CN108112866A - The acquisition methods of anthocyanidin sterling in a kind of gynura bicolor blade - Google Patents

The acquisition methods of anthocyanidin sterling in a kind of gynura bicolor blade Download PDF

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Publication number
CN108112866A
CN108112866A CN201711440827.4A CN201711440827A CN108112866A CN 108112866 A CN108112866 A CN 108112866A CN 201711440827 A CN201711440827 A CN 201711440827A CN 108112866 A CN108112866 A CN 108112866A
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CN
China
Prior art keywords
gynura bicolor
anthocyanidin
sterling
blade
gynura
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Pending
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CN201711440827.4A
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Chinese (zh)
Inventor
张少平
邱珊莲
郑开斌
张少华
应璐
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INSTITUTE OF SUBTROPICAL AGRICULTURE FUJIAN ACADEMY OF AGRICULTURAL SCIENCES
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INSTITUTE OF SUBTROPICAL AGRICULTURE FUJIAN ACADEMY OF AGRICULTURAL SCIENCES
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Priority to CN201711440827.4A priority Critical patent/CN108112866A/en
Publication of CN108112866A publication Critical patent/CN108112866A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/40Colouring or decolouring of foods
    • A23L5/41Retaining or modifying natural colour by use of additives, e.g. optical brighteners
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • A23L2/58Colouring agents
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105Plant extracts, their artificial duplicates or their derivatives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Botany (AREA)
  • Mycology (AREA)
  • General Preparation And Processing Of Foods (AREA)

Abstract

The invention belongs to natural pigment development fields, and in particular to the extraction of anthocyanidin sterling in gynura bicolor blade.Gynura bicolor tender leaf and top browse are taken, the measures such as clean, green removing in high temperature, dehydration, ultrasonic wave extraction, spray drying.The aubergine anthocyanidin sterling powder of acquisition can be directly used for the formulas such as food or beverage, it is also possible to be sealed after Brown Glass Brown glass bottles and jars only packing, 04 DEG C of environment lower long periods preserve.The gynura bicolor tender leaf annual output that the present invention takes is up to 2500Kg/666.7m2, for anthocyanidin sterling yield up to 7.5% 8.5%, the natural anthocyanidin sterling that the method obtains not only has very high nutritive value and health-care efficacy, and yield is high, color is gorgeous, stability is good, has good commercial value in tender leaf.

Description

The acquisition methods of anthocyanidin sterling in a kind of gynura bicolor blade
Technical field
The present invention relates to plant extracts technical fields, and in particular to the extraction of anthocyanidin sterling in a kind of gynura bicolor blade Method.
Background technology
Daily the eaten food additives pigment of people is divided into natural pigment and synthetic dyestuff, is sent out in synthetic food color Before bright, the mankind it is initially use be all natural pigment, later since synthetic food color is at low cost, use currently on the market In food color pigment nearly all be artificial color.With going deep into for research, it has been found that most artificial color food additive Add agent that there is side effect, some synthetic dyestuffs, which have, to be caused to let out even carcinogenic danger.Natural pigment such as anthocyanidin etc. has safety Property high and tool nutrition and health care and other effects, but the defects of natural anthocyanidin acquisition generally needs to expend higher cost and poor stability, And the extract that the technique that tradition extracts natural anthocyanidin obtains is typically liquid state, is unfavorable for storing and apply, therefore, opens Hair yield is high, it is good to stablize and is modern food industry development suitable for the solid-state like natural anthocyanidin sterling that the long period preserves There is an urgent need to.
Gynura bicolor(Cynura bicolor)Alias kwan-yin dish, red phoenix dish, red back of the body dish, red dish, Gynura bicolor etc., are composite family The ground such as gynura segetum category perennial herb plant, native to China, Japanese and Southeast Asia, in Fujian, Taiwan, Guangdong, Hainan Etc. ground be distributed.In recent years, gynura bicolor is as a kind of commercialization plantation eaten vegetables raw and have certain area.Artificial growth is purple It is few to carry on the back dish pest and disease damage, management is simple and yield is high, but eats gynura bicolor raw due to influencing it with peculiar taste as common Vegetables large area is planted.Gynura bicolor face of blade green, back side purple, therefore it contains outside chlorophyll also rich in anthocyanidin(Bag Include cyanidin, pelargonidin, delphinidin and high mallow element etc.), special anthocyanidin aqueous solution that gynura bicolor is rich in(Or it dries The dry anthocyanidin powder obtained) stability is strong, safe without toxic side effect, there is prevention cardiovascular and cerebrovascular disease, protect liver, anticancer, anti- The multiple efficacies such as oxidation and removing free radical and enhancing body immunity, meanwhile, gynura bicolor anthocyanidin is to bacterium and saccharomycete With apparent inhibitory action, there is good fresh-keeping effect, therefore natural food colour-cyanine is developed from gynura bicolor Plain sterling will have broad prospects.
The content of the invention
It is an object of the invention to obtain a kind of natural anthocyanidin sterling, using gynura bicolor blade as raw material, by finishing, The measures such as dehydration, ultrasonic wave extraction, spray drying obtain anthocyanidin sterling in gynura bicolor blade, this anthocyanidin sterling can conduct The additives such as luxury food beverage have the multiple efficacies such as nutrition and health care and color protection.
The acquisition methods of anthocyanidin sterling, are as follows in a kind of gynura bicolor blade:
(1)Choose the gynura bicolor rich in anthocyanidin(Front is dark green, the back side is dark purple)Seedling carries out domestication
Cultivating and growing, when such gynura bicolor length is to 22 ± 3cm, harvesting top young stem and leaf grows 18 ± 3cm;Take its tender leaf and top 3-5cm young stem and leafs are material, and 110 DEG C of tea baking machines are put into after cleaning drying(Model:
TYS-6CHG-6)Finish 25-30min, then adjusts curer temperature to continuing between 68-72 DEG C to bake 90-100 min, Make gynura bicolor leaves water loss 60% or so;
(2)Solvent is done using pure water, solid-liquid ratio is 1:3 to 1:4(g/mL), 80 DEG C of temperature, power
Pass through ultrasonic wave under 270W environment(Model:KQ-33DE )Extract 40-50min;
(3)Gynura bicolor mixture is squeezed with filtered through gauze and firmly, gained high concentration anthocyanidin aqueous solution carries out
Spray dryer is dried(Model:YC-1800 ;120 DEG C of wind turbine temperature;Pressure:0.2Mpa ), finally obtain purplish red dyeing defect Blue or green element sterling powder;
(4)The aubergine anthocyanidin sterling powder of acquisition can be directly used for the formula such as food or beverage or with brown
It is sealed after the packing of color vial, is preserved under 0-4 DEG C of environment and be used further to match somebody with somebody as food or beverage etc. within 6-8 months Side.
The beneficial effects of the present invention are:
(1)The present invention by finishing and making after its appropriate dehydration ultrasonic wave extraction again, is obtained using rich in anthocyanidin gynura bicolor tender leaf The anthocyanidin aqueous solution of higher concentration is obtained, is dried finally by spray dryer, acquisition stability is good within a short period of time, is suitable for The anthocyanidin sterling that long period preserves.
(2)The gynura bicolor tender leaf annual output that the present invention takes is up to 2500Kg/666.7m2, anthocyanidin sterling obtains in tender leaf Rate is up to 7.5%-8.5%, therefore, per 666.7m2The anthocyanidin sterling raw material that field can obtain 200Kg or so in 1 year, this flower The alternative part synthetic food color of blue or green element sterling, and develop the different functionalities food with health-care efficacy.Meanwhile this side The natural anthocyanidin sterling that method obtains not only has very high nutritive value and health-care efficacy, and yield is high, color is gorgeous, stablizes Property it is good, have good development prospect.
Specific embodiment
Below in conjunction with specific embodiment, the present invention will be further described, but the present invention is not limited only to these embodiments.
Embodiment 1
A kind of acquisition methods of gynura bicolor anthocyanidin sterling, specifically include following steps
(1)Choose the gynura bicolor rich in anthocyanidin(Front is dark green, the back side is dark purple)Seedling carries out domestication's high yield
Cultivating and growing when such gynura bicolor length is to 22 ± 3cm, harvests top young stem and leaf and grows 18 ± 3cm in time;
(2)Its branch is abandoned, it is material to take its blade and its top browse, and 110 DEG C of tealeaves are put into after cleaning drying
Curer finishes 25min, then adjusts curer temperature and continue to bake to 70 DEG C, and the time is 90 min, makes gynura bicolor blade Dehydration 60% or so;
(3)Solvent is done using pure water, solid-liquid ratio is 1:3(g/mL), 80 DEG C of temperature, lead under power 270W environment
Cross ultrasonic wave extraction 40min;
(4)Gynura bicolor mixture is squeezed with filtered through gauze and firmly, gained high concentration anthocyanidin aqueous solution is using spraying
Drying machine is dried, and finally obtains aubergine anthocyanidin sterling powder.
(5)For anthocyanidin yield up to 7.5%, the aubergine anthocyanidin of acquisition is pure in the gynura bicolor tender leaf that the method obtains
Product powder can be directly used for the formulas such as food or beverage;Or sealed after being dispensed with Brown Glass Brown glass bottles and jars only, it can be protected under 0 DEG C of environment There are the formulas such as food or beverage are used further within 8 months.
Embodiment 2
A kind of acquisition methods of gynura bicolor anthocyanidin sterling, specifically include following steps
(1)Choose the gynura bicolor rich in anthocyanidin(Front is dark green, the back side is dark purple)Seedling carries out domestication's high yield
Cultivating and growing when such gynura bicolor length is to 22 ± 3cm, harvests top young stem and leaf and grows 18 ± 3cm in time;
(2)Its branch is abandoned, it is material to take its blade and its top browse, and 110 DEG C of tealeaves are put into after cleaning drying
Curer finishes 30min, then adjusts curer temperature and continue to bake to 68 DEG C, and the time is 100 min, makes gynura bicolor blade Dehydration 60% or so;
(3)Solvent, solid-liquid ratio 1 are done using pure water:4(g/mL), 80 DEG C of temperature, pass through ultrasonic wave extraction under power 270W environment 50min;
(4)Gynura bicolor mixture is squeezed with filtered through gauze and firmly, gained high concentration anthocyanidin aqueous solution carries out
Spray dryer is dried, and finally obtains aubergine anthocyanidin sterling powder.
(5)For anthocyanidin yield up to 8.5%, the aubergine anthocyanidin of acquisition is pure in the gynura bicolor tender leaf that the method obtains
Product powder can be directly used for the formulas such as food or beverage;Or sealed after being dispensed with Brown Glass Brown glass bottles and jars only, it can be protected under 4 DEG C of environment It deposits and the formulas such as food or beverage is used further within 6 months.
Comparative example 1
(1)Choose the gynura bicolor rich in anthocyanidin(Front is dark green, the back side is dark purple)Seedling carries out domestication's high yield
Cultivating and growing when such gynura bicolor length is to 22 ± 3cm, harvests top young stem and leaf and grows 18 ± 3cm in time;
(2)Its branch is abandoned, it is material to take its blade and its top browse, and solvent, solid-liquid ratio 1 are done using pure water:5(g/ mL), 80 DEG C of temperature, under power 270W environment by ultrasonic wave extraction twice, each 50min merges filtrate twice;It is dry, it obtains Obtain anthocyanidin sterling powder.
(3)Anthocyanidin yield is 3.2% in the gynura bicolor tender leaf that the method obtains, and the anthocyanidin obtained with embodiment 1,2 obtains Rate is compared to more significant lower.Meanwhile the method is obtained in anthocyanidin powder process, since the anthocyanidin aqueous solution that early period obtains is dense Degree it is too low, cause the later stage drying obtain anthocyanidin powder spent time it is long, the anthocyanidin powder color of acquisition it is not gorgeous enough and Stability is poor, the shelf-life is short.

Claims (3)

1. a kind of acquisition methods of anthocyanidin sterling in gynura bicolor blade, it is characterised in that:Gynura bicolor tender leaf is taken, including top By clean, green removing in high temperature, dehydration, ultrasonic wave extraction, spray drying, it is pure to obtain gynura bicolor blade anthocyanidin for 3-5cm browses Product.
2. the acquisition methods of anthocyanidin sterling in a kind of gynura bicolor blade according to claim 1, it is characterised in that:Tool Body step is as follows:
(1)Dark green, back side darkviolet the gynura bicolor in plantation front, treats such gynura bicolor length to 22 ± 3cm
When, harvesting top young stem and leaf grows 18 ± 3cm;
(2)It is material to take its tender leaf and top 3-5cm sprays, and being put into 110 DEG C of tea baking machines after cleaning kills
Blue or green 25-30 min, then curer temperature is adjusted to 68-72 DEG C, drying time is 90-100 min, loses gynura bicolor blade Water 60% ~ 65%;
(3)With step(2)The gynura bicolor leaf of acquisition is extracting object, adds in pure water, is led under 80 DEG C of temperature, power 270W environment Cross ultrasonic wave extraction 40-50min;Filtering;
(4)Gained high concentration anthocyanidin aqueous solution carries out spray dryer drying, finally obtains purplish red dyeing defect
Blue or green element sterling powder.
3. the acquisition methods of anthocyanidin sterling in a kind of gynura bicolor blade according to claim 1, it is characterised in that:Step (3)The solid-liquid ratio of middle pure water and gynura bicolor leaf is 1:3 to 1:4, unit g/mL.
CN201711440827.4A 2017-12-27 2017-12-27 The acquisition methods of anthocyanidin sterling in a kind of gynura bicolor blade Pending CN108112866A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108743491A (en) * 2018-08-30 2018-11-06 福建春辉生物工程有限公司 A kind of antibacterial anti-inflammatory talcum powder
CN111685311A (en) * 2020-07-02 2020-09-22 中国计量大学 Processing method of gynura bicolor and lentinus edodes lotus root starch and product thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105062131A (en) * 2015-09-01 2015-11-18 福建省农业科学院甘蔗研究所 Method for extracting and using two natural pigments in gynura bicolor
CN105639548A (en) * 2016-01-07 2016-06-08 福建省农业科学院甘蔗研究所 Preparation method for jelly added with gynura bicolor anthocyanin
CN105949166A (en) * 2016-07-13 2016-09-21 吉林省普蓝高科技有限公司 Extraction method for blueberry anthocyanin
CN106189349A (en) * 2016-07-15 2016-12-07 广西顺帆投资有限公司 A kind of method extracting dyestuff based on Radix seu Folium Alchorneae trewioidis

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105062131A (en) * 2015-09-01 2015-11-18 福建省农业科学院甘蔗研究所 Method for extracting and using two natural pigments in gynura bicolor
CN105639548A (en) * 2016-01-07 2016-06-08 福建省农业科学院甘蔗研究所 Preparation method for jelly added with gynura bicolor anthocyanin
CN105949166A (en) * 2016-07-13 2016-09-21 吉林省普蓝高科技有限公司 Extraction method for blueberry anthocyanin
CN106189349A (en) * 2016-07-15 2016-12-07 广西顺帆投资有限公司 A kind of method extracting dyestuff based on Radix seu Folium Alchorneae trewioidis

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
栾娜等: "超声辅助提取紫甘蓝中原花青素工艺的优化", 《安徽农业科学》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108743491A (en) * 2018-08-30 2018-11-06 福建春辉生物工程有限公司 A kind of antibacterial anti-inflammatory talcum powder
CN111685311A (en) * 2020-07-02 2020-09-22 中国计量大学 Processing method of gynura bicolor and lentinus edodes lotus root starch and product thereof

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Application publication date: 20180605