CN102670458A - Oral care solution and preparation process thereof - Google Patents
Oral care solution and preparation process thereof Download PDFInfo
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- CN102670458A CN102670458A CN2012101839039A CN201210183903A CN102670458A CN 102670458 A CN102670458 A CN 102670458A CN 2012101839039 A CN2012101839039 A CN 2012101839039A CN 201210183903 A CN201210183903 A CN 201210183903A CN 102670458 A CN102670458 A CN 102670458A
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Abstract
The invention discloses an oral care solution. The oral care solution is characterized by comprising care ingredients, ingredients inhibiting dental plaque and dissolving pigment and base material ingredients; the care ingredients comprise angelica extract, shatian pomelo extract, halite, xylitol, turmeric extract and tea polyphenol; the ingredients inhibiting dental plaque comprise modified sodium phytate; the base material ingredients comprise water, moisturizers, saccharin sodium, essence and non-ionic surfactants; and the oral care solution also comprises anti-corrosive ingredients, and the anti-corrosive ingredients are positive-ionic surfactants, traditional Chinese medicine extract and parabens. The oral care solution can inhibit plaque, avoids tooth decay, repairs damaged oral mucosa, whitens teeth and freshens breath.
Description
Technical field
The invention belongs to the oral care product field, specifically, relate to a kind of oral nursing liquid and processing technology thereof.
Background technology
Oral nursing liquid is to be the liquid oral care product, mainly act as cleaning oral cavity, has covered not abnormal smells from the patient, and be the lasting remaining pure and fresh pleasant sensation in oral cavity.Oral cavity cleaning and nursing liquid on the market is the spirituosity prescription mostly, and oral mucosa is produced stimulates easily, and it is careful that the use of ethanol consumer hypersensitive is needed.In addition; Since the oral nursing liquid water content than higher generally more than 80%; Accomplish not contain alcohol and can have good antiseptic power again, need select, can influence the ability to accept of consumer because the use of antiseptic not only influences mouthfeel protective system.Therefore, have good bacteriostasis, adding the oral nursing liquid that Chinese herbal medicine extract can help to nurse gingiva, useful teeth surfaces bacterial plaque is that market is required.
Summary of the invention
The technical problem that the present invention will solve is to overcome above-mentioned defective, provide a kind of do not have alcohol, have cleaning bacterial plaque and nursing gingiva, gingivitis, periodontal disease are had the oral nursing liquid that contains Chinese herbal medicine extract of certain effect.This oral nursing liquid makes no pure product have good antiseptic property, in the shelf life of regulation, keeps steady quality, and makes the solubilising problem of tea polyphenols in no pure system that solved through emulsifying technology.
For addressing the above problem, the technical scheme that the present invention adopted is:
A kind of oral nursing liquid is characterized in that: comprise nursing composition, antipathogenic composition and base material composition;
Said nursing composition comprises following component by mass percent: Radix Angelicae Dahuricae extract 0.2 ~ 10%, shatian pomelo extract 0.1～5%, Halitum 0.5～10%, xylitol 0.3～10%, Rhizoma Curcumae Longae extract 0.1～2% and tea polyphenols 0～3%;
Said inhibition bacterial plaque and dissolving pigment composition comprise following component by mass percent: modification sodium phytate 0.2～5%;
Said base material composition comprises following component by mass percent: water 70～96%, wetting agent 5～15%, saccharin sodium 0～0.2%, essence 0.05～1.0%, non-ionic surface active agent 0.1～2%.
Said oral nursing liquid also contains anti-corrosion composition, and anti-corrosion composition is cationic surfactant, Chinese medicine extract and parabens.
Said wetting agent be glycerol or and sorbitol.
Said non-ionic surface active agent be as castor oil hydrogenated polyoxy ethanol-40 or and polysorbas20.
Said cationic surfactant is western arsenic oronain.
Further say:
Said nursing composition comprises following component by mass percent: 1% Radix Angelicae Dahuricae extract, 0.5% shatian pomelo extract, 1% Halitum, 1% Rhizoma Curcumae Longae extract and 0.5% tea polyphenols;
Said inhibition bacterial plaque and dissolving pigment composition comprise following component by mass percent: 1% modification sodium phytate;
Said anti-corrosion composition comprises following component by mass percent: 0.1% western arsenic oronain;
Said base material composition comprises following component by mass percent: 10% glycerol, 0.02% saccharin sodium, 0.2% essence, 1.5% are like castor oil hydrogenated polyoxy ethanol-40 and 1.0% polysorbas20;
Surplus is 0.1%EDTA disodium and water.
Further say:
Said nursing composition comprises following component by mass percent: 1% Radix Angelicae Dahuricae extract, 0.5% shatian pomelo extract, 1% Halitum, 1% Rhizoma Curcumae Longae extract and 3% xylitol;
Said inhibition bacterial plaque and dissolving pigment composition comprise following component by mass percent: 1% improved plant sodium;
Said anti-corrosion composition comprises following component by mass percent: 0.1% western arsenic oronain;
Said base material composition comprises following component by mass percent: 8% glycerol, 0.2% essence, 1.5% are like castor oil hydrogenated polyoxy ethanol-40;
Surplus is 0.1%EDTA disodium and water.
Further say:
Said nursing composition comprises following component by mass percent: 1% Radix Angelicae Dahuricae extract, 0.5% shatian pomelo extract, 1% Halitum, 1% Rhizoma Curcumae Longae extract and 5% xylitol;
Said inhibition bacterial plaque and dissolving pigment composition comprise following component by mass percent: 1% modification sodium phytate;
Said anti-corrosion composition comprises following component by mass percent: 0.1% western arsenic oronain;
Said base material composition comprises following component by mass percent: 8% glycerol, 0.2% essence, 1.5% are like castor oil hydrogenated polyoxy ethanol-40;
Surplus is 0.1%EDTA disodium and water.
A kind of processing technology of oral nursing liquid is characterized in that:
Comprise following steps:
1), industrial water must pass through reverse osmosis equipment and handle, and requires electrical conductivity≤10 μ s, total plate count≤80/g, water need use the circulation heating systems simultaneously, guaranteeing to get into the temperature of driving material emulsifying pot is 80 degree; After 10 minutes, need behind the entering emulsifying pot, water temperature is reduced to 50 degree through cooling system, for use;
2), a certain proportion of Radix Angelicae Dahuricae extract, Rhizoma Curcumae Longae extract is dissolved in the 50 degree hot water through sterilization back and a certain proportion of xylitol, Halitum and saccharin sodium;
3), a certain proportion of tea polyphenols is dissolved in separately in the hot water, back and a certain proportion of wetting agent (glycerol, the sorbitol) back of dissolving each other is for use;
4), dissolve each other a certain proportion of essence, shatian pomelo extract and emulsifying agent for use;
5), the mixture in the step 2 is added in the water in 1, and agitator speed is adjusted to low speed, stirs after 5 minutes, add the mixture in step 3, the step 4, and simultaneously mixing speed is adjusted at a high speed; Stir 40 minutes through discharging behind one 0.02 μ sterilization filter element;
6), the liquid that comes out of the filter element that will go out to sterilize, to storage tank, stored 4～8 hours, behind sterilization filter element and uviol lamp, fill.
Since adopted technique scheme, compared with prior art, among the present invention; The Radix Angelicae Dahuricae is the good medicine of treatment halitosis; Halitum has the effect of diminishing inflammation and clearing pharynx, and Rhizoma Curcumae Longae has the effect of quickening the mucosa healing and avoiding bacterial infection, and the shatian pomelo extract is the broad-spectrum antiseptic material; In prescription, both can play the effect that suppresses oral cavity bacterium and also can play certain antiseptic property, thereby xylitol reaches the purpose of preventing decayed tooth for the growth that can suppress Streptococcus mutans.Tea polyphenols has the effect that suppresses dental plaque and preventing decayed tooth.Above-mentioned, combination of compositions is the effect that oral nursing liquid has antiinflammatory, deodorization, sore-throat relieving and reparation oral ulcer together.
The pH value of modification sodium phytate can be stabilized between 5 ~ 9, and can be stable be present in the liquid and is unlikely to cause PH too high or low excessively, has avoided using phytic acid institute to cause easily and the perhaps bad outward appearance of float of deposition occurred.The modification sodium phytate plays good chelating agent dissolution to mottle on the facing or the alkaline bacterial plaque that is deposited on the facing; Help to remove the tooth stain and makes conditioning liquid in the process of using, though there is not the mechanical friction of toothbrush also can reach the effect of certain cleaning dental plaque.
Owing to use the cation antibacterial as anti-corrosion composition, avoid composition and cation in the Chinese medicine extract to react, causing deposition is that cation lost efficacy.The cation antibacterial also can reach and kill the purpose that oral cavity bacterium is safeguarded oral health in the rinsing the mouth process simultaneously.
The specific embodiment
Embodiment:
A kind of oral nursing liquid comprises nursing composition, antipathogenic composition and base material composition.
Said nursing composition comprises following component by mass percent: Radix Angelicae Dahuricae extract 0.2 ~ 10%, shatian pomelo extract 0.1～5%, Halitum 0.5～10%, xylitol 0.3～10%, Rhizoma Curcumae Longae extract 0.1～2% and tea polyphenols 0～3%;
Said inhibition bacterial plaque and dissolving pigment composition comprise following component by mass percent: modification sodium phytate 0.2～5%;
Said base material composition comprises following component by mass percent: water 70～96%, wetting agent 5～15%, saccharin sodium 0～0.2%, essence 0.05～1.0%, non-ionic surface active agent 0.1～2%.
In the present embodiment, said oral nursing liquid also contains anti-corrosion composition, and anti-corrosion composition is cationic surfactant, Chinese medicine extract and parabens.Said wetting agent be glycerol or and sorbitol.Said non-ionic surface active agent be as castor oil hydrogenated polyoxy ethanol-40 or and polysorbas20.Said cationic surfactant is western arsenic oronain.
Among the present invention; The Radix Angelicae Dahuricae is the good medicine of treatment halitosis; Halitum has the effect of diminishing inflammation and clearing pharynx, and Rhizoma Curcumae Longae has the effect of quickening the mucosa healing and avoiding bacterial infection, and the shatian pomelo extract is the broad-spectrum antiseptic material; In prescription, both can play the effect that suppresses oral cavity bacterium and also can play certain antiseptic property, thereby xylitol reaches the purpose of preventing decayed tooth for the growth that can suppress Streptococcus mutans.Tea polyphenols has the effect that suppresses dental plaque and preventing decayed tooth.Above-mentioned, combination of compositions is the effect that oral nursing liquid has antiinflammatory, deodorization, sore-throat relieving and reparation oral ulcer together.
The pH value of improved plant sodium can be stabilized between 5 ~ 9, and can be stable be present in the liquid and is unlikely to cause PH too high or low excessively, has avoided using phytic acid institute to cause easily and the perhaps bad outward appearance of float of deposition occurred.The modification sodium phytate plays good chelating agent dissolution to mottle on the facing or the alkaline bacterial plaque that is deposited on the facing; Help to remove the tooth stain and makes conditioning liquid in the process of using, though there is not the mechanical friction of toothbrush also can reach the effect of certain cleaning dental plaque.
Owing to use the cation antibacterial as anti-corrosion composition, avoid composition and cation in the Chinese medicine extract to react, causing deposition is that cation lost efficacy.The cation antibacterial also can reach and kill the purpose that oral cavity bacterium is safeguarded oral health in the rinsing the mouth process simultaneously.
The processing technology of present embodiment comprises following steps:
1), industrial water at first handles through reverse osmosis equipment, requires electrical conductivity≤10 μ s, total plate count≤80/g, water need use the circulation heating systems simultaneously, guaranteeing to get into the temperature of driving material emulsifying pot is 80 degree; After 10 minutes, need behind the entering emulsifying pot, water temperature is reduced to 50 degree through cooling system, for use;
2), a certain proportion of Radix Angelicae Dahuricae extract, Rhizoma Curcumae Longae extract is dissolved in the 50 degree hot water through sterilization back and a certain proportion of xylitol, Halitum and saccharin sodium;
3), a certain proportion of tea polyphenols is dissolved in separately in the hot water, back and a certain proportion of wetting agent (glycerol, the sorbitol) back of dissolving each other is for use;
4), dissolve each other a certain proportion of essence, shatian pomelo extract and emulsifying agent for use;
5), the mixture in the step 2 is added in the water in 1, and agitator speed is adjusted to low speed, stirs after 5 minutes, add the mixture in step 3, the step 4, and simultaneously mixing speed is adjusted at a high speed; Stir 40 minutes through discharging behind one 0.02 μ sterilization filter element;
6), the liquid that comes out of the filter element that will go out to sterilize, to storage tank, stored 4～8 hours, behind sterilization filter element and uviol lamp, fill.
According to practical situation, in the present embodiment, can choose following three kinds of prescriptions:
Prescription 1:
The nursing composition comprises following component by mass percent: 1% Radix Angelicae Dahuricae extract, 0.5% shatian pomelo extract, 1% Halitum, 1% Rhizoma Curcumae Longae extract and 0.5% tea polyphenols;
Suppress bacterial plaque and dissolve pigment composition to comprise following component by mass percent: 1% modification sodium phytate;
Anti-corrosion composition comprises following component by mass percent: 0.1% western arsenic oronain;
The base material composition comprises following component by mass percent: 10% glycerol, 0.02% saccharin sodium, 0.2% essence, 1.5% are like castor oil hydrogenated polyoxy ethanol-40 and 1.0% polysorbas20;
Surplus is 0.1%EDTA disodium and water.
Prescription 2:
The nursing composition comprises following component by mass percent: 1% Radix Angelicae Dahuricae extract, 0.5% shatian pomelo extract, 1% Halitum, 1% Rhizoma Curcumae Longae extract and 3% xylitol;
Suppress bacterial plaque and dissolve pigment composition to comprise following component by mass percent: 1% modification sodium phytate;
Anti-corrosion composition comprises following component by mass percent: 0.1% western arsenic oronain;
The base material composition comprises following component by mass percent: 8% glycerol, 0.2% essence, 1.5% are like castor oil hydrogenated polyoxy ethanol-40;
Surplus is 0.1%EDTA disodium and water.
Prescription 3:
Said nursing composition comprises following component by mass percent: 1% Radix Angelicae Dahuricae extract, 0.5% shatian pomelo extract, 1% Halitum, 1% Rhizoma Curcumae Longae extract and 5% xylitol;
Said inhibition bacterial plaque and dissolving pigment composition comprise following component by mass percent: 1% modification sodium phytate;
Said anti-corrosion composition comprises following component by mass percent: 0.1% western arsenic oronain;
Said base material composition comprises following component by mass percent: 8% glycerol, 0.2% essence, 1.5% are like castor oil hydrogenated polyoxy ethanol-40;
Surplus is 0.1%EDTA disodium and water.
In above prescription, add an amount of EDTA disodium as chelating agen, can play the purpose of stablizing conditioning liquid.
Oral nursing liquid according to above prescription is processed can suppress dental plaque, helps mothproofly, repairs impaired oral mucosa, brilliant white tooth, breath freshening.
Claims (9)
1. an oral nursing liquid is characterized in that: comprise nursing composition, antipathogenic composition and base material composition;
Said nursing composition comprises following component by mass percent: Radix Angelicae Dahuricae extract 0.2 ~ 10%, shatian pomelo extract 0.1～5%, Halitum 0.5～10%, xylitol 0.3～10%, Rhizoma Curcumae Longae extract 0.1～2% and tea polyphenols 0～3%;
Said antibacterial speckle and dissolving pigment composition comprise following component by mass percent: modification sodium phytate 0.2～5%;
Said base material composition comprises following component by mass percent: water 70～96%, wetting agent 5～15%, saccharin sodium 0～0.2%, essence 0.05～1.0%, non-ionic surface active agent 0.1～2%.
2. according to the oral nursing liquid described in the claim 1, it is characterized in that: said oral nursing liquid also contains anti-corrosion composition, and anti-corrosion composition is cationic surfactant, Chinese medicine extract and parabens.
3. according to the oral nursing liquid described in the claim 1, it is characterized in that: said wetting agent be glycerol or and sorbitol.
4. according to the oral nursing liquid described in the claim 1, it is characterized in that: non-ionic surface active agent for as castor oil hydrogenated polyoxy ethanol-40 or and polysorbas20.
5. according to the oral nursing liquid described in the claim 2, it is characterized in that: cationic surfactant is western arsenic oronain.
6. according to the oral nursing liquid described in claim 1 or 2, it is characterized in that:
Said nursing composition comprises following component by mass percent: 1% Radix Angelicae Dahuricae extract, 0.5% shatian pomelo extract, 1% Halitum, 1% Rhizoma Curcumae Longae extract and 0.5% tea polyphenols;
Said antibacterial speckle and dissolving pigment composition comprise following component by mass percent: 1% modification sodium phytate;
Said anti-corrosion composition comprises following component by mass percent: 0.1% western arsenic oronain;
Said base material composition comprises following component by mass percent: 10% glycerol, 0.02% saccharin sodium, 0.2% essence, 1.5% are like castor oil hydrogenated polyoxy ethanol-40 and 1.0% polysorbas20;
Surplus is 0.1%EDTA disodium and water.
7. according to the oral nursing liquid described in claim 1 or 2, it is characterized in that:
Said nursing composition comprises following component by mass percent: 1% Radix Angelicae Dahuricae extract, 0.5% shatian pomelo extract, 1% Halitum, 1% Rhizoma Curcumae Longae extract and 3% xylitol;
Said antibacterial speckle and dissolving pigment composition comprise following component by mass percent: 1% modification sodium phytate;
Said anti-corrosion composition comprises following component by mass percent: 0.1% western arsenic oronain;
Said base material composition comprises following component by mass percent: 8% glycerol, 0.2% essence, 1.5% are like castor oil hydrogenated polyoxy ethanol-40;
Surplus is 0.1%EDTA disodium and water.
8. according to the oral nursing liquid described in claim 1 or 2, it is characterized in that:
Said nursing composition comprises following component by mass percent: 1% Radix Angelicae Dahuricae extract, 0.5% shatian pomelo extract, 1% Halitum, 1% Rhizoma Curcumae Longae extract and 5% xylitol;
Said antibacterial speckle and dissolving mottle composition comprise following component by mass percent: 1% improved plant sodium;
Said anti-corrosion composition comprises following component by mass percent: 0.1% western arsenic oronain;
Said base material composition comprises following component by mass percent: 8% glycerol, 0.2% essence, 1.5% are like castor oil hydrogenated polyoxy ethanol-40;
Surplus is 0.1%EDTA disodium and water.
9. the processing technology of an oral nursing liquid is characterized in that:
Comprise following steps:
1), industrial water must pass through reverse osmosis equipment and handle, and requires electrical conductivity≤10 μ s, total plate count≤80/g, water need use the circulation heating systems simultaneously, guaranteeing to get into the temperature of driving material emulsifying pot is 80 degree; After 10 minutes, need behind the entering emulsifying pot, water temperature is reduced to 50 degree through cooling system, for use;
2), a certain proportion of Radix Angelicae Dahuricae extract, Rhizoma Curcumae Longae extract is dissolved in the 50 degree hot water through sterilization back and a certain proportion of xylitol, Halitum and saccharin sodium;
3), a certain proportion of tea polyphenols is dissolved in separately in the hot water, back and a certain proportion of wetting agent (glycerol, the sorbitol) back of dissolving each other is for use;
4), dissolve each other a certain proportion of essence, shatian pomelo extract and emulsifying agent for use;
5), the mixture in the step 2 is added in the water in 1, and agitator speed is adjusted to low speed, stirs after 5 minutes, add the mixture in step 3, the step 4, and simultaneously mixing speed is adjusted at a high speed; Stir 40 minutes through discharging behind one 0.02 μ sterilization filter element;
6), the liquid that comes out of the filter element that will go out to sterilize, to storage tank, stored 4～8 hours, behind sterilization filter element and uviol lamp, fill.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2012101839039A CN102670458A (en) | 2012-06-06 | 2012-06-06 | Oral care solution and preparation process thereof |
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| CN2012101839039A CN102670458A (en) | 2012-06-06 | 2012-06-06 | Oral care solution and preparation process thereof |
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| CN102670458A true CN102670458A (en) | 2012-09-19 |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103705912A (en) * | 2013-12-20 | 2014-04-09 | 江苏雪豹日化有限公司 | Composite lysozyme oral spray and preparation method thereof |
| CN103933401A (en) * | 2014-04-30 | 2014-07-23 | 马艺 | Applications of highland Barley malt fruit extract in preparation of oral antibacterial drug |
| CN104225485A (en) * | 2014-09-18 | 2014-12-24 | 吴岳泽 | Oral care solution for neurosurgery post-operation |
| CN106074341A (en) * | 2016-07-11 | 2016-11-09 | 周晗生 | Portable oral care liquid |
| CN106074274A (en) * | 2016-07-11 | 2016-11-09 | 周晗生 | Oral care substance |
| CN106727990A (en) * | 2017-02-14 | 2017-05-31 | 哈尔滨市第医院 | Oral nursing liquid and preparation method thereof |
| CN110013451A (en) * | 2019-05-16 | 2019-07-16 | 华纳时代健康科技（武汉）股份有限公司 | A kind of oral bacteriostasis liquid and production technology |
| WO2020118603A1 (en) * | 2018-12-13 | 2020-06-18 | Colgate-Palmolive Company | Oral care compositions including botanicals and methods for the same |
| CN111603418A (en) * | 2020-04-23 | 2020-09-01 | 广州宏康医药科技有限公司 | Oral care product capable of lasting freshness and bacteriostasis and preparation method thereof |
| WO2020181372A1 (en) * | 2019-03-11 | 2020-09-17 | Dosebiome Inc. | Compositions and methods for inhibiting growth of caries-, gingivitis- and halitosis-causing bacteria |
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2012
- 2012-06-06 CN CN2012101839039A patent/CN102670458A/en active Pending
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103705912A (en) * | 2013-12-20 | 2014-04-09 | 江苏雪豹日化有限公司 | Composite lysozyme oral spray and preparation method thereof |
| CN103705912B (en) * | 2013-12-20 | 2015-10-28 | 江苏雪豹日化有限公司 | A kind of composite lysozyme oral spray and preparation method thereof |
| CN103933401A (en) * | 2014-04-30 | 2014-07-23 | 马艺 | Applications of highland Barley malt fruit extract in preparation of oral antibacterial drug |
| CN103933401B (en) * | 2014-04-30 | 2016-08-24 | 张广德 | Wheat tiller extract purposes in preparing oral bacteriostasis medicine |
| CN104225485A (en) * | 2014-09-18 | 2014-12-24 | 吴岳泽 | Oral care solution for neurosurgery post-operation |
| CN106074274A (en) * | 2016-07-11 | 2016-11-09 | 周晗生 | Oral care substance |
| CN106074341A (en) * | 2016-07-11 | 2016-11-09 | 周晗生 | Portable oral care liquid |
| CN106727990A (en) * | 2017-02-14 | 2017-05-31 | 哈尔滨市第医院 | Oral nursing liquid and preparation method thereof |
| WO2020118603A1 (en) * | 2018-12-13 | 2020-06-18 | Colgate-Palmolive Company | Oral care compositions including botanicals and methods for the same |
| WO2020181372A1 (en) * | 2019-03-11 | 2020-09-17 | Dosebiome Inc. | Compositions and methods for inhibiting growth of caries-, gingivitis- and halitosis-causing bacteria |
| US11382850B2 (en) | 2019-03-11 | 2022-07-12 | Dosebiome Inc. | Compositions and methods for inhibiting growth of caries-, gingivitis- and halitosis-causing bacteria |
| CN110013451A (en) * | 2019-05-16 | 2019-07-16 | 华纳时代健康科技（武汉）股份有限公司 | A kind of oral bacteriostasis liquid and production technology |
| CN111603418A (en) * | 2020-04-23 | 2020-09-01 | 广州宏康医药科技有限公司 | Oral care product capable of lasting freshness and bacteriostasis and preparation method thereof |
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Application publication date: 20120919 |