CN108411616A - 一种抗皱防螨织物整理方法 - Google Patents

一种抗皱防螨织物整理方法 Download PDF

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CN108411616A
CN108411616A CN201810302292.2A CN201810302292A CN108411616A CN 108411616 A CN108411616 A CN 108411616A CN 201810302292 A CN201810302292 A CN 201810302292A CN 108411616 A CN108411616 A CN 108411616A
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胡玲
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Foshan Huichuang Zhengyuan New Mstar Technology Ltd
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Abstract

本发明公开了一种抗皱防螨织物整理方法，其包括以下步骤：抗皱整理液的配制；防螨整理液的配制；取棉麻织物，将纯棉织物浸入到抗皱整理液中，50℃下浸泡0.5～2h，两浸两轧，轧余率为65‑85％，在85℃下烘干；将上述烘干的织物浸入到防螨整理液中一浸一轧，浸轧液位70％，轧余率为70‑80％，在100℃下烘干，得到整理后的织物。本发明的织物抗皱防螨整理方法具有良好的无醛环保性，穿着安全、健康；经本发明整理方法整理得到的织物干、湿折皱回复角(度)增加30％以上，皂洗40次后折皱回复角度基本不变；经本发明整理方法整理得到的织物具有良好的防螨和杀菌能力，安全无残留，且具有天然的植物气味，织物的螨虫驱避率高达90％以上。

Description

一种抗皱防螨织物整理方法
技术领域
本发明涉及纺织材料整理方法领域，具体涉及一种用于棉麻织物的环保性优良的抗皱防螨整理方法。
背景技术
传统的棉织物抗皱整理剂N2羟甲基酰胺类化合物、环脲羟甲基衍生物等，此类整理剂防皱效果好，应用广泛，但在织物整理和储存时会释放出大量的游离甲醛，危害人体健康和安全。现有技术中新型棉织物交联防皱防缩整理剂为多元羧酸类，其中1，2，3，4-丁烷四羧酸(BTCA)和柠檬酸(CA)研究最多，这类整理剂处理的棉织物虽无甲醛释放，但整理后织物撕破强力下降显著。因此，开发新型无甲醛抗皱整理剂成为目前研究的重点。
当今，随着人们生活水平的提高以及纺织文化的发展，追求纺织品的美观、舒适、保健，甚至功能性成为时尚，但是现有的织物尤其是床单、被套等不能有效地阻止如螨虫等微生物的滋生，进而在一定程度上影响了人们正常的日常生活。
发明内容
针对现有技术不足，本发明提供了一种用于棉麻织物的环保性优良的抗皱防螨整理方法。
本发明解决上述技术问题采用的技术方案为：一种抗皱防螨织物整理方法，其包括以下步骤：
(1)抗皱整理液的配制：分别备取以下重量份数的原料，亲水性氨基硅油20～30份、烷基酚聚氧乙烯醚12～18份、烷基苯磺酸钠5～10份、碳酸氢钠1～3份、丙烯酸0.5～1.5份、三乙醇胺硼酸酯1～3份、次亚磷酸钠3～6份、乙醇10～15份、去离子水100～130份，将上述原料于50～70℃下混合均匀，冷却后为抗皱整理液；
(2)防螨整理液的配制：分别备取以下重量份数的原料，麝香草酚10～15份、水溶性壳聚糖季铵盐15～25份、聚丙烯酸钠5～10份、硫酸钠1～3份、甲基正壬基酮2～4份、去离子水80～120份，将上述原料常温下充分混合均匀，得到防螨整理液；
(3)取棉麻织物，将纯棉织物浸入到抗皱整理液中，50℃下浸泡0.5～2h，两浸两轧，轧余率为65-85％，在85℃下烘干；
(4)将经步骤(3)抗皱整理后的织物浸入到防螨整理液中一浸一轧，浸轧液位70％，轧余率为70-80％，在100℃下烘干，得到整理后的织物。
进一步地，所述的步骤(1)中，备取原料的重量份数为：亲水性氨基硅油25份、烷基酚聚氧乙烯醚15份、烷基苯磺酸钠8份、碳酸氢钠2份、丙烯酸1份、三乙醇胺硼酸酯2份、次亚磷酸钠5份、乙醇12份、去离子水115份。
进一步地，所述的步骤(2)中，备取原料的重量份数为：麝香草酚12份、水溶性壳聚糖季铵盐20份、聚丙烯酸钠8份、硫酸钠2份、甲基正壬基酮3份、去离子水100份。
进一步地，所述的步骤(3)中，轧余率为75％。
进一步地，所述的步骤(4)中，轧余率为75％。
与现有技术相比，本发明具备的优点为：本发明的织物抗皱防螨整理方法具有良好的无醛环保性，穿着安全、健康；经本发明整理方法整理得到的织物干、湿折皱回复角(度)增加30％以上，皂洗40次后折皱回复角度基本不变；经本发明整理方法整理得到的织物具有良好的防螨和杀菌能力，安全无残留，且具有天然的植物气味，织物的螨虫驱避率高达90％以上。
具体实施方式
下面结合具体实施例对本发明做进一步的说明。
实施例1：一种抗皱防螨织物整理方法，其包括以下步骤：
(1)抗皱整理液的配制：分别备取以下重量份数的原料，亲水性氨基硅油25份、烷基酚聚氧乙烯醚15份、烷基苯磺酸钠8份、碳酸氢钠2份、丙烯酸1份、三乙醇胺硼酸酯2份、次亚磷酸钠5份、乙醇12份、去离子水115份，将上述原料于50～70℃下混合均匀，冷却后为抗皱整理液；
(2)防螨整理液的配制：分别备取以下重量份数的原料，麝香草酚12份、水溶性壳聚糖季铵盐20份、聚丙烯酸钠8份、硫酸钠2份、甲基正壬基酮3份、去离子水100份，将上述原料常温下充分混合均匀，得到防螨整理液；
(3)取棉麻织物，将纯棉织物浸入到抗皱整理液中，50℃下浸泡1h，两浸两轧，浸轧余率为75％，在85℃下烘干；
(4)将经步骤(3)抗皱整理后的织物浸入到防螨整理液中一浸一轧，浸轧液位70％，轧余率为75％，在100℃下烘干，得到整理后的织物。
采用本实施例方法整理的纯棉织物的抗皱回复角为275，按照农药检(生测)函2003年45号《灭螨和驱螨药效试验方法和评价标准》检测采用本实施例方法整理的纯棉织物的螨虫驱避率达到98％。
实施例2：一种抗皱防螨织物整理方法，其包括以下步骤：
(1)抗皱整理液的配制：分别备取以下重量份数的原料，亲水性氨基硅油20份、烷基酚聚氧乙烯醚12份、烷基苯磺酸钠5份、碳酸氢钠1份、丙烯酸0.5份、三乙醇胺硼酸酯1份、次亚磷酸钠3份、乙醇10份、去离子水100份，将上述原料于50℃下混合均匀，冷却后为抗皱整理液；
(2)防螨整理液的配制：分别备取以下重量份数的原料，麝香草酚10份、水溶性壳聚糖季铵盐15份、聚丙烯酸钠5份、硫酸钠1份、甲基正壬基酮2份、去离子水80份，将上述原料常温下充分混合均匀，得到防螨整理液；
(3)取棉麻织物，将纯棉织物浸入到抗皱整理液中，50℃下浸泡0.5h，两浸两轧，轧余率为65％，在85℃下烘干；
(4)将经步骤(3)抗皱整理后的织物浸入到防螨整理液中一浸一轧，浸轧液位70％，轧余率为70％，在100℃下烘干，得到整理后的织物。
采用本实施例方法整理的纯棉织物的抗皱回复角为249，按照农药检(生测)函2003年45号《灭螨和驱螨药效试验方法和评价标准》检测采用本实施例方法整理的纯棉织物的螨虫驱避率达到95％。
实施例3：一种抗皱防螨织物整理方法，其包括以下步骤：
(1)抗皱整理液的配制：分别备取以下重量份数的原料，亲水性氨基硅油30份、烷基酚聚氧乙烯醚18份、烷基苯磺酸钠10份、碳酸氢钠3份、丙烯酸1.5份、三乙醇胺硼酸酯3份、次亚磷酸钠6份、乙醇15份、去离子水130份，将上述原料于70℃下混合均匀，冷却后为抗皱整理液；
(2)防螨整理液的配制：分别备取以下重量份数的原料，麝香草酚15份、水溶性壳聚糖季铵盐25份、聚丙烯酸钠10份、硫酸钠3份、甲基正壬基酮4份、去离子水120份，将上述原料常温下充分混合均匀，得到防螨整理液；
(3)取棉麻织物，将纯棉织物浸入到抗皱整理液中，50℃下浸泡2h，两浸两轧，轧余率为85％，在85℃下烘干；
(4)将经步骤(3)抗皱整理后的织物浸入到防螨整理液中一浸一轧，浸轧液位70％，轧余率为80％，在100℃下烘干，得到整理后的织物。
采用本实施例方法整理的纯棉织物的抗皱回复角为264，按照农药检(生测)函2003年45号《灭螨和驱螨药效试验方法和评价标准》检测采用本实施例方法整理的纯棉织物的螨虫驱避率达到96％。
实施例4：一种抗皱防螨织物整理方法，其包括以下步骤：
(1)抗皱整理液的配制：分别备取以下重量份数的原料，亲水性氨基硅油30份、烷基酚聚氧乙烯醚12份、烷基苯磺酸钠10份、碳酸氢钠1份、丙烯酸1.5份、三乙醇胺硼酸酯1份、次亚磷酸钠6份、乙醇10份、去离子水130份，将上述原料于50℃下混合均匀，冷却后为抗皱整理液；
(2)防螨整理液的配制：分别备取以下重量份数的原料，麝香草酚15份、水溶性壳聚糖季铵盐15份、聚丙烯酸钠10份、硫酸钠1份、甲基正壬基酮4份、去离子水80份，将上述原料常温下充分混合均匀，得到防螨整理液；
(3)取棉麻织物，将纯棉织物浸入到抗皱整理液中，50℃下浸泡2h，两浸两轧，轧余率为65％，在85℃下烘干；
(4)将经步骤(3)抗皱整理后的织物浸入到防螨整理液中一浸一轧，浸轧液位70％，轧余率为75％，在100℃下烘干，得到整理后的织物。
采用本实施例方法整理的纯棉织物的抗皱回复角为251，按照农药检(生测)函2003年45号《灭螨和驱螨药效试验方法和评价标准》检测采用本实施例方法整理的纯棉织物的螨虫驱避率达到92％。
实施例5：一种抗皱防螨织物整理方法，其包括以下步骤：
(1)抗皱整理液的配制：分别备取以下重量份数的原料，亲水性氨基硅油28份、烷基酚聚氧乙烯醚14份、烷基苯磺酸钠9份、碳酸氢钠2份、丙烯酸1.2份、三乙醇胺硼酸酯2份、次亚磷酸钠4份、乙醇14份、去离子水120份，将上述原料于65℃下混合均匀，冷却后为抗皱整理液；
(2)防螨整理液的配制：分别备取以下重量份数的原料，麝香草酚14份、水溶性壳聚糖季铵盐18份、聚丙烯酸钠9份、硫酸钠2份、甲基正壬基酮4份、去离子水90份，将上述原料常温下充分混合均匀，得到防螨整理液；
(3)取棉麻织物，将纯棉织物浸入到抗皱整理液中，50℃下浸泡100min，两浸两轧，轧余率为70％，在85℃下烘干；
(4)将经步骤(3)抗皱整理后的织物浸入到防螨整理液中一浸一轧，浸轧液位70％，轧余率为75％，在100℃下烘干，得到整理后的织物。
采用本实施例方法整理的纯棉织物的抗皱回复角为261，按照农药检(生测)函2003年45号《灭螨和驱螨药效试验方法和评价标准》检测采用本实施例方法整理的纯棉织物的螨虫驱避率达到94％。

Claims (5)

1.一种抗皱防螨织物整理方法，其特征在于，包括以下步骤：
(1)抗皱整理液的配制：分别备取以下重量份数的原料，亲水性氨基硅油20～30份、烷基酚聚氧乙烯醚12～18份、烷基苯磺酸钠5～10份、碳酸氢钠1～3份、丙烯酸0.5～1.5份、三乙醇胺硼酸酯1～3份、次亚磷酸钠3～6份、乙醇10～15份、去离子水100～130份，将上述原料于50～70℃下混合均匀，冷却后为抗皱整理液；
(2)防螨整理液的配制：分别备取以下重量份数的原料，麝香草酚10～15份、水溶性壳聚糖季铵盐15～25份、聚丙烯酸钠5～10份、硫酸钠1～3份、甲基正壬基酮2～4份、去离子水80～120份，将上述原料常温下充分混合均匀，得到防螨整理液；
(3)取棉麻织物，将纯棉织物浸入到抗皱整理液中，50℃下浸泡0.5～2h，两浸两轧，轧余率为65-85％，在85℃下烘干；
(4)将经步骤(3)抗皱整理后的织物浸入到防螨整理液中一浸一轧，浸轧液位70％，轧余率为70-80％，在100℃下烘干，得到整理后的织物。
2.根据权利要求1所述的一种抗皱防螨织物整理方法，其特征在于：所述的步骤(1)中，备取原料的重量份数为：亲水性氨基硅油25份、烷基酚聚氧乙烯醚15份、烷基苯磺酸钠8份、碳酸氢钠2份、丙烯酸1份、三乙醇胺硼酸酯2份、次亚磷酸钠5份、乙醇12份、去离子水115份。
3.根据权利要求1所述的一种抗皱防螨织物整理方法，其特征在于：所述的步骤(2)中，备取原料的重量份数为：麝香草酚12份、水溶性壳聚糖季铵盐20份、聚丙烯酸钠8份、硫酸钠2份、甲基正壬基酮3份、去离子水100份。
4.根据权利要求1所述的一种抗皱防螨织物整理方法，其特征在于：所述的步骤(3)中，轧余率为75％。
5.根据权利要求1所述的一种抗皱防螨织物整理方法，其特征在于：所述的步骤(4)中，轧余率为75％。
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