CN108112866A - The acquisition methods of anthocyanidin sterling in a kind of gynura bicolor blade - Google Patents
The acquisition methods of anthocyanidin sterling in a kind of gynura bicolor blade Download PDFInfo
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- CN108112866A CN108112866A CN201711440827.4A CN201711440827A CN108112866A CN 108112866 A CN108112866 A CN 108112866A CN 201711440827 A CN201711440827 A CN 201711440827A CN 108112866 A CN108112866 A CN 108112866A
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- gynura bicolor
- anthocyanidin
- sterling
- blade
- gynura
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- 229930014669 anthocyanidin Natural products 0.000 title claims abstract description 53
- 150000001452 anthocyanidin derivatives Chemical class 0.000 title claims abstract description 53
- 235000008758 anthocyanidins Nutrition 0.000 title claims abstract description 53
- 241000123865 Gynura bicolor Species 0.000 title claims abstract description 48
- 238000000034 method Methods 0.000 title claims abstract description 17
- 239000000843 powder Substances 0.000 claims abstract description 13
- 238000000605 extraction Methods 0.000 claims abstract description 10
- 230000018044 dehydration Effects 0.000 claims abstract description 6
- 238000006297 dehydration reaction Methods 0.000 claims abstract description 6
- 238000001694 spray drying Methods 0.000 claims abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000007864 aqueous solution Substances 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 6
- 238000003306 harvesting Methods 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- 239000007921 spray Substances 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 claims description 4
- 230000007547 defect Effects 0.000 claims description 3
- 238000004043 dyeing Methods 0.000 claims description 2
- 241001122767 Theaceae Species 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 235000013305 food Nutrition 0.000 abstract description 11
- 235000013361 beverage Nutrition 0.000 abstract description 8
- 244000061458 Solanum melongena Species 0.000 abstract description 6
- 239000011521 glass Substances 0.000 abstract description 6
- 239000000049 pigment Substances 0.000 abstract description 6
- 230000000050 nutritive effect Effects 0.000 abstract description 2
- 238000012856 packing Methods 0.000 abstract description 2
- 229920003266 Leaf® Polymers 0.000 description 12
- 235000002864 food coloring agent Nutrition 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000000284 extract Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- VEVZSMAEJFVWIL-UHFFFAOYSA-O cyanidin cation Chemical compound [O+]=1C2=CC(O)=CC(O)=C2C=C(O)C=1C1=CC=C(O)C(O)=C1 VEVZSMAEJFVWIL-UHFFFAOYSA-O 0.000 description 2
- 235000013373 food additive Nutrition 0.000 description 2
- 239000002778 food additive Substances 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 241000030710 Cynura Species 0.000 description 1
- GCPYCNBGGPHOBD-UHFFFAOYSA-N Delphinidin Natural products OC1=Cc2c(O)cc(O)cc2OC1=C3C=C(O)C(=O)C(=C3)O GCPYCNBGGPHOBD-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241001530884 Gynura segetum Species 0.000 description 1
- 240000002129 Malva sylvestris Species 0.000 description 1
- 235000006770 Malva sylvestris Nutrition 0.000 description 1
- 241000233805 Phoenix Species 0.000 description 1
- 241000235342 Saccharomycetes Species 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 208000026106 cerebrovascular disease Diseases 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000019804 chlorophyll Nutrition 0.000 description 1
- 229930002875 chlorophyll Natural products 0.000 description 1
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 235000007336 cyanidin Nutrition 0.000 description 1
- JKHRCGUTYDNCLE-UHFFFAOYSA-O delphinidin Chemical compound [O+]=1C2=CC(O)=CC(O)=C2C=C(O)C=1C1=CC(O)=C(O)C(O)=C1 JKHRCGUTYDNCLE-UHFFFAOYSA-O 0.000 description 1
- 235000007242 delphinidin Nutrition 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- HKUHOPQRJKPJCJ-UHFFFAOYSA-N pelargonidin Natural products OC1=Cc2c(O)cc(O)cc2OC1c1ccc(O)cc1 HKUHOPQRJKPJCJ-UHFFFAOYSA-N 0.000 description 1
- 235000006251 pelargonidin Nutrition 0.000 description 1
- XVFMGWDSJLBXDZ-UHFFFAOYSA-O pelargonidin Chemical compound C1=CC(O)=CC=C1C(C(=C1)O)=[O+]C2=C1C(O)=CC(O)=C2 XVFMGWDSJLBXDZ-UHFFFAOYSA-O 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 239000009685 tusanqi Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
- A23L5/41—Retaining or modifying natural colour by use of additives, e.g. optical brighteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/58—Colouring agents
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Botany (AREA)
- Mycology (AREA)
- General Preparation And Processing Of Foods (AREA)
Abstract
The invention belongs to natural pigment development fields, and in particular to the extraction of anthocyanidin sterling in gynura bicolor blade.Gynura bicolor tender leaf and top browse are taken, the measures such as clean, green removing in high temperature, dehydration, ultrasonic wave extraction, spray drying.The aubergine anthocyanidin sterling powder of acquisition can be directly used for the formulas such as food or beverage, it is also possible to be sealed after Brown Glass Brown glass bottles and jars only packing, 04 DEG C of environment lower long periods preserve.The gynura bicolor tender leaf annual output that the present invention takes is up to 2500Kg/666.7m2, for anthocyanidin sterling yield up to 7.5% 8.5%, the natural anthocyanidin sterling that the method obtains not only has very high nutritive value and health-care efficacy, and yield is high, color is gorgeous, stability is good, has good commercial value in tender leaf.
Description
Technical field
The present invention relates to plant extracts technical fields, and in particular to the extraction of anthocyanidin sterling in a kind of gynura bicolor blade
Method.
Background technology
Daily the eaten food additives pigment of people is divided into natural pigment and synthetic dyestuff, is sent out in synthetic food color
Before bright, the mankind it is initially use be all natural pigment, later since synthetic food color is at low cost, use currently on the market
In food color pigment nearly all be artificial color.With going deep into for research, it has been found that most artificial color food additive
Add agent that there is side effect, some synthetic dyestuffs, which have, to be caused to let out even carcinogenic danger.Natural pigment such as anthocyanidin etc. has safety
Property high and tool nutrition and health care and other effects, but the defects of natural anthocyanidin acquisition generally needs to expend higher cost and poor stability,
And the extract that the technique that tradition extracts natural anthocyanidin obtains is typically liquid state, is unfavorable for storing and apply, therefore, opens
Hair yield is high, it is good to stablize and is modern food industry development suitable for the solid-state like natural anthocyanidin sterling that the long period preserves
There is an urgent need to.
Gynura bicolor(Cynura bicolor)Alias kwan-yin dish, red phoenix dish, red back of the body dish, red dish, Gynura bicolor etc., are composite family
The ground such as gynura segetum category perennial herb plant, native to China, Japanese and Southeast Asia, in Fujian, Taiwan, Guangdong, Hainan
Etc. ground be distributed.In recent years, gynura bicolor is as a kind of commercialization plantation eaten vegetables raw and have certain area.Artificial growth is purple
It is few to carry on the back dish pest and disease damage, management is simple and yield is high, but eats gynura bicolor raw due to influencing it with peculiar taste as common
Vegetables large area is planted.Gynura bicolor face of blade green, back side purple, therefore it contains outside chlorophyll also rich in anthocyanidin(Bag
Include cyanidin, pelargonidin, delphinidin and high mallow element etc.), special anthocyanidin aqueous solution that gynura bicolor is rich in(Or it dries
The dry anthocyanidin powder obtained) stability is strong, safe without toxic side effect, there is prevention cardiovascular and cerebrovascular disease, protect liver, anticancer, anti-
The multiple efficacies such as oxidation and removing free radical and enhancing body immunity, meanwhile, gynura bicolor anthocyanidin is to bacterium and saccharomycete
With apparent inhibitory action, there is good fresh-keeping effect, therefore natural food colour-cyanine is developed from gynura bicolor
Plain sterling will have broad prospects.
The content of the invention
It is an object of the invention to obtain a kind of natural anthocyanidin sterling, using gynura bicolor blade as raw material, by finishing,
The measures such as dehydration, ultrasonic wave extraction, spray drying obtain anthocyanidin sterling in gynura bicolor blade, this anthocyanidin sterling can conduct
The additives such as luxury food beverage have the multiple efficacies such as nutrition and health care and color protection.
The acquisition methods of anthocyanidin sterling, are as follows in a kind of gynura bicolor blade:
(1)Choose the gynura bicolor rich in anthocyanidin(Front is dark green, the back side is dark purple)Seedling carries out domestication
Cultivating and growing, when such gynura bicolor length is to 22 ± 3cm, harvesting top young stem and leaf grows 18 ± 3cm;Take its tender leaf and top
3-5cm young stem and leafs are material, and 110 DEG C of tea baking machines are put into after cleaning drying(Model:
TYS-6CHG-6)Finish 25-30min, then adjusts curer temperature to continuing between 68-72 DEG C to bake 90-100 min,
Make gynura bicolor leaves water loss 60% or so;
(2)Solvent is done using pure water, solid-liquid ratio is 1:3 to 1:4(g/mL), 80 DEG C of temperature, power
Pass through ultrasonic wave under 270W environment(Model:KQ-33DE )Extract 40-50min;
(3)Gynura bicolor mixture is squeezed with filtered through gauze and firmly, gained high concentration anthocyanidin aqueous solution carries out
Spray dryer is dried(Model:YC-1800 ;120 DEG C of wind turbine temperature;Pressure:0.2Mpa ), finally obtain purplish red dyeing defect
Blue or green element sterling powder;
(4)The aubergine anthocyanidin sterling powder of acquisition can be directly used for the formula such as food or beverage or with brown
It is sealed after the packing of color vial, is preserved under 0-4 DEG C of environment and be used further to match somebody with somebody as food or beverage etc. within 6-8 months
Side.
The beneficial effects of the present invention are:
(1)The present invention by finishing and making after its appropriate dehydration ultrasonic wave extraction again, is obtained using rich in anthocyanidin gynura bicolor tender leaf
The anthocyanidin aqueous solution of higher concentration is obtained, is dried finally by spray dryer, acquisition stability is good within a short period of time, is suitable for
The anthocyanidin sterling that long period preserves.
(2)The gynura bicolor tender leaf annual output that the present invention takes is up to 2500Kg/666.7m2, anthocyanidin sterling obtains in tender leaf
Rate is up to 7.5%-8.5%, therefore, per 666.7m2The anthocyanidin sterling raw material that field can obtain 200Kg or so in 1 year, this flower
The alternative part synthetic food color of blue or green element sterling, and develop the different functionalities food with health-care efficacy.Meanwhile this side
The natural anthocyanidin sterling that method obtains not only has very high nutritive value and health-care efficacy, and yield is high, color is gorgeous, stablizes
Property it is good, have good development prospect.
Specific embodiment
Below in conjunction with specific embodiment, the present invention will be further described, but the present invention is not limited only to these embodiments.
Embodiment 1
A kind of acquisition methods of gynura bicolor anthocyanidin sterling, specifically include following steps
(1)Choose the gynura bicolor rich in anthocyanidin(Front is dark green, the back side is dark purple)Seedling carries out domestication's high yield
Cultivating and growing when such gynura bicolor length is to 22 ± 3cm, harvests top young stem and leaf and grows 18 ± 3cm in time;
(2)Its branch is abandoned, it is material to take its blade and its top browse, and 110 DEG C of tealeaves are put into after cleaning drying
Curer finishes 25min, then adjusts curer temperature and continue to bake to 70 DEG C, and the time is 90 min, makes gynura bicolor blade
Dehydration 60% or so;
(3)Solvent is done using pure water, solid-liquid ratio is 1:3(g/mL), 80 DEG C of temperature, lead under power 270W environment
Cross ultrasonic wave extraction 40min;
(4)Gynura bicolor mixture is squeezed with filtered through gauze and firmly, gained high concentration anthocyanidin aqueous solution is using spraying
Drying machine is dried, and finally obtains aubergine anthocyanidin sterling powder.
(5)For anthocyanidin yield up to 7.5%, the aubergine anthocyanidin of acquisition is pure in the gynura bicolor tender leaf that the method obtains
Product powder can be directly used for the formulas such as food or beverage;Or sealed after being dispensed with Brown Glass Brown glass bottles and jars only, it can be protected under 0 DEG C of environment
There are the formulas such as food or beverage are used further within 8 months.
Embodiment 2
A kind of acquisition methods of gynura bicolor anthocyanidin sterling, specifically include following steps
(1)Choose the gynura bicolor rich in anthocyanidin(Front is dark green, the back side is dark purple)Seedling carries out domestication's high yield
Cultivating and growing when such gynura bicolor length is to 22 ± 3cm, harvests top young stem and leaf and grows 18 ± 3cm in time;
(2)Its branch is abandoned, it is material to take its blade and its top browse, and 110 DEG C of tealeaves are put into after cleaning drying
Curer finishes 30min, then adjusts curer temperature and continue to bake to 68 DEG C, and the time is 100 min, makes gynura bicolor blade
Dehydration 60% or so;
(3)Solvent, solid-liquid ratio 1 are done using pure water:4(g/mL), 80 DEG C of temperature, pass through ultrasonic wave extraction under power 270W environment
50min;
(4)Gynura bicolor mixture is squeezed with filtered through gauze and firmly, gained high concentration anthocyanidin aqueous solution carries out
Spray dryer is dried, and finally obtains aubergine anthocyanidin sterling powder.
(5)For anthocyanidin yield up to 8.5%, the aubergine anthocyanidin of acquisition is pure in the gynura bicolor tender leaf that the method obtains
Product powder can be directly used for the formulas such as food or beverage;Or sealed after being dispensed with Brown Glass Brown glass bottles and jars only, it can be protected under 4 DEG C of environment
It deposits and the formulas such as food or beverage is used further within 6 months.
Comparative example 1
(1)Choose the gynura bicolor rich in anthocyanidin(Front is dark green, the back side is dark purple)Seedling carries out domestication's high yield
Cultivating and growing when such gynura bicolor length is to 22 ± 3cm, harvests top young stem and leaf and grows 18 ± 3cm in time;
(2)Its branch is abandoned, it is material to take its blade and its top browse, and solvent, solid-liquid ratio 1 are done using pure water:5(g/
mL), 80 DEG C of temperature, under power 270W environment by ultrasonic wave extraction twice, each 50min merges filtrate twice;It is dry, it obtains
Obtain anthocyanidin sterling powder.
(3)Anthocyanidin yield is 3.2% in the gynura bicolor tender leaf that the method obtains, and the anthocyanidin obtained with embodiment 1,2 obtains
Rate is compared to more significant lower.Meanwhile the method is obtained in anthocyanidin powder process, since the anthocyanidin aqueous solution that early period obtains is dense
Degree it is too low, cause the later stage drying obtain anthocyanidin powder spent time it is long, the anthocyanidin powder color of acquisition it is not gorgeous enough and
Stability is poor, the shelf-life is short.
Claims (3)
1. a kind of acquisition methods of anthocyanidin sterling in gynura bicolor blade, it is characterised in that:Gynura bicolor tender leaf is taken, including top
By clean, green removing in high temperature, dehydration, ultrasonic wave extraction, spray drying, it is pure to obtain gynura bicolor blade anthocyanidin for 3-5cm browses
Product.
2. the acquisition methods of anthocyanidin sterling in a kind of gynura bicolor blade according to claim 1, it is characterised in that:Tool
Body step is as follows:
(1)Dark green, back side darkviolet the gynura bicolor in plantation front, treats such gynura bicolor length to 22 ± 3cm
When, harvesting top young stem and leaf grows 18 ± 3cm;
(2)It is material to take its tender leaf and top 3-5cm sprays, and being put into 110 DEG C of tea baking machines after cleaning kills
Blue or green 25-30 min, then curer temperature is adjusted to 68-72 DEG C, drying time is 90-100 min, loses gynura bicolor blade
Water 60% ~ 65%;
(3)With step(2)The gynura bicolor leaf of acquisition is extracting object, adds in pure water, is led under 80 DEG C of temperature, power 270W environment
Cross ultrasonic wave extraction 40-50min;Filtering;
(4)Gained high concentration anthocyanidin aqueous solution carries out spray dryer drying, finally obtains purplish red dyeing defect
Blue or green element sterling powder.
3. the acquisition methods of anthocyanidin sterling in a kind of gynura bicolor blade according to claim 1, it is characterised in that:Step
(3)The solid-liquid ratio of middle pure water and gynura bicolor leaf is 1:3 to 1:4, unit g/mL.
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CN201711440827.4A CN108112866A (en) | 2017-12-27 | 2017-12-27 | The acquisition methods of anthocyanidin sterling in a kind of gynura bicolor blade |
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Cited By (2)
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CN108743491A (en) * | 2018-08-30 | 2018-11-06 | 福建春辉生物工程有限公司 | A kind of antibacterial anti-inflammatory talcum powder |
CN111685311A (en) * | 2020-07-02 | 2020-09-22 | 中国计量大学 | Processing method of gynura bicolor and lentinus edodes lotus root starch and product thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108743491A (en) * | 2018-08-30 | 2018-11-06 | 福建春辉生物工程有限公司 | A kind of antibacterial anti-inflammatory talcum powder |
CN111685311A (en) * | 2020-07-02 | 2020-09-22 | 中国计量大学 | Processing method of gynura bicolor and lentinus edodes lotus root starch and product thereof |
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Application publication date: 20180605 |