CN108096116B - Preparation method of antibacterial lip balm containing natural pigment - Google Patents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses a preparation method of a natural pigment-containing antibacterial lip balm, which comprises the steps of extracting carrot pigment from carrots, extracting onosma paniculatum with sweet almond oil as a solvent to obtain the onosma paniculatum pigment, dissolving the carrot pigment in the onosma paniculatum pigment, adding butter, natural beeswax, rose essential oil, vitamin E, a vitamin B1/B6 mixture and other humectants, and freezing and molding the obtained mixture to obtain the lip balm. The method does not add any heavy metal and toxic chemical substances, the Yunnan alkanna tinctoria pigment is compounded with the carrot pigment, the sweet almond oil, the ghee, the rose essential oil, the vitamin E, the mixture of the vitamin B1/B6 and the natural beeswax are used as active raw materials, and the obtained lip balm is natural red after being smeared, and has the characteristics of strong tinting strength, heat resistance and light resistance; the obtained lip balm has good moisturizing effect, is mild to lip skin, has no irritation, and also has antibacterial, antiallergic, blood circulation promoting, and lip skin protecting effects.
Description
Technical Field
The invention belongs to the technical field of lip care, and particularly relates to a preparation method of a natural pigment-containing antibacterial lip balm.
Background
The lip balm is one of the cosmetics commonly used in daily life, and is very easy to eat into the body because the lip balm is directly applied to the lips, so that the safety of the lip balm component is closely related to the health. The existing colored lip balm contains complex dye components, can cause lip chap and lip skin peeling after long-term application, has great damage to lip skin, even can cause anaphylactic reaction, and has great threat to human health. Today's health pursuit is more important, so simple lip balms that provide decoration and enhance lip moisturization to the lips have not met the consumer expectations of most women. The effective components extracted from natural plants, particularly from Chinese medicinal plant with health care and health preserving functions are applied to the lip balm, so that the lip balm not only can achieve the beautifying effect, but also has certain nutritive value and medical value, and accords with the green consumption concept pursued by modern people.
Disclosure of Invention
The invention aims to overcome the defects and provides a preparation method of the bacteriostatic lip balm containing the natural pigment.
The second purpose of the invention is to provide the lip gloss obtained by the method.
The purpose of the invention is realized by the following technical scheme:
a method for preparing antibacterial lip balm containing natural pigment comprises extracting radix Dauci Sativae pigment from radix Dauci Sativae, extracting radix Onosporae with sweet almond oil as solvent to obtain radix Onosporae Yunnanensis pigment, dissolving radix Dauci Sativae pigment in the radix Onosporae Yunnanensis pigment, adding ghee, natural Cera flava, oleum Rosae Rugosae, vitamin E, vitamin B1/B6 mixture and other humectant, and freezing and molding the obtained mixture to obtain lip balm.
Further, the method specifically comprises the following steps:
(1) extraction of carrot pigment
Cleaning carrot, performing ultrasonic-assisted extraction, filtering, collecting filtrate, evaporating and concentrating at 40 deg.C, and freeze drying to obtain carrot pigment;
(2) extraction of erythronium erythrorhizon pigment
Weighing 10-20 parts of onosma paniculatum in parts by weight, cleaning, vacuum drying, crushing, sieving with a 50-mesh sieve, performing ultrasonic-assisted extraction with sweet almond oil, and collecting supernatant oil liquid to obtain the erythronium paniculatum pigment;
(3) preparation of lip balm
Weighing 0.8-1 part by weight of the carrot pigment obtained in the step (1), adding the carrot pigment into the Yunnan arnebia euchroma pigment obtained in the step (2), stirring until the carrot pigment is completely dissolved, adding 1-2 parts by weight of ghee and 2.6-4.2 parts by weight of natural beewax, heating for dissolving, naturally cooling to 50 ℃, adding 0.2-0.5 part by weight of rose essential oil, 0.2-0.5 part by weight of vitamin E, 0.2-0.3 part by weight of a vitamin B1/B6 mixture and 0.6-1 part by weight of other humectants, and uniformly stirring;
pouring the obtained liquid composite base material into a mold, freezing and molding, inserting the formed lip balm into a lip balm tube, and vacuumizing to separate the lip balm from the lip balm tube to obtain the antibacterial lip balm containing the natural pigment.
Furthermore, in the step (1), the ultrasonic-assisted extraction conditions include that the extraction solvent is 95 vt% ethanol, the material-liquid ratio g/m L is 1: 5-1: 15, the ultrasonic temperature is 20-40 ℃, the ultrasonic time is 60-120min, the ultrasonic power is 150-.
Furthermore, in the step (2), the ultrasonic-assisted extraction conditions are that the material-liquid ratio g/m L of the longhua lithospermum and the sweet almond oil is 2: 1-1: 2, the ultrasonic temperature is 20-40 ℃, the ultrasonic time is 30-60min, the ultrasonic power is 150-.
Further, in the step (3), the other moisturizers include white petrolatum, glycerin and/or sorbitol.
Further, in the step (3), the heating and dissolving are carried out at 65-75 ℃.
Further, in the step (3), the freeze forming is frozen for 5-10min at an ultralow temperature of-20 ℃.
The bacteriostatic lip balm containing the natural pigment is obtained by any one of the methods.
The Tibetan medicine onosma paniculatum and lithospermum is a medicine and food dual-purpose plant, has a long history, is recorded at first in the Tibetan medicine classic 'treatment precious materia medica', and is recorded in all past generations of materia medica. Is currently collected in Tibetan medicine (first volume) in drug Standard of Ministry of public health of the people's republic of China; the Tibetan medicine is sweet in nature and cool in flavor, has the effects of clearing heat and cooling blood, nourishing lung and inhibiting bacteria, has a long history of medication in China, is commonly used for pneumonia, tuberculosis cavity and high mountain hyperemia, and belongs to common Tibetan medicine materials which are frequently used. In addition, the Yunnan alkanna tinctoria is also a food pigment source used by Tibetan nationality.
Carrot has various health care functions on human body, is known as 'xiao ren', and has the efficacies of strengthening spleen, tonifying liver and improving eyesight. Carrot pigment is one of main nutrients in human food, is considered as a food additive with excellent A-class nutrition, is widely used in the fields of beverages, cosmetics and medicines, and can also be eaten as a health-care product for treating various diseases.
The natural beewax is a substance secreted by four pairs of wax glands under the abdomen of the worker bee, and can increase the skin elasticity of lips; the sweet almond oil is rich in vitamins and has the miraculous effects of nourishing and moisturizing and relieving allergy; the rose essential oil has the effects of resisting aging, preventing wrinkle and keeping moisture.
In order to enhance the moistening and moisturizing performance of the lip balm, butter and other moisturizing agents are added, the butter is fat extracted from cow or sheep milk, is essence of Tibetan food, is rich in energy substances such as fat and the like and important trace elements such as selenium and zinc, has the functions of regulating qi, moisturizing and plasticity, and other moisturizing agents adopt traditional moisturizing agent components such as medicinal white vaseline, glycerin, sorbitol and the like. In order to enhance the antioxidant properties of the lip balm, the natural antioxidant vitamin E is added. In order to improve the health-care characteristics of the lip balm, a vitamin B1/B6 mixture is added.
The invention has the following beneficial effects:
compared with the prior art, the preparation method of the bacteriostatic lip balm containing the natural pigment has the following advantages:
(1) the lip balm does not contain any heavy metal and toxic chemical substances, the active ingredients in the onosma paniculatum are extracted to be compounded with carrot pigment for color matching, sweet almond oil, butter, rose essential oil, vitamin E, a vitamin B1/B6 mixture and natural beeswax are used as active raw materials for composing, the effects of the ingredients are synergistic, the prepared lip balm presents natural red after being smeared, and the lip balm has the characteristics of strong tinting strength, heat resistance and light resistance;
(2) the prepared lip balm has the moisturizing effect higher than that of the conventional lip balm, is mild to the skin of lips, has no stimulation, has excellent effects of inhibiting bacteria, resisting allergy and promoting blood circulation, has certain health-care effects of preventing angular cheilitis and protecting the skin of the lips, and is a pure natural edible antibacterial lip balm.
Detailed Description
The following description of the preferred embodiments of the present invention is provided for the purpose of illustration and description, and is in no way intended to limit the invention.
Example 1
An antibacterial lip balm containing natural pigment comprises 20.0g of onosma paniculatum, 10.0m L of sweet almond oil, 1.5g of ghee, 3.5g of natural beeswax, 1.0g of white vaseline, 0.2g of vitamin E, 0.8g of carrot pigment, 0.2g of rose essential oil and 0.2g of a vitamin B1/B6 mixture.
The preparation method comprises the following steps:
(1) the carrot pigment is extracted by washing carrot, extracting with 95 vt% ethanol under the assistance of ultrasonic waves at the material-liquid ratio (g/m L) of 1: 5 and the ultrasonic temperature of 20 ℃ for 120min and the ultrasonic power of 150W for 2 times, filtering, collecting filtrate, concentrating at 40 ℃ by a rotary evaporator, and freeze-drying to obtain the carrot pigment.
(2) The extraction of the erythrorhizon paniculatum pigment comprises cleaning erythrorhizon paniculatum with distilled water, vacuum drying, pulverizing, sieving with 50 mesh sieve, extracting with sweet almond oil as solvent at a material-liquid ratio (g/m L) of 2: 1 under the assistance of ultrasonic waves at 20 deg.C for 60min at 150W for 1 time, and collecting supernatant to obtain erythrorhizon paniculatum pigment.
(3) Preparing lip balm: placing carrot pigment in sweet almond oil containing Onosma paniculatum pigment, and stirring until completely dissolved; adding butter and natural Cera flava, and heating the solution in a constant temperature water bath at 65-75 deg.C to obtain liquid composite base material; naturally cooling to 50 deg.C, adding rose essential oil, vitamin E, vitamin B1/B6 mixture, and white vaseline, and stirring; pouring the liquid composite base material into a mold, and placing the mold in an ultralow temperature environment of-20 ℃ for freezing and molding for 5-10 min; inserting the formed lip balm into the lip balm tube, and separating the lip balm from the lip balm tube by using the vacuum pumping principle to obtain the bacteriostatic lip balm containing the natural pigment.
Example 2
An antibacterial lip balm containing natural pigment comprises 10.0g of Yunnan arnebia euchroma, 20m L of sweet almond oil, 1g of ghee, 2.6g of natural beeswax, 0.6g of sorbitol, 0.35g of vitamin E, 1.0g of carrot pigment, 0.3g of rose essential oil and 0.3g of a vitamin B1/B6 mixture.
The preparation method comprises the following steps:
(1) extracting carrot pigment by washing carrot, extracting with 95 vt% ethanol under the assistance of ultrasonic waves at a feed-liquid ratio (g/m L) of 1: 10 at 30 ℃ for 90min under the ultrasonic power of 250W for 3 times, filtering, collecting filtrate, concentrating at 40 ℃ by a rotary evaporator, and freeze-drying to obtain the carrot pigment.
(2) The extraction of the erythronium paniculatum pigment comprises the steps of cleaning the erythronium paniculatum with distilled water, drying in vacuum, crushing, sieving with a 50-mesh sieve, extracting the pigment with sweet almond oil as a solvent in a material-liquid ratio (g/m L) of 1: 2, extracting for 1 time by ultrasonic waves at an ultrasonic temperature of 40 ℃ for 45min and an ultrasonic power of 250W, and collecting supernatant oil liquid to obtain the erythronium paniculatum pigment.
(3) Preparing lip balm: placing carrot pigment in sweet almond oil containing Onosma paniculatum pigment, and stirring until completely dissolved; adding butter and natural Cera flava, and heating the solution in a constant temperature water bath at 65-75 deg.C to obtain liquid composite base material; naturally cooling to 50 deg.C, adding rose essential oil, vitamin E, vitamin B1/B6 mixture, and sorbitol, and stirring; pouring the liquid composite base material into a mold, and placing the mold in an ultralow temperature environment of-20 ℃ for freezing and molding for 5-10 min; inserting the formed lip balm into the lip balm tube, and separating the lip balm from the lip balm tube by using the vacuum pumping principle to obtain the bacteriostatic lip balm containing the natural pigment.
Example 3
An antibacterial lip balm containing natural pigment comprises 10.0g of Yunnan arnebia euchroma, 10.0m L of sweet almond oil, 2.0g of ghee, 4.2g of natural beeswax, 0.8g of glycerin, 0.5g of vitamin E, 1.0g of carrot pigment, 0.5g of rose essential oil and 0.3g of a vitamin B1/B6 mixture.
The preparation method comprises the following steps:
(1) extracting carrot pigment by washing carrot, extracting with 95 vt% ethanol under the assistance of ultrasonic waves at a feed-liquid ratio (g/m L) of 1: 15 at 40 ℃ for 60min under the ultrasonic power of 350W for 4 times, filtering, collecting filtrate, concentrating at 40 ℃ by a rotary evaporator, and freeze-drying to obtain the carrot pigment.
(2) The extraction of the erythronium paniculatum pigment comprises the steps of cleaning the erythronium paniculatum with distilled water, drying in vacuum, crushing, sieving with a 50-mesh sieve, extracting the pigment with sweet almond oil as a solvent in a material-liquid ratio (g/m L) of 1: 1, extracting for 1 time by ultrasonic waves at an ultrasonic temperature of 30 ℃ for 30min and an ultrasonic power of 350W, and collecting supernatant oil liquid to obtain the erythronium paniculatum pigment.
(3) Preparing lip balm: placing carrot pigment in sweet almond oil containing Onosma paniculatum pigment, and stirring until completely dissolved; adding butter and natural Cera flava, and heating the solution in a constant temperature water bath at 65-75 deg.C to obtain liquid composite base material; naturally cooling to 50 deg.C, adding rose essential oil, vitamin E, vitamin B1/B6 mixture, and glycerol, and stirring; pouring the liquid composite base material into a mold, and placing the mold in an ultralow temperature environment of-20 ℃ for freezing and molding for 5-10 min; inserting the formed lip balm into the lip balm tube, and separating the lip balm from the lip balm tube by using the vacuum pumping principle to obtain the bacteriostatic lip balm containing the natural pigment.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (7)
1. A preparation method of an antibacterial lip balm containing a natural pigment is characterized in that carrot pigment is extracted from carrots, longhuayunnan arnebia root is extracted by taking sweet almond oil as a solvent to obtain the longhuayunnan arnebia root pigment, the carrot pigment is dissolved in the longhuayunnan arnebia root pigment, ghee, natural beeswax, rose essential oil, vitamin E, a vitamin B1/B6 mixture and other humectants are added, and the obtained mixture is frozen and formed to obtain the lip balm;
the method specifically comprises the following steps:
(1) extraction of carrot pigment
Washing carrots, performing ultrasonic-assisted extraction, filtering, collecting filtrate, evaporating and concentrating at 40 ℃, and freeze-drying to obtain the carrot pigment, wherein the extraction solvent is 95 vt% ethanol, and the material-liquid ratio is 1: 5-1: 15;
(2) extraction of erythronium erythrorhizon pigment
Weighing 10-20 parts of longhua Yunnan alkanna tinctoria, cleaning, drying in vacuum, crushing, sieving with a 50-mesh sieve, carrying out ultrasonic-assisted extraction with sweet almond oil, collecting supernatant oil liquid to obtain longhua Yunnan alkanna tinctoria pigment, wherein the material-liquid ratio of the longhua Yunnan alkanna tinctoria to the sweet almond oil is 2: 1-1: 2;
(3) preparation of lip balm
Weighing 0.8-1 part by weight of the carrot pigment obtained in the step (1), adding the carrot pigment into the Yunnan arnebia euchroma pigment obtained in the step (2), stirring until the carrot pigment is completely dissolved, adding 1-2 parts by weight of ghee and 2.6-4.2 parts by weight of natural beewax, heating for dissolving, naturally cooling to 50 ℃, adding 0.2-0.5 part by weight of rose essential oil, 0.2-0.5 part by weight of vitamin E, 0.2-0.3 part by weight of a vitamin B1/B6 mixture and 0.6-1 part by weight of other humectants, and uniformly stirring;
pouring the obtained liquid composite base material into a mold, freezing and molding, inserting the formed lip balm into a lip balm tube, and vacuumizing to separate the lip balm from the lip balm tube to obtain the antibacterial lip balm containing the natural pigment.
2. The preparation method of the bacteriostatic lip balm containing natural pigment according to claim 1, wherein in the step (1), the ultrasonic-assisted extraction conditions are as follows: the ultrasonic temperature is 20-40 ℃, the ultrasonic time is 60-120min, the ultrasonic power is 150-.
3. The preparation method of the bacteriostatic lip balm containing natural pigment according to claim 1, wherein in the step (2), the ultrasonic-assisted extraction conditions are as follows: the ultrasonic temperature is 20-40 ℃, the ultrasonic time is 30-60min, the ultrasonic power is 150-.
4. The method for preparing bacteriostatic lip balm containing natural pigment according to claim 1, wherein in the step (3), the other moisturizers comprise white vaseline, glycerin and/or sorbitol.
5. The method for preparing bacteriostatic lip balm containing natural pigment according to claim 1, wherein the heating and dissolving in step (3) is carried out at 65-75 ℃.
6. The method for preparing the bacteriostatic lip balm containing the natural pigment according to claim 1, wherein in the step (3), the freeze forming is frozen for 5-10min at an ultra-low temperature of-20 ℃.
7. A bacteriostatic lip balm containing a natural pigment obtained by the method according to any one of claims 1 to 6.
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| CN108619022A (en) * | 2018-06-20 | 2018-10-09 | 钟里梅 | A kind of fruit extraction lip care glaze formula |
| CN109044885B (en) * | 2018-08-10 | 2021-07-23 | 三明学院 | Chinese herbal medicine lipstick capable of improving effective components and preparation method thereof |
| CN108852910A (en) * | 2018-08-17 | 2018-11-23 | 张雨阳 | A kind of lipstick and preparation method thereof |
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| CN109303757A (en) * | 2018-11-15 | 2019-02-05 | 新疆农业大学 | A kind of horseshoe oil and its preparation method and application |
| CN110025561A (en) * | 2019-06-03 | 2019-07-19 | 西藏圣雪生物科技有限公司 | A kind of method that butter extract prepares lipstick, lipstick |
| CN113559021B (en) * | 2021-09-03 | 2023-06-13 | 河南省商业科学研究所有限责任公司 | Peony seed oil lip balm and preparation method thereof |
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| JP5020122B2 (en) * | 2007-02-28 | 2012-09-05 | 株式会社コーセー | Topical skin preparation |
| CN104352396A (en) * | 2014-11-23 | 2015-02-18 | 李文渊 | Tibetan yak butter plateau lip protector |
| CN104983654A (en) * | 2015-06-19 | 2015-10-21 | 邓毅敏 | Pure plant lipstick type rouge and preparing method thereof |
| CN105802754A (en) * | 2016-03-21 | 2016-07-27 | 广州市南大实业有限公司 | Hand-protecting antimicrobial detergent and preparation method and application thereof |
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