-05-05 2016-10-12 常州大学 Self-cleaning solid toothpaste and preparation method thereof
CN106361588A (en) * 2016-10-27 2017-02-01 陆腾蛟 Tooth cleaning product and production device and process
CN109010090A (en) * 2018-09-20 2018-12-18 江苏雪豹日化有限公司 A kind of sodium bicarbonate biological complex enzyme toothpaste
CN111821218A (en) * 2020-08-04 2020-10-27 安徽克菱保健科技有限公司 Chewing foaming slow-release toothpaste tablet
CN112237564A (en) * 2020-10-16 2021-01-19 浙江神英科技股份有限公司 Toothpaste and preparation method thereof

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013072932A3 (en) * 2011-09-30 2013-08-08 Rubicon Research Private Limited Oral care compositions
US10806685B2 (en) 2011-09-30 2020-10-20 Rubicon Research Private Limited Oral care compositions
CN103432044A (en) * 2013-09-05 2013-12-11 桂林三金西瓜霜生态制品有限责任公司 Watermelon emulsum toothpaste and preparation method thereof
CN103767990A (en) * 2014-01-13 2014-05-07 赵君友 Oral cleaning grain and preparation method thereof
CN103830145A (en) * 2014-03-18 2014-06-04 林彤 Toothpaste containing biological peptides and traditional Chinese medicines
CN103830145B (en) * 2014-03-18 2015-10-28 林彤 A kind of toothpaste containing biological peptide and Chinese medicine
WO2015158638A1 (en) * 2014-04-17 2015-10-22 Unilever Plc Solid oral care compositions
CN106456498A (en) * 2014-04-17 2017-02-22 荷兰联合利华有限公司 Solid oral care compositions
CN104997660B (en) * 2015-07-21 2018-01-23 重庆登康口腔护理用品股份有限公司 A kind of oral cavity composition, preparation method, oral preparation and its application
CN104997660A (en) * 2015-07-21 2015-10-28 重庆登康口腔护理用品股份有限公司 Oral cavity composition, preparation method and oral cavity preparation and application thereof
CN105748369A (en) * 2016-04-11 2016-07-13 马鞍山中粮生物化学有限公司 Mouth wash for diminishing inflammation and removing halitosis
CN105997605A (en) * 2016-05-05 2016-10-12 常州大学 Self-cleaning solid toothpaste and preparation method thereof
CN106361588A (en) * 2016-10-27 2017-02-01 陆腾蛟 Tooth cleaning product and production device and process
CN109010090A (en) * 2018-09-20 2018-12-18 江苏雪豹日化有限公司 A kind of sodium bicarbonate biological complex enzyme toothpaste
CN111821218A (en) * 2020-08-04 2020-10-27 安徽克菱保健科技有限公司 Chewing foaming slow-release toothpaste tablet
CN112237564A (en) * 2020-10-16 2021-01-19 浙江神英科技股份有限公司 Toothpaste and preparation method thereof

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