CN108815014A - Skin care item and preparation method thereof containing swan-mussel polysaccharide and precious Rogor - Google Patents
Skin care item and preparation method thereof containing swan-mussel polysaccharide and precious Rogor Download PDFInfo
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- CN108815014A CN108815014A CN201810930869.4A CN201810930869A CN108815014A CN 108815014 A CN108815014 A CN 108815014A CN 201810930869 A CN201810930869 A CN 201810930869A CN 108815014 A CN108815014 A CN 108815014A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
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- A61P37/08—Antiallergic agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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Abstract
The present invention provides a kind of skin care item containing swan-mussel polysaccharide and precious Rogor, and preparation method thereof.The skin care item include the raw material of following mass percentage：Swan-mussel polysaccharide 1.0%~5.0%, precious Rogor powder 1.0%~8.0%, surplus are other skin care ingredients and auxiliary agent.The skin care item can be inhibited tyrosinase activity effectively, keep skin moisture, have good whitening, moisture-keeping efficacy.
Description
Technical field
The invention belongs to technical field of skin care.More particularly to a kind of skin care item containing swan-mussel polysaccharide and precious Rogor, and
Preparation method and use.
Background technique
Swan-mussel polysaccharide is a kind of white obtained from extracting, purifying in the freshwater mussel meat of fresh water bivalve mollusks hydriopsis cumingii
Powdered natural polysaccharide substance has beauty, beauty treatment, anti-senescence function and a kind of national new resource food.Swan-mussel polysaccharide category
In acid mucopolysaccharide, excellent moisture-keeping functions can be used as a kind of ideal natural moisturizing factor, be suitable for different skin quality, weather,
It is used under environment.Swan-mussel polysaccharide can also improve skin physiology condition, for dermal collagen and elastomer synthesis provide it is superior
External environment, reinforced nutrition matter supply, play the effect of skin-protecting face nursing.In addition, swan-mussel polysaccharide can also prevent one in cell
The generation of a little enzymes reduces free radical and is formed, and plays in terms of preventing free radical from destroying eucaryotic cell structure and causing skin aging important
Effect.
Precious Rogor（Borojo patinoi Cuatrec）It is the ripening fruits of Rubiaceae woods fruit platymiscium, originates in South America
Tropical rain forest.Treasured Rogor is mainly by the way that using the pulp of precious Rogor as raw material, through peeling, deseeding, pectinase enzymatic hydrolysis concentration is sprayed at present
Mist is dried to powder in food or cosmetics.It is had shown that through research, precious Rogor powder is rich in natural iridoid glycosides, polyphenol and Huang
Ketone antioxidant and rare B family vitamin in general tropical fruit (tree), minerals etc., as science in precious Rogor powder
Anti-oxidant composition known to boundary plays crucial positive effect in terms of human health and prevention disease, can help tissue
Cellular damage caused by free radical is resisted, mankind's ageing process is controlled.Current result of study also shows precious Rogor powder and is changing
In cosmetic field, have the function of moisturizing, anti-aging, uvioresistant, antiallergy and whitening.
Swan-mussel polysaccharide or precious Rogor have been machined on various skin care item, but currently, about swan-mussel polysaccharide and precious Rogor
Combination compounds rare research with other skin care ingredients.
Summary of the invention
Inventor has found after further research, by swan-mussel polysaccharide and precious Rogor be combined and with other skin care ingredients
It is compounded, has the function of good synergy moisturizing, whitening.
To achieve the above object, the present invention provides a kind of skin care item containing swan-mussel polysaccharide and precious Rogor, comprising following
The raw material of mass percentage：Swan-mussel polysaccharide 1.0%~5.0%, precious Rogor powder 1.0%~8.0%, Sodium Hyaluronate 0.1%~
0.3%, emulsifier 2.0%~7.0%, moisturizing composition 14.1%~30.3%, thickener 0.3%~1.2%, solubilizer 0.3%
~0.6%, vitamin C 0.05%~0.15%, vitamin E 0.1%~0.8%, EDTA-2Na 0.01%~0.08%, 1,3- the third two
Alcohol 2.0%~6.0%, methyl hydroxybenzoate 0.1%~0.3%, Nipasol 0.05%~0.15%, glycerol 2.0%~6.0%, essence 0.02%
~0.08%, surplus is purified water；
The swan-mussel polysaccharide, using hydriopsis cumingii meat as raw material, extracted, enzymatic hydrolysis, ultrafiltration, alcohol precipitation, drying, crushing and etc. system
At, and Thick many candies（With glucose meter）Content is greater than 70%；
The treasured Rogor powder is using the pulp of precious Rogor as raw material, and through peeling, deseeding, pectinase enzymatic hydrolysis concentration is spray dried to
Powder is made.
Preferably, the skin care item include lotion, Essence, toner, face cream, facial mask, mildy wash and facial cleanser.
Preferably, the skin care item are lotion.
Preferably, mass percentage of each substance in skin care item is respectively in the emulsifier：Laruyl alcohol polyoxy second
Alkene ether 0.5%~2.0% and Tween-80 1.5%~5.0%；
Mass percentage of each substance in skin care item is respectively in the moisturizing composition：Shea butter 2.5%~
5.5%, carbonic acid dioctyl ester 2.5%~6.0%, maleic acid ricinolein 2.5%~5.5%, plant bionic sebum 0.3%~1.2%, pungent
Acid/Triglyceride DDD 3.2%~5.5%, saualane 3.0%~6.0% and allantoin 0.1%~0.6%；
Mass percentage of each substance in skin care item is respectively in the thickener：Xanthan gum 0.1%~0.6% and ethoxy
Cellulose 0.2%~0.6%；
The solubilizer is glycol distearate 0.1%~0.3%, Cremophor RH40 0.2%~0.3%.
The present invention also provides a kind of preparation method of skin care item containing swan-mussel polysaccharide and precious Rogor, the skin care item are used
Following steps are prepared：
(1) in water phase pot, swan-mussel polysaccharide is added（In advance with appropriate 80 DEG C of hot water dissolving）, precious Rogor powder（In advance with appropriate
Purified water dissolution）, EDTA-2Na, allantoin, glycerol, xanthan gum, 1,3- propylene glycol, hydroxyethyl cellulose（In advance with whole
The dispersion of 1,3- propylene glycol）, Sodium Hyaluronate and appropriate purified water, be heated to 85 DEG C, stirring is uniformly dispersed to dissolving；
(2) in oily phase pot, methyl hydroxybenzoate, Nipasol, saualane, carbonic acid dioctyl ester, maleic acid ricinolein, plant is added
Bionical sebum, shea butter, glycol distearate, Cremophor RH40, olive oil, caprylic/capric glycerol
Three esters, ethoxylated dodecyl alcohol, Tween-80, vitamin E are heated to 85 DEG C, and stir abundant to dissolving；
(3) material in oily phase pot is added in water phase pot, starts homogenizer, speed is 1000~6000rpm, emulsifying homogeneous
3~8min, it is rear to cool down；
(4) 30 DEG C are cooled to, vitamin C, essence and appropriate purified water is added, it is quantitative, it is sufficiently stirred, is down to room temperature；
(5) it vacuumizes, discharges, it is filling to get the skin care item.
Compared with prior art, the present invention has the advantages that：The present invention by by swan-mussel polysaccharide and precious Rogor into
Row is combined and is compounded with other skin care ingredients, and resulting composition can be inhibited tyrosinase activity effectively, keeps skin water
Point, there is good whitening, moisture-keeping efficacy, by test, under formula of the invention, swan-mussel polysaccharide has good with precious Rogor powder
Good synergistic function.
Specific embodiment
In the implementation of the present invention, those of ordinary skill in the art are not departing from scope and spirit of the present invention reality
The various embodiments generated on the basis of matter and modification are obvious and are easy to perform.Pass through following implementation
Example is further elaborated with application of the invention etc., it is not intended that embodiment limitation of the present invention.
Embodiment 1, skin care item containing swan-mussel polysaccharide and precious Rogor and preparation method thereof
Raw material comprising following mass percentage：
Swan-mussel polysaccharide 3.0%, precious Rogor powder 4.2%, Sodium Hyaluronate 0.18%, ethoxylated dodecyl alcohol 0.8%, Tween-80
2.5%, saualane 5.8%, carbonic acid dioctyl ester 3.8%, maleic acid ricinolein 3.6%, plant bionic sebum 0.8%, caprylic/capric
Triglycerides 3.5%, shea butter 3.8%, allantoin 0.4%, xanthan gum 0.3, hydroxyethyl cellulose 0.6%, ethylene glycol distearyl
Acid esters 0.15%, Cremophor RH40 0.45%, vitamin C 0.1%, vitamin E 0.6%, EDTA-2Na 0.06%, 1,3-
Propylene glycol 3.8%, methyl hydroxybenzoate 0.2%, Nipasol 0.1%, glycerol 5%, essence 0.05%, surplus are purified water；
Preparation method is as follows：
(1) in water phase pot, swan-mussel polysaccharide is added（In advance with appropriate 80 DEG C of hot water dissolving）, precious Rogor powder（In advance with appropriate
Purified water dissolution）, EDTA-2Na, allantoin, glycerol, xanthan gum, 1,3- propylene glycol, hydroxyethyl cellulose（In advance with whole
The dispersion of 1,3- propylene glycol）, Sodium Hyaluronate and appropriate purified water, be heated to 85 DEG C, stirring is uniformly dispersed to dissolving；
(2) in oily phase pot, methyl hydroxybenzoate, Nipasol, saualane, carbonic acid dioctyl ester, maleic acid ricinolein, plant is added
Bionical sebum, shea butter, glycol distearate, Cremophor RH40, olive oil, caprylic/capric glycerol
Three esters, ethoxylated dodecyl alcohol, Tween-80, vitamin E are heated to 85 DEG C, and stir abundant to dissolving；
(3) material in oily phase pot is added in water phase pot, starts homogenizer, speed is 1000~6000rpm, emulsifying homogeneous
3~8min, it is rear to cool down；
(4) 30 DEG C are cooled to, vitamin C, essence and appropriate purified water is added, it is quantitative, it is sufficiently stirred, is down to room temperature；
(5) it vacuumizes, discharges, it is filling to get the skin care item.
Embodiment 2, the moisturizing of skin care item containing swan-mussel polysaccharide and precious Rogor, whitening effect
1. sample preparation
1. preparing resulting skin care item as observation group's sample using the formula of embodiment 1；
2. swan-mussel polysaccharide is not added in the formula of embodiment 1 using its same preparation method preparation gained sample as reference group
Sample 1；
3. precious Rogor powder is not added in the formula of embodiment 1 using its same preparation method preparation gained sample as reference group
Sample 2；
4. swan-mussel polysaccharide is not added in the formula of embodiment 1 with precious Rogor powder with its same preparation method preparation gained sample
As reference group sample 3.
2. moistening effect is tested
Its moisture-keeping efficacy is evaluated by the moisturizing rate of skin care item, moisturizing rate is higher, illustrates that moisture-absorbing moisture-keeping effect is better.
Fill saturation (NH4)2SO4Environment (RH=81%) of the drier inner cavity of aqueous solution as relative humidity 81%, will contain
There is saturation K2SO4Environment (RH=43%) of the drier inner cavity of aqueous solution as relative humidity 43%, then accurately weighs respectively
0.5g is dry to observation group's sample of constant weight, reference group sample 1, reference group sample 2, reference group sample 3, above four groups of samples point
Not Jia Yang quality 10% deionized water, be placed in small weighing bottle, and be put in above-mentioned 2 driers respectively, by 2 dryings
Device is placed in 20 DEG C of isoperibols, is stood for 24 hours, and the quality of each sample is weighed, and calculates moisturizing rate：
Moisturizing rate=m4/m3×100%
m3It is the initial biodiversity of sample, m4It is the biodiversity of rear sample for 24 hours.
3. whitening effect is tested
Its white-skinned face function is evaluated to the inhibitory effect of tyrosinase activity by detecting skin care item；Tyrosinase residual activity is got over
It is low, illustrate that skin care item are better to the inhibitory effect of tyrosinase activity, white-skinned face function is better.
Test is with ultraviolet spectrophotometry（The selective absorbing of light is analyzed with substance）To measure sample pair
The inhibiting effect of tyrosinase and the activity of tyrosinase；This experiment using ultra-violet (UV) band by tyrosinase and DOPA enzymatically
Oxidation product dopachrome is formed, dopachrome has absorption maximum at 475nm, and absorptivity ε=3700 (cmmol/L) comes
It carries out.
Draw the L-3,4 dihydroxyphenylalanine and 2.6mL phosphate buffer solution of 1.0mL 2mmoL/L respectively using hand-held liquid-transfering gun（PH=
6.8）It is placed in cuvette, the constant temperature 10min in 30 DEG C of waters bath with thermostatic control, 0.2mL observation group sample, reference group sample is then added
1,100 μ g/mL tyrosinase solution of reference group sample 2, reference group sample 3 and 0.2mL constitutes 4mL solution system；In wavelength
It changes with time value to measure the absorbance in solution system 8min at 475nm, tyrosinase residual activity (U) calculates public affairs
Formula is as follows：
U=[(OD1-OD3)/OD2-OD4]×100%
In formula:OD1Refer to the absorbance of the live body system containing substrate, tyrosinase, sample solution；OD3Refer to and contains only bottom
The absorbance of the live body system of object, sample solution；OD2Refer to the extinction for containing only the live body system of substrate, tyrosinase solution
Degree；OD4Refer to the absorbance for containing only the live body system of substrate solution.
4. testing result
The testing result of sample moisturizing whitening effect in observation group, reference group is shown in Table 1.
Table 1
From the above results, the skin care item containing swan-mussel polysaccharide and precious Rogor can be inhibited tyrosinase activity effectively, be had good
Moisturizing well, white-skinned face function, while swan-mussel polysaccharide and precious Rogor have good synergistic function.
Claims (7)
1. the skin care item containing swan-mussel polysaccharide and precious Rogor, which is characterized in that the raw material comprising following mass percentage：Freshwater mussel meat
Polysaccharide 1.0%~5.0%, precious Rogor powder 1.0%~8.0%, Sodium Hyaluronate 0.1%~0.3%, emulsifier 2.0%~7.0%, moisturizing
Moist composition 14.1%~30.3%, thickener 0.3%~1.2%, solubilizer 0.3%~0.6%, vitamin C 0.05%~
0.15%, vitamin E 0.1%~0.8%, EDTA-2Na 0.01%~0.08%, 1,3- propylene glycol 2.0%~6.0%, methyl hydroxybenzoate
0.1%~0.3%, Nipasol 0.05%~0.15%, glycerol 2.0%~6.0%, essence 0.02%~0.08%, surplus are purified water.
2. the skin care item according to claim 1 containing swan-mussel polysaccharide and precious Rogor, which is characterized in that the skin care item packet
Include lotion, Essence, toner, face cream, facial mask, mildy wash and facial cleanser.
3. the skin care item according to claim 2 containing swan-mussel polysaccharide and precious Rogor, which is characterized in that the skin care item are
Lotion.
4. the skin care item according to claim 3 containing swan-mussel polysaccharide and precious Rogor, which is characterized in that in the emulsifier
Mass percentage of each substance in skin care item be respectively：Ethoxylated dodecyl alcohol 0.5%~2.0% and Tween-80 1.5%
~5.0%；
Mass percentage of each substance in skin care item is respectively in the moisturizing composition：Shea butter 2.5%~
5.5%, carbonic acid dioctyl ester 2.5%~6.0%, maleic acid ricinolein 2.5%~5.5%, plant bionic sebum 0.3%~1.2%, pungent
Acid/Triglyceride DDD 3.2%~5.5%, saualane 3.0%~6.0% and allantoin 0.1%~0.6%；
Mass percentage of each substance in skin care item is respectively in the thickener：Xanthan gum 0.1%~0.6% and ethoxy
Cellulose 0.2%~0.6%；
The solubilizer is glycol distearate 0.1%~0.3%, Cremophor RH40 0.2%~0.3%.
5. the preparation method of the skin care item containing swan-mussel polysaccharide and precious Rogor according to claim 3-4, which is characterized in that
Include the following steps：
(1) in water phase pot, swan-mussel polysaccharide is added（In advance with appropriate 80 DEG C of hot water dissolving）, precious Rogor powder（In advance with appropriate
Purified water dissolution）, EDTA-2Na, allantoin, glycerol, xanthan gum, 1,3- propylene glycol, hydroxyethyl cellulose（In advance with whole
The dispersion of 1,3- propylene glycol）, Sodium Hyaluronate and appropriate purified water, be heated to 85 DEG C, stirring is uniformly dispersed to dissolving；
(2) in oily phase pot, methyl hydroxybenzoate, Nipasol, saualane, carbonic acid dioctyl ester, maleic acid ricinolein, plant is added
Bionical sebum, shea butter, glycol distearate, Cremophor RH40, olive oil, caprylic/capric glycerol
Three esters, ethoxylated dodecyl alcohol, Tween-80, vitamin E are heated to 85 DEG C, and stir abundant to dissolving；
(3) material in oily phase pot is added in water phase pot, starts homogenizer, speed is 1000~6000rpm, emulsifying homogeneous
3~8min, it is rear to cool down；
(4) 30 DEG C are cooled to, vitamin C, essence and appropriate purified water is added, it is quantitative, it is sufficiently stirred, is down to room temperature；
(5) it vacuumizes, discharges, it is filling to get the skin care item.
6. a kind of skin care item and preparation method thereof containing swan-mussel polysaccharide and precious Rogor, which is characterized in that include following quality hundred
Divide the raw material of content：
Swan-mussel polysaccharide 3.0%, precious Rogor powder 4.2%, Sodium Hyaluronate 0.18%, ethoxylated dodecyl alcohol 0.8%, Tween-80
2.5%, saualane 5.8%, carbonic acid dioctyl ester 3.8%, maleic acid ricinolein 3.6%, plant bionic sebum 0.8%, caprylic/capric
Triglycerides 3.5%, shea butter 3.8%, allantoin 0.4%, xanthan gum 0.3, hydroxyethyl cellulose 0.6%, ethylene glycol distearyl
Acid esters 0.15%, Cremophor RH40 0.45%, vitamin C 0.1%, vitamin E 0.6%, EDTA-2Na 0.06%, 1,3-
Propylene glycol 3.8%, methyl hydroxybenzoate 0.2%, Nipasol 0.1%, glycerol 5%, essence 0.05%, surplus are purified water；
Preparation method is as follows：
(1) in water phase pot, swan-mussel polysaccharide is added（In advance with appropriate 80 DEG C of hot water dissolving）, precious Rogor powder（In advance with appropriate
Purified water dissolution）, EDTA-2Na, allantoin, glycerol, xanthan gum, 1,3- propylene glycol, hydroxyethyl cellulose（In advance with whole
The dispersion of 1,3- propylene glycol）, Sodium Hyaluronate and appropriate purified water, be heated to 85 DEG C, stirring is uniformly dispersed to dissolving；
(2) in oily phase pot, methyl hydroxybenzoate, Nipasol, saualane, carbonic acid dioctyl ester, maleic acid ricinolein, plant is added
Bionical sebum, shea butter, glycol distearate, Cremophor RH40, olive oil, caprylic/capric glycerol
Three esters, ethoxylated dodecyl alcohol, Tween-80, vitamin E are heated to 85 DEG C, and stir abundant to dissolving；
(3) material in oily phase pot is added in water phase pot, starts homogenizer, speed is 1000~6000rpm, emulsifying homogeneous
3~8min, it is rear to cool down；
(4) 30 DEG C are cooled to, vitamin C, essence and appropriate purified water is added, it is quantitative, it is sufficiently stirred, is down to room temperature；
(5) it vacuumizes, discharges, it is filling to get the skin care item.
7. the skin care item described in -6 containing swan-mussel polysaccharide and precious Rogor according to claim 1, which is characterized in that the skin care item
It can effectively inhibit tyrosinase activity, keep skin moisture, there is good whitening, moisture-keeping efficacy.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109568243A (en) * | 2019-01-31 | 2019-04-05 | 张鹭云 | A kind of waterless nano vitamin C face cream and preparation method thereof |
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Application publication date: 20181116 |