CN108186413A - A kind of sun water with antiperspirant effect and preparation method thereof - Google Patents
A kind of sun water with antiperspirant effect and preparation method thereof Download PDFInfo
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- CN108186413A CN108186413A CN201810234497.1A CN201810234497A CN108186413A CN 108186413 A CN108186413 A CN 108186413A CN 201810234497 A CN201810234497 A CN 201810234497A CN 108186413 A CN108186413 A CN 108186413A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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Abstract
The invention belongs to cosmetic technical fields more particularly to a kind of sun water with antiperspirant effect and preparation method thereof.A kind of sun water with antiperspirant effect, which is characterized in that including following parts by weight of component：5 20 parts of aminobenzoic acid menthyl ester, 45 65 parts of ethylglycol salicylate, 40 70 parts of sorbierite, 500 900 parts of alcohol, 13 parts of morpholine, 7 21 parts of shellac, 7 21 parts of sodium stearate, 10 15 parts of essence, 20 50 parts of lactic acid, 15 parts of polyoxyethylene aliphatic alcohol ether, 200 400 parts of deionized water.The present invention provides a kind of sun waters with antiperspirant effect and preparation method thereof, the formula of traditional sun water is upgraded, the proteins coagulation of skin surface is realized by adding suitable lactic acid, expand sweat gland, block the circulation of sweat, so as to generate inhibition or reduce the effect of sweat secretion amount.
Description
Technical field
The invention belongs to cosmetic technical field more particularly to a kind of sun waters and its preparation side with antiperspirant effect
Method.
Background technology
Sun care preparations is a kind of for preventing the product of skin sunburn, from formulation composition, mainly in various bases
Various sun-screening agents are added in agent.In presently commercially available sun care preparations, mainly there are sunblock lotion, sun water, sunscreen by form
Liquid and suncream etc..Most sun care preparations is sun-screening agent to be dissolved in vegetable oil sunblock lotion is made, although sun-proof result one
As it is good and more due to containing oil, be not easy to be washed out by water, but skin can be made to have greasy feeling, easily glutinous ash is airtight.Therefore, it is
It avoids the greasy feeling of sunblock lotion on the skin, sun-screening agent can be dissolved with alcohol, sun water be made.
Conventional sun water technology contents as disclosed in Chinese patent CN102743311A：Include the original of following mass fraction
Material：40-50 parts of alcohol, 3-5 parts of sorbic acid, 1-2 parts of triethanolamine, 2-3 parts of ethylglycol salicylate, 0.1-0.3 parts of essence,
8-10 parts of bitter leaves tea extract, 50-60 parts of deionized water.Although its cost of manufacture is cheap, in the work of ethylglycol salicylate
It can stop ultraviolet light to a certain extent under, but its cost is too simple, sun-proof result is not excellent, and acts on single.
Invention content
The technical problems to be solved by the invention are to provide a kind of sun water with antiperspirant effect and preparation method thereof, right
The formula of traditional sun water is upgraded, and is realized the proteins coagulation of skin surface by adding suitable lactic acid, is made sweat
Gland expands, and blocks the circulation of sweat, so as to generate inhibition or reduce the effect of sweat secretion amount.For this purpose, the present invention is using following
Technical solution：
A kind of sun water with antiperspirant effect, including following parts by weight of component：
Aminobenzoic acid menthyl ester（CAS 61597-98-6）5-20 parts,
Ethylglycol salicylate（CAS 87-28-5）45-65 parts,
Sorbierite（CAS 50-70-4）40-70 parts,
Alcohol（CAS 64-17-5）500-900 parts,
Morpholine（CAS 110-91-8）1-3 parts,
Shellac（CAS 9000-59-3）7-21 parts,
Sodium stearate（CAS 822-16-2）7-21 parts,
10-15 parts of essence,
Lactic acid（CAS 50-21-5）20-50 parts,
Polyoxyethylene aliphatic alcohol ether（CAS 68213-23-0）1-5 parts,
Deionized water（CAS 7732-18-5）200-400 parts.
Shellac is film forming agent, can form protective film with sorbierite combination sun-screening agent to be helped to attach on skin, together
When, shellac has certain water repelling property, remaining after treating part morpholine volatilization after adding morpholine and sodium stearate
Sun water contains a small amount of soap, and not only water-resistance is good but also easy to clean；Morpholine to a certain extent can be anti-with organic acid meeting
Salt or amide should be generated, sun water is not influenced if a small amount of salt is generated, if a small amount of amide of generation can enhance it is sun-proof
The dissolubility of substance in water so that sun water mixing is more uniformly distributed, quality is more smooth；Polyoxyethylene aliphatic alcohol ether is nonionic
Surfactant can not only increase the solubility property of essence so that sun water forms uniform solution, and can reduce acid
The irritation of confrontation skin.
On the basis of using above-mentioned technical proposal, technical solution further below also can be used in the present invention：
Further, including following parts by weight of component：
10 parts of aminobenzoic acid menthyl ester,
60 parts of ethylglycol salicylate,
50 parts of sorbierite,
600 parts of alcohol,
1 part of morpholine,
7 parts of shellac,
7 parts of sodium stearate,
12 parts of essence,
35 parts of lactic acid,
2 parts of polyoxyethylene aliphatic alcohol ether,
280 parts of deionized water.
Wherein, the weight ratio between the morpholine, shellac and sodium stearate is 1：7：7.Morpholine is colourless hygroscopicity
Oily liquids, be good solvent, although it can volatilize with air, because it is with certain toxicity, therefore protecting
The weight ratio between morpholine, shellac and sodium stearate is controlled 1 under the premise of demonstrate,proving water-resistance：7：7 best ratios.
To achieve the above object, the present invention also provides following technical schemes：
A kind of preparation method of the sun water with antiperspirant effect, includes the following steps：
A., liquid is added in solid after mixing and is stirred；
B. the old storage of the mixture obtained by step a after stirring evenly 7-10 days；
C. the mixture obtained by step b is refrigerated to 0 DEG C to place 24 hours；
D. it is packed after the mixture obtained by step c being thawed and filtered.
Further, the old storage time is 9 days in the step b
It is an advantage of the invention that：Suitable organic acid-lactic acid is increased on the basis of traditional sun water formula, lactic acid this
The effect of antiperspirant can be generated under the action of kind astringent, and since its cost is appropriate, sun water entirety pH will not be relatively low, to skin
There is no stimulation, sun-proof result is good, applies salubrious non-greasy.Meanwhile after sun water is coated on skin the preceding paragraph time, portion
Divide morpholine that can volatilize, work with the sodium stearate one of addition, the sunscreen film containing a small amount of soap can be formed, not only have sun water
There is certain water-resistance, and when needing cleaning, need to be only coated on skin with appropriate warm water, and light with finger or cotton pads
Light rubbing can generate a small amount of foam and clean up sun water.
Specific embodiment
A kind of sun water with antiperspirant effect provided by the invention and preparation method thereof is described further below.
Essence can be selected according to production, such as need to produce the sun water of jasmine taste, you can addition is natural
Jasmine essential oil（CAS 8022-96-6）.
Embodiment one：
A kind of sun water with antiperspirant effect, including following parts by weight of component：
5 parts of aminobenzoic acid menthyl ester,
45 parts of ethylglycol salicylate,
70 parts of sorbierite,
500 parts of alcohol,
1 part of morpholine,
7 parts of shellac,
7 parts of sodium stearate,
10 parts of essence,
20 parts of lactic acid,
1 part of polyoxyethylene aliphatic alcohol ether,
200 parts of deionized water.
Its specific preparation method is：
A kind of preparation method of the sun water with antiperspirant effect, includes the following steps：
A., liquid is added in solid after mixing and is stirred；
B. the old storage of the mixture obtained by step a after stirring evenly 7 days；
C. the mixture obtained by step b is refrigerated to 0 DEG C to place 24 hours；
D. it is packed after the mixture obtained by step c being thawed and filtered.
Embodiment two：
A kind of sun water with antiperspirant effect, including following parts by weight of component：
20 parts of aminobenzoic acid menthyl ester,
65 parts of ethylglycol salicylate,
40 parts of sorbierite,
900 parts of alcohol,
3 parts of morpholine,
21 parts of shellac,
21 parts of sodium stearate,
15 parts of essence,
50 parts of lactic acid,
5 parts of polyoxyethylene aliphatic alcohol ether,
400 parts of deionized water.
Its specific preparation method is：
A kind of preparation method of the sun water with antiperspirant effect, includes the following steps：
A., liquid is added in solid after mixing and is stirred；
B. the old storage of the mixture obtained by step a after stirring evenly 10 days；
C. the mixture obtained by step b is refrigerated to 0 DEG C to place 24 hours；
D. it is packed after the mixture obtained by step c being thawed and filtered.
Embodiment three：
A kind of sun water with antiperspirant effect, including following parts by weight of component：
10 parts of aminobenzoic acid menthyl ester,
60 parts of ethylglycol salicylate,
50 parts of sorbierite,
600 parts of alcohol,
1 part of morpholine,
7 parts of shellac,
7 parts of sodium stearate,
12 parts of essence,
35 parts of lactic acid,
2 parts of polyoxyethylene aliphatic alcohol ether,
280 parts of deionized water.
Its specific preparation method is：
A kind of preparation method of the sun water with antiperspirant effect, includes the following steps：
A., liquid is added in solid after mixing and is stirred；
B. the old storage of the mixture obtained by step a after stirring evenly 9 days；
C. the mixture obtained by step b is refrigerated to 0 DEG C to place 24 hours；
D. it is packed after the mixture obtained by step c being thawed and filtered.
Example IV：
A kind of sun water with antiperspirant effect, including following parts by weight of component：
8 parts of aminobenzoic acid menthyl ester,
50 parts of ethylglycol salicylate,
55 parts of sorbierite,
550 parts of alcohol,
1 part of morpholine,
7 parts of shellac,
7 parts of sodium stearate,
11 parts of essence,
25 parts of lactic acid,
1 part of polyoxyethylene aliphatic alcohol ether,
250 parts of deionized water.
Its specific preparation method is：
A kind of preparation method of the sun water with antiperspirant effect, includes the following steps：
A., liquid is added in solid after mixing and is stirred；
B. the old storage of the mixture obtained by step a after stirring evenly 8 days；
C. the mixture obtained by step b is refrigerated to 0 DEG C to place 24 hours；
D. it is packed after the mixture obtained by step c being thawed and filtered.
Embodiment five：
A kind of sun water with antiperspirant effect, including following parts by weight of component：
12 parts of aminobenzoic acid menthyl ester,
55 parts of ethylglycol salicylate,
60 parts of sorbierite,
800 parts of alcohol,
2 parts of morpholine,
14 parts of shellac,
14 parts of sodium stearate,
14 parts of essence,
45 parts of lactic acid,
4 parts of polyoxyethylene aliphatic alcohol ether,
320 parts of deionized water.
Its specific preparation method is：
A kind of preparation method of the sun water with antiperspirant effect, includes the following steps：
A., liquid is added in solid after mixing and is stirred；
B. the old storage of the mixture obtained by step a after stirring evenly 9 days；
C. the mixture obtained by step b is refrigerated to 0 DEG C to place 24 hours；
D. it is packed after the mixture obtained by step c being thawed and filtered.
Embodiment six：
A kind of sun water with antiperspirant effect, including following parts by weight of component：
15 parts of aminobenzoic acid menthyl ester,
63 parts of ethylglycol salicylate,
65 parts of sorbierite,
750 parts of alcohol,
1 part of morpholine,
7 parts of shellac,
7 parts of sodium stearate,
3 parts of carboxymethyl cellulose,
14 parts of essence,
40 parts of lactic acid,
3 parts of polyoxyethylene aliphatic alcohol ether,
350 parts of deionized water.
Its specific preparation method is：
A kind of preparation method of the sun water with antiperspirant effect, includes the following steps：
A., liquid is added in solid after mixing and is stirred；
B. the old storage of the mixture obtained by step a after stirring evenly 10 days；
C. the mixture obtained by step b is refrigerated to 0 DEG C to place 24 hours；
D. it is packed after the mixture obtained by step c being thawed and filtered.
Comparative example 1：
A kind of sun water, including following weight percentage components：
40-50 parts of alcohol,
3-5 parts of sorbic acid,
1-2 parts of triethanolamine,
2-3 parts of ethylglycol salicylate,
0.1-0.3 parts of essence,
8-10 parts of bitter leaves tea extract,
50-60 parts of deionized water.
Its specific preparation method includes the following steps：
Liquid is added in solid by step 1 after mixing；
Step 2, by the old storage of the mixture being uniformly mixed in step 28 days；
Step 3, by the mixture obtained by step 2 be refrigerated to 0 DEG C place 24 hours after thaw.
Experiment：The present invention is prepared using the sun water that embodiment 1-6 is prepared as test specimen 1-6 using comparative example 1
Obtained sun water is as control sample 1.
Test method：
1. water-resistance is tested：Test specimen 1-6 and control sample 1 are taken respectively in the material of the long 10cm of human body skin of dorsum of hand surface smear
Film carries out Crystal drops were dripping down to material film with the drop pot for being inoculated with clear water and covers, the number of drop pot drippage water droplet when record material film starts shedding off, often
Group sample repeats experiment 20 times, takes the average value of 20 experiments.
2. cleaning experiment：Test specimen 1-6 and control sample 1 are taken respectively the long 10cm's of human body skin of dorsum of hand surface smear
Expect film, rub material film repeatedly with the cotton pads for being stained with clear water, the time that record material film is completely removed, every group of sample repeats to test
20 times, take the average value of 20 experiments.Test data is as shown in the table：
Result of the test：The water-resistance of control sample 1 is poor, although longer the time required to being cleaned by clear water；Test specimen
The water-resistance of middle test specimen 3 is best, but the water-resistance of test specimen 4-6 is also relatively good；Except 2 scavenging period of test specimen compared with
Except length, the scavenging period of other test specimens approaches, and is all easier to clean.
Although the present invention is described by reference to preferred embodiment, those skilled in the art should
Work as understanding, in the range of claims, various variation in form and details can be made.
Claims (5)
1. a kind of sun water with antiperspirant effect, which is characterized in that including following parts by weight of component：
5-20 parts of aminobenzoic acid menthyl ester,
45-65 parts of ethylglycol salicylate,
40-70 parts of sorbierite,
500-900 parts of alcohol,
1-3 parts of morpholine,
7-21 parts of shellac,
7-21 parts of sodium stearate,
10-15 parts of essence,
20-50 parts of lactic acid,
1-5 parts of polyoxyethylene aliphatic alcohol ether,
200-400 parts of deionized water.
2. a kind of sun water with antiperspirant effect according to claim 1, which is characterized in that including following parts by weight group
Point：
10 parts of aminobenzoic acid menthyl ester,
60 parts of ethylglycol salicylate,
50 parts of sorbierite,
600 parts of alcohol,
1 part of morpholine,
7 parts of shellac,
7 parts of sodium stearate,
12 parts of essence,
35 parts of lactic acid,
2 parts of polyoxyethylene aliphatic alcohol ether,
280 parts of deionized water.
3. a kind of sun water with antiperspirant effect according to claim 1, which is characterized in that the morpholine, shellac and
Weight ratio between sodium stearate is 1：7：7.
4. a kind of preparation method of the sun water with antiperspirant effect in 1-3 such as claim as described in any one, feature
It is, includes the following steps：
A., liquid is added in solid after mixing and is stirred；
B. the old storage of the mixture obtained by step a after stirring evenly 7-10 days；
C. the mixture obtained by step b is refrigerated to 0 DEG C to place 24 hours；
D. it is packed after the mixture obtained by step c being thawed and filtered.
A kind of 5. preparation method of sun water with antiperspirant effect according to claim 4, which is characterized in that step b
In it is old storage the time be 9 days.
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| CN201810234497.1A CN108186413A (en) | 2018-03-21 | 2018-03-21 | A kind of sun water with antiperspirant effect and preparation method thereof |
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| CN201810234497.1A CN108186413A (en) | 2018-03-21 | 2018-03-21 | A kind of sun water with antiperspirant effect and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113968411A (en) * | 2021-11-09 | 2022-01-25 | 厦门乾沣电子有限公司 | Novel television buffering packaging material |
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2018
- 2018-03-21 CN CN201810234497.1A patent/CN108186413A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113968411A (en) * | 2021-11-09 | 2022-01-25 | 厦门乾沣电子有限公司 | Novel television buffering packaging material |
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