CN108178991A - Novel heat-conducting adhesive tape and preparation method thereof - Google Patents

Novel heat-conducting adhesive tape and preparation method thereof Download PDF

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Publication number
CN108178991A
CN108178991A CN201711458197.3A CN201711458197A CN108178991A CN 108178991 A CN108178991 A CN 108178991A CN 201711458197 A CN201711458197 A CN 201711458197A CN 108178991 A CN108178991 A CN 108178991A
Authority
CN
China
Prior art keywords
sensitive adhesive
pressure sensitive
heat
conducting
adhesive tape
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711458197.3A
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Chinese (zh)
Inventor
李长顺
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhangjiagang Kangdexin Optronics Material Co Ltd
Original Assignee
Zhangjiagang Kangdexin Optronics Material Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhangjiagang Kangdexin Optronics Material Co Ltd filed Critical Zhangjiagang Kangdexin Optronics Material Co Ltd
Priority to CN201711458197.3A priority Critical patent/CN108178991A/en
Publication of CN108178991A publication Critical patent/CN108178991A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/02Elements
    • C08K3/08Metals
    • C08K2003/085Copper
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2203/00Applications of adhesives in processes or use of adhesives in the form of films or foils
    • C09J2203/318Applications of adhesives in processes or use of adhesives in the form of films or foils for the production of liquid crystal displays
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2301/00Additional features of adhesives in the form of films or foils
    • C09J2301/30Additional features of adhesives in the form of films or foils characterized by the chemical, physicochemical or physical properties of the adhesive or the carrier
    • C09J2301/312Additional features of adhesives in the form of films or foils characterized by the chemical, physicochemical or physical properties of the adhesive or the carrier parameters being the characterizing feature
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2301/00Additional features of adhesives in the form of films or foils
    • C09J2301/40Additional features of adhesives in the form of films or foils characterized by the presence of essential components
    • C09J2301/408Additional features of adhesives in the form of films or foils characterized by the presence of essential components additives as essential feature of the adhesive layer
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2400/00Presence of inorganic and organic materials
    • C09J2400/10Presence of inorganic materials
    • C09J2400/16Metal
    • C09J2400/163Metal in the substrate

Landscapes

  • Adhesives Or Adhesive Processes (AREA)
  • Adhesive Tapes (AREA)

Abstract

A kind of novel heat-conducting adhesive tape in function tape technology field and preparation method thereof, the heat-conducting glue band includes heat conduction functional layer and the pressure sensitive adhesive for being coated on one side surface of heat conduction functional layer, the pressure sensitive adhesive has diffusion micro-structure on the surface far from heat conduction functional layer side, and the pressure sensitive adhesive for being mixed with metal powder is filled in the diffusion micro-structure.The present invention in pressure sensitive adhesive by setting metal powder to improve the heat conductivility of pressure sensitive adhesive, and so as to improve the radiating efficiency of heat-conducting glue band entirety, radiating efficiency can improve 10%~30%.

Description

Novel heat-conducting adhesive tape and preparation method thereof
Technical field
The present invention relates to a kind of technology of function adhesive tape area, specifically a kind of novel heat-conducting adhesive tape and its preparation side Method.
Background technology
OLED technology is widely used in portable device at present.In the design of OLED screen curtain, often using glass or PI is as substrate, and the radiating efficiency of glass and PI is not high, needs to take cooling measure, is typically employed in OLED screen backstage face paste The mode of heat-conducting glue band reaches heat dissipation effect.
Current heat-conducting glue band needs pressure-sensitive adhesive coating mainly using copper foil as functional layer.Although copper foil radiating efficiency It is higher, but pressure sensitive adhesive is high-molecular compound, heat transfer efficiency is relatively low, therefore current heat-conducting glue band synthesis radiating efficiency is not It is high.
Invention content
The present invention is directed to deficiencies of the prior art, it is proposed that a kind of novel heat-conducting adhesive tape and preparation method thereof, The heat conductivility of pressure sensitive adhesive can be improved, so as to improve the radiating efficiency of heat-conducting glue band entirety.
The present invention is achieved by the following technical solutions:
The present invention relates to a kind of novel heat-conducting adhesive tape, the heat-conducting glue band includes heat conduction functional layer and is coated on heat conduction work( The pressure sensitive adhesive of one side surface of ergosphere, the pressure sensitive adhesive have diffusion micro-structure, institute on the surface far from heat conduction functional layer side Filled with the pressure sensitive adhesive for being mixed with metal powder in the diffusion micro-structure stated.
The pressure sensitive adhesive for being mixed with metal powder is fitted with release film on the surface far from heat conduction functional layer side.
The heat conduction functional layer is copper foil or aluminium foil, it is preferable that is copper foil;
The metal powder is copper powder, aluminium powder, silver powder or the mixed metal powder including three;Preferably, it is copper powder.
The present invention relates to a kind of preparation method of heat-conducting glue band, including:
A then) the pressure-sensitive adhesive coating on diffusion micro-structure master mold is bonded heat conduction functional layer, stripping diffusion micro-structure master mold The semi-finished product with diffusion micro-structure are made afterwards;
B) metal powder is dispersed in volatile organic solvent, adds in pressure sensitive adhesive and is uniformly mixed, treat that organic solvent is waved Send out spare;
C) semi-finished product with diffusion micro-structure are placed on screen printing platform, in diffusion micro-structure surface coating mixing Pressure sensitive adhesive, is finally bonded by the pressure sensitive adhesive of metal powder with release film, and novel heat-conducting adhesive tape is made.
In the step B, in parts by weight, metal powder is 10~20 parts, and volatile organic solvent is 60~80 parts, Pressure sensitive adhesive is 80~100 parts.
Preferably, the volatile organic solvent is selected from ethyl acetate, butyl acetate, butanone, toluene, ethyl alcohol.
The diffusion micro-structure master mold is any one diffusion barrier, and surface is coated with silicone oil;Preferably, the diffusion Prism spacing is 20~30 microns in film, and depth is 8~10 microns.
Technique effect
Compared with prior art, the present invention in pressure sensitive adhesive by setting metal powder to improve the thermal conductivity of pressure sensitive adhesive Can, so as to improve the radiating efficiency of heat-conducting glue band entirety, radiating efficiency can improve 10%~30%.
Description of the drawings
Fig. 1 is the structural diagram of the present invention;
Fig. 2 is the process flow chart of the present invention;
In figure:Heat conduction functional layer 1, pressure sensitive adhesive 2, diffusion micro-structure 3, release film 4, diffusion barrier 5.
Specific embodiment
Below in conjunction with the accompanying drawings and specific embodiment the present invention will be described in detail.
Embodiment 1
As shown in Figure 1, the present embodiment is related to a kind of novel heat-conducting adhesive tape, the heat-conducting glue band includes heat conduction functional layer 1 With the pressure sensitive adhesive 2 for being coated on 1 one side surface of heat conduction functional layer, the pressure sensitive adhesive 2 is on the surface far from 1 side of heat conduction functional layer With diffusion micro-structure 3, exist in the diffusion micro-structure 3 filled with the pressure sensitive adhesive for being mixed with metal powder, the pressure sensitive adhesive Release film 4 is fitted with far from heat conduction functional layer side.
The thermal conductivity factor of the heat-conducting glue band is 10w/ (mk), and 180 ° of peeling forces are 600gf.
Preferably, the heat conduction functional layer 1 is copper foil.
Preferably, the metal powder is copper powder.
As shown in Fig. 2, the present embodiment is related to a kind of preparation method of novel heat-conducting adhesive tape, include the following steps:
S1, 30 microns of prism spacing, 10 microns of depth diffusion barrier 5 on, be coated with silicone oil, be made off-type force 10gf a left side Right diffusion micro-structure master mold;
S2, the pressure-sensitive adhesive coating 2 on diffusion micro-structure master mold is bonded 9 microns of copper foil on pressure sensitive adhesive 2, then removes expansion Micro-structure master mold is dissipated, obtains semi-finished product;
S3, semi-finished product are placed on screen printing platform, is coated in micro-structure 3 is spread and is mixed with the pressure-sensitive of copper powder Pressure sensitive adhesive is finally bonded by glue with release film 4, and novel heat-conducting adhesive tape is made.
The pressure sensitive adhesive for being mixed with copper powder is prepared with the following method, in parts by weight, 20 parts of copper powders is dispersed in 80 In part butanone, the pressure sensitive adhesive of 100 parts of soken Co., Ltd. model C 502C is then added in, passes through high speed dispersor or ultrasonic wavelength-division It dissipates and is uniformly mixed, and is spare after organic matter volatilizees completely.
It is emphasized that:It the above is only presently preferred embodiments of the present invention, not the present invention made in any form Limitation, any simple modification, equivalent change and modification that every technical spirit according to the present invention makees above example, In the range of still falling within technical solution of the present invention.

Claims (9)

1. a kind of novel heat-conducting adhesive tape, which is characterized in that the heat-conducting glue band includes heat conduction functional layer and is coated on heat conduction work( The pressure sensitive adhesive of one side surface of ergosphere, the pressure sensitive adhesive have diffusion micro-structure, institute on the surface far from heat conduction functional layer side Filled with the pressure sensitive adhesive for being mixed with metal powder in the diffusion micro-structure stated.
2. heat-conducting glue band according to claim 1, it is characterized in that, the pressure sensitive adhesive for being mixed with metal powder is led separate The surface of hot merit ergosphere side is fitted with release film.
3. heat-conducting glue band according to claim 1, it is characterized in that, the heat conduction functional layer is copper foil or aluminium foil, preferably Ground is copper foil;The metal powder is copper powder, aluminium powder, silver powder or the mixed metal powder including three, it is preferable that is copper Powder.
4. a kind of preparation method of novel heat-conducting adhesive tape described in any of the above-described claim, which is characterized in that including:
A then) the pressure-sensitive adhesive coating on diffusion micro-structure master mold is bonded heat conduction functional layer, is made after stripping diffusion micro-structure master mold Obtain the semi-finished product with diffusion micro-structure;
B) metal powder is dispersed in volatile organic solvent, adds in pressure sensitive adhesive and is uniformly mixed;
C) semi-finished product with diffusion micro-structure are placed on screen printing platform, gold is mixed in diffusion micro-structure surface coating Belong to the pressure sensitive adhesive of powder, be finally bonded pressure sensitive adhesive with release film, novel heat-conducting adhesive tape is made.
5. the preparation method of novel heat-conducting adhesive tape according to claim 4, it is characterized in that, the metal powder that is mixed with In pressure sensitive adhesive, in parts by weight, the metal powder is 10~20 parts, and the pressure sensitive adhesive is 80~100 parts.
6. the preparation method of novel heat-conducting adhesive tape according to claim 5, it is characterized in that, in parts by weight, described waves Hair property organic solvent is 60~80 parts.
7. the preparation method of novel heat-conducting adhesive tape according to claim 5, it is characterized in that, the volatile organic solvent Selected from ethyl acetate, butyl acetate, butanone, toluene, two propyl alcohol methyl ethers.
8. the preparation method of novel heat-conducting adhesive tape according to claim 4, it is characterized in that, the diffusion micro-structure master mold For any one diffusion barrier, surface is coated with silicone oil.
9. the preparation method of novel heat-conducting adhesive tape according to claim 8, it is characterized in that, prism spacing in the diffusion barrier It it is 20~30 microns, depth is 8~10 microns.
CN201711458197.3A 2017-12-28 2017-12-28 Novel heat-conducting adhesive tape and preparation method thereof Pending CN108178991A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711458197.3A CN108178991A (en) 2017-12-28 2017-12-28 Novel heat-conducting adhesive tape and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711458197.3A CN108178991A (en) 2017-12-28 2017-12-28 Novel heat-conducting adhesive tape and preparation method thereof

Publications (1)

Publication Number Publication Date
CN108178991A true CN108178991A (en) 2018-06-19

Family

ID=62548196

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711458197.3A Pending CN108178991A (en) 2017-12-28 2017-12-28 Novel heat-conducting adhesive tape and preparation method thereof

Country Status (1)

Country Link
CN (1) CN108178991A (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0924761A1 (en) * 1997-12-22 1999-06-23 Nitto Denko Corporation Heat-conductive and pressure-sensitive adhesive sheets and method for fixing electronic parts to heat-radiating members with the use of the same
CN106189912A (en) * 2016-08-12 2016-12-07 斯迪克新型材料(江苏)有限公司 A kind of Copper Foil conduction, the preparation method of heat conduction one-faced tapes

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0924761A1 (en) * 1997-12-22 1999-06-23 Nitto Denko Corporation Heat-conductive and pressure-sensitive adhesive sheets and method for fixing electronic parts to heat-radiating members with the use of the same
CN106189912A (en) * 2016-08-12 2016-12-07 斯迪克新型材料(江苏)有限公司 A kind of Copper Foil conduction, the preparation method of heat conduction one-faced tapes

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Application publication date: 20180619

RJ01 Rejection of invention patent application after publication