CN108158881A - A kind of skin care item comprising precious Rogor powder and preparation method and application - Google Patents
A kind of skin care item comprising precious Rogor powder and preparation method and application Download PDFInfo
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- CN108158881A CN108158881A CN201711492498.8A CN201711492498A CN108158881A CN 108158881 A CN108158881 A CN 108158881A CN 201711492498 A CN201711492498 A CN 201711492498A CN 108158881 A CN108158881 A CN 108158881A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/738—Cyclodextrins
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/004—Aftersun preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract
The invention discloses a kind of skin care item comprising precious Rogor powder and preparation method and application.A kind of skin care item for including precious Rogor powder, based on 100 parts of quality, are made of the component of following mass fractions：0.1~1.0 part of vitamin E, 1~10 part of mannitol ester silanol C, 0.1~2 part of precious Rogor powder, surplus is auxiliary agent, and auxiliary agent is made of component A, B component, component C and D components.It by the component A heating stirring of water and auxiliary agent, is mixed after the B component of auxiliary agent and vitamin E heating stirring, adds in the emulsification of D components, the cooling of auxiliary agent, the skin care item are prepared in the rear component C for adding in auxiliary agent, mannitol ester silanol C and precious Rogor powder.The skin care item can effectively improve skin moisture content and with good wrinkle improvement effect, and preparation method is simple and practicable, mild condition, in addition, the skin care item are particularly suitable for the skin care of the middle-aged and the old.
Description
Technical field
The present invention relates to skin care field more particularly to a kind of skin care item comprising precious Rogor powder and preparation method thereof with answering
With.
Background technology
Research shows that human skin after 25~30 years old will gradual aging with advancing age, about 35
It just will appear obvious damped exponential model after~40 years old.Skin moisture-keeping mechanism is damaged, skin tissue cell and cell
Moisture between tissue is reduced, when the moisture of cuticula is dropped to below 10%, skin just will appear dry, follow the string,
Corrugated symptom；In addition, fibroblastic quantity gradually decreases in human skin, and the collagen and elastic fibers secreted
Albumen is also gradually decreased because of being aoxidized, is broken, and so as to disappear to the supporting role of epidermis, skin corium starts thinning, skin
Elastic force be deteriorated, therefore cause it is inhomogenous cave in, generate wrinkle；In addition, the elastic fibers and collagen of ageing skin skin corium are fine
Dimension is reduced, thicker, aging, and skin elasticity reduces, and subcutaneous fat is reduced, and skin is made to reduce support, shows old application on human skin knot
Structure feature：It is dry, coarse, corrugate, relax.
Well-known anti-aging product main composition on the market includes ubiquinone, vitamins, polypeptide protein class, plants at present
Extract extract etc., by supplementing the nutrients, increasing skin water lock moisture-retaining capacity and oxidation resistance, decline so as to slow down skin
Always, the purpose of skin is waken up.
However above-mentioned anti-aging product has the following problems：1st, the extracting method of extraction extract is planted to active in plant component
Object component has important influence, is applied to the influence of its rear stability to product in cosmetics and also needs to be paid close attention to；Polypeptide
Protide component is the nutrition composition of needed by human body, is applied in cosmetics, and whether active ingredient can be by pH, temperature etc.
Influence, can be absorbed and merit attention by human body completely；2nd, the said goods are mainly locked by supplementing the nutrients, increasing skin
Water moisture-retaining capacity and the mode of anti-oxidant energy carry out slowing down skin aging, and there is no the reconstruction considered to fibrocyte, inside and outside knots
Conjunction fundamentally slows down aging.
Precious Rogor (Borojo) belongs to the tropical fruit (tree) of Rubiaceae woods fruit category, fresh Borojo extremely sour (pH2.74), low water
Divide (69.22%), high carbohydrate (28.02%), low sugar (9.72%), high protein (1.22%), high dietary-fiber
(2.98%) fruit.The content of B1, B2, niacin, folic acid and vitamin E in B family vitamin are far above most fruits.Trip
Isolated amino acid total content be 1.35%, 25 kinds；Containing 19 kinds of amino acid substances after hydrolysis, total amount is up to 2.51%, wherein containing 5 kinds of human bodies
Necessary amino acid, 2 kinds of conditions must amino acid.Trace element is abundant in Borojo, 3500mg/kg containing potassium, magnesium 280mg/kg, iron
160mg/kg and zinc 0.64mg/kg；Contain micro elements needed by human zinc, copper, cobalt, iron, it may be necessary to trace element manganese, silicon,
Rare trivalent chromium and nickel in nickel, boron and vegetable and fruit.Total amount of rare earth and 16 kinds of rare earth element contents are all in normal range (NR)
It is interior, to human health without potential hazard.Harmful heavy metal lead is 24 μ g/kg, and mercury, arsenic, cadmium are below minimum detection limit.Borojo
Containing abundant linoleic acid needed by human (9.91%) and leukotrienes (0.89%), general flavone reaches 335.2mg/kg, 8,9- cyclenes
Ether terpene glycosides reaches 1.92g/100g, and polyphenol reaches 270mg/kg.From the foregoing, it will be observed that precious Rogor contains abundant nutrient, higher albumen
Matter content and essential amino acid and P elements, and it is immune with enhancing, it is anti-inflammatory and anti-oxidant and other effects, it can come for skin tape
Sufficient nutrition and moisture.
At present, the research that skin care item are applied to for precious Rogor is less, and CN103860429 discloses a kind of precious Rogor skin care
Product are combined with different substrates by precious Rogor and realize the skin-protecting functions such as whitening and anti-aging, moisturizing；CN103948530 is then disclosed
A kind of precious Rogor moisture-keeping composition with treasured Rogor compounds to obtain good with moistening effect by vegetalitas xylose glucose glycosides
Good composition；CN103919706 discloses a kind of precious Rogor lightening compositions, is found pleasure in by 3-o- ethylascorbyls and treasured
Fruit compounds in proportion so that precious Rogor can utmostly inhibit the activity of tyrosinase, can effectively prevent l-tyrosine hydroxylating
It is changed into DOPA quinone, so as to achieve the effect that whitening, but passes through the moisturizing of precious Rogor and other substances compounding realization longer time
And apparent wrinkle improvement effect has not been reported, in addition there is no the weights considered to fibrocyte for the above-mentioned skin care item containing precious Rogor
It builds, enhances the water lock moisture-retaining capacity of skin, improve skin moisture content, the combination of inner and outside provides sufficient nutrient and water for skin
Point, fundamentally slow down aging.
Invention content
The purpose of the present invention is to provide a kind of skin care item comprising the precious powder of fruit pleasure and preparation method and application.The skin care
Product can effectively improve moisture content of skin and with apparent wrinkle improvement effect.
One of the objects of the present invention is to provide a kind of skin care item for including precious Rogor powder, pass through vitamin E, mannitol
Ester silanol C and precious Rogor powder compound to obtain for main composition.
The technical solution used in the present invention is：
A kind of skin care item for including precious Rogor powder, based on 100 parts of quality, are made of the component of following mass fractions：0.1~
1.0 parts of vitamin Es, 1~10 part of mannitol ester silanol C, 0.1~2 part of precious Rogor powder, surplus is auxiliary agent.
Preferably, a kind of skin care item for including precious Rogor powder, by 100 parts of mass flowmeters, mass fraction is：0.3
~0.7 part of vitamin E, 3~7 parts of mannitol ester silanol C, 0.3~1.0 part of precious Rogor powder, surplus is auxiliary agent.
Scheme more preferably, a kind of skin care item for including precious Rogor powder, based on 100 parts of quality, mass fraction is：
0.4~0.6 part of vitamin E, 4~6 parts of mannitol ester silanol C, 0.4~0.6 part of precious Rogor powder, surplus is auxiliary agent.
Preferably, add in what beta-cyclodextrin was handled after precious Rogor powder is digested by precious Rogor pulp.
Preferably, above-mentioned auxiliary agent is made of component A, B component, component C and D components, and component A is selected from glycerine, butanediol, small
At least one of pyrenomycetes glue, antierythrite, allantoin, xylitol, urea；B component be selected from rapeseed oil, shea butter, beeswax,
At least one of dimethyl silicone polymer；Component C is selected from least one of preservative, essence；D components are selected from emulsifier.
Preferably, component A is made of glycerine, butanediol, Scleroglucan, antierythrite, allantoin, xylitol, urea；B
Component is made of rapeseed oil, shea butter, beeswax, dimethyl silicone polymer；Component C is made of preservative, essence；D components by
Emulsifier forms.
Preferably, the mass fraction of each substance of component A is：3~6 parts of glycerine, 2~4 parts of 1,3 butylene glycols, 0.01~0.1
Part Scleroglucan, 1~4 part of antierythrite, 0.05~0.2 part of allantoin, 0.02~0.1 part of xylitol, 0~4 part of urea；B groups
The mass fraction of point each substance is：5~8 portions of rapeseed oils, 1~5 part of shea butter, 0.1~1.0 part of beeswax, 3~5 parts of poly- diformazans
Radical siloxane；The mass fraction of each substance of component C is：0.1~1.0 portion of preservative, 0.01~0.05 part of essence；D component materials
Mass fraction be：1~4 part of emulsifier.
Preferably, emulsifier is selected from stearic acid, sodium hydroxide, triethanolamine, siloxanes, polyoxyethylene laurel ether, polyoxy
At least one of ethylene octadecyl alcolol, polyoxyethylene ether, Vinlub 73.
Preferably, preservative be selected from methyl p-hydroxybenzoate, ethyl-para-hydroxybenzoate, propylparaben,
At least one of butyl p-hydroxybenzoate, benzyl alcohol, dichloroxylenol, Bian chlorophenol.
Preferably, essence is selected from tea flavour essence, fruity flavor, spends at least one of savory essence, vegetation essence.
Wherein, precious Rogor powder contains abundant nutrient, higher protein content and essential amino acid and phosphorus member
Element, and it is immune with enhancing, it is anti-inflammatory and anti-oxidant and other effects, sufficient nutrition and moisture can be come for skin tape.
Vitamin E prevents the readily oxidizable substances such as cell membrane and intracellular unrighted acid during body metabolism
It is aoxidized, it, can conduct so as to protect the complete of cell membrane and then prevent the effect of aging, and vitamin E has stronger reproducibility
Antioxidant as internal antioxidant, eliminates interior free yl, reduces injury of the ultraviolet light to human body.
Vitamin E of the present invention is preferably tocopherol acetate.
(molecular formula is mannitol ester silanol C：C7H14O7Si it is) a kind of multi-functional skin care active constituent, energy
Framework skin support structure, repairs elastic collagen, and bioactivity silicon is provided for good skin utilization rate, can combine
Intracellular water, creates moisture structure, stimulates more newly-generated, the reconstruction skin connective tissue of fibrocyte and collagen,
The elasticity and compactness of skin are kept, optimizes the metabolism of Skin Cell, therefore it is integrate reparation, moisturizing etc. more
Functional mass.
It is of the invention first to reveal hydrone in sugar alcohol silanol C combination cells, stimulate the update of fibrocyte and collagen
Generation, rebuild skin connective tissue, Rosemary Extract, after using vitamin E as antioxidant eliminate interior free yl, reduction it is ultraviolet
Injury of the line to human body, recycling precious Rogor powder, three's complementation collaboration increases as comprehensive skin repair nutritional ingredient and moisture
Effect the combination of inner and outside be truly realized for skin supplement the nutrients and moisture, reconstituted cell barrier, optimize Skin Cell metabolism, prolong
The purpose of slow aging.
It is contemplated that based on above-mentioned consideration those skilled in the art and is replaced again using the substance with above-mentioned function
Match, each substance synergy combination of inner and outside is really achieved the effect of moisturizing smoothing wrinkle.
Another object of the present invention is to provide a kind of preparation method of the skin care item comprising precious Rogor powder, including walking as follows
Suddenly：
(1) various raw materials in precise formula, are contained in vessel；
(2) component A of water and auxiliary agent is added in water phase agitated kettle, stirring, heating is heated and stirred, and is kept the temperature
It is spare；
(3) by the B component of auxiliary agent, vitamin E input oil phase agitated kettle, stirring, heating is heated and is stirred,
It keeps the temperature spare；
(4) raw material in water phase agitated kettle is pumped into vacuum emulsification pot, is pumped into oil phase agitated kettle after stirring evenly
Raw material adds in D components, is stirred after emulsifying, cools down after constant temperature stirring defoaming；
(5) component C, mannitol ester silanol C and the precious Rogor powder of auxiliary agent are added in, discharges after stirring, is quiet
It puts；
(6) after the assay was approved, filling, packaging, coding, storage.
Preferably：The heating temperature of step (2) and step (3) is：80~85 DEG C.
Preferably：The emulsifying time in step (4) is 5~8min.
Preferably：Step (5) adds each substance when being cooled to below 45 DEG C.
Wherein precious Rogor powder is prepared by a method comprising the following steps：
(a) precious Rogor fresh fruit, cleaning peeling, separation fruit, core are taken；
(b) add water in pulp, grinding adds in pectase, makes pulp enzymolysis, digestion afterwards；
(c) the pulp press filtration after enzymolysis, digestion is cleaned, enzyme is killed in heating；
(d) pH is adjusted, is concentrated in vacuo；
(e) beta-cyclodextrin is added in, rear spray drying is to get precious Rogor powder.
Preferably：The weight that step (b) adds in water is the 10% of pulp weight, and the weight of pectase is pulp weight
1‰。
Preferably：Step (c) heating kills the condition setting of enzyme and is：80 DEG C of holding 5min.
Preferably：Step (d) is concentrated in vacuo to BRIX up to 20%.
Preferably：The weight that step (e) adds in beta-cyclodextrin is the 1% of pulp weight.
Another object of the present invention is to provide the above-mentioned skin care item comprising precious Rogor powder in middle-aged and the old's skin care
Using.
The beneficial effects of the invention are as follows：
1st, it is of the invention that restriction for primary efficacy substance and is pressed by vitamin E, mannitol ester silanol C and precious Rogor powder
Ratio compounded, gained skin care item can effectively improve skin moisture content, when tocopherol acetate be 0.5 part, mannose
Alcohol ester silanol C is 5.0 parts, precious Rogor powder is, 0.5 part when, moisture lifting capacity is up to 100.32%, and with good
Wrinkle improvement effect.
2nd, precious Rogor powder can give full play to its moisturizing smoothing wrinkle active function under the ratio of the present invention, with vitamin E and sweet
Reveal sugar alcohol ester silanol C and generate synergistic effect, the combination of inner and outside is truly realized the effect of moisturizing smoothing wrinkle.
3rd, the preparation method of the skin care item is simple and practicable, and conditioned response is mild, which is particularly suitable for the middle-aged and the old
Skin care.
Description of the drawings
When the content of Fig. 1 tocopherol acetates is 0.5 part, the mannitol ester silanol C of different content and precious Rogor powder
Sample is before use and using surrounding inner skin moisture change rate with the change curve of usage time；
When the content of Fig. 2 tocopherol acetates is 0.8 part, the mannitol ester silanol C of different content and precious Rogor powder
Sample is before use and using surrounding inner skin moisture change rate with the change curve of usage time；
When the content of Fig. 3 tocopherol acetates is 1.0 parts, the mannitol ester silanol C of different content and precious Rogor powder
Sample is before use and using surrounding inner skin moisture change rate with the change curve of usage time；
When Fig. 4 mannitol ester silanols C content is 1.0 parts, the tocopherol acetate of different content and precious Rogor powder sample
Product are before use and using surrounding inner skin moisture change rate with the change curve of usage time；
When Fig. 5 mannitol ester silanols C content is 3.0 parts, the tocopherol acetate of different content and precious Rogor powder sample
Product are before use and using surrounding inner skin moisture change rate with the change curve of usage time；
When Fig. 6 mannitol ester silanols C content is 5.0 parts, the tocopherol acetate of different content and precious Rogor powder sample
Product are before use and using surrounding inner skin moisture change rate rate with the change curve of usage time；
The sample that Fig. 7 is formulated using embodiment 3 is before use and using face wrinkles' area accounting in 2 weeks with usage time
Change curve；
The sample that Fig. 8 is formulated using embodiment 3 is before use and using face wrinkles' variation diagram after 2 weeks.
Note：In the present invention (0.5,1.0,0.1) represent 0.5 part of tocopherol acetate, 1.0 parts of mannitol ester silanol C,
0.1 part of precious Rogor powder, the rest may be inferred for remaining.
Specific embodiment
Some nonessential modifications and adaptations that the principle that invention illustrates is made all belong to the scope of protection of the present invention.It is following
Specific technological parameter of example etc. is also only an example in OK range, i.e. those skilled in the art can pass through this paper's
Illustrate to do the selection in OK range, and do not really want to be defined in hereafter exemplary specific data.
Embodiment 1：
Skin care item formula is：0.5 part of tocopherol acetate, 1.0 parts of mannitol ester silanol C, 0.1 part of precious Rogor powder,
1.0 parts of precious Rogor, 4.0 parts of glycerine, 3.0 parts of 1,3 butylene glycols, 1.0 parts of urea, 0.03 part of Scleroglucan, 2.0 parts of antierythrites,
0.1 part of allantoin, 2.0 parts of stearic acid, 6.0 portions of rapeseed oils, 2.0 parts of shea butters, 0.5 part of beeswax, 4.0 parts of polydimethylsiloxanes
Alkane, 0.05 part of xylitol, 0.5 part of methyl p-hydroxybenzoate, 0.03 part of cream jasmin france, surplus are water.
Embodiment 2：
Skin care item formula is：0.5 part of tocopherol acetate, 3.0 parts of mannitol ester silanol C, 1.0 parts of precious Rogor powder,
4.0 parts of glycerine, 3.0 parts of 1,3 butylene glycols, 1.0 parts of urea, 0.03 part of Scleroglucan, 2.0 parts of antierythrites, 0.1 part of allantoin,
2.0 parts of stearic acid, 6.0 portions of rapeseed oils, 2.0 parts of shea butters, 0.5 part of beeswax, 4.0 parts of dimethyl silicone polymers, 0.05 part of wood
Sugar alcohol, 0.5 part of methyl p-hydroxybenzoate, 0.03 part of cream jasmin france, surplus are water.
Embodiment 3：
Skin care item formula is：0.5 part of tocopherol acetate, 5.0 parts of mannitol ester silanol C, 0.5 part of precious Rogor powder,
1.0 parts of precious Rogor, 4.0 parts of glycerine, 3.0 parts of 1,3 butylene glycols, 1.0 parts of urea, 0.03 part of Scleroglucan, 2.0 parts of antierythrites,
0.1 part of allantoin, 2.0 parts of stearic acid, 6.0 portions of rapeseed oils, 2.0 parts of shea butters, 0.5 part of beeswax, 4.0 parts of polydimethylsiloxanes
Alkane, 0.05 part of xylitol, 0.5 part of methyl p-hydroxybenzoate, 0.03 part of cream jasmin france, surplus are water.
Embodiment 4：
Skin care item formula is：0.8 part of tocopherol acetate, 1.0 parts of mannitol ester silanol C, 1.0 parts of precious Rogor powder,
3.0 parts of glycerine, 2.0 parts of 1,3 butylene glycols, 0.01 part of Scleroglucan, 1.0 parts of antierythrites, 0.05 part of allantoin, 1.0 parts of polyoxies
Ethylene bay ether, 5 portions of rapeseed oils, 1.0 parts of shea butters, 0.1 part of beeswax, 3.0 parts of dimethyl silicone polymers, 0.02 part of xylose
Alcohol, 0.1 part of ethyl-para-hydroxybenzoate, 0.01 part of Mint Essence, surplus are water.
Embodiment 5：
Skin care item formula is：0.8 part of tocopherol acetate, 3.0 parts of mannitol ester silanol C, 0.5 part of precious Rogor powder,
3.0 parts of glycerine, 2.0 parts of 1,3 butylene glycols, 0.01 part of Scleroglucan, 1.0 parts of antierythrites, 0.05 part of allantoin, 1.0 parts of polyoxies
Ethylene bay ether, 5 portions of rapeseed oils, 1.0 parts of shea butters, 0.1 part of beeswax, 3.0 parts of dimethyl silicone polymers, 0.02 part of xylose
Alcohol, 0.1 part of ethyl-para-hydroxybenzoate, 0.01 part of Mint Essence, surplus are water.
Embodiment 6：
Skin care item formula is：0.8 part of tocopherol acetate, 5.0 parts of mannitol ester silanol C, 0.1 part of precious Rogor powder,
3.0 parts of glycerine, 2.0 parts of 1,3 butylene glycols, 0.01 part of Scleroglucan, 1.0 parts of antierythrites, 0.05 part of allantoin, 1.0 parts of polyoxies
Ethylene bay ether, 5 portions of rapeseed oils, 1.0 parts of shea butters, 0.1 part of beeswax, 3.0 parts of dimethyl silicone polymers, 0.02 part of xylose
Alcohol, 0.1 part of ethyl-para-hydroxybenzoate, 0.01 part of Mint Essence, surplus are water.
Embodiment 7：
Skin care item formula is：1.0 parts of tocopherol acetates, 1.0 parts of mannitol ester silanol C, 0.5 part of precious Rogor powder,
6.0 parts of glycerine, 4.0 parts of 1,3 butylene glycols, 4.0 parts of urea, 0.1 part of Scleroglucan, 4.0 parts of antierythrites, 0.2 part of allantoin,
4.0 parts of siloxanes, 8.0 portions of rapeseed oils, 5.0 parts of shea butters, 1.0 parts of beeswaxs, 5.0 parts of dimethyl silicone polymers, 0.1 part of xylose
Alcohol, 1.0 parts of propylparabens, 0.05 part of flavoring rose essence, surplus are water.
Embodiment 8：
Skin care item formula is：1.0 parts of tocopherol acetates, 3.0 parts of mannitol ester silanol C, 0.1 part of precious Rogor powder,
6.0 parts of glycerine, 4.0 parts of 1,3 butylene glycols, 4.0 parts of urea, 0.1 part of Scleroglucan, 4.0 parts of antierythrites, 0.2 part of allantoin,
4.0 parts of siloxanes, 8.0 portions of rapeseed oils, 5.0 parts of shea butters, 1.0 parts of beeswaxs, 5.0 parts of dimethyl silicone polymers, 0.1 part of xylose
Alcohol, 1.0 parts of propylparabens, 0.05 part of flavoring rose essence, surplus are water.
Embodiment 9：
Skin care item formula is：1.0 parts of tocopherol acetates, 5.0 parts of mannitol ester silanol C, 1.0 parts of precious Rogor powder,
6.0 parts of glycerine, 4.0 parts of 1,3 butylene glycols, 4.0 parts of urea, 0.1 part of Scleroglucan, 4.0 parts of antierythrites, 0.2 part of allantoin,
4.0 parts of siloxanes, 8.0 portions of rapeseed oils, 5.0 parts of shea butters, 1.0 parts of beeswaxs, 5.0 parts of dimethyl silicone polymers, 0.1 part of xylose
Alcohol, 1.0 parts of propylparabens, 0.05 part of flavoring rose essence, surplus are water.
Comparative example 1：
Skin care item formula is：0.5 part of tocopherol acetate, 5.0 parts of mannitol ester silanol C, 4.0 parts of glycerine, 3.0 parts
1,3 butylene glycol, 1.0 parts of urea, 0.03 part of Scleroglucan, 2.0 parts of antierythrites, 0.1 part of allantoin, 2.0 parts of stearic acid, 6.0
Portion rapeseed oil, 2.0 parts of shea butters, 0.5 part of beeswax, 4.0 parts of dimethyl silicone polymers, 0.05 part of xylitol, 0.5 part to hydroxyl
Methyl benzoate, 0.03 part of cream jasmin france, surplus are water.
Comparative example 2：
Skin care item formula is：5.0 parts of mannitol ester silanol C, 0.5 part of precious Rogor powder, 4.0 parts of glycerine, 3.0 part 1,3-
Butanediol, 1.0 parts of urea, 0.03 part of Scleroglucan, 2.0 parts of antierythrites, 0.1 part of allantoin, 2.0 parts of stearic acid, 6.0 portions of dishes
Seed oil, 2.0 parts of shea butters, 0.5 part of beeswax, 4.0 parts of dimethyl silicone polymers, 0.05 part of xylitol, 0.5 part of para hydroxybenzene first
Sour methyl esters, 0.03 part of cream jasmin france, surplus are water.
Comparative example 3：
Skin care item formula is：0.5 part of tocopherol acetate, 0.5 part of precious Rogor powder, 4.0 parts of glycerine, 3.0 parts of 1,3- fourths two
Alcohol, 1.0 parts of urea, 0.03 part of Scleroglucan, 2.0 parts of antierythrites, 0.1 part of allantoin, 2.0 parts of stearic acid, 6.0 parts of vegetable seed
Oil, 2.0 parts of shea butters, 0.5 part of beeswax, 4.0 parts of dimethyl silicone polymers, 0.05 part of xylitol, 0.5 part of P-hydroxybenzoic acid
Methyl esters, 0.03 part of cream jasmin france, surplus are water.
1st, moisture percutaneously scatter rate (TEWL) test：
The percutaneous rate of scattering and disappearing of moisture (TEWL) is carried out using CK Multi-functional skins tester to test.Two products are chosen every time to exist
The hairless skin part of same subject face the same area is tested, and skip test is also by this execution.
The percutaneous rate of scattering and disappearing of the sample of different formulations moisture after four weeks is used such as the following table 1：
Table 1
| Sample | Before use | After 1h | After 6h | After one day | After a week | After two weeks | After three weeks | After four weeks |
| Embodiment 1 (0.5,1.0,0.1) | 13.8 | 18.7 | 19.2 | 13.6 | 8.8 | 16.3 | 16.2 | 15.5 |
| Embodiment 2 (0.5,3.0,1.0) | 15.8 | 16.8 | 17.6 | 17.5 | 9.3 | 13.4 | 12.3 | 18.3 |
| Embodiment 3 (0.5,5.0,0.5) | 15.4 | 17.6 | 17.8 | 18.8 | 10.1 | 14.8 | 15.9 | 21.5 |
| Embodiment 4 (0.8,1.0,1.0) | 10.1 | 16.3 | 13.3 | 10.3 | 11.1 | 12.2 | 18.0 | 20.3 |
| Embodiment 5 (0.8,3.0,0.5) | 21.5 | 26.8 | 13.0 | 17.3 | 18.4 | 16.6 | 17.1 | 14.9 |
| Embodiment 6 (0.8,5.0,0.1) | 13.3 | 19.4 | 12.8 | 12.3 | 15.1 | 18.6 | 16.8 | 7.4 |
| Embodiment 7 (1.0,1.0,0.5) | 21.4 | 16 | 14.8 | 16.8 | 17.8 | 13.4 | 19.0 | 14.7 |
| Embodiment 8 (1.0,3.0,0.1) | 21.7 | 15.8 | 20.5 | 16.4 | 15.1 | 15.1 | 22.7 | 14.9 |
| Embodiment 9 (1.0,5.0,1.0) | 15.2 | 18.1 | 13.3 | 20.0 | 13.8 | 19.3 | 16.5 | 12.8 |
Note：In the present invention (0.5,1.0,0.1) represent 0.5 part of tocopherol acetate, 1.0 parts of mannitol ester silanol C,
0.1 part of precious Rogor powder, the rest may be inferred for remaining.
As can be seen from Table 1, subject percutaneously scatters rate 10 using the moisture in the skin-protection product surrounding of different formulations
It is fluctuated between~25, maintains essentially in normal level.
2nd, moisture is tested：
Moisture test is carried out using CK Multi-functional skins tester.Two products are chosen every time in same subject's face
Portion's the same area is tested, and skin moisture content is averaged after the same area selects 5 fixed points to be tested every time
Value, and tested in hairless skin part, skip test is also to be performed by this, wherein, amplification (enhancing rate/change rate)=
(moisture after using N hours-uses moisture before product)/using moisture * 100% before product.
When the content of tocopherol acetate is fixed as 0.5 part, different mannitol ester silanol C, precious Rogor powder content
Skin moisture content of the sample within the time for using surrounding sees below table 2, moisture amplification (enhancing rate/change rate) variation
See Fig. 1：
Table 2
When the content of tocopherol acetate is fixed as 0.8 part, different mannitol ester silanol C, precious Rogor powder content
Skin moisture content of the sample within the time for using surrounding sees below table 3, moisture amplification (enhancing rate/change rate) variation
See Fig. 2：
Table 3
When the content of tocopherol acetate is fixed as 1.0 parts, different mannitol ester silanol C, precious Rogor powder content
Skin moisture content of the sample within the time for using surrounding sees below table 4, moisture amplification (enhancing rate/change rate) variation
See Fig. 3：
Table 4
By table 2 and Fig. 1 it is found that subject's moisture after product is used has apparent rising, when mannitol ester silicon
Alkanol C content and precious Rogor powder content at 5.0 parts, 0.5 part, are better than respectively using overall moisture lifting capacity in the time of surrounding
Other 2 group of formula, and herein be formulated when moisture raising amount be up to 100.32%.
By table 3 and Fig. 2 it is found that subject's moisture after product is used is fluctuated, there is promotion substantially, work as mannose
Alcohol ester silanol C content and precious Rogor powder content at 3.0 parts, 0.5 part, are promoted respectively using overall moisture in the time of surrounding
Amount is better than other 2 group of formula, and moisture improves up to 69.34% in this formula, but its moisture raising amount is not as good as fertility
The content of phenol acetic acid esters is fixed as overall moisture raising amount at 0.5 part.
By table 4 and Fig. 3 it is found that subject's moisture content fluctuation after product is used is more apparent, hydraulic lift amount unobvious,
When mannitol ester silanol C content and precious Rogor powder content respectively at 3.0 parts, 0.1 part when, using whole in the time of surrounding
Body hydraulic lift amount be better than other 2 group of formula, and herein be formulated when moisture raising amount highest be also only 29.91%.
When the content of mannitol ester silanol C is fixed as 1.0 parts, different bearing phenol acetic acid esters, precious Rogor powder content
Fig. 4 is shown in skin moisture content enhancing rate variation of the sample within the time for using surrounding, and as shown in Figure 4, subject is using production
Moisture is promoted after product, when tocopheryl acetate ester content and precious Rogor content respectively at 0.5 part, 0.1 part when, use
In the time of surrounding overall moisture lifting capacity be better than other 2 group of formula, and herein be formulated when moisture raising amount be up to
53.76%.
When the content of mannitol ester silanol C is fixed as 3.0 parts, different bearing phenol acetic acid esters, precious Rogor powder content
Fig. 5 is shown in skin moisture content enhancing rate variation of the sample within the time for using surrounding, and as shown in Figure 5, subject is using production
Moisture is promoted more apparent after product, when tocopheryl acetate ester content and precious Rogor powder content respectively at 0.8 part, 0.5 part when, make
It is more steady with overall moisture lifting capacity in the time of surrounding, but when tocopheryl acetate ester content and precious Rogor powder content exist respectively
At 0.5 part, 1.0 parts, when using the 3-4 weeks, clearly, in 4th week, hydraulic lift amount reaches hydraulic lift amount
99.80%.
When the content of mannitol ester silanol C is fixed as 5.0 parts, different bearing phenol acetic acid esters, precious Rogor powder content
Fig. 6 is shown in skin moisture content enhancing rate variation of the sample within the time for using surrounding, it will be appreciated from fig. 6 that subject is using production
Moisture is promoted more apparent after product, when tocopheryl acetate ester content and precious Rogor powder content respectively at 0.5 part, 0.5 part when, make
Moisture raising amount is up to when being better than other 2 group of formula with overall moisture lifting capacity in the time of surrounding, and being formulated herein
100.32%.
3rd, skin wrinkle resisting is tested：
Optimal case is selected according to above test, skin wrinkle resisting test is carried out to optimal case.Using first being carried out before product
Skip test to make later product effect comparison, carries out test of taking pictures in face's the same area every time, and skip test is also by this
It performs, during test, it is desirable that bright and clear, it is clear to take pictures.
Rate of percutaneously being scattered according to moisture (TEWL) is tested and moisture test data, chooses cost performance optimal case
(0.5,5.0,0.5), i.e.,：0.5 part of tocopherol acetate, 5.0 parts of mannitol ester silanol C, 0.5 part of precious Rogor powder, i.e., in fact
The formula in example 3 is applied as wrinkle of skin test sample, subject records initial pictures with VISIA imaging systems before use
Perform an analysis artwork, and subject is daily using product, and 2 weeks by a definite date, choosing the same photo opporunity in any one day weekly made subject
Photograph to record comparing with the face after product, experiment flow, image and data analysis are as follows：
1st, material and instrument
Without effect facial cleanser, test specimen, VISIA-CR skin of face analyzers.
2nd, volunteer requires：Age, face had the women of apparent wrinkle or microgroove between 26~55 years old.
3rd, experimental design：
Subject face is tried out into sample, daily sooner or later using once, the trial employment period, which does not use, has effects that anti-ageing Eradicates wrinkles
Product, before use, using 7 days, 14 days when pay a return visit and photograph to record, the area percentage of the same constituency wrinkle of integrated image analysis
Than.
4th, testing process：Before test, after subject cleans test position, 15 are sat quietly in the environment of constant temperature and humidity system
~20 minutes, then carry out photographic analysis.
Crease-resistant test the results are shown in Table 5, Fig. 7, Fig. 8：
Table 5
| User | Use position | Age | 0d | 7d | 14d |
| Pan | Face | 54 | 12.26% | 8.64% | 8.61% |
It can be seen that from above-mentioned chart：The trend that decreased significantly using wrinkle measurer after this product 2 weeks, this illustrates this
Product has good wrinkle improvement effect.
Claims (10)
1. a kind of skin care item for including precious Rogor powder, it is characterised in that：Based on 100 parts of quality, by the component of following mass fractions
Composition：0.1~1.0 part of vitamin E, 1~10 part of mannitol ester silanol C, 0.1~2 part of precious Rogor powder, surplus is auxiliary agent.
2. a kind of skin care item for including precious Rogor powder according to claim 1, it is characterised in that：The mass fraction is：
0.3~0.7 part of vitamin E, 3~7 parts of mannitol ester silanol C, 0.3~1.0 part of precious Rogor powder, surplus is auxiliary agent.
3. a kind of skin care item for including precious Rogor powder according to claim 1, it is characterised in that：The mass fraction is：
0.4~0.6 part of vitamin E, 4~6 parts of mannitol ester silanol C, 0.4~0.6 part of precious Rogor powder, surplus is auxiliary agent.
4. according to a kind of skin care item for including precious Rogor powder of claims 1 to 3 any one of them, it is characterised in that：The treasured
Rogor powder adds in beta-cyclodextrin after being digested by precious Rogor pulp and handles to obtain.
5. according to a kind of skin care item for including precious Rogor powder of claims 1 to 3 any one of them, it is characterised in that：It is described to help
Agent is made of component A, B component, component C and D components, and component A is selected from glycerine, butanediol, Scleroglucan, antierythrite, allantois
At least one of element, xylitol, urea；B component in rapeseed oil, shea butter, beeswax, dimethyl silicone polymer extremely
Few one kind；Component C is selected from least one of preservative, essence；D components are selected from emulsifier.
6. a kind of skin care item for including precious Rogor powder according to claim 5, it is characterised in that：The component A by glycerine,
Butanediol, Scleroglucan, antierythrite, allantoin, xylitol, urea composition；B component by rapeseed oil, shea butter, beeswax,
Dimethyl silicone polymer forms；Component C is made of preservative, essence；D components are made of emulsifier.
7. a kind of skin care item for including precious Rogor powder according to claim 6, it is characterised in that：Each substance of component A
Mass fraction be：3~6 parts of glycerine, 2~4 parts of 1,3 butylene glycols, 0.01~0.1 part of Scleroglucan, 1~4 part of antierythrite,
0.05~0.2 part of allantoin, 0.02~0.1 part of xylitol, 0~4 part of urea；The mass fraction of each substance of B component is：5
~8 portions of rapeseed oils, 1~5 part of shea butter, 0.1~1.0 part of beeswax, 3~5 parts of dimethyl silicone polymers；Each object of component C
The mass fraction of matter is：0.1~1.0 portion of preservative, 0.01~0.05 part of essence；The mass fraction of the D component materials is：1
~4 parts of emulsifiers.
A kind of 8. preparation method of the skin care item comprising precious Rogor powder of claim 5-7 any one of them, which is characterized in that packet
Include following steps：
(1) various raw materials in precise formula, are contained in vessel；
(2) component A of water and auxiliary agent is added in water phase agitated kettle, stirring, heating is heated and stirred, and heat preservation is standby
With；
(3) by the B component of auxiliary agent, vitamin E input oil phase agitated kettle, stirring, heating is heated and is stirred, and is kept the temperature
It is spare；
(4) raw material in water phase agitated kettle is pumped into vacuum emulsification pot, the raw material being pumped into after stirring evenly in oil phase agitated kettle,
D components are added in, are stirred after emulsifying, are cooled down after constant temperature stirring defoaming；
(5) component C, mannitol ester silanol C and the precious Rogor powder of auxiliary agent are added in, discharges, stand after stirring；
(6) after the assay was approved, filling, packaging, coding, storage.
9. a kind of preparation method of skin care item comprising precious Rogor powder according to claim 8, it is characterised in that：It is wherein precious
Rogor powder is prepared by a method comprising the following steps：
(a) precious Rogor fresh fruit, cleaning peeling, separation fruit, core are taken；
(b) add water in pulp, grinding adds in pectase, makes pulp enzymolysis, digestion afterwards；
(c) the pulp press filtration after enzymolysis, digestion is cleaned, enzyme is killed in heating；
(d) pH is adjusted, is concentrated in vacuo；
(e) beta-cyclodextrin is added in, rear spray drying is to get precious Rogor powder.
10. according to a kind of skin care item comprising precious Rogor powder of claim 1~7 any one of them in middle-aged and the old's skin care
Using.
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| CN108815014A (en) * | 2018-08-15 | 2018-11-16 | 白东跃 | Skin care item and preparation method thereof containing swan-mussel polysaccharide and precious Rogor |
| CN109966202A (en) * | 2019-03-27 | 2019-07-05 | 广州博罗霍生物科技有限公司 | Purposes of the precious Rogor in Transdermal absorption |
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