CN108309862A - Pudilan whitening moisturizing face masque - Google Patents

Pudilan whitening moisturizing face masque Download PDF

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Publication number
CN108309862A
CN108309862A CN201810372226.2A CN201810372226A CN108309862A CN 108309862 A CN108309862 A CN 108309862A CN 201810372226 A CN201810372226 A CN 201810372226A CN 108309862 A CN108309862 A CN 108309862A
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Prior art keywords
extract
pudilan
whitening
moisturizing face
phases
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CN201810372226.2A
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CN108309862B (en
Inventor
曹龙祥
田刚
董自波
夏立武
许佳
蔡虎
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Jiangsu Pudilan Daily Chemical Co.,Ltd.
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JUMPCAN PHARMACEUTICAL GROUP Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

Abstract

The invention discloses a kind of Pudilan whitening moisturizing face masques, the facial mask is mainly by deionized water, polyglycereol 10, 1.2 pentanediol, beta glucan, EDETATE SODIUM, glycine betaine, allantoin, dipotassium glycyrrhizinate, carbomer, Sodium Hyaluronate, niacinamide, polyquaternium 51, triethanolamine, 1.3 butanediol, 60 rilanit specials of PEG, PHL, glycerol caprylate, essence, potassium hydroxide, citric acid, ascorbic acid glucoside, rose extract, Ginseng extract, Purslane extract, dandelion extract, Herba Violae extract, woaded blue root extract, radix scutellariae root extract, glycyrrhiza glabra root extract, reed fragrant plant oil is prepared;Pudilan whitening moisturizing face masque disclosed by the invention has and makes the whitening of skin nature, moisturizing and whitening effect outstanding feature, at the same have enrich blood foster the spirit of nobility, the alimentary health-care functions such as promoting blood circulation to remove blood stasis, more agree with current consumer and pursue natural skin care this consumption concept.

Description

Pudilan whitening moisturizing face masque
Technical field
The present invention relates to technical field of skin care more particularly to a kind of Pudilan whitening moisturizing face masques.
Background technology
Facial mask is a classification in skin care item, and most basic and most important purpose is to make up makeup removing and wash one's face still Right insufficient cleaning coordinates other essential ingredients to realize other maintenance functions, such as replenishing water and preserving moisture, U.S. on this basis In vain, anti-aging, Sage Extract etc..The principle of facial mask is temporarily isolating the external world exactly using the of short duration time for being covered in face Air and pollution, improve skin temperature, and the pore expansion of skin promotes sweat gland secretion and metabolism, makes the oxygen content of skin Rise, be conducive to the oil substances that skin excludes the product and accumulation of epidermal cell metabolism, the moisture in facial mask penetrates into The cuticula of epidermis, skin become soft, and skin is naturally bright flexible.
Melanin is a kind of biochrome, is that tyrosine forms DOPA under the action of tyrosinase, and then is oxidized to black Pigment is widely present in skin, mucous membrane, retina, pia mater and the gall-bladder and ovary etc. of people.The generation of melanin mostly with it is interior Dyssecretosis, solar radiation are related, and the number of melanocyte depends primarily on heredity.Melanin is present in skin base layer Among cell, also referred to as chromoplast, chromoplast secretes Mai Laning pigments, when ultraviolet light is irradiated on skin, skin The state of " self-protection " is would be at, i.e., Mai Laning pigments is stimulated by ultraviolet light, the activity of tyrosinase is activated, to protect me Skin Cell.DOPA is exactly the predecessor of melanin in fact, is formed through oxidizing tyrosine, releases melanin, melanin is again Via moving layer by layer for cell metabolism, skin epidermis is arrived and has formed freckle, sunburn, blackspot etc..
It is read because the tradition of " a white screening three is ugly " is beautiful, Asia women has whitening persistent pursuit.Whitening can be from The following aspects carries out:1, inhibit the activity of TYR enzyme needed for melanin production, to inhibit the generation of melanin, still It needs to penetrate into the effect of skin bottom competence exertion;2, melanin is inhibited to be transported to horn cell from melanocyte, such as dimension life Plain B3;3, skin darkening generates spot, is the process of skin oxidation in itself, and vitamin C and its derivative known to us are Strong anti-oxidant small bodyguard, it can restore back oxidized process, inhibit the oxidation reaction of melanin;4. generation Thank to melanin, the cuticula excessive by peeling off skin makes skin newborn to which melanin is taken away from skin.
Whitening mask refers to being added to promote melanin metabolism, inhibit and destroy melanin production, prevent tyrosine Enzyme activation or the facial mask for restoring melanin intermediates and other functional ingredient.The process of whitening is also skin renewal and clean mistake in fact Journey, and the cuticula for getting rid of aging can allow skin to become drying, and dry skin is easy to generate melanin, institute To need to supplement the nutrients in time and moisture, moisturizing could also say that the basic homework that any skin quality is required for doing.And existing U.S. Fine flour film usually all focuses on ingredient of the addition with white-skinned face function, and has ignored the importance of moisturizing, merely by addition Some moisturizer carry out moisturizing, such as Natrulon H-10, butanediol, propylene glycol, although the 15- that these moisturizer are used in facial mask There is in 25min certain replenishing water and preserving moisture effect, but facial mask after use, these ingredients can largely be flush with water stream Lose, can not lasting moisturizing in the follow-up process, cause white-skinned face function to reduce, and existing whitening mask whitening mode is more single, Whitening effect is poor.Also, presently commercially available facial treatment mask type is more, but it is to pursue a certain effect to have many facial masks, past There are the chemical substance or hormone of larger stimulation to skin toward some are added, sugared skin such as is added to pursue short-term freckle effect Matter hormone, long-time service can lead to telangiectasis, and skin contraction, forming side effects, some such as skin dependence dermatitis is It pursues short-term whitening effect to be added in facial mask containing heavy metals such as lead, mercury, arsenic, although short run effect is notable, be used for a long time It can make one neurasthenia, weak, anorexia, diplopia, expiratory dyspnea etc..Therefore providing one kind not only having skin whitening, moisturizing effect, It is healthy and beneficial to human body simultaneously to pursue natural skin care this consumption such as the facial mask with healthcare function to agree with current consumer Theory be very it is necessary to.
A kind of skin whitening, moisturizing tencel facial mask essence containing lecithin is disclosed in Chinese patent application 201410268341.7 Skin whitening, moisturizing Essence containing lecithin is stored in tencel (TENCEL) facial mask cloth by liquid, and Essence coordinates facial mask cloth soft Soft sticking nature, gas permeability and comfort do not have nutritional health function only up to the effect for keeping skin whitening, moisturizing better, Its cold-resistant heat resistance is poor simultaneously;Disclosed in Chinese patent application 201711050700.1 a kind of whitening moisturizing face masque and its Preparation method, disclosed facial mask only can whitening effect skin, moisturizings, moreover it is possible to lighten the stain, desalinate microgroove, make for a long time With skin smooth, delicacy and high resilience can be made, but it equally exists cold-resistant heat resistance equistability difference and is protected without nutrition The problem of strong effect.
Based on above-mentioned realistic problem, those skilled in the art are dedicated to disclosing a kind of Pudilan whitening moisturizing face masque, to reach Have the effect of making skin nature whitening and enriching blood to foster the spirit of nobility simultaneously to it, the alimentary health-care functions such as promoting blood circulation to remove blood stasis, the present invention is thus It generates.
Invention content
Present invention aims at providing a kind of Pudilan whitening moisturizing face masque, having to reach the facial mask makes skin natural beauty In vain, moisturizing and whitening effect outstanding feature, can be simultaneously reached the facial mask have enrich blood foster the spirit of nobility, the nutrition and health cares such as promoting blood circulation to remove blood stasis Function and cold resistance and the good purpose of heat resistance stability make it more agree with current consumer and pursue natural skin care this disappears Take theory.
Involved in the present invention to term " PHL " be the U.S. whole world INOLEX Ying Dishi Specialty Chemicals product, Its trade name SpectrastatTMPHL, specific ingredient are decoyl hydroximic acid, 1,2 hexylene glycols and 1,3 propylene glycol.
To achieve the goals above, the present invention provides following technical solutions:
It is heretofore described rose extract, Ginseng extract, Purslane extract, dandelion extract, pale reddish brown Chinese violet extract, woaded blue root extract, radix scutellariae root extract and glycyrrhiza glabra root extract are normal by those skilled in the art What physical extracting method obtained.
A kind of Pudilan whitening moisturizing face masque, it is characterised in that:The Pudilan whitening moisturizing face masque is by following weight Content at being grouped as:Natrulon H-10 0.5-3%, 1.2- pentanediol 0.5-3%, beta glucan 0.5-2%, EDETATE SODIUM 0.01-0.08%, glycine betaine 0.3-2%, allantoin 0.01-0.1%, dipotassium glycyrrhizinate 0.01-0.15%, carbomer 0.05- 0.8%, Sodium Hyaluronate 0.005-0.08%, niacinamide 1-5%, -51 0.05-0.6% of polyquaternium, triethanolamine 0.1- 0.5%, 1.3 butanediol 2-10%, PEG-60 rilanit special 0.05-0.5%, PHL 0.15-0.95%, glycerol caprylate 0.01-0.1%, essence 0.001-0.025%, potassium hydroxide 0.01-0.1%, citric acid 0.01-0.12%, ascorbic acid Portugal Glucosides 0.1-0.5%, rose extract 0.01-0.1%, Ginseng extract 0.01-0.1%, Purslane extract 0.01- 0.1%, dandelion extract 0.0005-0.0025%, Herba Violae extract 0.0005-0.0025%, woaded blue root extract 0.0005-0.0025%, glycyrrhiza glabra root extract 0.00005-0.00025%, reed fragrant plant oil 0.1-1.5%, scutellariae,radix extraction Object 0.005-0.03% and water surplus.
Further, the Pudilan whitening moisturizing face masque by following weight content at being grouped as:Natrulon H-10 1-2.5%, 1.2- pentanediol 1-2.5%, beta glucan 0.8-1.5%, EDETATE SODIUM 0.02-0.04%, glycine betaine 0.7- 1.3%, allantoin 0.03-0.08%, dipotassium glycyrrhizinate 0.03-0.1%, carbomer 0.1-0.3%, Sodium Hyaluronate 0.01- 0.03%, niacinamide 1.5-3.5%, -51 0.1-0.3% of polyquaternium, triethanolamine 0.15-0.3%, 1.3 butanediol 4- 8%, PEG-60 rilanit specials 0.15-0.25%, PHL 0.4-0.8%, glycerol caprylate 0.03-0.08%, essence 0.005-0.015%, potassium hydroxide 0.03-0.08%, citric acid 0.02-0.08%, ascorbic acid glucoside 0.15- 0.35%, rose extract 0.05-0.07%, Ginseng extract 0.04-0.07%, Purslane extract 0.05-0.08%, Dandelion extract 0.0008-0.0015%, Herba Violae extract 0.001-0.002%, woaded blue root extract 0.001- 0.0018%, glycyrrhiza glabra root extract 0.00008-0.00012%, reed fragrant plant oil 0.3-1%, radix scutellariae root extract 0.008- 0.015% and water surplus.
Further, the one kind or several of the carbomer in carbomer 934, Acritamer 940 and Carbopol 941 Kind.
Water typically serves to the effect of solvent in the ingredient that this field prepares whitening moisturizing face masque.
Natrulon H-10,1.2- pentanediols, beta glucan, glycine betaine, Sodium Hyaluronate, polyquaternium -51 and 1.3 fourths two Alcohol typically serves to the effect of moisturizer, moisturizer commonly used in the art in the ingredient that this field prepares whitening moisturizing face masque Also amino acid, collagen and PCA- sodium.
EDETATE SODIUM typically serves to the effect of chelating agent in the ingredient that this field prepares whitening moisturizing face masque.
Allantoin, dipotassium glycyrrhizinate, Flos Rosae Rugosae extract, ginseng extract, purslane extract, dandelion extract, Reed fragrant plant oil and radix scutellariae root extract typically serve to the work of skin conditioning agent in the ingredient that this field prepares whitening moisturizing face masque With.
Carbomer typically serves to the effect of thickener in the ingredient that this field prepares whitening moisturizing face masque, in this field Common thickener also has xanthans, cellulose.
Triethanolamine, potassium hydroxide and citric acid typically serve to PH in the ingredient that this field prepares whitening moisturizing face masque The effect of conditioning agent.
Niacinamide, ascorbic acid glucoside and glycyrrhiza glabra root extract prepare the ingredient of whitening moisturizing face masque in this field In, typically serve to the effect of whitening agent.
PEG-60 rilanit specials typically serve to the work of solubilizer in the ingredient that this field prepares whitening moisturizing face masque With.
PHL and glycerol caprylate typically serve to the effect of preservative in the ingredient that this field prepares whitening moisturizing face masque, Preservative commonly used in the art also has benzoic acid and sorbic acid.
A kind of preparation method of above-mentioned Pudilan whitening moisturizing face masque, includes the following steps:
(1) by Natrulon H-10 0.5-3%, 1.2- pentanediol 0.5-3% of weight content, beta glucan 0.5-2%, EDETATE SODIUM 0.01-0.08%, glycine betaine 0.3-2%, allantoin 0.01-0.1%, dipotassium glycyrrhizinate 0.01-0.15%, card wave Breast is added in nurse 0.05-0.8%, Sodium Hyaluronate 0.005-0.08%, niacinamide 1-5% and -51 0.05-0.6% of polyquaternium Change in pot, is heated to 60-90 DEG C, dissolving of blunging is denoted as A phases;
(2) by 1.3 butanediol 2-10%, PEG-60 rilanit special 0.05-0.5%, PHL 0.15- of weight content 0.95%, glycerol caprylate 0.01-0.1%, essence 0.001-0.025% and glycyrrhiza glabra root extract 0.00005- 0.00025% is stirred to being completely dispersed, and is denoted as B phases, spare;
(3) by the potassium hydroxide 0.01-0.1% of weight content, citric acid 0.01-0.12% and ascorbic acid glucoside 0.1-0.5% water dissolutions stir to being completely dispersed, are denoted as C phases, spare;
(4) the A phases of gained in step (1) are stirred and is cooled to 30-70 DEG C, then by the triethanolamine 0.1- of weight content 0.5% input emulsification pot, homogeneous mixing, then by obtained by the B phases and step (3) of gained in step (2) C phases and weight contain The rose extract 0.05-0.07% of amount, Ginseng extract 0.04-0.07%, Purslane extract 0.05-0.08%, Pu Public English extract 0.0008-0.0015%, Herba Violae extract 0.001-0.002%, woaded blue root extract 0.001- 0.0018%, reed fragrant plant oil 0.1-1.5% and radix scutellariae root extract 0.005-0.03% is put into one by one in emulsification pot pot, more than addition Water is measured to 100%, obtains mixture D;
(5) the mixture D stirring obtained by step (4) is cooled to 10-50 DEG C, and vacuumizes degassing, filtering, when discharging adopts Sample does the inspection of semifinished product;
(6) carried out by measure with bottle placer after the inspection of semifinished product qualification obtained by step (5) it is filling, in assembly line upper cover bottle Lid fills firework, then fills outer container;
(7) packaging is dispatched from the factory after completing after product inspection qualification.
Heating temperature in the step (1) is preferably 70-80 DEG C.
Further, the A phases obtained by step (1) are stirred in the step (4) and is cooled to 40-60 DEG C.
Further, the mixture D stirring obtained by step (4) is cooled to 20-40 DEG C in the step (5).
Beneficial effects of the present invention are:Heretofore described Pudilan whitening moisturizing face masque, Chinese tradition Chinese medicine is managed It is organically combined by with facial mask, it is professional and both effectiveness that its is protruded compared with traditional facial mask.Heretofore described Pudilan Whitening moisturizing face masque has and makes the whitening of skin nature, moisturizing and whitening effect outstanding feature, while having to enrich blood and fosters the spirit of nobility, invigorates blood circulation Dissipate alimentary health-care functions and the good cold resistance and heat resistance stability such as the stasis of blood;Product imparts plant skin care this concept, More agree with current consumer and pursues natural skin care this consumption concept.
Description of the drawings
Fig. 1 is a kind of production technology schematic diagram of Pudilan whitening moisturizing face masque.
Specific embodiment
The present invention can further be well understood by specific examples presented below, but they are not to the present invention Restriction.
The carbomer used in 1-17 of the embodiment of the present invention and comparative example 1-9 is Carbopol 941.
Rose extract, Ginseng extract in the embodiment of the present invention, Purslane extract, dandelion extract, purple Flower Chinese violet extract, woaded blue root extract, radix scutellariae root extract and glycyrrhiza glabra root extract are produced by the following method, It is as follows:
(1) respectively by rose, ginseng, purslane, dandelion, Chinese violet, woaded blue root, scutellariae,radix and glycyrrhiza glabra root It weighs, dry, pulverize, with 90-95% ethanol percolations, be percolated 3-4 hours, ethanol filtrate, the dregs of a decoction is taken to retain, filtrate decompression recycling Ethyl alcohol obtains concentrate 1 to no alcohol taste.
(2) respectively by the rose obtained by step (1), ginseng, purslane, dandelion, Chinese violet, woaded blue root, radix scutellariae The water of 10 times of amounts is added in root and the glycyrrhiza glabra root dregs of a decoction, boils 1 hour, extracts 2 times, merging filtrate, but to 40 DEG C hereinafter, must filter Liquid 2;By chelate resin column on filtrate 2, the feed liquid in resin is cemented out with 7% sodium chloride solution after upper prop, Efflux is collected, is recovered under reduced pressure, specific gravity control obtains concentrate 2 in 1.08-1.1.
(3) it is spray-dried, obtains after mixing the concentrate 1 obtained by above-mentioned steps (1) and the concentrate 2 obtained by step (2) Rose extract, Ginseng extract, Purslane extract, dandelion extract, Herba Violae extract, the extraction of woaded blue root Object, radix scutellariae root extract and glycyrrhiza glabra root extract.
A kind of 1 Pudilan whitening moisturizing face masque of embodiment is by following weight content at being grouped as:Natrulon H-10 2%, 1.2- pentanediols 2%, beta glucan 1%, EDETATE SODIUM 0.03%, glycine betaine 1%, allantoin 0.05%, dipotassium glycyrrhizinate 0.05%, carbomer 0.2%, Sodium Hyaluronate 0.02%, niacinamide 2.5%, polyquaternium -51 0.2%, triethanolamine 0.25%, 1.3 butanediols 6%, PEG-60 rilanit specials 0.2%, PHL 0.6%, glycerol caprylate 0.05%, essence 0.01%, potassium hydroxide 0.05%, citric acid 0.04%, ascorbic acid glucoside 0.22%, rose extract 0.06%, people Join extracting solution 0.05%, Purslane extract 0.07%, dandelion extract 0.001%, Herba Violae extract 0.0015%, woaded blue root extract 0.0015%, glycyrrhiza glabra root extract 0.0001%, reed fragrant plant oil 0.5%, scutellariae,radix extraction Object 0.01% and water surplus.
The preparation method of above-mentioned Pudilan whitening moisturizing face masque, includes the following steps:
(1) by the Natrulon H-10 of weight content 2%, 1.2- pentanediols 2%, beta glucan 1%, EDETATE SODIUM 0.03%, glycine betaine 1%, allantoin 0.05%, dipotassium glycyrrhizinate 0.05%, carbomer 0.2%, Sodium Hyaluronate 0.02%, Niacinamide 2.5% and polyquaternium -51 0.2% are added in emulsification pot, are heated to 75 DEG C, dissolving of blunging is denoted as A phases;
(2) by 1.3 butanediols 6% of weight content, PEG-60 rilanit specials 0.2%, PHL 0.6%, glycerine octanoic acid Ester 0.05%, essence 0.01% and glycyrrhiza glabra root extract 0.0001% are stirred to being completely dispersed, and are denoted as B phases, spare;
(3) by the potassium hydroxide of weight content 0.05%, citric acid 0.04%, ascorbic acid glucoside 0.22% with water-soluble Solution stirs to being completely dispersed, is denoted as C phases, spare;
(4) the A phases of gained in step (1) are stirred and is cooled to 50 DEG C, then by the triethanolamine of weight content 0.25% Input emulsification pot, homogeneous mixing, then by the rose of C phases and weight content obtained by the B phases and step (3) of gained in step (2) It is rare colored extracting solution 0.06%, Ginseng extract 0.05%, Purslane extract 0.07%, dandelion extract 0.001%, pale reddish brown Chinese violet extract 0.0015%, woaded blue root extract 0.0015%, reed fragrant plant oil 0.5% and radix scutellariae root extract 0.01% are one by one In input emulsification pot pot, excess water is added to 100%, obtains mixture D;
(5) the mixture D stirring obtained by step (4) is cooled to 30 DEG C, and vacuumizes degassing, filtering, when discharging samples Do the inspection of semifinished product;
(6) carried out by measure with bottle placer after the inspection of semifinished product qualification obtained by step (5) it is filling, in assembly line upper cover bottle Lid fills firework, then fills outer container;
(7) packaging is dispatched from the factory after completing after product inspection qualification.
A kind of 2 Pudilan whitening moisturizing face masque of embodiment is by following weight content at being grouped as:Natrulon H-10 1%, 1.2- pentanediols 1%, beta glucan 0.8%, EDETATE SODIUM 0.02%, glycine betaine 0.7%, allantoin 0.03%, glycyrrhizic acid two Potassium 0.03%, carbomer 0.1%, Sodium Hyaluronate 0.01%, niacinamide 1.5%, polyquaternium -51 0.1%, triethanolamine 0.15%, 1.3 butanediols 4%, PEG-60 rilanit specials 0.15%, PHL 0.4%, glycerol caprylate 0.03%, essence 0.005%, potassium hydroxide 0.03%, citric acid 0.02%, ascorbic acid glucoside 0.15%, rose extract 0.05%, Ginseng extract 0.04%, Purslane extract 0.05%, dandelion extract 0.0008%, Herba Violae extract 0.001%, woaded blue root extract 0.001%, glycyrrhiza glabra root extract 0.00008%, reed fragrant plant oil 0.3%, scutellariae,radix extraction Object 0.008% and water surplus.
The preparation method of above-mentioned Pudilan whitening moisturizing face masque, includes the following steps:
(1) by the Natrulon H-10 of weight content 1%, 1.2- pentanediols 1%, beta glucan 0.8%, EDTA disodiums 0.02%, glycine betaine 0.7%, allantoin 0.03%, dipotassium glycyrrhizinate 0.03%, carbomer 0.1%, Sodium Hyaluronate 0.01%, niacinamide 1.5%, polyquaternium -51 0.1% are added in emulsification pot, are heated to 75 DEG C, dissolving of blunging is denoted as A phases;
(2) by 1.3 butanediols 4% of weight content, PEG-60 rilanit specials 0.15%, PHL 0.4%, glycerine octanoic acid Ester 0.03%, essence 0.005% and glycyrrhiza glabra root extract 0.00008% are stirred to being completely dispersed, and are denoted as B phases, standby With;
(3) by the potassium hydroxide of weight content 0.03%, citric acid 0.02%, ascorbic acid glucoside 0.15% with water-soluble Solution stirs to being completely dispersed, is denoted as C phases, spare;
(4) the A phases of gained in step (1) are stirred and is cooled to 50 DEG C, then by the triethanolamine of weight content 0.15% Input emulsification pot, homogeneous mixing, then by the rose of C phases and weight content obtained by the B phases and step (3) of gained in step (2) Rare colored extracting solution 0.05%, Ginseng extract 0.04%, Purslane extract 0.05%, dandelion extract 0.0008%, purple Flower Chinese violet extract 0.001%, woaded blue root extract 0.001%, reed fragrant plant oil 0.3% and radix scutellariae root extract 0.008% are one by one In input emulsification pot pot, excess water is added to 100%, obtains mixture D;
(5) the mixture D stirring obtained by step (4) is cooled to 30 DEG C, and vacuumizes degassing, filtering, when discharging samples Do the inspection of semifinished product;
(6) carried out by measure with bottle placer after the inspection of semifinished product qualification obtained by step (5) it is filling, in assembly line upper cover bottle Lid fills firework, then fills outer container;
(7) packaging is dispatched from the factory after completing after product inspection qualification.
A kind of 3 Pudilan whitening moisturizing face masque of embodiment is by following weight content at being grouped as:Natrulon H-10 2.5%, 1.2- pentanediols 2.5%, beta glucan 1.5%, EDETATE SODIUM 0.04%, glycine betaine 1.3%, allantoin 0.08%, Dipotassium glycyrrhizinate 0.1%, carbomer 0.3%, Sodium Hyaluronate 0.03%, niacinamide 3.5%, polyquaternium -51 0.3%, three Ethanol amine 0.3%, 1.3 butanediols 8%, PEG-60 rilanit specials 0.25%, PHL 0.8%, glycerol caprylate 0.08%, Essence 0.015%, potassium hydroxide 0.08%, citric acid 0.08%, ascorbic acid glucoside 0.35%, rose extract 0.07%, Ginseng extract 0.07%, Purslane extract 0.08%, dandelion extract 0.0015%, Chinese violet extraction Object 0.002%, woaded blue root extract 0.0018%, glycyrrhiza glabra root extract 0.00012%, reed fragrant plant oil 1%, scutellariae,radix carry Take object 0.015% and water surplus.
The preparation method of above-mentioned Pudilan whitening moisturizing face masque, includes the following steps:
(1) by the Natrulon H-10 of weight content 2.5%, 1.2- pentanediols 2.5%, beta glucan 1.5%, EDTA bis- Sodium 0.04%, glycine betaine 1.3%, allantoin 0.08%, dipotassium glycyrrhizinate 0.1%, carbomer 0.3%, Sodium Hyaluronate 0.03%, niacinamide 3.5%, polyquaternium -51 0.3% are added in emulsification pot, are heated to 75 DEG C, dissolving of blunging is denoted as A phases;
(2) by 1.3 butanediols 8% of weight content, PEG-60 rilanit specials 0.25%, PHL 0.8%, glycerine octanoic acid Ester 0.08%, essence 0.015% and glycyrrhiza glabra root extract 0.00012% are stirred to being completely dispersed, and are denoted as B phases, standby With;
(3) by the potassium hydroxide of weight content 0.08%, citric acid 0.08%, ascorbic acid glucoside 0.35% with water-soluble Solution stirs to being completely dispersed, is denoted as C phases, spare;
(4) the A phases of gained in step (1) are stirred and is cooled to 50 DEG C, then throw the triethanolamine of weight content 0.3% Enter and emulsifies pot, homogeneous mixing, then by the rose of C phases and weight content obtained by the B phases and step (3) of gained in step (2) It is flower extracting solution 0.07%, Ginseng extract 0.07%, Purslane extract 0.08%, dandelion extract 0.0015%, pale reddish brown Chinese violet extract 0.002%, woaded blue root extract 0.0018%, reed fragrant plant oil 1%, radix scutellariae root extract 0.015% are put into one by one It emulsifies in pot pot, excess water is added to 100%, obtains mixture D;
(5) the mixture D stirring obtained by step (4) is cooled to 30 DEG C, and vacuumizes degassing, filtering, when discharging samples Do the inspection of semifinished product;
(6) carried out by measure with bottle placer after the inspection of semifinished product qualification obtained by step (5) it is filling, in assembly line upper cover bottle Lid fills firework, then fills outer container;
(7) packaging is dispatched from the factory after completing after product inspection qualification.
A kind of 4 Pudilan whitening moisturizing face masque of embodiment is by following weight content at being grouped as:Natrulon H-10 0.5%, 1.2- pentanediols 0.5%, beta glucan 0.5%, EDETATE SODIUM 0.01%, glycine betaine 0.3%, allantoin 0.01%, Dipotassium glycyrrhizinate 0.01%, carbomer 0.05%, Sodium Hyaluronate 0.005%, niacinamide 1%, polyquaternium -51 0.05%, Triethanolamine 0.1%, 1.3 butanediols 2%, PEG-60 rilanit specials 0.05%, PHL 0.15%, glycerol caprylate 0.01%, essence 0.001%, potassium hydroxide 0.01%, citric acid 0.01%, ascorbic acid glucoside 0.1%, rose extraction Liquid 0.01%, Ginseng extract 0.01%, Purslane extract 0.01%, dandelion extract 0.0005%, Chinese violet carry Take object 0.0005%, woaded blue root extract 0.0005%, glycyrrhiza glabra root extract 0.00005%, reed fragrant plant oil 0.1%, radix scutellariae Root extract 0.005% and water surplus.
The preparation method of above-mentioned Pudilan whitening moisturizing face masque, includes the following steps:
(1) by the Natrulon H-10 of weight content 0.5%, 1.2- pentanediols 0.5%, beta glucan 0.5%, EDTA bis- Sodium 0.01%, glycine betaine 0.3%, allantoin 0.01%, dipotassium glycyrrhizinate 0.01%, carbomer 0.05%, Sodium Hyaluronate 0.005%, niacinamide 1%, polyquaternium -51 0.05% are added in emulsification pot, are heated to 75 DEG C, dissolving of blunging is denoted as A phases;
(2) by 1.3 butanediols 2%, PEG-60 rilanit specials 0.05%, PHL 0.15%, the caprylic of weight content Acid esters 0.01%, essence 0.001% and glycyrrhiza glabra root extract 0.00005% are stirred to being completely dispersed, and are denoted as B phases, It is spare;
(3) by the potassium hydroxide of weight content 0.01%, citric acid 0.01%, ascorbic acid glucoside 0.1% with water-soluble Solution stirs to being completely dispersed, is denoted as C phases, spare;
(4) the A phases of gained in step (1) are stirred and is cooled to 50 DEG C, then throw the triethanolamine of weight content 0.1% Enter and emulsifies pot, homogeneous mixing, then by the rose of C phases and weight content obtained by the B phases and step (3) of gained in step (2) It is flower extracting solution 0.01%, Ginseng extract 0.01%, Purslane extract 0.01%, dandelion extract 0.0005%, pale reddish brown Chinese violet extract 0.0005%, woaded blue root extract 0.0005%, reed fragrant plant oil 0.1%, radix scutellariae root extract 0.005% are one by one In input emulsification pot pot, excess water is added to 100%, obtains mixture D;
(5) the mixture D stirring obtained by step (4) is cooled to 30 DEG C, and vacuumizes degassing, filtering, when discharging samples Do the inspection of semifinished product;
(6) carried out by measure with bottle placer after the inspection of semifinished product qualification obtained by step (5) it is filling, in assembly line upper cover bottle Lid fills firework, then fills outer container;
(7) packaging is dispatched from the factory after completing after product inspection qualification.
A kind of 5 Pudilan whitening moisturizing face masque of embodiment is by following weight content at being grouped as:Natrulon H-10 3%, 1.2- pentanediols 3%, beta glucan 2%, EDETATE SODIUM 0.08%, glycine betaine 2%, allantoin 0.1%, dipotassium glycyrrhizinate 0.15%, carbomer 0.8%, Sodium Hyaluronate 0.08%, niacinamide 5%, polyquaternium -51 0.6%, triethanolamine 0.5%, 1.3 butanediols 10%, PEG-60 rilanit specials 0.5%, PHL 0.95%, glycerol caprylate 0.1%, essence 0.025%, potassium hydroxide 0.1%, citric acid 0.12%, ascorbic acid glucoside 0.5%, rose extract 0.1%, ginseng Extracting solution 0.1%, Purslane extract 0.1%, dandelion extract 0.0025%, Herba Violae extract 0.0025%, ancient name for Chinese cabbage Blue root extract 0.0025%, glycyrrhiza glabra root extract 0.00025%, reed fragrant plant oil 1.5%, 0.03% and of radix scutellariae root extract Water surplus.
The preparation method of above-mentioned Pudilan whitening moisturizing face masque, includes the following steps:
(1) by the Natrulon H-10 of weight content 3%, 1.2- pentanediols 3%, beta glucan 2%, EDETATE SODIUM 0.08%, glycine betaine 2%, allantoin 0.1%, dipotassium glycyrrhizinate 0.15%, carbomer 0.8%, Sodium Hyaluronate 0.08%, cigarette Amide 5%, polyquaternium -51 0.6% are added in emulsification pot, are heated to 75 DEG C, dissolving of blunging is denoted as A phases;
(2) by 1.3 butanediols 10%, PEG-60 rilanit specials 0.5%, PHL 0.95%, the caprylic of weight content Acid esters 0.1%, essence 0.025% and glycyrrhiza glabra root extract 0.00025% are stirred to being completely dispersed, and are denoted as B phases, standby With;
(3) by the potassium hydroxide of weight content 0.1%, citric acid 0.12%, ascorbic acid glucoside 0.5% with water-soluble Solution stirs to being completely dispersed, is denoted as C phases, spare;
(4) the A phases of gained in step (1) are stirred and is cooled to 50 DEG C, then throw the triethanolamine of weight content 0.5% Enter and emulsifies pot, homogeneous mixing, then by the rose of C phases and weight content obtained by the B phases and step (3) of gained in step (2) It is flower extracting solution 0.1%, Ginseng extract 0.1%, Purslane extract 0.1%, dandelion extract 0.0025%, pale reddish brown Fourth extract 0.0025%, woaded blue root extract 0.0025%, reed fragrant plant oil 1.5%, radix scutellariae root extract 0.03% are put into one by one It emulsifies in pot pot, excess water is added to 100%, obtains mixture D;
(5) the mixture D stirring obtained by step (4) is cooled to 30 DEG C, and vacuumizes degassing, filtering, when discharging samples Do the inspection of semifinished product;
(6) carried out by measure with bottle placer after the inspection of semifinished product qualification obtained by step (5) it is filling, in assembly line upper cover bottle Lid fills firework, then fills outer container;
(7) packaging is dispatched from the factory after completing after product inspection qualification.
Embodiment 6
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque Heating temperature in step (1) is 70 DEG C.
Embodiment 7
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque Heating temperature in step (1) is 80 DEG C.
Embodiment 8
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque Heating temperature in step (1) is 60 DEG C.
Embodiment 9
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque Heating temperature in step (1) is 90 DEG C.
Embodiment 10
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque The A phases obtained by step (1) are stirred in step (4) and are cooled to 40 DEG C.
Embodiment 11
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque The A phases obtained by step (1) are stirred in step (4) and are cooled to 60 DEG C.
Embodiment 12
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque The A phases obtained by step (1) are stirred in step (4) and are cooled to 30 DEG C.
Embodiment 13
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque The A phases obtained by step (1) are stirred in step (4) and are cooled to 70 DEG C.
Embodiment 14
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque The mixture D stirring obtained by step (4) is cooled to 20 DEG C in step (5).
Embodiment 15
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque The mixture D stirring obtained by step (4) is cooled to 40 DEG C in step (5).
Embodiment 16
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque The mixture D stirring obtained by step (4) is cooled to 10 DEG C in step (5).
Embodiment 17
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque The mixture D stirring obtained by step (4) is cooled to 50 DEG C in step (5).
Comparative example 1
With embodiment only difference is that:The Pudilan whitening moisturizing face masque is by following weight content at grouping At:Natrulon H-10 0.3%, 1.2- pentanediols 0.3%, beta glucan 0.2%, EDETATE SODIUM 0.008%, glycine betaine 0.2%, Allantoin 0.008%, dipotassium glycyrrhizinate 0.008%, carbomer 0.03%, Sodium Hyaluronate 0.003%, niacinamide 0.8%, Polyquaternium -51 0.03%, triethanolamine 0.08%, 1.3 butanediols 1.7%, PEG-60 rilanit specials 0.03%, PHL0.1%, glycerol caprylate 0.008%, essence 0.0008%, potassium hydroxide 0.008%, citric acid 0.008%, Vitamin C Sour glucoside 0.08%, rose extract 0.008%, Ginseng extract 0.008%, Purslane extract 0.008%, Pu Gong English extract 0.0003%, Herba Violae extract 0.0003%, woaded blue root extract 0.0003%, glycyrrhiza glabra root extract 0.00003%, reed fragrant plant oil 0.08%, radix scutellariae root extract 0.003% and water surplus.
Comparative example 2
With embodiment only difference is that:The Pudilan whitening moisturizing face masque is by following weight content at grouping At:Natrulon H-10 5%, 1.2- pentanediols 6%, beta glucan 4%, EDETATE SODIUM 0.1%, glycine betaine 3%, allantoin 0.3%, dipotassium glycyrrhizinate 0.3%, carbomer 0.9%, Sodium Hyaluronate 0.1%, niacinamide 7%, polyquaternium -51 0.8%, triethanolamine 0.7%, 1.3 butanediols 12%, PEG-60 rilanit specials 0.8%, PHL 1%, glycerol caprylate 0.3%, essence 0.03%, potassium hydroxide 0.3%, citric acid 0.15%, ascorbic acid glucoside 0.7%, rose extract 0.3%, Ginseng extract 0.3%, Purslane extract 0.4%, dandelion extract 0.004%, Herba Violae extract 0.0035%, woaded blue root extract 0.004%, glycyrrhiza glabra root extract 0.0005%, reed fragrant plant oil 1.8%, scutellariae,radix extraction Object 0.05% and water surplus.
Comparative example 3
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque Heating temperature in step (1) is 50 DEG C.
Comparative example 4
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque Heating temperature in step (1) is 100 DEG C.
Comparative example 5
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque The A phases obtained by step (1) are stirred in step (4) and are cooled to 20 DEG C.
Comparative example 6
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque The A phases obtained by step (1) are stirred in step (4) and are cooled to 90 DEG C.
Comparative example 7
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque The mixture D stirring obtained by step (4) is cooled to 5 DEG C in step (5).
Comparative example 8
With embodiment 1 it is unique difference lies in:It is described in the preparation method of the Pudilan whitening moisturizing face masque The mixture D stirring obtained by step (4) is cooled to 60 DEG C in step (5).
Comparative example 9
With embodiment 1 only difference is that:The Pudilan whitening moisturizing face masque at being grouped as in, use amino Acid, collagen replace beta glucan, glycine betaine.
Comparative example 10
With embodiment 1 only difference is that:The Pudilan whitening moisturizing face masque at being grouped as in, the card Wave nurse is carbomer 934.
Comparative example 11
With embodiment 1 only difference is that:The Pudilan whitening moisturizing face masque at being grouped as in, the card Wave nurse is Acritamer 940.
Contrast test
Pudilan whitening moisturizing face masque made from 1-17 of the embodiment of the present invention, it is transparent (faint yellow) to estimate its appearance, nose It is mixing fruity to smell its fragrance, meets regulation fragrance, has good heat-resisting, cold resistance.
(1) the Pudilan whitening moisturizing face masque for using 1-5 of the embodiment of the present invention and comparative example 1-2 to prepare, to 20 18- 40 years old volunteers carry out facial application experiment, using 1h, 5h, 18h after the detection facial mask application of MY18-MDS800 type skinanalysis apparatus Moisture content of skin, be averaged, testing result see the table below.
As can be seen from the above table, the skin after Pudilan whitening moisturizing face masque prepared by application embodiment of the present invention 1-5 Water content reaches 30% or more, and after 18h, and moisture content of skin can still keep higher level, and moistening effect is notable and holds Long.
(2) the Pudilan whitening moisturizing face masque for using 1-5 of the embodiment of the present invention and comparative example 1-2 to prepare, to 140 18- The deeper volunteer of 40 years old colours of skin carries out facial application experiment in 10 weeks, wherein 70 males, 70 women are divided into seven at random Group, the Pudilan whitening moisturizing face masque that respectively prepared by application embodiment 1-5 and comparative example 1-2, application facial mask twice weekly, every time 15-20min after experiment, evaluates the skin of face of volunteer, as a result such as following table.
As can be seen from the above table, the Pudilan whitening moisturizing face masque white-skinned face function that prepared by 1-5 of the embodiment of the present invention is notable, uses Family is fed back, and whitening moisturizing face masque comfort of the present invention, gas permeability, compactness are good, after long-time service, non-stimulated allergic reaction hair It is raw.
(3) the Pudilan whitening moisturizing face masque for using 1-17 of the embodiment of the present invention and comparative example 1-9 to prepare, has 100 There is the volunteer of the symptoms such as different degrees of insufficiency of vital energy and blood and hemostasis illness to carry out facial application experiment in 5 weeks, finds using the present invention The symptoms such as the insufficiency of vital energy and blood of the volunteer of Pudilan whitening moisturizing face masque prepared by embodiment 1-17 and hemostasis illness are eased, And using the symptom of the volunteer of the comparative example 1-11 Pudilan whitening moisturizing face masques prepared without significant change or exacerbation.
(4) Pudilan whitening moisturizing face masque prepared by Example 6-9 and comparative example 3-4, the high temperature item in (40 ± 1) DEG C It is placed under part for 24 hours, then restores room temperature, range estimation finds Pudilan whitening moisturizing face masque no significant difference prepared by embodiment 6-9, And Pudilan whitening moisturizing face masque prepared by comparative example 3-4 loses fragrance, appearance is presented buff, it is placed in hot conditions Before have apparent difference, illustrate that Pudilan whitening moisturizing face masque prepared by 6-9 of the embodiment of the present invention has heat-resistant stability.
Example 11-12, embodiment 16-17, comparative example 5 and comparative example 8, the cryogenic conditions decentralization in (- 8 ± 2) DEG C Set for 24 hours, then restore room temperature, range estimation find Pudilan whitening moisturizing face masque prepared by embodiment 11-12, embodiment 16-17 without Notable difference, and Pudilan whitening moisturizing face masque prepared by comparative example 5 and comparative example 8 loses fragrance, buff is presented in appearance, with There is apparent difference before cryogenic conditions placement, illustrates Pudilan prepared by 11-12 of the embodiment of the present invention, embodiment 16-17 Whitening moisturizing face masque has cold-resistant stability.
(5) the Pudilan whitening moisturizing face masque for taking 1-3 of the embodiment of the present invention and comparative example 9 to prepare, to 20 18-40 Sui The deeper volunteer of the colour of skin carries out facial application experiment, using 5h after the detection facial mask application of MY18-MDS800 type skinanalysis apparatus Moisture content of skin, be averaged;Facial application experiment in 5 weeks is carried out to it simultaneously, facial mask, experiment terminate twice for application weekly Afterwards, the skin of face of volunteer is evaluated, as a result such as following table:
Comparative example 9 and embodiment 1 only difference is that:The Pudilan whitening moisturizing face masque at being grouped as in, With amino acid, collagen replaces beta glucan, glycine betaine.
Beta glucan, glycine betaine, amino acid, collagen is in the ingredient that this field prepares whitening moisturizing face masque, usually Play the role of moisturizer, as seen from the above table, when replacing beta glucan, glycine betaine with amino acid collagen, finds The performance of keeping humidity of facial mask has the decrease of degree very little, and its whitening effect is much weaker than embodiment 1-3.
(6) the Pudilan whitening moisturizing face masque for taking the embodiment of the present invention 1 and comparative example 10-11 to prepare, to 50 18-40 Year, the deeper volunteer of the colour of skin carried out facial application experiment, after detecting facial mask application using MY18-MDS800 type skinanalysis apparatus The moisture content of skin of 10h, is averaged;Facial application experiment in 6 weeks is carried out to it simultaneously, facial mask, experiment are tied twice for application weekly Shu Hou evaluates the skin of face of volunteer, as a result such as following table:
Carbomer used in Example 1 is Carbopol 941, and the carbomer that comparative example 10 uses is right for carbomer 934 The carbomer that ratio 11 uses is Acritamer 940.As can be seen from the above table, it is protected using Pudilan whitening made from Carbopol 941 Wet facial mask makes volunteer after facial mask application when 10h, and moisture content of skin can still keep higher level, and moistening effect is notable and holds Long, while also there is significant whitening effect.

Claims (7)

1. a kind of Pudilan whitening moisturizing face masque, it is characterised in that:The Pudilan whitening moisturizing face masque is contained by following weight Amount at being grouped as:Natrulon H-10 0.5-3%, 1.2- pentanediol 0.5-3%, beta glucan 0.5-2%, EDETATE SODIUM 0.01-0.08%, glycine betaine 0.3-2%, allantoin 0.01-0.1%, dipotassium glycyrrhizinate 0.01-0.15%, carbomer 0.05- 0.8%, Sodium Hyaluronate 0.005-0.08%, niacinamide 1-5%, -51 0.05-0.6% of polyquaternium, triethanolamine 0.1- 0.5%, 1.3 butanediol 2-10%, PEG-60 rilanit special 0.05-0.5%, PHL 0.15-0.95%, glycerol caprylate 0.01-0.1%, essence 0.001-0.025%, potassium hydroxide 0.01-0.1%, citric acid 0.01-0.12%, ascorbic acid Portugal Glucosides 0.1-0.5%, rose extract 0.01-0.1%, Ginseng extract 0.01-0.1%, Purslane extract 0.01- 0.1%, dandelion extract 0.0005-0.0025%, Herba Violae extract 0.0005-0.0025%, woaded blue root extract 0.0005-0.0025%, glycyrrhiza glabra root extract 0.00005-0.00025%, reed fragrant plant oil 0.1-1.5%, scutellariae,radix extraction Object 0.005-0.03% and water surplus.
2. Pudilan whitening moisturizing face masque according to claim 1, it is characterised in that:The Pudilan skin whitening, moisturizing face Film is by following weight content at being grouped as:Natrulon H-10 1-2.5%, 1.2- pentanediol 1-2.5%, beta glucan 0.8- 1.5%, EDETATE SODIUM 0.02-0.04%, glycine betaine 0.7-1.3%, allantoin 0.03-0.08%, dipotassium glycyrrhizinate 0.03- 0.1%, carbomer 0.1-0.3%, Sodium Hyaluronate 0.01-0.03%, niacinamide 1.5-3.5%, -51 0.1- of polyquaternium 0.3%, triethanolamine 0.15-0.3%, 1.3 butanediol 4-8%, PEG-60 rilanit special 0.15-0.25%, PHL 0.4- 0.8%, glycerol caprylate 0.03-0.08%, essence 0.005-0.015%, potassium hydroxide 0.03-0.08%, citric acid 0.02- 0.08%, ascorbic acid glucoside 0.15-0.35%, rose extract 0.05-0.07%, Ginseng extract 0.04- 0.07%, Purslane extract 0.05-0.08%, dandelion extract 0.0008-0.0015%, Herba Violae extract 0.001-0.002%, woaded blue root extract 0.001-0.0018%, glycyrrhiza glabra root extract 0.00008-0.00012%, reed Fragrant plant oil 0.3-1%, radix scutellariae root extract 0.008-0.015% and water surplus.
3. Pudilan whitening moisturizing face masque according to claim 1, it is characterised in that:The carbomer is selected from carbomer 934, one or more of Acritamer 940 and Carbopol 941.
4. a kind of preparation method of Pudilan whitening moisturizing face masque as described in claim 1-3, it is characterised in that:Including following Step:
(1) by Natrulon H-10 0.5-3%, 1.2- pentanediol 0.5-3%, beta glucan 0.5-2%, EDTA bis- of weight content Sodium 0.01-0.08%, glycine betaine 0.3-2%, allantoin 0.01-0.1%, dipotassium glycyrrhizinate 0.01-0.15%, carbomer Emulsification is added in 0.05-0.8%, Sodium Hyaluronate 0.005-0.08%, niacinamide 1-5% and -51 0.05-0.6% of polyquaternium In pot, it is heated to 60-90 DEG C, dissolving of blunging is denoted as A phases;
(2) by 1.3 butanediol 2-10%, PEG-60 rilanit special 0.05-0.5%, PHL0.15-0.95% of weight content, Glycerol caprylate 0.01-0.1%, essence 0.001-0.025% and glycyrrhiza glabra root extract 0.00005-0.00025% are carried out Stirring is denoted as B phases to being completely dispersed, spare;
(3) by the potassium hydroxide 0.01-0.1% of weight content, citric acid 0.01-0.12% and ascorbic acid glucoside 0.1- 0.5% uses water dissolution, stirs to being completely dispersed, is denoted as C phases, spare;
(4) the A phases of gained in step (1) are stirred and is cooled to 30-70 DEG C, then by the triethanolamine 0.1- of weight content 0.5% input emulsification pot, homogeneous mixing, then by the C phases and weight content obtained by the B phases and step (3) of gained in step (2) Rose extract 0.01-0.1%, Ginseng extract 0.01-0.1%, Purslane extract 0.01-0.1%, dandelion carry Take object 0.0005-0.0025%, Herba Violae extract 0.0005-0.0025%, woaded blue root extract 0.0005- 0.0025%, reed fragrant plant oil 0.1-1.5% and radix scutellariae root extract 0.005-0.03% is put into one by one in emulsification pot pot, and surplus is added Water obtains mixture D to 100%;
(5) the mixture D stirring obtained by step (4) is cooled to 10-50 DEG C, and vacuumizes degassing, filters, when discharging, which samples, does The inspection of semifinished product;
(6) carried out by measure with bottle placer after the inspection of semifinished product qualification obtained by step (5) it is filling, in assembly line upper cover bottle cap, Firework is filled, outer container is then filled;
(7) packaging is dispatched from the factory after completing after product inspection qualification.
5. the preparation method of Pudilan whitening moisturizing face masque according to claim 4, it is characterised in that:The step (1) heating temperature in is 70-80 DEG C.
6. the preparation method of Pudilan whitening moisturizing face masque according to claim 4, it is characterised in that:The step (4) the A phases obtained by step (1) are stirred in and are cooled to 40-60 DEG C.
7. the preparation method of Pudilan whitening moisturizing face masque according to claim 4, it is characterised in that:The step (5) the mixture D stirring obtained by step (4) is cooled to 20-40 DEG C in.
CN201810372226.2A 2018-04-24 2018-04-24 Pudilan blue whitening and moisturizing mask Active CN108309862B (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109044874A (en) * 2018-10-17 2018-12-21 郑玉波 A kind of facial mask of the factor containing spontaneous growth and preparation method thereof
CN109620782A (en) * 2018-11-02 2019-04-16 广州市爱百伊生物技术有限公司 A kind of plant composition with Whitening, spot effect
CN110192996A (en) * 2019-06-27 2019-09-03 福建师范大学 A kind of viola mandshurica moisturizer and preparation method thereof and the moisturizing moisturizing sleep mask containing the moisturizer
CN110664658A (en) * 2019-11-16 2020-01-10 菏泽新东方日化科技有限公司 Whitening antibacterial composition and cosmetic containing same
CN113069387A (en) * 2020-01-06 2021-07-06 广州樱奈儿化妆品有限公司 Anti-fatigue mask and preparation method thereof
CN115177576A (en) * 2022-09-09 2022-10-14 广州优理氏生物科技有限公司 Composition for moisturizing, repairing and anti-aging of skin, application of composition and facial mask liquid

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103637939A (en) * 2013-11-29 2014-03-19 大连创达技术交易市场有限公司 Purslane smoothing toner
CN105434282A (en) * 2015-12-31 2016-03-30 天津达仁堂京万红药业有限公司 Moisturizing and nourishing toner and preparation method thereof
CN105640845A (en) * 2016-03-30 2016-06-08 韩玉逍 Skin age multi-effect silk mask liquid
CN105748354A (en) * 2016-03-09 2016-07-13 广东芭薇生物科技股份有限公司 Facial mask liquid and preparation method thereof
CN107468634A (en) * 2017-10-16 2017-12-15 徐宏伟 A kind of anti-acne moisture saver mask and its preparation technology

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103637939A (en) * 2013-11-29 2014-03-19 大连创达技术交易市场有限公司 Purslane smoothing toner
CN105434282A (en) * 2015-12-31 2016-03-30 天津达仁堂京万红药业有限公司 Moisturizing and nourishing toner and preparation method thereof
CN105748354A (en) * 2016-03-09 2016-07-13 广东芭薇生物科技股份有限公司 Facial mask liquid and preparation method thereof
CN105640845A (en) * 2016-03-30 2016-06-08 韩玉逍 Skin age multi-effect silk mask liquid
CN107468634A (en) * 2017-10-16 2017-12-15 徐宏伟 A kind of anti-acne moisture saver mask and its preparation technology

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109044874A (en) * 2018-10-17 2018-12-21 郑玉波 A kind of facial mask of the factor containing spontaneous growth and preparation method thereof
CN109620782A (en) * 2018-11-02 2019-04-16 广州市爱百伊生物技术有限公司 A kind of plant composition with Whitening, spot effect
CN109620782B (en) * 2018-11-02 2021-12-21 广州市爱百伊生物技术有限公司 Plant composition with whitening and spot-fading effects
CN110192996A (en) * 2019-06-27 2019-09-03 福建师范大学 A kind of viola mandshurica moisturizer and preparation method thereof and the moisturizing moisturizing sleep mask containing the moisturizer
CN110664658A (en) * 2019-11-16 2020-01-10 菏泽新东方日化科技有限公司 Whitening antibacterial composition and cosmetic containing same
CN113069387A (en) * 2020-01-06 2021-07-06 广州樱奈儿化妆品有限公司 Anti-fatigue mask and preparation method thereof
CN115177576A (en) * 2022-09-09 2022-10-14 广州优理氏生物科技有限公司 Composition for moisturizing, repairing and anti-aging of skin, application of composition and facial mask liquid

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