CN108298820A - A kind of production method of anion fine pottery color glaze - Google Patents
A kind of production method of anion fine pottery color glaze Download PDFInfo
- Publication number
- CN108298820A CN108298820A CN201810450638.3A CN201810450638A CN108298820A CN 108298820 A CN108298820 A CN 108298820A CN 201810450638 A CN201810450638 A CN 201810450638A CN 108298820 A CN108298820 A CN 108298820A
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- Prior art keywords
- glaze
- anion
- fine pottery
- color glaze
- anion fine
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Abstract
The invention discloses a kind of production methods of anion fine pottery color glaze, the described method comprises the following steps：（1）According to base glaze proportioning and processing method, parent glaze is got ready；（2）Ceramic paint and water are mixed and made into color glaze in mass ratio；（3）Anion raw mineral materials is directly added into color glaze, uniform anion fine pottery color glaze is made；（4）A biscuit after high-temperature firing is crossed into clear water, is then immersed in anion fine pottery color glaze；（5）By the color base drying after leaching anion fine pottery color glaze, then carry out secondary glaze firing；（6）By vanning after the secondary molding product natural cooling of glaze firing to get anion fine pottery color glaze product.The present invention fully considers the industry characteristics of anion ore, and suitable machined parameters, anion fine pottery color glaze product anion number >=3100/cm are adjusted according to proportioning2。
Description
Technical field
The present invention relates to fine pottery color glaze proprietary formula technical field more particularly to a kind of making sides of anion fine pottery color glaze
Method.
Background technology
With the improvement of living standards, requirement of the people to ornament materials is also sent out towards multifunctional direction and environmentally friendly direction
Exhibition.Anion is that the oxygen molecule in air combines free electron formation, carries negative electrical charge, has extra electronics, has " empty
The good reputation of gas vitamin ", " air vitamin ".Its main function is shown：1, it is influence to nervous system.It can make brain
Function of cortex and mental activity are reinforced, in high spirits, and working efficiency improves, and sleep quality can be made to be improved.2, it is to painstaking effort
The influence of guard system.It is observed according to scholar, anion has apparent expansion blood vessel function, can release arteries spasm, reach reduction
The effect of blood pressure, anion for improve cardiovascular function and improve myocardial nutrition also have very big benefit, be conducive to hypertension and
The state of an illness of cardio-cerebrovascular disorder patient is restored.3, it is influence to hematological system.Research confirms that anion has and makes blood pool stream
Speed is slack-off, extends the effect in clotting time, and oxygen content in blood can be made to increase, and is conducive to blood oxygen conveying, absorbs and utilizes.
Therefore, developing a kind of can discharge the negative aeroion ceramic glaze beneficial to health and have wide application
Foreground.
Invention content
The technical problem to be solved in the present invention is to provide a kind of production methods of anion fine pottery color glaze.Made from this method
Fine pottery color glaze will be applied in combination rich in negative ion mineral raw material according to corresponding proportioning, not only meet corresponding industry technology mark
Standard, while negative ion concentration can also be made to increase in use environment, promote human metabolism, improves health.
In order to solve the above technical problems, the technical solution adopted by the present invention is that：A kind of making side of anion fine pottery color glaze
Method the described method comprises the following steps：
（1）According to base glaze proportioning and processing method, parent glaze is got ready；
（2）By ceramic paint and water in mass ratio 10:1 ratio mixes, and normal temperature state is sufficiently stirred 1~2h, crosses 200 mesh sieve, so
After be added in parent glaze 4~5h of stirring, according to parent glaze:Ceramic paint mass ratio 9:1 is made color glaze, the ceramic paint
For package series；
（3）Anion raw mineral materials is directly added into color glaze, 2~3h is stirred, uniform anion fine pottery color glaze is made；
（4）A biscuit clamping device after high-temperature firing is submerged in clear water and stagnates 3~5s, water excessively is uniform, nothing
Water dryin-up point is not crossed, is then immersed in anion fine pottery color glaze；
（5）After color base after leaching anion fine pottery color glaze is dried 48~52h, then carry out secondary glaze firing；
（6）By vanning after the secondary molding product natural cooling of glaze firing to get anion fine pottery color glaze product.
Step of the present invention（1）Middle base glaze matches：Frit 95~97%, Suzhou soil 3~5%.
Step of the present invention（1）The frit chemical composition of middle base glaze forms and mass percentage is：SiO2：45
~50%, Al2O3：6~7%, CaO：4.5~5.0%, K2O：5~6%, Na2O：2~3%, ZnO：7~8%.
Step of the present invention（1）Middle base glaze processing method, by material:Ball:Water=1:2.5:Ball is added in 0.5 ratio
In grinding machine, 30~35h of ball milling, more than grain fineness 0.03~0.05g/ 10000-hole sieves.
Step of the present invention（3）Middle anion raw mineral materials is by containing rare earth element and natural primordial radionuclide
Mineral composition.
Step of the present invention（3）Middle color glaze is 4 with anion raw mineral materials quality ratio:1；The step（4）Middle biscuit
1100~1150 DEG C of a biscuiting temperature.
Step of the present invention（4）Middle anion fine pottery color glaze modulation proportion is 1.70~1.75kg/cm3, soak the glaze time
3-3.5s, 1.0~1.2mm of glazed thickness.
Step of the present invention（5）40~50 DEG C of color base drying temperature after middle leaching anion fine pottery color glaze.
Step of the present invention（5）The secondary glaze firing firing temperature of anion fine pottery color glaze color base after middle drying 1050~
1080 DEG C, the firing time is 8~9h.
Anion fine pottery color glaze product anion number >=3100/cm of the method for the invention production2。
Product testing canonical reference GB/T10815-2002 of the present invention《Domestic fine pottory device》, hardness of glaze surface detection numerical value 510
~535kg/cm2.Anion raw mineral materials of the present invention selects the anion product of Shanghai great Hong enamel frit makeing Co., Ltd production, model
DH8001。
Anion fine pottery glaze activity porcelain series of the present invention is combined with Ceramic glaze by repetition test, by anion
Element incorporates in original fine pottery glaze, is attached on fine pottery green body through high-temperature firing perfection, is detected by national authority department, wax
Candlestick anion glaze anion number is up to 3100/cm2More than, it can effectively increase body immunity and antibacterial ability.
Anion quantity is detected using HD-3200 type anionic textiles instrument.
Anion color glaze proprietary formula of the present invention will make rich in negative ion mineral raw material according to the combination of corresponding proportioning
With, so that negative ion concentration is increased in use environment, promote human metabolism, improve health, while fully considering anion
The industry characteristics of ore adjust suitable machined parameters according to proportioning, improve production efficiency, improve the quality of production.
It is using advantageous effect caused by above-mentioned technical proposal：1, the present invention is special by fully considering the production of color glaze
Property, different colours are adjusted out according to proportioning, improve ornamental value.2, the present invention uses anion color glaze proprietary formula, will be rich in negative
Ion mineral matter raw material is applied in combination according to corresponding proportioning, so that negative ion concentration is increased in use environment, promotes human body new
Old metabolism, improves health.3, production method of the present invention fully considers the industry characteristics of anion ore, is closed according to proportioning adjustment
Suitable machined parameters improve production efficiency, improve the quality of production.4, the anion fine pottery color glaze product of the method for the present invention production is negative
Ion number >=3100/cm2。
Specific implementation mode
With reference to specific embodiment, the present invention is described in further detail.
Embodiment 1
A kind of production method of anion fine pottery color glaze includes the following steps：
（1）Base glaze matches：Frit 95%, Suzhou soil 5%；By material:Ball:Water=1:2.5:Ball mill is added in 0.5 ratio
In, ball milling 30h, more than grain fineness 0.03~0.05g/ 10000-hole sieves；
（2）By ceramic paint and water in mass ratio 10:1 ratio mixes, and 2h is sufficiently stirred under room temperature, crosses 200 mesh sieve, is then added
To 4h is stirred in parent glaze, according to parent glaze:Ceramic paint (package series) mass ratio 9:1 is made color glaze；
（3）It is 4 by the mineral composition of rare earth element and natural primordial radionuclide:1 anion raw mineral materials is directly added into
In color glaze, 3h is stirred, uniform anion fine pottery color glaze is made；
（4）By a biscuit after high-temperature firing（1130 DEG C of a biscuiting temperature）3s is stagnated in submergence in clear water, crosses water
Uniformly, without water dryin-up point is not crossed, it is then immersed in anion fine pottery color glaze, it is 1.75kg/ that anion fine pottery color glaze, which modulates proportion,
cm3, soak glaze time 3s, glazed thickness 1.0mm；
（5）By the color base after leaching anion fine pottery color glaze after 40 DEG C of dry 52h, then secondary glaze firing is carried out, secondary glaze firing is fired
1050 DEG C of temperature, firing time 8h；
（6）By vanning after the secondary molding product natural cooling of glaze firing to get anion fine pottery color glaze.After testing, anion glaze
Anion number is up to 3180/cm in face2, hardness of glaze surface detection numerical value 520kg/cm2。
Embodiment 2
A kind of production method of anion fine pottery color glaze includes the following steps：
（1）Base glaze matches：Frit 97%, Suzhou soil 3%；By material:Ball:Water=1:2.5:Ball mill is added in 0.5 ratio
In, ball milling 35h, more than grain fineness 0.03~0.05g/ 10000-hole sieves；
（2）By ceramic paint and water in mass ratio 10:1 ratio mixes, and 1h is sufficiently stirred under room temperature, crosses 200 mesh sieve, is then added
To 5h is stirred in parent glaze, according to parent glaze:Ceramic paint (package series) mass ratio 9:1 is made color glaze；
（3）It is 4 by the mineral composition of rare earth element and natural primordial radionuclide:1 anion raw mineral materials is directly added into
In color glaze, 2h is stirred, uniform anion fine pottery color glaze is made；
（4）By a biscuit after high-temperature firing（1120 DEG C of a biscuiting temperature）5s is stagnated in submergence in clear water, crosses water
Uniformly, without water dryin-up point is not crossed, it is then immersed in anion fine pottery color glaze, it is 1.70kg/ that anion fine pottery color glaze, which modulates proportion,
cm3, soak glaze time 3.5s, glazed thickness 1.2mm；
（5）By the color base after leaching anion fine pottery color glaze after 50 DEG C of dry 48h, then secondary glaze firing is carried out, secondary glaze firing is fired
1080 DEG C of temperature, firing time 9h；
（6）By vanning after the secondary molding product natural cooling of glaze firing to get anion fine pottery color glaze.After testing, anion glaze
Anion number is up to 3120/cm in face2, hardness of glaze surface detection numerical value 530kg/cm2。
Embodiment 3
A kind of production method of anion fine pottery color glaze includes the following steps：
（1）Base glaze matches：Frit 96%, Suzhou soil 4%；By material:Ball:Water=1:2.5:Ball mill is added in 0.5 ratio
In, ball milling 32h, more than grain fineness 0.03~0.04g/ 10000-hole sieves；
（2）By ceramic paint and water in mass ratio 10:1 ratio mixes, and 1.5h is sufficiently stirred under room temperature, crosses 200 mesh sieve, then adds
Enter and stir 4.5h into parent glaze, according to parent glaze:Ceramic paint (package series) mass ratio 9:1 is made color glaze；
（3）It is 4 by the mineral composition of rare earth element and natural primordial radionuclide:1 anion raw mineral materials is directly added into
In color glaze, 2.5h is stirred, uniform anion fine pottery color glaze is made；
（4）By a biscuit after high-temperature firing（1100 DEG C of a biscuiting temperature）4s is stagnated in submergence in clear water, crosses water
Uniformly, without water dryin-up point is not crossed, it is then immersed in anion fine pottery color glaze, it is 1.72kg/ that anion fine pottery color glaze, which modulates proportion,
cm3, soak glaze time 3.2s, glazed thickness 1.1mm；
（5）By the color base after leaching anion fine pottery color glaze after 43 DEG C of dry 50h, then secondary glaze firing is carried out, secondary glaze firing is fired
1065 DEG C of temperature, firing time 8.5h；
（6）After testing to get anion fine pottery color glaze by vanning after the secondary molding product natural cooling of glaze firing, anion glaze
Middle anion number is up to 3200/cm2, hardness of glaze surface detection numerical value 535kg/cm2。
Embodiment 4
A kind of production method of anion fine pottery color glaze includes the following steps：
（1）Base glaze matches：Frit 95.5%, Suzhou soil 4.5%；By material:Ball:Water=1:2.5:Ball milling is added in 0.5 ratio
In machine, ball milling 33h, more than grain fineness 0.04~0.05g/ 10000-hole sieves；
（2）By ceramic paint and water in mass ratio 10:1 ratio mixes, and 2h is sufficiently stirred under room temperature, crosses 200 mesh sieve, is then added
To 4h is stirred in parent glaze, according to parent glaze:Ceramic paint (package series) mass ratio 9:1 is made color glaze；
（3）It is 4 by the mineral composition of rare earth element and natural primordial radionuclide:1 anion raw mineral materials is directly added into
In color glaze, 3h is stirred, uniform anion fine pottery color glaze is made；
（4）By a biscuit after high-temperature firing（1150 DEG C of a biscuiting temperature）5s is stagnated in submergence in clear water, crosses water
Uniformly, without water dryin-up point is not crossed, it is then immersed in anion fine pottery color glaze, it is 1.74kg/ that anion fine pottery color glaze, which modulates proportion,
cm3, soak glaze time 3.4s, glazed thickness 1.2mm；
（5）By the color base after leaching anion fine pottery color glaze after 47 DEG C of dry 51h, then secondary glaze firing is carried out, secondary glaze firing is fired
1075 DEG C of temperature, firing time 9h；
（6）After testing to get anion fine pottery color glaze by vanning after the secondary molding product natural cooling of glaze firing, anion glaze
Middle anion number is up to 3150/cm2, hardness of glaze surface detection numerical value 515kg/cm2。
The above embodiments are only used to illustrate and not limit the technical solutions of the present invention, although with reference to above-described embodiment to this hair
It is bright to be described in detail, it will be understood by those of ordinary skill in the art that：Still can the present invention be modified or be waited
With replacing, without departing from the spirit or scope of the invention, or any substitutions, the power in the present invention should all be covered
In sharp claimed range.
Claims (10)
1. a kind of production method of anion fine pottery color glaze, which is characterized in that the described method comprises the following steps：
（1）According to base glaze proportioning and processing method, parent glaze is got ready；
（2）By ceramic paint and water in mass ratio 10:1 ratio mixes, and normal temperature state is sufficiently stirred 1~2h, crosses 200 mesh sieve, so
After be added in parent glaze 4~5h of stirring, according to parent glaze:Ceramic paint mass ratio 9:1 is made color glaze, the ceramic paint
For package series；
（3）Anion raw mineral materials is directly added into color glaze, 2~3h is stirred, uniform anion fine pottery color glaze is made；
（4）A biscuit clamping device after high-temperature firing is submerged in clear water and stagnates 3~5s, water excessively is uniform, nothing
Water dryin-up point is not crossed, is then immersed in anion fine pottery color glaze；
（5）After color base after leaching anion fine pottery color glaze is dried 48~52h, then carry out secondary glaze firing；
（6）By vanning after the secondary molding product natural cooling of glaze firing to get anion fine pottery color glaze product.
2. a kind of production method of anion fine pottery color glaze according to claim 1, which is characterized in that the step（1）
Middle base glaze matches：Frit 95~97%, Suzhou soil 3~5%.
3. a kind of production method of anion fine pottery color glaze according to claim 1, which is characterized in that the step（1）
The frit chemical composition of middle base glaze forms and mass percentage is：SiO2：45~50%, Al2O3：6~7%, CaO：4.5
~5.0%, K2O：5~6%, Na2O：2~3%, ZnO：7~8%.
4. a kind of production method of anion fine pottery color glaze according to claim 1, which is characterized in that the step（1）
Middle base glaze processing method, by material:Ball:Water=1:2.5:0.5 ratio is added in ball mill, 30~35h of ball milling, and particle is thin
It spends more than 0.03~0.05g/ 10000-hole sieves.
5. a kind of production method of anion fine pottery color glaze according to any one of claims 1-4, which is characterized in that institute
State step（3）Middle anion raw mineral materials is by the mineral composition containing rare earth element and natural primordial radionuclide.
6. a kind of production method of anion fine pottery color glaze according to any one of claims 1-4, which is characterized in that institute
State step（3）Middle color glaze is 4 with anion raw mineral materials quality ratio:1；The step（4）Biscuiting temperature 1100 of middle biscuit
~1150 DEG C.
7. a kind of production method of anion fine pottery color glaze according to any one of claims 1-4, which is characterized in that institute
State step（4）Middle anion fine pottery color glaze modulation proportion is 1.70~1.75kg/cm3, soak glaze time 3-3.5s, glazed thickness
1.0~1.2mm.
8. a kind of production method of anion fine pottery color glaze according to any one of claims 1-4, which is characterized in that institute
State step（5）40~50 DEG C of color base drying temperature after middle leaching anion fine pottery color glaze.
9. a kind of production method of anion fine pottery color glaze according to any one of claims 1-4, which is characterized in that institute
State step（5）Secondary 1050~1080 DEG C of the glaze firing firing temperature of anion fine pottery color glaze color base after middle drying, firing time 8
~9h.
10. a kind of production method of anion fine pottery color glaze according to any one of claims 1-4, which is characterized in that
Anion fine pottery color glaze product anion number >=3100/cm of the method production2。
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|---|---|---|---|
| CN201810450638.3A CN108298820B (en) | 2018-05-11 | 2018-05-11 | Method for preparing negative ion fine ceramic glaze |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810450638.3A CN108298820B (en) | 2018-05-11 | 2018-05-11 | Method for preparing negative ion fine ceramic glaze |
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| CN108298820B CN108298820B (en) | 2021-07-13 |
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| CN107288293A (en) * | 2017-06-21 | 2017-10-24 | 信益陶瓷(中国)有限公司 | A kind of negative ion health ceramic tile |
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2018
- 2018-05-11 CN CN201810450638.3A patent/CN108298820B/en active Active
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| CN103396167A (en) * | 2013-08-05 | 2013-11-20 | 李涛 | Porous building decoration material capable of adjusting humidity, reducing harm and releasing negative ions |
| CN103408327A (en) * | 2013-08-08 | 2013-11-27 | 李涛 | Building decoration material and production method thereof |
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| CN107288293A (en) * | 2017-06-21 | 2017-10-24 | 信益陶瓷(中国)有限公司 | A kind of negative ion health ceramic tile |
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