A kind of bulb of thunberg fritillary plantation substrate, preparation process and system
Technical field
The present invention relates to a kind of cultivation matrixes, and in particular to a kind of bulb of thunberg fritillary plantation substrate, preparation system and technique.Belong to
In bulb of thunberg fritillary technical field of cultivation.
Background technology
The solution efficiently emerged for bulb of thunberg fritillary is not found at present, is all traditional nursery means, from agrotechnical angle
Degree goes to improve planting percent.Bulb of thunberg fritillary is usually to form bulb in summer, and more after the summer, nursery will be used as in 10 annual~November
The bulb on basis digs up to rearrange again and is seeded into ground namely forms bulb to sowing (intermediate meeting next time in bulb of thunberg fritillary
The high bulb of a collection of commodity is dug out to be peddled) during, the bulb as seedling substrate will be embedded in ground borough chief up to 2~3
As long as month, encounter the time more than rainwater, bulb it is rotten be it is very serious, directly result in the reduction of the yield of bulb of thunberg fritillary, bring through
Loss in Ji.
Bulb of thunberg fritillary mainly realizes that expansion is numerous by bulb breeding and tissue cultures in process of production.It is low for bulb of thunberg fritillary emergence rate
The problem of, it is related to the nursery of bulb of thunberg fritillary, is badly in need of a kind of seedling medium at present, according to the nutrient demand in bulb of thunberg fritillary bulb plumule emergence
Promote bulb seedling to formulate efficient formula.
Invention content
The purpose of the present invention is to overcome above-mentioned the deficiencies in the prior art, provide a kind of bulb of thunberg fritillary plantation substrate, prepare
Technique and system.
To achieve the above object, the present invention uses following technical proposals:
A kind of preparation process of bulb of thunberg fritillary plantation substrate, is as follows:
(1) by air-dried high mountain mao bamboon and cow dung according to mass ratio 8:1 input retort, connect the gas outlet of retort with
Condensing plant opens condensing plant, closes bamboo charcoal discharge port and activated carbon discharge nozzle, and material is heated with the heating rate of 0.1 DEG C/s
Temperature is to 250~350 DEG C, charing process 15~20 minutes in this temperature range, and the condensed equipment of bamboo vinegar steam stream of generation is cold
It coagulates for crude bamboo vinegar, and the bottom for passing through condensing plant is expelled to distilling apparatus;
(2) continue to heat material temperature to 300~350 DEG C, open bamboo charcoal discharge port, the bamboo charcoal of discharge is collected using tray,
And the cooling that tiles;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray, until residual in retort
1/20 that quality is input amount is stayed, closes bamboo charcoal discharge port;
(4) continue to heat material temperature to 700 DEG C or more, raw material is further cracked into activated carbon in retort, connects activated carbon
Discharge nozzle makes activated carbon slowly enter the distilling apparatus for being connected to crude bamboo vinegar, treats that crude bamboo vinegar collection finishes, closes condensation
Equipment exports, and avoids flowing back;
(5) distilling apparatus is warming up to 120 DEG C, is come into full contact with by stirring activated carbon with crude bamboo vinegar, generation
Enter refined bamboo vinegar reception device after the condensed conduit condensation of steam, stand 24 hours, filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary as primary raw material with refined bamboo vinegar obtained by step (5) using bamboo charcoal obtained by step (3)
Plantation substrate.
Preferably, in step (1), pressure reducing valve is opened slightly, for adjusting pressure in retort;In step (3), bamboo is closed
Pressure reducing valve is also turn off while charcoal discharge port.
Preferably, in step (1), the bamboo vinegar steam of generation is followed by two condensers, respectively from two condensers
The crude bamboo vinegar that condensation obtains is expelled to distilling apparatus by bottom.
Preferably, in step (4), in distilling apparatus, the mass ratio of activated carbon and crude bamboo vinegar is 1:12.
Preferably, in step (5), pH=3.4~4.8 of refined bamboo vinegar.
Preferably, the specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2~3 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 3~5 hours, cross 40 mesh sieve, obtain
Scorched clay dust powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, standby
With;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), is then spread evenly
Mineral powders obtained by step (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar while stirring, measure simultaneously
The pH of system, until pH=5~5.8, stop sprinkling bamboo vinegar to get.
It is further preferred that in step (6-2), thickness of earth covering is 1cm on hay.
It is further preferred that in step (6-4), the mass ratio of mineral powders, bamboo charcoal powder and scorched clay dust powder is 1:4:
8。
It is further preferred that the whole-process control moisture in the preparation process of cultivation matrix, the water of final gained cultivation matrix
Weight content is divided to be less than 15%.
It is further preferred that step (6-4) is also granulated after stopping spraying bamboo vinegar, controls the appearance of cultivation matrix
Weight ranging from 1.15~1.27g/cm3。
A kind of bulb of thunberg fritillary plantation substrate, is obtained by above-mentioned preparation process.
Bulb of thunberg fritillary bulb nursery is carried out using above-mentioned cultivation matrix, specific method is:In late October, bulb of thunberg fritillary bulb is embedded in
In the cultivation matrix, institute's buried depth degree is 2 times, about 5~7cm of bulb of thunberg fritillary bulb diameter, and seedling raise period is 14~20 days.
The corresponding a kind of preparation system of bulb of thunberg fritillary plantation substrate of above-mentioned preparation process, including bamboo charcoal preparation facilities and bamboo
Vinegar liquid preparation facilities two parts, the bamboo charcoal preparation facilities are retort, and the main body of bamboo vinegar preparation facilities is condensing plant, charcoal
Change and be respectively equipped with gas outlet and bamboo charcoal discharge port at the top and bottom of stove, the lower section setting tray of bamboo charcoal discharge port, it is described go out
Gas port is connected to the top of condensing plant, and the bottom of condensing plant is connected with distilling apparatus;The bottom of the retort is additionally provided with
Activated carbon discharge nozzle, activated carbon discharge nozzle are connected to distilling apparatus;The distilling apparatus passes through condensation pipe and refined bamboo vinegar
Reception device connects.
Preferably, the bottom of the retort is additionally provided with pressure reducing valve, and the bamboo vinegar steam that being arranged on bottom can prevent leads to
Pressure reducing valve is crossed to lose.
Preferably, the condensing plant includes the first condenser and the second condenser of series connection, and the gas outlet of retort connects
It is connected to the top of the first condenser, the bottom of the first condenser is equipped with leakage fluid dram I and exhaust outlet, exhaust outlet and the second condenser
Top connects, and the bottom of the second condenser is equipped with leakage fluid dram II, and the leakage fluid dram I and leakage fluid dram II are respectively connected to distillation dress
It puts.
It is further preferred that the outside of first condenser and the second condenser be respectively arranged the first condensing water conduit and
Second condensing water conduit, condensed water enter from the bottom of the second condensing water conduit, and top outflow then flows into the first condensate pipe
The bottom in road is finally flowed out via the top of the first condensing water conduit.
Preferably, the material of the tray is stainless steel, is conducive to collected bamboo charcoal tiling heat dissipation.
Preferably, stirring rod is equipped in the distilling apparatus.
Beneficial effects of the present invention:
The present invention compounds to obtain a kind of bulb of thunberg fritillary plantation substrate using bamboo charcoal and refined bamboo vinegar as primary raw material, both can be with
The nursery of bulb is directly used in, while can directly apply plot conduct again and accompany fertilizer ground substance.Zhejiang is realized using the cultivation matrix
The maximization compounding of nutrient needed for the breeding of shellfish bulb, ensures maximally utilizing for critical nutrients, it is asexual numerous finally to realize bulb of thunberg fritillary
Grow the raising of emergence rate.The key problem in technology of the present invention is that the quality of bamboo charcoal and refined bamboo vinegar improves, and corresponding is to prepare work
The innovation of skill, it is specific as follows:
1st, bulb of thunberg fritillary growth is more sensitive for elements such as N, K, Mg, Zn, Cu, therefore in the process of cultivation matrix raw material compounding
It is middle to need to add in the more raw material of available nutrient, the high mountain mao bamboon of special ratios is formed with cow dung by specific calcine technology
The maximized bamboo charcoal of nutrient is imitated, makes it have physically better absorption property, fertilizer conservation effect is good, and the nutrient of compounding is avoided quickly to flow
It loses, slow release nutrient is more advantageous to bulb of thunberg fritillary bulb seedling.Wherein, the addition of cow dung helps to improve the ash content of gained bamboo charcoal,
Increase effective nitrogen content.
2nd, the difference of bamboo vinegar refines mode and is affected for the property of itself, needs to control the refined bamboo vinegar of gained
PH=3.4~4.8 of liquid are proper, organic matter mass content 8% or so (organic acid, phenols, ketone, aldehydes, alcohols, three
Terpene, heterocyclic compound), the bamboo vinegar of such quality can play its maximum effect when matrix compounds, and be conducive to bulb of thunberg fritillary bulb
Seedling.In addition, the bamboo vinegar of the present invention can effectively kill harmful bacteria, the relatively low miscellaneous bacteria rate of matrix is controlled.
3rd, the activated carbon that retort is generated at 700 DEG C or more mixes distillation with crude bamboo vinegar, on the one hand can adsorb thick
Harmful substance and impurity in bamboo vinegar processed, on the other hand can effectively improve gained refined bamboo vinegar pH, adjusted to
PH=3.4~4.8, avoid refined bamboo vinegar peracid, so in compound process by the pH of matrix it is too fast be reduced to reasonable value with
Under, simultaneously so that refined bamboo vinegar retains ammonium ions more as possible, reduces the loss late of nitrogen.
4th, the habit grown according to bulb of thunberg fritillary, it is desirable that growing environment slant acidity, nutrient content are high, can by granulating technique,
Matrix unit weight is controlled in 1.15~1.27g/cm3, pH=5~5.8 can ensure good fertilizer conservation water storage performance, to promote squama
Stem-root.
Description of the drawings
Fig. 1 is the preparation system structure diagram of the present invention;
Wherein, 1 is retort, and 11 be gas outlet, and 12 be bamboo charcoal discharge port, and 13 be activated carbon discharge nozzle, and 14 be pressure reducing valve,
2 be tray, and 3 be the first condenser, and 31 be leakage fluid dram I, and 32 be exhaust outlet, and 4 be the second condenser, and 41 be leakage fluid dram II, and 5 are
Distilling apparatus, 6 be refined bamboo vinegar reception device, and 7 be condensed water, and 8 be condensation pipe.
Specific embodiment
The present invention will be further elaborated with reference to the accompanying drawings and examples, it should which explanation, the description below is only
It is to explain the present invention, its content is not defined.
Embodiment 1:
As shown in Figure 1, a kind of preparation process of bulb of thunberg fritillary plantation substrate, is as follows:
(1) by air-dried high mountain mao bamboon and cow dung according to mass ratio 8:1 input retort 1 connects the gas outlet of retort 1
11 and condensing plant, condensing plant is opened, closes bamboo charcoal discharge port 12 and activated carbon discharge nozzle 13, with the heating speed of 0.1 DEG C/s
Rate heats material temperature to 250 DEG C, charing process 15 minutes in this temperature range, the condensed equipment condensation of bamboo vinegar steam stream of generation
For crude bamboo vinegar, and the bottom for passing through condensing plant is expelled to distilling apparatus 5;
(2) continue to heat material temperature to 300 DEG C, open bamboo charcoal discharge port 12, the bamboo charcoal of discharge is collected using tray 2, and
Tile cooling;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray 2, until in retort 1
Residual mass is the 1/20 of input amount, closes bamboo charcoal discharge port 12;
(4) continue to heat material temperature to 700 DEG C or more, raw material is further cracked into activated carbon in retort 1, connects activated carbon
Discharge nozzle 13 makes activated carbon slowly enter the distilling apparatus 5 for being connected to crude bamboo vinegar, treats that crude bamboo vinegar collection finishes, closes
Condensing plant exports, and avoids flowing back;
(5) distilling apparatus 5 is warming up to 120 DEG C, is come into full contact with by stirring activated carbon with crude bamboo vinegar, generation
The condensed conduit 8 of steam enters refined bamboo vinegar reception device 6 after condensing, and stands 24 hours, and filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary as primary raw material with refined bamboo vinegar obtained by step (5) using bamboo charcoal obtained by step (3)
Plantation substrate.
It is pico- to open pressure reducing valve 14 in step (1), for adjusting pressure in retort 1;In step (3), close bamboo charcoal and go out
Pressure reducing valve 14 is also turn off while material mouth 12.
In step (1), the bamboo vinegar steam of generation, respectively will be cold from the bottom of two condensers followed by two condensers
Solidifying obtained crude bamboo vinegar is expelled to distilling apparatus 5.
In step (4), in distilling apparatus 5, the mass ratio of activated carbon and crude bamboo vinegar is 1:12.
In step (5), the pH=3.4 of refined bamboo vinegar.
The specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 3 hours, cross 40 mesh sieve, obtain burnt mud
Grey powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, standby
With;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), is then spread evenly
Mineral powders obtained by step (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar while stirring, measure simultaneously
The pH of system, until pH=5, stop sprinkling bamboo vinegar to get.
In step (6-2), thickness of earth covering is 1cm on hay.
In step (6-4), the mass ratio of mineral powders, bamboo charcoal powder and scorched clay dust powder is 1:4:8.
The whole-process control moisture in the preparation process of cultivation matrix, the moisture weight content of final gained cultivation matrix are less than
15%.
A kind of bulb of thunberg fritillary plantation substrate, is obtained by above-mentioned preparation process.
The corresponding a kind of preparation system of bulb of thunberg fritillary plantation substrate of above-mentioned preparation process, including bamboo charcoal preparation facilities and bamboo
Vinegar liquid preparation facilities two parts, bamboo charcoal preparation facilities are retort 1, and the main body of bamboo vinegar preparation facilities is condensing plant, is carbonized
The top and bottom of stove 1 are respectively equipped with gas outlet 11 and bamboo charcoal discharge port 12, and the lower section of bamboo charcoal discharge port 12 sets tray 2,
Gas outlet 11 is connected to the top of condensing plant, and the bottom of condensing plant is connected with distilling apparatus 5;The bottom of retort 1 is also set
Active charcoal discharge nozzle 13, activated carbon discharge nozzle 13 are connected to distilling apparatus 5;Distilling apparatus 5 passes through condensation pipe 8 and refined bamboo
Vinegar liquid reception device 6 connects.
The bottom of retort 1 is additionally provided with pressure reducing valve 14, and the bamboo vinegar steam that being arranged on bottom can prevent passes through pressure reducing valve
14 lose.
Condensing plant includes the first condenser 3 and the second condenser 4 of series connection, and the gas outlet 11 of retort 1 is connected to the
The top of one condenser 3, the bottom of the first condenser 3 are equipped with leakage fluid dram I 31 and exhaust outlet 32,32 and second condenser of exhaust outlet
4 top connection, the bottom of the second condenser 4 are equipped with leakage fluid dram II 41, and leakage fluid dram I 31 and leakage fluid dram II 41 are respectively connected to steam
Distillation unit 5.
The outside of first condenser 3 and the second condenser 4 is respectively arranged the first condensing water conduit and the second condensing water conduit,
Condensed water 7 enters from the bottom of the second condensing water conduit, top outflow, then flows into the bottom of the first condensing water conduit, finally
It is flowed out via the top of the first condensing water conduit.
The material of tray 2 is stainless steel, is conducive to collected bamboo charcoal tiling heat dissipation.
Stirring rod is equipped in distilling apparatus 5.
Embodiment 2:
As shown in Figure 1, a kind of preparation process of bulb of thunberg fritillary plantation substrate, is as follows:
(1) by air-dried high mountain mao bamboon and cow dung according to mass ratio 8:1 input retort 1 connects the gas outlet of retort 1
11 and condensing plant, condensing plant is opened, closes bamboo charcoal discharge port 12 and activated carbon discharge nozzle 13, with the heating speed of 0.1 DEG C/s
Rate heats material temperature to 350 DEG C, charing process 20 minutes in this temperature range, the condensed equipment condensation of bamboo vinegar steam stream of generation
For crude bamboo vinegar, and the bottom for passing through condensing plant is expelled to distilling apparatus 5;
(2) continue to heat material temperature to 350 DEG C, open bamboo charcoal discharge port 12, the bamboo charcoal of discharge is collected using tray 2, and
Tile cooling;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray 2, until in retort 1
Residual mass is the 1/20 of input amount, closes bamboo charcoal discharge port 12;
(4) continue to heat material temperature to 700 DEG C or more, raw material is further cracked into activated carbon in retort 1, connects activated carbon
Discharge nozzle 13 makes activated carbon slowly enter the distilling apparatus 5 for being connected to crude bamboo vinegar, treats that crude bamboo vinegar collection finishes, closes
Condensing plant exports, and avoids flowing back;
(5) distilling apparatus 5 is warming up to 120 DEG C, is come into full contact with by stirring activated carbon with crude bamboo vinegar, generation
The condensed conduit 8 of steam enters refined bamboo vinegar reception device 6 after condensing, and stands 24 hours, and filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary as primary raw material with refined bamboo vinegar obtained by step (5) using bamboo charcoal obtained by step (3)
Plantation substrate.
It is pico- to open pressure reducing valve 14 in step (1), for adjusting pressure in retort 1;In step (3), close bamboo charcoal and go out
Pressure reducing valve 14 is also turn off while material mouth 12.
In step (1), the bamboo vinegar steam of generation, respectively will be cold from the bottom of two condensers followed by two condensers
Solidifying obtained crude bamboo vinegar is expelled to distilling apparatus 5.
In step (4), in distilling apparatus 5, the mass ratio of activated carbon and crude bamboo vinegar is 1:12.
In step (5), the pH=4.8 of refined bamboo vinegar.
The specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 3 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 5 hours, cross 40 mesh sieve, obtain burnt mud
Grey powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, standby
With;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), is then spread evenly
Mineral powders obtained by step (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar while stirring, measure simultaneously
The pH of system, until pH=5.8, stop sprinkling bamboo vinegar to get.
In step (6-2), thickness of earth covering is 1cm on hay.
In step (6-4), the mass ratio of mineral powders, bamboo charcoal powder and scorched clay dust powder is 1:4:8.
The whole-process control moisture in the preparation process of cultivation matrix, the moisture weight content of final gained cultivation matrix are less than
15%.
A kind of bulb of thunberg fritillary plantation substrate, is obtained by above-mentioned preparation process.
The corresponding a kind of preparation system of bulb of thunberg fritillary plantation substrate of above-mentioned preparation process, including bamboo charcoal preparation facilities and bamboo
Vinegar liquid preparation facilities two parts, bamboo charcoal preparation facilities are retort 1, and the main body of bamboo vinegar preparation facilities is condensing plant, is carbonized
The top and bottom of stove 1 are respectively equipped with gas outlet 11 and bamboo charcoal discharge port 12, and the lower section of bamboo charcoal discharge port 12 sets tray 2,
Gas outlet 11 is connected to the top of condensing plant, and the bottom of condensing plant is connected with distilling apparatus 5;The bottom of retort 1 is also set
Active charcoal discharge nozzle 13, activated carbon discharge nozzle 13 are connected to distilling apparatus 5;Distilling apparatus 5 passes through condensation pipe 8 and refined bamboo
Vinegar liquid reception device 6 connects.
The bottom of retort 1 is additionally provided with pressure reducing valve 14, and the bamboo vinegar steam that being arranged on bottom can prevent passes through pressure reducing valve
14 lose.
Condensing plant includes the first condenser 3 and the second condenser 4 of series connection, and the gas outlet 11 of retort 1 is connected to the
The top of one condenser 3, the bottom of the first condenser 3 are equipped with leakage fluid dram I 31 and exhaust outlet 32,32 and second condenser of exhaust outlet
4 top connection, the bottom of the second condenser 4 are equipped with leakage fluid dram II 41, and leakage fluid dram I 31 and leakage fluid dram II 41 are respectively connected to steam
Distillation unit 5.
The outside of first condenser 3 and the second condenser 4 is respectively arranged the first condensing water conduit and the second condensing water conduit,
Condensed water 7 enters from the bottom of the second condensing water conduit, top outflow, then flows into the bottom of the first condensing water conduit, finally
It is flowed out via the top of the first condensing water conduit.
The material of tray 2 is stainless steel, is conducive to collected bamboo charcoal tiling heat dissipation.
Stirring rod is equipped in distilling apparatus 5.
Embodiment 3:
As shown in Figure 1, a kind of preparation process of bulb of thunberg fritillary plantation substrate, is as follows:
(1) by air-dried high mountain mao bamboon and cow dung according to mass ratio 8:1 input retort 1 connects the gas outlet of retort 1
11 and condensing plant, condensing plant is opened, closes bamboo charcoal discharge port 12 and activated carbon discharge nozzle 13, with the heating speed of 0.1 DEG C/s
Rate heats material temperature to 300 DEG C, charing process 18 minutes in this temperature range, the condensed equipment condensation of bamboo vinegar steam stream of generation
For crude bamboo vinegar, and the bottom for passing through condensing plant is expelled to distilling apparatus 5;
(2) continue to heat material temperature to 320 DEG C, open bamboo charcoal discharge port 12, the bamboo charcoal of discharge is collected using tray 2, and
Tile cooling;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray 2, until in retort 1
Residual mass is the 1/20 of input amount, closes bamboo charcoal discharge port 12;
(4) continue to heat material temperature to 700 DEG C or more, raw material is further cracked into activated carbon in retort 1, connects activated carbon
Discharge nozzle 13 makes activated carbon slowly enter the distilling apparatus 5 for being connected to crude bamboo vinegar, treats that crude bamboo vinegar collection finishes, closes
Condensing plant exports, and avoids flowing back;
(5) distilling apparatus 5 is warming up to 120 DEG C, is come into full contact with by stirring activated carbon with crude bamboo vinegar, generation
The condensed conduit 8 of steam enters refined bamboo vinegar reception device 6 after condensing, and stands 24 hours, and filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary as primary raw material with refined bamboo vinegar obtained by step (5) using bamboo charcoal obtained by step (3)
Plantation substrate.
It is pico- to open pressure reducing valve 14 in step (1), for adjusting pressure in retort 1;In step (3), close bamboo charcoal and go out
Pressure reducing valve 14 is also turn off while material mouth 12.
In step (1), the bamboo vinegar steam of generation, respectively will be cold from the bottom of two condensers followed by two condensers
Solidifying obtained crude bamboo vinegar is expelled to distilling apparatus 5.
In step (4), in distilling apparatus 5, the mass ratio of activated carbon and crude bamboo vinegar is 1:12.
In step (5), the pH=4 of refined bamboo vinegar.
The specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 4 hours, cross 40 mesh sieve, obtain burnt mud
Grey powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, standby
With;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), is then spread evenly
Mineral powders obtained by step (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar while stirring, measure simultaneously
The pH of system, until pH=5.5, stop sprinkling bamboo vinegar to get.
In step (6-2), thickness of earth covering is 1cm on hay.
In step (6-4), the mass ratio of mineral powders, bamboo charcoal powder and scorched clay dust powder is 1:4:8.
The whole-process control moisture in the preparation process of cultivation matrix, the moisture weight content of final gained cultivation matrix are less than
15%.
Step (6-4) is also granulated after stopping spraying bamboo vinegar, controls the unit weight ranging from 1.2g/ of cultivation matrix
cm3。
A kind of bulb of thunberg fritillary plantation substrate, is obtained by above-mentioned preparation process.
The corresponding a kind of preparation system of bulb of thunberg fritillary plantation substrate of above-mentioned preparation process, including bamboo charcoal preparation facilities and bamboo
Vinegar liquid preparation facilities two parts, bamboo charcoal preparation facilities are retort 1, and the main body of bamboo vinegar preparation facilities is condensing plant, is carbonized
The top and bottom of stove 1 are respectively equipped with gas outlet 11 and bamboo charcoal discharge port 12, and the lower section of bamboo charcoal discharge port 12 sets tray 2,
Gas outlet 11 is connected to the top of condensing plant, and the bottom of condensing plant is connected with distilling apparatus 5;The bottom of retort 1 is also set
Active charcoal discharge nozzle 13, activated carbon discharge nozzle 13 are connected to distilling apparatus 5;Distilling apparatus 5 passes through condensation pipe 8 and refined bamboo
Vinegar liquid reception device 6 connects.
The bottom of retort 1 is additionally provided with pressure reducing valve 14, and the bamboo vinegar steam that being arranged on bottom can prevent passes through pressure reducing valve
14 lose.
Condensing plant includes the first condenser 3 and the second condenser 4 of series connection, and the gas outlet 11 of retort 1 is connected to the
The top of one condenser 3, the bottom of the first condenser 3 are equipped with leakage fluid dram I 31 and exhaust outlet 32,32 and second condenser of exhaust outlet
4 top connection, the bottom of the second condenser 4 are equipped with leakage fluid dram II 41, and leakage fluid dram I 31 and leakage fluid dram II 41 are respectively connected to steam
Distillation unit 5.
The outside of first condenser 3 and the second condenser 4 is respectively arranged the first condensing water conduit and the second condensing water conduit,
Condensed water 7 enters from the bottom of the second condensing water conduit, top outflow, then flows into the bottom of the first condensing water conduit, finally
It is flowed out via the top of the first condensing water conduit.
The material of tray 2 is stainless steel, is conducive to collected bamboo charcoal tiling heat dissipation.
Stirring rod is equipped in distilling apparatus 5.
Comparative example 1
A kind of preparation process of bulb of thunberg fritillary plantation substrate, is as follows:
(1) air-dried high mountain mao bamboon is put into retort, connects gas outlet and the condensing plant of retort, opened condensation and set
It is standby, bamboo charcoal discharge port and activated carbon discharge nozzle are closed, material temperature is heated to 300 DEG C with the heating rate of 0.1 DEG C/s, in this temperature model
Enclose interior charing process 18 minutes, the condensed equipment of bamboo vinegar steam stream of generation is condensed into crude bamboo vinegar, and pass through condensing plant
Bottom be expelled to distilling apparatus;
(2) continue to heat material temperature to 320 DEG C, open bamboo charcoal discharge port, the bamboo charcoal of discharge is collected using tray, and tile
Cooling;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray, until residual in retort
1/20 that quality is input amount is stayed, closes bamboo charcoal discharge port;
(4) continue to heat material temperature to 700 DEG C or more, raw material is further cracked into activated carbon in retort, connects activated carbon
Discharge nozzle makes activated carbon slowly enter the distilling apparatus for being connected to crude bamboo vinegar, treats that crude bamboo vinegar collection finishes, closes condensation
Equipment exports, and avoids flowing back;
(5) distilling apparatus is warming up to 120 DEG C, is come into full contact with by stirring activated carbon with crude bamboo vinegar, generation
Enter refined bamboo vinegar reception device after the condensed conduit condensation of steam, stand 24 hours, filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary as primary raw material with refined bamboo vinegar obtained by step (5) using bamboo charcoal obtained by step (3)
Plantation substrate.
In step (1), pressure reducing valve is opened slightly, for adjusting pressure in retort;In step (3), bamboo charcoal discharging is closed
Pressure reducing valve is also turn off while mouth.
In step (1), the bamboo vinegar steam of generation, respectively will be cold from the bottom of two condensers followed by two condensers
Solidifying obtained crude bamboo vinegar is expelled to distilling apparatus.
In step (4), in distilling apparatus, the mass ratio of activated carbon and crude bamboo vinegar is 1:12.
In step (5), the pH=4 of refined bamboo vinegar.
The specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 4 hours, cross 40 mesh sieve, obtain burnt mud
Grey powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, standby
With;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), is then spread evenly
Mineral powders obtained by step (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar while stirring, measure simultaneously
The pH of system, until pH=5.5, stop sprinkling bamboo vinegar to get.
In step (6-2), thickness of earth covering is 1cm on hay.
In step (6-4), the mass ratio of mineral powders, bamboo charcoal powder and scorched clay dust powder is 1:4:8.
The whole-process control moisture in the preparation process of cultivation matrix, the moisture weight content of final gained cultivation matrix are less than
15%.
Step (6-4) is also granulated after stopping spraying bamboo vinegar, controls the unit weight ranging from 1.2g/ of cultivation matrix
cm3。
A kind of bulb of thunberg fritillary plantation substrate, is obtained by above-mentioned preparation process.
Comparative example 2
A kind of preparation process of bulb of thunberg fritillary plantation substrate, is as follows:
(1) by air-dried high mountain mao bamboon and cow dung according to mass ratio 8:1 input retort, connect the gas outlet of retort with
Condensing plant opens condensing plant, closes bamboo charcoal discharge port and activated carbon discharge nozzle, and material is heated with the heating rate of 0.1 DEG C/s
Temperature is to 300 DEG C, charing process 18 minutes in this temperature range, and the condensed equipment of bamboo vinegar steam stream of generation is condensed into crude bamboo
Vinegar liquid, and the bottom for passing through condensing plant is expelled to distilling apparatus;
(2) continue to heat material temperature to 320 DEG C, open bamboo charcoal discharge port, the bamboo charcoal of discharge is collected using tray, and tile
Cooling;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray, until residual in retort
1/20 that quality is input amount is stayed, closes bamboo charcoal discharge port;
(4) condensing plant outlet is closed, avoids flowing back;
(5) distilling apparatus is warming up to 120 DEG C, and entering refined bamboo vinegar after the condensed conduit condensation of steam of generation receives dress
It puts, stands 24 hours, filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary as primary raw material with refined bamboo vinegar obtained by step (5) using bamboo charcoal obtained by step (3)
Plantation substrate.
In step (1), pressure reducing valve is opened slightly, for adjusting pressure in retort;In step (3), bamboo charcoal discharging is closed
Pressure reducing valve is also turn off while mouth.
In step (1), the bamboo vinegar steam of generation, respectively will be cold from the bottom of two condensers followed by two condensers
Solidifying obtained crude bamboo vinegar is expelled to distilling apparatus.
The specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 4 hours, cross 40 mesh sieve, obtain burnt mud
Grey powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, standby
With;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), is then spread evenly
Mineral powders obtained by step (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar while stirring, measure simultaneously
The pH of system, until pH=5.5, stop sprinkling bamboo vinegar to get.
In step (6-2), thickness of earth covering is 1cm on hay.
In step (6-4), the mass ratio of mineral powders, bamboo charcoal powder and scorched clay dust powder is 1:4:8.
The whole-process control moisture in the preparation process of cultivation matrix, the moisture weight content of final gained cultivation matrix are less than
15%.
Step (6-4) is also granulated after stopping spraying bamboo vinegar, controls the unit weight ranging from 1.2g/ of cultivation matrix
cm3。
A kind of bulb of thunberg fritillary plantation substrate, is obtained by above-mentioned preparation process.
Comparative example 3
A kind of cultivation matrix is according to mass ratio 4 by bamboo charcoal powder and scorched clay dust powder:8 are obtained by mixing.The preparation of bamboo charcoal powder
Method:Bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2 hours, obtain bamboo charcoal powder.The preparation method of scorched clay dust powder:It utilizes
The soil of hay overlying 1cm thickness, with fiery smoke curing into scorched clay dust, 105 DEG C dry 4 hours, cross 40 mesh sieve, obtain scorched clay dust powder.
Test example
The cultivation matrix for preparing Examples 1 to 3 or comparative example 1~3 carries out bulb of thunberg fritillary bulb nursery, and specific method is:10
In the last ten-days period moon, bulb of thunberg fritillary bulb (diameter 3cm) is embedded in cultivation matrix, institute's buried depth degree is 6cm, and seedling raise period is 15 days.It investigates and plants
It trains the miscellaneous bacteria rate of matrix and carries out the emergence rate of bulb of thunberg fritillary bulb nursery using it, the results are shown in Table 1.
The miscellaneous bacteria rate of 1. cultivation matrix of table and the emergence rate using its progress bulb of thunberg fritillary bulb nursery
|
Miscellaneous bacteria rate (%) |
Emergence rate (%) |
Embodiment 1 |
≤0.5 |
97 |
Embodiment 2 |
≤0.5 |
97 |
Embodiment 3 |
≤0.5 |
99 |
Comparative example 1 |
≤0.5 |
85 |
Comparative example 2 |
12 |
83 |
Comparative example 3 |
25 |
65 |
As shown in Table 1, the cultivation matrix of Examples 1 to 3 has relatively low miscellaneous bacteria rate, and bulb of thunberg fritillary bulb nursery is carried out using it
Emergence rate it is high.Comparative example 1 omits cow dung, and emergence rate is substantially reduced;Comparative example 2, which omits, to be generated activated carbon and is conducted into
The step of crude bamboo vinegar, the miscellaneous bacteria rate of cultivation matrix significantly rise, and it is apparent to carry out the emergence rate of bulb of thunberg fritillary bulb nursery using it
It reduces;The cultivation matrix of comparative example 3 is not added with bamboo charcoal and bamboo vinegar, and miscellaneous bacteria rate and emergence rate two indices are undesirable.
Above-mentioned, although the foregoing specific embodiments of the present invention is described with reference to the accompanying drawings, not protects model to the present invention
The limitation enclosed, based on the technical solutions of the present invention, those skilled in the art are not needed to make the creative labor and can be done
The various modifications or changes gone out are still within protection scope of the present invention.