CN108243900A - A kind of bulb of thunberg fritillary plantation substrate, preparation process and system - Google Patents

A kind of bulb of thunberg fritillary plantation substrate, preparation process and system Download PDF

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Publication number
CN108243900A
CN108243900A CN201810100209.3A CN201810100209A CN108243900A CN 108243900 A CN108243900 A CN 108243900A CN 201810100209 A CN201810100209 A CN 201810100209A CN 108243900 A CN108243900 A CN 108243900A
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bamboo
bulb
bamboo charcoal
bamboo vinegar
retort
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CN108243900B (en
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黄盼盼
蒲加兴
蒲加军
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SEEK BIO-TECHNOLOGY (SHANGHAI) Co Ltd
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SEEK BIO-TECHNOLOGY (SHANGHAI) Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00Other inorganic fertilisers
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10CWORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
    • C10C5/00Production of pyroligneous acid distillation of wood, dry distillation of organic waste
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/10Biofuels, e.g. bio-diesel

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cultivation Of Plants (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of bulb of thunberg fritillary plantation substrate, preparation process and systems, it compounds to obtain a kind of bulb of thunberg fritillary plantation substrate using bamboo charcoal and refined bamboo vinegar as primary raw material, not only the nursery of bulb had been used directly for, but also can directly apply plot conduct and accompany fertilizer ground substance.The maximization that nutrient needed for the breeding of bulb of thunberg fritillary bulb is realized using the cultivation matrix is compounded, and is ensured maximally utilizing for critical nutrients, is finally realized the raising of bulb of thunberg fritillary vegetative propagation emergence rate.

Description

A kind of bulb of thunberg fritillary plantation substrate, preparation process and system
Technical field
The present invention relates to a kind of cultivation matrixes, and in particular to a kind of bulb of thunberg fritillary plantation substrate, preparation system and technique.Belong to In bulb of thunberg fritillary technical field of cultivation.
Background technology
The solution efficiently emerged for bulb of thunberg fritillary is not found at present, is all traditional nursery means, from agrotechnical angle Degree goes to improve planting percent.Bulb of thunberg fritillary is usually to form bulb in summer, and more after the summer, nursery will be used as in 10 annual~November The bulb on basis digs up to rearrange again and is seeded into ground namely forms bulb to sowing (intermediate meeting next time in bulb of thunberg fritillary The high bulb of a collection of commodity is dug out to be peddled) during, the bulb as seedling substrate will be embedded in ground borough chief up to 2~3 As long as month, encounter the time more than rainwater, bulb it is rotten be it is very serious, directly result in the reduction of the yield of bulb of thunberg fritillary, bring through Loss in Ji.
Bulb of thunberg fritillary mainly realizes that expansion is numerous by bulb breeding and tissue cultures in process of production.It is low for bulb of thunberg fritillary emergence rate The problem of, it is related to the nursery of bulb of thunberg fritillary, is badly in need of a kind of seedling medium at present, according to the nutrient demand in bulb of thunberg fritillary bulb plumule emergence Promote bulb seedling to formulate efficient formula.
Invention content
The purpose of the present invention is to overcome above-mentioned the deficiencies in the prior art, provide a kind of bulb of thunberg fritillary plantation substrate, prepare Technique and system.
To achieve the above object, the present invention uses following technical proposals:
A kind of preparation process of bulb of thunberg fritillary plantation substrate, is as follows:
(1) by air-dried high mountain mao bamboon and cow dung according to mass ratio 8:1 input retort, connect the gas outlet of retort with Condensing plant opens condensing plant, closes bamboo charcoal discharge port and activated carbon discharge nozzle, and material is heated with the heating rate of 0.1 DEG C/s Temperature is to 250~350 DEG C, charing process 15~20 minutes in this temperature range, and the condensed equipment of bamboo vinegar steam stream of generation is cold It coagulates for crude bamboo vinegar, and the bottom for passing through condensing plant is expelled to distilling apparatus;
(2) continue to heat material temperature to 300~350 DEG C, open bamboo charcoal discharge port, the bamboo charcoal of discharge is collected using tray, And the cooling that tiles;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray, until residual in retort 1/20 that quality is input amount is stayed, closes bamboo charcoal discharge port;
(4) continue to heat material temperature to 700 DEG C or more, raw material is further cracked into activated carbon in retort, connects activated carbon Discharge nozzle makes activated carbon slowly enter the distilling apparatus for being connected to crude bamboo vinegar, treats that crude bamboo vinegar collection finishes, closes condensation Equipment exports, and avoids flowing back;
(5) distilling apparatus is warming up to 120 DEG C, is come into full contact with by stirring activated carbon with crude bamboo vinegar, generation Enter refined bamboo vinegar reception device after the condensed conduit condensation of steam, stand 24 hours, filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary as primary raw material with refined bamboo vinegar obtained by step (5) using bamboo charcoal obtained by step (3) Plantation substrate.
Preferably, in step (1), pressure reducing valve is opened slightly, for adjusting pressure in retort;In step (3), bamboo is closed Pressure reducing valve is also turn off while charcoal discharge port.
Preferably, in step (1), the bamboo vinegar steam of generation is followed by two condensers, respectively from two condensers The crude bamboo vinegar that condensation obtains is expelled to distilling apparatus by bottom.
Preferably, in step (4), in distilling apparatus, the mass ratio of activated carbon and crude bamboo vinegar is 1:12.
Preferably, in step (5), pH=3.4~4.8 of refined bamboo vinegar.
Preferably, the specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2~3 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 3~5 hours, cross 40 mesh sieve, obtain Scorched clay dust powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, standby With;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), is then spread evenly Mineral powders obtained by step (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar while stirring, measure simultaneously The pH of system, until pH=5~5.8, stop sprinkling bamboo vinegar to get.
It is further preferred that in step (6-2), thickness of earth covering is 1cm on hay.
It is further preferred that in step (6-4), the mass ratio of mineral powders, bamboo charcoal powder and scorched clay dust powder is 1:4: 8。
It is further preferred that the whole-process control moisture in the preparation process of cultivation matrix, the water of final gained cultivation matrix Weight content is divided to be less than 15%.
It is further preferred that step (6-4) is also granulated after stopping spraying bamboo vinegar, controls the appearance of cultivation matrix Weight ranging from 1.15~1.27g/cm3
A kind of bulb of thunberg fritillary plantation substrate, is obtained by above-mentioned preparation process.
Bulb of thunberg fritillary bulb nursery is carried out using above-mentioned cultivation matrix, specific method is:In late October, bulb of thunberg fritillary bulb is embedded in In the cultivation matrix, institute's buried depth degree is 2 times, about 5~7cm of bulb of thunberg fritillary bulb diameter, and seedling raise period is 14~20 days.
The corresponding a kind of preparation system of bulb of thunberg fritillary plantation substrate of above-mentioned preparation process, including bamboo charcoal preparation facilities and bamboo Vinegar liquid preparation facilities two parts, the bamboo charcoal preparation facilities are retort, and the main body of bamboo vinegar preparation facilities is condensing plant, charcoal Change and be respectively equipped with gas outlet and bamboo charcoal discharge port at the top and bottom of stove, the lower section setting tray of bamboo charcoal discharge port, it is described go out Gas port is connected to the top of condensing plant, and the bottom of condensing plant is connected with distilling apparatus;The bottom of the retort is additionally provided with Activated carbon discharge nozzle, activated carbon discharge nozzle are connected to distilling apparatus;The distilling apparatus passes through condensation pipe and refined bamboo vinegar Reception device connects.
Preferably, the bottom of the retort is additionally provided with pressure reducing valve, and the bamboo vinegar steam that being arranged on bottom can prevent leads to Pressure reducing valve is crossed to lose.
Preferably, the condensing plant includes the first condenser and the second condenser of series connection, and the gas outlet of retort connects It is connected to the top of the first condenser, the bottom of the first condenser is equipped with leakage fluid dram I and exhaust outlet, exhaust outlet and the second condenser Top connects, and the bottom of the second condenser is equipped with leakage fluid dram II, and the leakage fluid dram I and leakage fluid dram II are respectively connected to distillation dress It puts.
It is further preferred that the outside of first condenser and the second condenser be respectively arranged the first condensing water conduit and Second condensing water conduit, condensed water enter from the bottom of the second condensing water conduit, and top outflow then flows into the first condensate pipe The bottom in road is finally flowed out via the top of the first condensing water conduit.
Preferably, the material of the tray is stainless steel, is conducive to collected bamboo charcoal tiling heat dissipation.
Preferably, stirring rod is equipped in the distilling apparatus.
Beneficial effects of the present invention:
The present invention compounds to obtain a kind of bulb of thunberg fritillary plantation substrate using bamboo charcoal and refined bamboo vinegar as primary raw material, both can be with The nursery of bulb is directly used in, while can directly apply plot conduct again and accompany fertilizer ground substance.Zhejiang is realized using the cultivation matrix The maximization compounding of nutrient needed for the breeding of shellfish bulb, ensures maximally utilizing for critical nutrients, it is asexual numerous finally to realize bulb of thunberg fritillary Grow the raising of emergence rate.The key problem in technology of the present invention is that the quality of bamboo charcoal and refined bamboo vinegar improves, and corresponding is to prepare work The innovation of skill, it is specific as follows:
1st, bulb of thunberg fritillary growth is more sensitive for elements such as N, K, Mg, Zn, Cu, therefore in the process of cultivation matrix raw material compounding It is middle to need to add in the more raw material of available nutrient, the high mountain mao bamboon of special ratios is formed with cow dung by specific calcine technology The maximized bamboo charcoal of nutrient is imitated, makes it have physically better absorption property, fertilizer conservation effect is good, and the nutrient of compounding is avoided quickly to flow It loses, slow release nutrient is more advantageous to bulb of thunberg fritillary bulb seedling.Wherein, the addition of cow dung helps to improve the ash content of gained bamboo charcoal, Increase effective nitrogen content.
2nd, the difference of bamboo vinegar refines mode and is affected for the property of itself, needs to control the refined bamboo vinegar of gained PH=3.4~4.8 of liquid are proper, organic matter mass content 8% or so (organic acid, phenols, ketone, aldehydes, alcohols, three Terpene, heterocyclic compound), the bamboo vinegar of such quality can play its maximum effect when matrix compounds, and be conducive to bulb of thunberg fritillary bulb Seedling.In addition, the bamboo vinegar of the present invention can effectively kill harmful bacteria, the relatively low miscellaneous bacteria rate of matrix is controlled.
3rd, the activated carbon that retort is generated at 700 DEG C or more mixes distillation with crude bamboo vinegar, on the one hand can adsorb thick Harmful substance and impurity in bamboo vinegar processed, on the other hand can effectively improve gained refined bamboo vinegar pH, adjusted to PH=3.4~4.8, avoid refined bamboo vinegar peracid, so in compound process by the pH of matrix it is too fast be reduced to reasonable value with Under, simultaneously so that refined bamboo vinegar retains ammonium ions more as possible, reduces the loss late of nitrogen.
4th, the habit grown according to bulb of thunberg fritillary, it is desirable that growing environment slant acidity, nutrient content are high, can by granulating technique, Matrix unit weight is controlled in 1.15~1.27g/cm3, pH=5~5.8 can ensure good fertilizer conservation water storage performance, to promote squama Stem-root.
Description of the drawings
Fig. 1 is the preparation system structure diagram of the present invention;
Wherein, 1 is retort, and 11 be gas outlet, and 12 be bamboo charcoal discharge port, and 13 be activated carbon discharge nozzle, and 14 be pressure reducing valve, 2 be tray, and 3 be the first condenser, and 31 be leakage fluid dram I, and 32 be exhaust outlet, and 4 be the second condenser, and 41 be leakage fluid dram II, and 5 are Distilling apparatus, 6 be refined bamboo vinegar reception device, and 7 be condensed water, and 8 be condensation pipe.
Specific embodiment
The present invention will be further elaborated with reference to the accompanying drawings and examples, it should which explanation, the description below is only It is to explain the present invention, its content is not defined.
Embodiment 1:
As shown in Figure 1, a kind of preparation process of bulb of thunberg fritillary plantation substrate, is as follows:
(1) by air-dried high mountain mao bamboon and cow dung according to mass ratio 8:1 input retort 1 connects the gas outlet of retort 1 11 and condensing plant, condensing plant is opened, closes bamboo charcoal discharge port 12 and activated carbon discharge nozzle 13, with the heating speed of 0.1 DEG C/s Rate heats material temperature to 250 DEG C, charing process 15 minutes in this temperature range, the condensed equipment condensation of bamboo vinegar steam stream of generation For crude bamboo vinegar, and the bottom for passing through condensing plant is expelled to distilling apparatus 5;
(2) continue to heat material temperature to 300 DEG C, open bamboo charcoal discharge port 12, the bamboo charcoal of discharge is collected using tray 2, and Tile cooling;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray 2, until in retort 1 Residual mass is the 1/20 of input amount, closes bamboo charcoal discharge port 12;
(4) continue to heat material temperature to 700 DEG C or more, raw material is further cracked into activated carbon in retort 1, connects activated carbon Discharge nozzle 13 makes activated carbon slowly enter the distilling apparatus 5 for being connected to crude bamboo vinegar, treats that crude bamboo vinegar collection finishes, closes Condensing plant exports, and avoids flowing back;
(5) distilling apparatus 5 is warming up to 120 DEG C, is come into full contact with by stirring activated carbon with crude bamboo vinegar, generation The condensed conduit 8 of steam enters refined bamboo vinegar reception device 6 after condensing, and stands 24 hours, and filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary as primary raw material with refined bamboo vinegar obtained by step (5) using bamboo charcoal obtained by step (3) Plantation substrate.
It is pico- to open pressure reducing valve 14 in step (1), for adjusting pressure in retort 1;In step (3), close bamboo charcoal and go out Pressure reducing valve 14 is also turn off while material mouth 12.
In step (1), the bamboo vinegar steam of generation, respectively will be cold from the bottom of two condensers followed by two condensers Solidifying obtained crude bamboo vinegar is expelled to distilling apparatus 5.
In step (4), in distilling apparatus 5, the mass ratio of activated carbon and crude bamboo vinegar is 1:12.
In step (5), the pH=3.4 of refined bamboo vinegar.
The specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 3 hours, cross 40 mesh sieve, obtain burnt mud Grey powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, standby With;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), is then spread evenly Mineral powders obtained by step (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar while stirring, measure simultaneously The pH of system, until pH=5, stop sprinkling bamboo vinegar to get.
In step (6-2), thickness of earth covering is 1cm on hay.
In step (6-4), the mass ratio of mineral powders, bamboo charcoal powder and scorched clay dust powder is 1:4:8.
The whole-process control moisture in the preparation process of cultivation matrix, the moisture weight content of final gained cultivation matrix are less than 15%.
A kind of bulb of thunberg fritillary plantation substrate, is obtained by above-mentioned preparation process.
The corresponding a kind of preparation system of bulb of thunberg fritillary plantation substrate of above-mentioned preparation process, including bamboo charcoal preparation facilities and bamboo Vinegar liquid preparation facilities two parts, bamboo charcoal preparation facilities are retort 1, and the main body of bamboo vinegar preparation facilities is condensing plant, is carbonized The top and bottom of stove 1 are respectively equipped with gas outlet 11 and bamboo charcoal discharge port 12, and the lower section of bamboo charcoal discharge port 12 sets tray 2, Gas outlet 11 is connected to the top of condensing plant, and the bottom of condensing plant is connected with distilling apparatus 5;The bottom of retort 1 is also set Active charcoal discharge nozzle 13, activated carbon discharge nozzle 13 are connected to distilling apparatus 5;Distilling apparatus 5 passes through condensation pipe 8 and refined bamboo Vinegar liquid reception device 6 connects.
The bottom of retort 1 is additionally provided with pressure reducing valve 14, and the bamboo vinegar steam that being arranged on bottom can prevent passes through pressure reducing valve 14 lose.
Condensing plant includes the first condenser 3 and the second condenser 4 of series connection, and the gas outlet 11 of retort 1 is connected to the The top of one condenser 3, the bottom of the first condenser 3 are equipped with leakage fluid dram I 31 and exhaust outlet 32,32 and second condenser of exhaust outlet 4 top connection, the bottom of the second condenser 4 are equipped with leakage fluid dram II 41, and leakage fluid dram I 31 and leakage fluid dram II 41 are respectively connected to steam Distillation unit 5.
The outside of first condenser 3 and the second condenser 4 is respectively arranged the first condensing water conduit and the second condensing water conduit, Condensed water 7 enters from the bottom of the second condensing water conduit, top outflow, then flows into the bottom of the first condensing water conduit, finally It is flowed out via the top of the first condensing water conduit.
The material of tray 2 is stainless steel, is conducive to collected bamboo charcoal tiling heat dissipation.
Stirring rod is equipped in distilling apparatus 5.
Embodiment 2:
As shown in Figure 1, a kind of preparation process of bulb of thunberg fritillary plantation substrate, is as follows:
(1) by air-dried high mountain mao bamboon and cow dung according to mass ratio 8:1 input retort 1 connects the gas outlet of retort 1 11 and condensing plant, condensing plant is opened, closes bamboo charcoal discharge port 12 and activated carbon discharge nozzle 13, with the heating speed of 0.1 DEG C/s Rate heats material temperature to 350 DEG C, charing process 20 minutes in this temperature range, the condensed equipment condensation of bamboo vinegar steam stream of generation For crude bamboo vinegar, and the bottom for passing through condensing plant is expelled to distilling apparatus 5;
(2) continue to heat material temperature to 350 DEG C, open bamboo charcoal discharge port 12, the bamboo charcoal of discharge is collected using tray 2, and Tile cooling;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray 2, until in retort 1 Residual mass is the 1/20 of input amount, closes bamboo charcoal discharge port 12;
(4) continue to heat material temperature to 700 DEG C or more, raw material is further cracked into activated carbon in retort 1, connects activated carbon Discharge nozzle 13 makes activated carbon slowly enter the distilling apparatus 5 for being connected to crude bamboo vinegar, treats that crude bamboo vinegar collection finishes, closes Condensing plant exports, and avoids flowing back;
(5) distilling apparatus 5 is warming up to 120 DEG C, is come into full contact with by stirring activated carbon with crude bamboo vinegar, generation The condensed conduit 8 of steam enters refined bamboo vinegar reception device 6 after condensing, and stands 24 hours, and filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary as primary raw material with refined bamboo vinegar obtained by step (5) using bamboo charcoal obtained by step (3) Plantation substrate.
It is pico- to open pressure reducing valve 14 in step (1), for adjusting pressure in retort 1;In step (3), close bamboo charcoal and go out Pressure reducing valve 14 is also turn off while material mouth 12.
In step (1), the bamboo vinegar steam of generation, respectively will be cold from the bottom of two condensers followed by two condensers Solidifying obtained crude bamboo vinegar is expelled to distilling apparatus 5.
In step (4), in distilling apparatus 5, the mass ratio of activated carbon and crude bamboo vinegar is 1:12.
In step (5), the pH=4.8 of refined bamboo vinegar.
The specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 3 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 5 hours, cross 40 mesh sieve, obtain burnt mud Grey powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, standby With;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), is then spread evenly Mineral powders obtained by step (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar while stirring, measure simultaneously The pH of system, until pH=5.8, stop sprinkling bamboo vinegar to get.
In step (6-2), thickness of earth covering is 1cm on hay.
In step (6-4), the mass ratio of mineral powders, bamboo charcoal powder and scorched clay dust powder is 1:4:8.
The whole-process control moisture in the preparation process of cultivation matrix, the moisture weight content of final gained cultivation matrix are less than 15%.
A kind of bulb of thunberg fritillary plantation substrate, is obtained by above-mentioned preparation process.
The corresponding a kind of preparation system of bulb of thunberg fritillary plantation substrate of above-mentioned preparation process, including bamboo charcoal preparation facilities and bamboo Vinegar liquid preparation facilities two parts, bamboo charcoal preparation facilities are retort 1, and the main body of bamboo vinegar preparation facilities is condensing plant, is carbonized The top and bottom of stove 1 are respectively equipped with gas outlet 11 and bamboo charcoal discharge port 12, and the lower section of bamboo charcoal discharge port 12 sets tray 2, Gas outlet 11 is connected to the top of condensing plant, and the bottom of condensing plant is connected with distilling apparatus 5;The bottom of retort 1 is also set Active charcoal discharge nozzle 13, activated carbon discharge nozzle 13 are connected to distilling apparatus 5;Distilling apparatus 5 passes through condensation pipe 8 and refined bamboo Vinegar liquid reception device 6 connects.
The bottom of retort 1 is additionally provided with pressure reducing valve 14, and the bamboo vinegar steam that being arranged on bottom can prevent passes through pressure reducing valve 14 lose.
Condensing plant includes the first condenser 3 and the second condenser 4 of series connection, and the gas outlet 11 of retort 1 is connected to the The top of one condenser 3, the bottom of the first condenser 3 are equipped with leakage fluid dram I 31 and exhaust outlet 32,32 and second condenser of exhaust outlet 4 top connection, the bottom of the second condenser 4 are equipped with leakage fluid dram II 41, and leakage fluid dram I 31 and leakage fluid dram II 41 are respectively connected to steam Distillation unit 5.
The outside of first condenser 3 and the second condenser 4 is respectively arranged the first condensing water conduit and the second condensing water conduit, Condensed water 7 enters from the bottom of the second condensing water conduit, top outflow, then flows into the bottom of the first condensing water conduit, finally It is flowed out via the top of the first condensing water conduit.
The material of tray 2 is stainless steel, is conducive to collected bamboo charcoal tiling heat dissipation.
Stirring rod is equipped in distilling apparatus 5.
Embodiment 3:
As shown in Figure 1, a kind of preparation process of bulb of thunberg fritillary plantation substrate, is as follows:
(1) by air-dried high mountain mao bamboon and cow dung according to mass ratio 8:1 input retort 1 connects the gas outlet of retort 1 11 and condensing plant, condensing plant is opened, closes bamboo charcoal discharge port 12 and activated carbon discharge nozzle 13, with the heating speed of 0.1 DEG C/s Rate heats material temperature to 300 DEG C, charing process 18 minutes in this temperature range, the condensed equipment condensation of bamboo vinegar steam stream of generation For crude bamboo vinegar, and the bottom for passing through condensing plant is expelled to distilling apparatus 5;
(2) continue to heat material temperature to 320 DEG C, open bamboo charcoal discharge port 12, the bamboo charcoal of discharge is collected using tray 2, and Tile cooling;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray 2, until in retort 1 Residual mass is the 1/20 of input amount, closes bamboo charcoal discharge port 12;
(4) continue to heat material temperature to 700 DEG C or more, raw material is further cracked into activated carbon in retort 1, connects activated carbon Discharge nozzle 13 makes activated carbon slowly enter the distilling apparatus 5 for being connected to crude bamboo vinegar, treats that crude bamboo vinegar collection finishes, closes Condensing plant exports, and avoids flowing back;
(5) distilling apparatus 5 is warming up to 120 DEG C, is come into full contact with by stirring activated carbon with crude bamboo vinegar, generation The condensed conduit 8 of steam enters refined bamboo vinegar reception device 6 after condensing, and stands 24 hours, and filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary as primary raw material with refined bamboo vinegar obtained by step (5) using bamboo charcoal obtained by step (3) Plantation substrate.
It is pico- to open pressure reducing valve 14 in step (1), for adjusting pressure in retort 1;In step (3), close bamboo charcoal and go out Pressure reducing valve 14 is also turn off while material mouth 12.
In step (1), the bamboo vinegar steam of generation, respectively will be cold from the bottom of two condensers followed by two condensers Solidifying obtained crude bamboo vinegar is expelled to distilling apparatus 5.
In step (4), in distilling apparatus 5, the mass ratio of activated carbon and crude bamboo vinegar is 1:12.
In step (5), the pH=4 of refined bamboo vinegar.
The specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 4 hours, cross 40 mesh sieve, obtain burnt mud Grey powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, standby With;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), is then spread evenly Mineral powders obtained by step (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar while stirring, measure simultaneously The pH of system, until pH=5.5, stop sprinkling bamboo vinegar to get.
In step (6-2), thickness of earth covering is 1cm on hay.
In step (6-4), the mass ratio of mineral powders, bamboo charcoal powder and scorched clay dust powder is 1:4:8.
The whole-process control moisture in the preparation process of cultivation matrix, the moisture weight content of final gained cultivation matrix are less than 15%.
Step (6-4) is also granulated after stopping spraying bamboo vinegar, controls the unit weight ranging from 1.2g/ of cultivation matrix cm3
A kind of bulb of thunberg fritillary plantation substrate, is obtained by above-mentioned preparation process.
The corresponding a kind of preparation system of bulb of thunberg fritillary plantation substrate of above-mentioned preparation process, including bamboo charcoal preparation facilities and bamboo Vinegar liquid preparation facilities two parts, bamboo charcoal preparation facilities are retort 1, and the main body of bamboo vinegar preparation facilities is condensing plant, is carbonized The top and bottom of stove 1 are respectively equipped with gas outlet 11 and bamboo charcoal discharge port 12, and the lower section of bamboo charcoal discharge port 12 sets tray 2, Gas outlet 11 is connected to the top of condensing plant, and the bottom of condensing plant is connected with distilling apparatus 5;The bottom of retort 1 is also set Active charcoal discharge nozzle 13, activated carbon discharge nozzle 13 are connected to distilling apparatus 5;Distilling apparatus 5 passes through condensation pipe 8 and refined bamboo Vinegar liquid reception device 6 connects.
The bottom of retort 1 is additionally provided with pressure reducing valve 14, and the bamboo vinegar steam that being arranged on bottom can prevent passes through pressure reducing valve 14 lose.
Condensing plant includes the first condenser 3 and the second condenser 4 of series connection, and the gas outlet 11 of retort 1 is connected to the The top of one condenser 3, the bottom of the first condenser 3 are equipped with leakage fluid dram I 31 and exhaust outlet 32,32 and second condenser of exhaust outlet 4 top connection, the bottom of the second condenser 4 are equipped with leakage fluid dram II 41, and leakage fluid dram I 31 and leakage fluid dram II 41 are respectively connected to steam Distillation unit 5.
The outside of first condenser 3 and the second condenser 4 is respectively arranged the first condensing water conduit and the second condensing water conduit, Condensed water 7 enters from the bottom of the second condensing water conduit, top outflow, then flows into the bottom of the first condensing water conduit, finally It is flowed out via the top of the first condensing water conduit.
The material of tray 2 is stainless steel, is conducive to collected bamboo charcoal tiling heat dissipation.
Stirring rod is equipped in distilling apparatus 5.
Comparative example 1
A kind of preparation process of bulb of thunberg fritillary plantation substrate, is as follows:
(1) air-dried high mountain mao bamboon is put into retort, connects gas outlet and the condensing plant of retort, opened condensation and set It is standby, bamboo charcoal discharge port and activated carbon discharge nozzle are closed, material temperature is heated to 300 DEG C with the heating rate of 0.1 DEG C/s, in this temperature model Enclose interior charing process 18 minutes, the condensed equipment of bamboo vinegar steam stream of generation is condensed into crude bamboo vinegar, and pass through condensing plant Bottom be expelled to distilling apparatus;
(2) continue to heat material temperature to 320 DEG C, open bamboo charcoal discharge port, the bamboo charcoal of discharge is collected using tray, and tile Cooling;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray, until residual in retort 1/20 that quality is input amount is stayed, closes bamboo charcoal discharge port;
(4) continue to heat material temperature to 700 DEG C or more, raw material is further cracked into activated carbon in retort, connects activated carbon Discharge nozzle makes activated carbon slowly enter the distilling apparatus for being connected to crude bamboo vinegar, treats that crude bamboo vinegar collection finishes, closes condensation Equipment exports, and avoids flowing back;
(5) distilling apparatus is warming up to 120 DEG C, is come into full contact with by stirring activated carbon with crude bamboo vinegar, generation Enter refined bamboo vinegar reception device after the condensed conduit condensation of steam, stand 24 hours, filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary as primary raw material with refined bamboo vinegar obtained by step (5) using bamboo charcoal obtained by step (3) Plantation substrate.
In step (1), pressure reducing valve is opened slightly, for adjusting pressure in retort;In step (3), bamboo charcoal discharging is closed Pressure reducing valve is also turn off while mouth.
In step (1), the bamboo vinegar steam of generation, respectively will be cold from the bottom of two condensers followed by two condensers Solidifying obtained crude bamboo vinegar is expelled to distilling apparatus.
In step (4), in distilling apparatus, the mass ratio of activated carbon and crude bamboo vinegar is 1:12.
In step (5), the pH=4 of refined bamboo vinegar.
The specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 4 hours, cross 40 mesh sieve, obtain burnt mud Grey powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, standby With;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), is then spread evenly Mineral powders obtained by step (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar while stirring, measure simultaneously The pH of system, until pH=5.5, stop sprinkling bamboo vinegar to get.
In step (6-2), thickness of earth covering is 1cm on hay.
In step (6-4), the mass ratio of mineral powders, bamboo charcoal powder and scorched clay dust powder is 1:4:8.
The whole-process control moisture in the preparation process of cultivation matrix, the moisture weight content of final gained cultivation matrix are less than 15%.
Step (6-4) is also granulated after stopping spraying bamboo vinegar, controls the unit weight ranging from 1.2g/ of cultivation matrix cm3
A kind of bulb of thunberg fritillary plantation substrate, is obtained by above-mentioned preparation process.
Comparative example 2
A kind of preparation process of bulb of thunberg fritillary plantation substrate, is as follows:
(1) by air-dried high mountain mao bamboon and cow dung according to mass ratio 8:1 input retort, connect the gas outlet of retort with Condensing plant opens condensing plant, closes bamboo charcoal discharge port and activated carbon discharge nozzle, and material is heated with the heating rate of 0.1 DEG C/s Temperature is to 300 DEG C, charing process 18 minutes in this temperature range, and the condensed equipment of bamboo vinegar steam stream of generation is condensed into crude bamboo Vinegar liquid, and the bottom for passing through condensing plant is expelled to distilling apparatus;
(2) continue to heat material temperature to 320 DEG C, open bamboo charcoal discharge port, the bamboo charcoal of discharge is collected using tray, and tile Cooling;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray, until residual in retort 1/20 that quality is input amount is stayed, closes bamboo charcoal discharge port;
(4) condensing plant outlet is closed, avoids flowing back;
(5) distilling apparatus is warming up to 120 DEG C, and entering refined bamboo vinegar after the condensed conduit condensation of steam of generation receives dress It puts, stands 24 hours, filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary as primary raw material with refined bamboo vinegar obtained by step (5) using bamboo charcoal obtained by step (3) Plantation substrate.
In step (1), pressure reducing valve is opened slightly, for adjusting pressure in retort;In step (3), bamboo charcoal discharging is closed Pressure reducing valve is also turn off while mouth.
In step (1), the bamboo vinegar steam of generation, respectively will be cold from the bottom of two condensers followed by two condensers Solidifying obtained crude bamboo vinegar is expelled to distilling apparatus.
The specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 4 hours, cross 40 mesh sieve, obtain burnt mud Grey powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, standby With;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), is then spread evenly Mineral powders obtained by step (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar while stirring, measure simultaneously The pH of system, until pH=5.5, stop sprinkling bamboo vinegar to get.
In step (6-2), thickness of earth covering is 1cm on hay.
In step (6-4), the mass ratio of mineral powders, bamboo charcoal powder and scorched clay dust powder is 1:4:8.
The whole-process control moisture in the preparation process of cultivation matrix, the moisture weight content of final gained cultivation matrix are less than 15%.
Step (6-4) is also granulated after stopping spraying bamboo vinegar, controls the unit weight ranging from 1.2g/ of cultivation matrix cm3
A kind of bulb of thunberg fritillary plantation substrate, is obtained by above-mentioned preparation process.
Comparative example 3
A kind of cultivation matrix is according to mass ratio 4 by bamboo charcoal powder and scorched clay dust powder:8 are obtained by mixing.The preparation of bamboo charcoal powder Method:Bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2 hours, obtain bamboo charcoal powder.The preparation method of scorched clay dust powder:It utilizes The soil of hay overlying 1cm thickness, with fiery smoke curing into scorched clay dust, 105 DEG C dry 4 hours, cross 40 mesh sieve, obtain scorched clay dust powder.
Test example
The cultivation matrix for preparing Examples 1 to 3 or comparative example 1~3 carries out bulb of thunberg fritillary bulb nursery, and specific method is:10 In the last ten-days period moon, bulb of thunberg fritillary bulb (diameter 3cm) is embedded in cultivation matrix, institute's buried depth degree is 6cm, and seedling raise period is 15 days.It investigates and plants It trains the miscellaneous bacteria rate of matrix and carries out the emergence rate of bulb of thunberg fritillary bulb nursery using it, the results are shown in Table 1.
The miscellaneous bacteria rate of 1. cultivation matrix of table and the emergence rate using its progress bulb of thunberg fritillary bulb nursery
Miscellaneous bacteria rate (%) Emergence rate (%)
Embodiment 1 ≤0.5 97
Embodiment 2 ≤0.5 97
Embodiment 3 ≤0.5 99
Comparative example 1 ≤0.5 85
Comparative example 2 12 83
Comparative example 3 25 65
As shown in Table 1, the cultivation matrix of Examples 1 to 3 has relatively low miscellaneous bacteria rate, and bulb of thunberg fritillary bulb nursery is carried out using it Emergence rate it is high.Comparative example 1 omits cow dung, and emergence rate is substantially reduced;Comparative example 2, which omits, to be generated activated carbon and is conducted into The step of crude bamboo vinegar, the miscellaneous bacteria rate of cultivation matrix significantly rise, and it is apparent to carry out the emergence rate of bulb of thunberg fritillary bulb nursery using it It reduces;The cultivation matrix of comparative example 3 is not added with bamboo charcoal and bamboo vinegar, and miscellaneous bacteria rate and emergence rate two indices are undesirable.
Above-mentioned, although the foregoing specific embodiments of the present invention is described with reference to the accompanying drawings, not protects model to the present invention The limitation enclosed, based on the technical solutions of the present invention, those skilled in the art are not needed to make the creative labor and can be done The various modifications or changes gone out are still within protection scope of the present invention.

Claims (9)

1. a kind of preparation process of bulb of thunberg fritillary plantation substrate, which is characterized in that be as follows:
(1) by air-dried high mountain mao bamboon and cow dung according to mass ratio 8:1 input retort, connects gas outlet and the condensation of retort Equipment opens condensing plant, closes bamboo charcoal discharge port and activated carbon discharge nozzle, with the heating rate heating material temperature of 0.1 DEG C/s extremely 250~350 DEG C, charing process 15~20 minutes in this temperature range, the condensed equipment of bamboo vinegar steam stream of generation is condensed into Crude bamboo vinegar, and the bottom for passing through condensing plant is expelled to distilling apparatus;
(2) continue to heat material temperature to 300~350 DEG C, open bamboo charcoal discharge port, the bamboo charcoal of discharge is collected using tray, and put down Spread cooling;
(3) continue to heat material temperature to 400 DEG C, and weigh the quality of collected bamboo charcoal in tray, until residual matter in retort 1/20 for input amount is measured, closes bamboo charcoal discharge port;
(4) continue to heat material temperature to 700 DEG C or more, raw material is further cracked into activated carbon, connection activated carbon discharging in retort Pipe, makes activated carbon slowly enter the distilling apparatus for being connected to crude bamboo vinegar, treats that crude bamboo vinegar collection finishes, closes condensing plant Outlet, avoids flowing back;
(5) distilling apparatus is warming up to 120 DEG C, is come into full contact with by stirring activated carbon with crude bamboo vinegar, the steam of generation Enter refined bamboo vinegar reception device after condensed conduit condensation, stand 24 hours, filtering is spare;
(6) it compounds to obtain a kind of bulb of thunberg fritillary using bamboo charcoal obtained by step (3) and step (5) gained refined bamboo vinegar as primary raw material special Cultivation matrix.
2. preparation process according to claim 1, which is characterized in that in step (1), pressure reducing valve is opened slightly, for adjusting Save pressure in retort;In step (3), pressure reducing valve is also turn off while closing bamboo charcoal discharge port.
3. preparation process according to claim 1, which is characterized in that in step (1), the bamboo vinegar steam of generation followed by Two condensers are expelled to distilling apparatus from the bottom of two condensers by the crude bamboo vinegar that condensation obtains respectively.
4. preparation process according to claim 1, which is characterized in that the specific method of step (6) is as follows:
(6-1) bamboo charcoal drying and crushing crosses 20 mesh sieve, and 100 DEG C dry 2~3 hours, obtain bamboo charcoal powder, spare;
(6-2) using earthing on hay, with fiery smoke curing into scorched clay dust, 105 DEG C dry 3~5 hours, cross 40 mesh sieve, obtain burnt mud Grey powder, it is spare;
(6-3) is by lime stone and potassium ore with mass ratio 2:3 mixing, crush, and cross 15 mesh sieve, obtain mineral powders, spare;
The bamboo charcoal powder of step (6-1) is uniformly mixed by (6-4) with the scorched clay dust powder of step (6-2), then spreads evenly step Mineral powders obtained by (6-3), are uniformly mixed, and then uniformly spray refined bamboo vinegar, while measurement system while stirring PH, until pH=5~5.8, stop sprinkling bamboo vinegar to get.
5. a kind of bulb of thunberg fritillary plantation substrate, which is characterized in that be by preparation work according to any one of claims 1 to 4 What skill obtained.
6. a kind of corresponding preparation system of bulb of thunberg fritillary plantation substrate of preparation process according to any one of claims 1 to 4, It is characterised in that it includes bamboo charcoal preparation facilities and bamboo vinegar preparation facilities two parts, the bamboo charcoal preparation facilities is retort, bamboo The main body of vinegar liquid preparation facilities is condensing plant, and gas outlet and bamboo charcoal discharge port, bamboo are respectively equipped at the top and bottom of retort The lower section setting tray of charcoal discharge port, the gas outlet is connected to the top of condensing plant, the bottom of condensing plant and distillation Device connects;The bottom of the retort is additionally provided with activated carbon discharge nozzle, and activated carbon discharge nozzle is connected to distilling apparatus;The steaming Distillation unit is connect by condensation pipe with refined bamboo vinegar reception device.
7. preparation system according to claim 6, which is characterized in that the bottom of the retort is additionally provided with pressure reducing valve.
8. preparation system according to claim 6, which is characterized in that the condensing plant includes the first condenser of series connection With the second condenser, the gas outlet of retort is connected to the top of the first condenser, and the bottom of the first condenser is equipped with leakage fluid dram I And exhaust outlet, exhaust outlet are connect with the top of the second condenser, the bottom of the second condenser is equipped with leakage fluid dram II, the drain Mouth I and leakage fluid dram II are respectively connected to distilling apparatus.
9. preparation system according to claim 8, which is characterized in that the outside of first condenser and the second condenser The first condensing water conduit and the second condensing water conduit are respectively arranged, condensed water enters from the bottom of the second condensing water conduit, top Outflow then flows into the bottom of the first condensing water conduit, is finally flowed out via the top of the first condensing water conduit.
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