CN108060047A - Small water turtle wine and preparation method thereof - Google Patents
Small water turtle wine and preparation method thereof Download PDFInfo
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- CN108060047A CN108060047A CN201711440514.9A CN201711440514A CN108060047A CN 108060047 A CN108060047 A CN 108060047A CN 201711440514 A CN201711440514 A CN 201711440514A CN 108060047 A CN108060047 A CN 108060047A
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Abstract
The invention discloses small water turtle wine and preparation method thereof, 1) feedstock processing；2) pre-treatment；3) Subcritical Water Extraction：The material that upper step obtains is concentrated into raw material weight, it is placed in extraction kettle, adds in sodium carboxymethylcellulose, deionized deoxygenated water is injected in kettle, it is extracted, 150 160 DEG C of extraction temperature, 5 8MPa of pressure, 10 15min of extraction time, extraction terminates, pressure release, extract liquor are flowed into collecting tank and are cooled to room temperature, and obtain extract liquor；4) mix, blend, small water turtle wine is made.
Description
Technical field
The present invention relates to health liquor technical fields, and in particular to the preparation method and use this method of small water turtle wine obtain
The pearl wine obtained.
Background technology
Small water turtle (scientific name：Cyclemys trifasciata), one kind of Testudinidae is called Cuora trifasciata, disconnected plate tortoise, red
Tripe tortoise, golden head tortoise etc. belong to rare tortoise kind, belong to Reptilia Chelonia Testudinidae, are a kind of ornamental tortoises.Meat flavour is delicious, has very high
Edible and medicinal value, be the terrapin that development prospect is had an optimistic view of.The cloudy place covered of selection is liked to inhabit, there is gregarious habit,
Annual winter wants hibernation.Wild small water turtle is extremely rare, in great demand on international, domestic market.Because having feeding habits wide, disease-resistant
The features such as power and Hunger tolerance are strong, viability is strong, artificial feeding is convenient, has considerable economic value.In addition, small water turtle also has pole
High medical value is traditional Chinese medicine, is one of the exporting of Chinese tradition.Move in water, mainly using earthworm as
Food, also eats fish, shrimp, insect and some plant foods in river in addition.World's distribution of small water turtle is very narrow, main
It is distributed in subtropical countries and the areas such as Chinese Guangdong, Guangxi, Fujian, Hainan, Hong Kong, Macao and north and south portion of Vietnam.
China national two level lays special stress on protecting animal；Hong-Kong fishman administration was classified as protection animal varieties in 2004；It is arranged
Enter《Endangered species of wild fauna and flora international trade pact》Two classes protect species；World Conservation Union's pole danger species.Artificial breeding
There are two types of the modes of small water turtle, and one kind is to imitate wild cultivation, exactly copies ingest feature and the growth and development rule of wild small water turtle
Rule cultivation small water turtle, the small water turtle that this mode cultivates can keep strong wild small water turtle disease resistance, long lifespan, laying period long
The advantages of, it is the first choice that kind is made in artificial breeding.Another kind is commercialization cultivation, by heating cultivation or cold water culture but to gold
Money tortoise largely feeds food, allows small water turtle fast-growth fast-ripenin, and the small water turtle disease resistance that this mode cultivates is low, the service life
Short, laying period is short not to lay eggs even, is generally used for edible and medicinal.
Modern times using edible small water turtle as disease preventing and treating, improve constitution, antifatigue diet trend.In China, three lines close
Shell small water turtle is favored be subject to south China and Hong Kong, Macao, Taiwan area and Southeast Asia and Overseas Chinese, except because there is higher nourishing
Outside nutrition, labor illness hectic fever due to yin, chronic cough spitting of blood, bloody flux, hemorrhoid blood, arthralgia and myalgia etc. can be controlled.Small water turtle is particularly suitable for tumor patients,
Postoperative rehabilitation person；Hepatopathy, nephrotic, weak, frequent flu, insomniac；The rheumatic bones such as woman puerperal fever headache, scapulohumeral periarthritis
Bitterly, tatanic spondylitis of lumbar vertebra patient；Chronic gastritis, chronic pharyngitis, chronic stomatocace, rhinitis chronic patient and overstrain one's nerves etc.
Sub-health population to adjust function of human body, improves the immunity of the human body and anti-fatigue ability.The clinical application of binding of pathological, gold
Money tortoise has the special efficacy for keeping human body yin-yang balancing.The content of small water turtle active factors is higher, active factors and various members
Element, which combines, forms one strong fresh combatants, can cure cell and lose extremely, decrease of platelet, and inhibits growth of cancer cells, reaches
Cancer-resisting, the effect for eliminating tumour.Promote blood circulation of human body, while also promote human body cell growth.
Alcoholic strength temperature, acrid flavour and bitter sweet have a warm promoting blood circulation, the surname dissipate efficacy of a drug, warm stomach, and dispersing wind and cold of dispelling rouses oneself yang-energy, eliminates
The effects that tired.Responsible drinking can be added to the fun with happy feelings, but cross drink then unrest, and excessive drinking then consumes vigour, even loses one's life.Doctor
Why hobby wine, be to take its benefaction medicine gesture up in the property of internal organs, four limbs bones of the body collectively, therefore have saying for " length that wine is hundred medicines "
Method.By the Chinese medicine to keep fit and healthy and wine " molten " in the medicinal liquor of one, not only preparation is convenient, pharmacological property is stable, safely and effectively, Er Qieyin
It is a kind of good semi-polarity organic solvent for alcohol, the various active ingredients of Chinese medicine are all soluble in wherein, and wine assisting drug, wine help
Medicine gesture and give full play to its effect, improve curative effect.In fact, wine is a kind of best solvent, many to be difficult to other processing methods
The drug that its active ingredient is precipitated can be extracted by means of this characteristic of wine, and can give full play to its prevention mostly
Disease, the drug effect promoted longevity, here it is medicinal liquor after where cause of many decades without subtracting its glamour.
It has often been said that " prolonged illness is how empty ".Sick deep chronic disease with the passing of time, often leads to the loss of human body gas, blood, yin, yang,
As soon as and its when forming all non-one days, treatment recovers also to be difficult to morning and evening to make contributions, and accomplishes in one move, is typically necessary a process.
Traditional Chinese medicine thinks " pathogen usually intruding into collateral in protracted disease ".Various chronic deficient diseases, are usually present that different degrees of qi and blood is not smooth, passages through which vital energy circulates is not smooth,
Treatment needs assistant with drug promoting blood circulation and removing obstruction in channels to heighten the effect of a treatment often.And the main compatibility of help medicinal liquor has blood-enrich, enriching yin temperature
The tonic food of sun, therefore it is relatively beneficial to the treatment of chronic disease.Personal qi and blood is valued for logical tune.Though it if obtaining help, and cannot flow
It is logical, then the profit of help is can not receive, the evil of anti-raw stasis.
Help medicinal liquor is not only widely used in the prevention of various chronic deficient diseases, moreover it is possible to which anti-aging is promoted longevity.Modern age
Research has shown that many of China's traditional Chinese medicine help drug has effects that premature senescence resistance, promotes longevity.Such as：The fruit of Chinese wolfberry, energy
Reduce blood glucose, cholesterol；The fleece-flower root can reduce cholesterol, prevent artery sclerosis；Cortex Eucommiae can reduce the absorption of cholesterol, centering
Pivot nervous system has adjustment effect；Radix Angelicae Sinensis, can anti-anemia action, can prevent hepatic glycogen from reducing, increase coronary blood flow；Glutinous rehmannia,
Energy Li Shui, blood pressure lowering；Radix Astragali plays the role of anticancer, can improve immune function, antifatigue, expands blood vessel, improves skin blood and follows
Ring reduces blood pressure；Ginseng can promote protein to synthesize, and reduce blood glucose, enhance hematopoiesis function, improve immune function, antifatigue energy
Power inhibits the generation that high courage consolidates mass formed by blood stasis.Help medicinal liquor made of these drugs is selected, frequent appropriate drink-service has anti-aging and prolongs
The effect that year lengthens one's life.
The content of the invention
It is an object of the invention to provide small water turtle wine and preparation method thereof, drink product of the present invention, can effectively improve calcium
Absorptivity.
The present invention is achieved through the following technical solutions:
The preparation method of small water turtle wine, includes the following steps：
1) feedstock processing：Small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat；
2) pre-treatment：Upper step is obtained into crushing material, pure water is added in, is handled with high-speed shearing emulsion machine, Ran Houyong
High pressure microjet Ultra-Micro Grinding Equipment is handled in 25 DEG C, obtains paste serous material；
3) Subcritical Water Extraction：The material that upper step obtains is concentrated into raw material weight, is placed in extraction kettle, adds in carboxylic first
Deionized deoxygenated water is injected in kettle, extracted, 150-160 DEG C of extraction temperature, pressure 5-8MPa by base sodium cellulosate, is extracted
Time 10-15min, extraction terminate, pressure release, and extract liquor is flowed into collecting tank and is cooled to room temperature, and obtains extract liquor；
4) mix, blend：The extract liquor that upper step is obtained, with 53-60 ° of white wine according to 1:The weight ratio of 4-5 is mixed
It closes and obtains small water turtle wine stoste, stand, then the white wine with 30-36 ° after the filtering of small water turtle wine stoste is pressed 1：The weight ratio of 2-4 into
Row mixing is blent, that is, small water turtle wine is made.
Small water turtle described in step 1) of the present invention, preferably Qiezhou stone small water turtle.
Upper step is preferably obtained crushing material, according to 1 by the pre-treatment described in step 2):1 weight ratio adds in pure
Water handles 10-20min, rotating speed 8000-12000r/min, then with high pressure microjet Ultramicro-powder with high-speed shearing emulsion machine
Broken equipment is handled in 25 DEG C, processing pressure 80-120MPa, and number of processes is 2-4 times, obtains paste serous material.
Mixing described in step 4) is blent, the extract liquor for preferably obtaining upper step, with 53-60 ° of rice spirit according to
1:The weight ratio of 4-5 carries out mixing and obtains small water turtle wine stoste, stands 6-12 months, then after small water turtle wine stoste is filtered with
30-36 ° of rice spirit presses 1：The weight ratio of 2-4 carries out mixing and blends, that is, small water turtle wine is made.
The invention further relates to the small water turtle wine obtained using preparation method of the present invention.
Compared to the prior art, the advantage of the invention is that：
1st, the prior art, the processing to small water turtle tortoise plastron directly crush after usually dry or are according to Chinese medicine tortoiseshell
Modern conventional concocting method, the method or the preparation method using vinegar tortoiseshell quenched using sand stir-fry wine, such processing method, and
The effect of small water turtle cannot be played.Inventor is by comparing, the small water turtle wine that method using the present invention obtains, hence it is evident that
Wine is obtained better than being impregnated after conventional immersion or hydrolysis, the product calcium absorptivity that the present invention obtains is higher, and the absorptivity of calcium is two
The wine that the prior art obtains is all remarkably higher than in kind calcium intake level.
2nd, for the present invention when carrying out Subcritical Water Extraction, it is to close that a certain amount of sodium carboxymethylcellulose is added in material
Key, can be to Ca in solution2+Package is formed, prevents it from generating precipitation, blocks extraction equipment pipeline, meanwhile, Ca2+It is abundant, it is beneficial to
The absorption in later stage.
Specific embodiment
With embodiment, the present invention will be described below, but the invention is not limited in these embodiments.
Embodiment 1
The preparation method of small water turtle wine, includes the following steps：
1) feedstock processing：Small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat；
2) pre-treatment：Upper step is obtained into crushing material, according to 1:1 weight ratio adds in pure water, with high speed shear breast
Change machine handles 10min, rotating speed 8000r/min, is then handled with high pressure microjet Ultra-Micro Grinding Equipment in 25 DEG C, handles
Pressure is 80MPa, and number of processes is 2 times, obtains paste serous material；
2) decompose calcareous：The material that upper step is obtained adds in 12mol/L hydrochloric acid, stirs, until no longer precipitation is generated,
Precipitation is obtained by filtration, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The material that upper step obtains is concentrated into raw material weight, is placed in extraction kettle, adds in carboxylic first
Deionized deoxygenated water is injected in kettle, extracted, 150-160 DEG C of extraction temperature, pressure 5-8MPa by base sodium cellulosate, is extracted
Time 10-15min, extraction terminate, pressure release, and extract liquor is flowed into collecting tank and is cooled to room temperature, and obtains extract liquor；
4) mix, blend：The extract liquor that upper step is obtained, with 53-60 ° of rice spirit according to 1:4 weight ratio into
Row mixing obtains small water turtle wine stoste, stands 6 months, then the rice spirit with 30-36 ° after the filtering of small water turtle wine stoste is pressed
1：3 weight ratio carries out mixing and blends, that is, small water turtle wine is made.
Embodiment 2
The preparation method of small water turtle wine, includes the following steps：
1) feedstock processing：Small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat；
2) pre-treatment：Upper step is obtained into crushing material, according to 1:1 weight ratio adds in pure water, with high speed shear breast
Change machine handles 20min, rotating speed 12000r/min, is then handled with high pressure microjet Ultra-Micro Grinding Equipment in 25 DEG C, locates
Reason pressure is 120MPa, and number of processes is 4 times, obtains paste serous material；
3) Subcritical Water Extraction：The material that upper step obtains is concentrated into raw material weight, is placed in extraction kettle, adds in carboxylic first
Deionized deoxygenated water is injected in kettle, extracted, 150-160 DEG C of extraction temperature, pressure 5-8MPa by base sodium cellulosate, is extracted
Time 10-15min, extraction terminate, pressure release, and extract liquor is flowed into collecting tank and is cooled to room temperature, and obtains extract liquor；
4) mix, blend：The extract liquor that upper step is obtained, with 53-60 ° of rice spirit according to 1:5 weight ratio into
Row mixing obtains small water turtle wine stoste, stands 9 months, then the rice spirit with 30-36 ° after the filtering of small water turtle wine stoste is pressed
1：4 weight ratio carries out mixing and blends, that is, small water turtle wine is made.
Embodiment 3
The preparation method of small water turtle wine, includes the following steps：
1) feedstock processing：Qiezhou stone small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat；
2) pre-treatment：Upper step is obtained into crushing material, according to 1:1 weight ratio adds in pure water, with high speed shear breast
Change machine handles 15min, rotating speed 10000r/min, is then handled with high pressure microjet Ultra-Micro Grinding Equipment in 25 DEG C, locates
Reason pressure is 100MPa, and number of processes is 3 times, obtains paste serous material；
3) Subcritical Water Extraction：The material that upper step obtains is concentrated into raw material weight, is placed in extraction kettle, adds in carboxylic first
Deionized deoxygenated water is injected in kettle, extracted, 150-160 DEG C of extraction temperature, pressure 5-8MPa by base sodium cellulosate, is extracted
Time 10-15min, extraction terminate, pressure release, and extract liquor is flowed into collecting tank and is cooled to room temperature, and obtains extract liquor；
4) mix, blend：The extract liquor that upper step is obtained, with 53-60 ° of rice spirit according to 1:4 weight ratio into
Row mixing obtains small water turtle wine stoste, stands 12 months, then rice spirit with 30-36 ° after small water turtle wine stoste is filtered
By 1：2 weight ratio carries out mixing and blends, that is, small water turtle wine is made.
Comparative example 1：
Method, in Subcritical Water Extraction, does not add in sodium carboxymethylcellulose with embodiment 3.
Comparative example 2：
1) feedstock processing：Small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat, is crushed；
2) with 53-60 ° of rice spirit according to 1:4 weight ratio carries out mixing and obtains small water turtle wine stoste, stands 12
Month, then the rice spirit with 30-36 ° after the filtering of small water turtle wine stoste is pressed 1：2 weight ratio carries out mixing and blends, and obtains.
Comparative example 3：
1) feedstock processing：Qiezhou stone small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat；
2) pre-treatment：Upper step is obtained into crushing material, according to 1:1 weight ratio adds in pure water, with high speed shear breast
Change machine handles 15min, rotating speed 10000r/min, is then handled with high pressure microjet Ultra-Micro Grinding Equipment in 25 DEG C, locates
Reason pressure is 100MPa, and number of processes is 3 times, obtains paste serous material；
3) mix, blend：The slurries that upper step is obtained, with 53-60 ° of rice spirit according to 1:4 weight ratio carries out
Mixing obtains small water turtle wine stoste, stands 12 months, then the rice spirit with 30-36 ° after the filtering of small water turtle wine stoste is pressed
1：2 weight ratio carries out mixing and blends, and obtains.
Experimental example：
Calcium uptake is tested
Experimental method：
1st, material：The wine that embodiment 3 and comparative example obtain.
2nd, it is grouped：Everyone 50mL/d of the food ration of wine by adult's 60kg batheroom scales, can be converted as 0.83mL/kgBw, sample
Product are given in a manner of oral gavage.Embodiment 3 presses 5,10 times of the daily recommended amounts of human body, comparative example according to health food design flow
5 times of the daily recommended amounts of human body are pressed according to health food design flow, totally 5 groups.
3rd, after rat adaptability feeds 6d, 5 groups are randomly divided by weight, every group 8, per 4, cage, after feeding 8 weeks, in succession
The metabolism of 3d, claims the food-intake of 3d, excrement weight, and excrement is milled after drying, is surveyed after digestion with atomic absorption spectrophotometer
Calcium content in feed and excrement.
Experiment feed formula, low calcium basal feed formula use semisynthetic feed formula.It is real with bone substance density improving function is increased
Proved recipe method：That is casein：Edible bone powder 20.0%, 16.0%, corn flour 33.3%, analysis for soybean powder 15.0%, sucrose 5.5%, jade
Rice bran oil 4.0%, cellulose 2.0%, DL- METHIONINE 0.2%, choline chloride 0.2%, AIN-93G salt-mixtures 2.6%, AIN-93G
Mixed vitamin 1.0%.
Data processing：With the one-way analysis of variance in SPSS statistical packages, the comparison between each group is carried out, is examined with LSD
It tests, carries out group and comparison among groups.
4th, interpretation of result
Calcium metabolism is tested：
The apparent absorptivity of calcium=(intake calcium-excrement calcium)/intake calcium × 100%
It can be with the high dose group effect of 3 groups of embodiment is best, low dose group, and the apparent absorptivity of calcium is high from upper table
In the comparative example group of matched doses, through statistical test P ＜ 0.05.Simultaneously we according to calcium uptake experimental result judgement mark
Standard if the absorptivity of given the test agent calcium is all remarkably higher than phase same level calcium carbonate in two kinds of calcium intake levels, can be determined that
Given the test agent is " calcium absorptivity is higher ".
Claims (5)
1. the preparation method of small water turtle wine, which is characterized in that include the following steps：
1) feedstock processing：Small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat；
2) pre-treatment：Upper step is obtained into crushing material, pure water is added in, is handled with high-speed shearing emulsion machine, then use high pressure
Microjet Ultra-Micro Grinding Equipment is handled in 25 DEG C, obtains paste serous material；
3) Subcritical Water Extraction：The material that upper step obtains is concentrated into raw material weight, is placed in extraction kettle, it is fine to add in carboxymethyl
The plain sodium of dimension, deionized deoxygenated water is injected in kettle, is extracted, 150-160 DEG C of extraction temperature, pressure 5-8MPa, extraction time
10-15min, extraction terminate, pressure release, and extract liquor is flowed into collecting tank and is cooled to room temperature, and obtains extract liquor；
4) mix, blend：The extract liquor that upper step is obtained, with 53-60 ° of white wine according to 1:The weight ratio of 4-5 carries out mixing and obtains
Small water turtle wine stoste is taken, is stood, then the white wine with 30-36 ° after the filtering of small water turtle wine stoste is pressed 1：The weight ratio of 2-4 is mixed
Conjunction is blent, that is, small water turtle wine is made.
2. the preparation method of small water turtle wine according to claim 1, it is characterised in that：Small water turtle described in step 1) is
Qiezhou stone small water turtle.
3. the preparation method of small water turtle wine according to claim 1, it is characterised in that：Pre-treatment described in step 2) is
Upper step is obtained into crushing material, according to 1:1 weight ratio adds in pure water, and 10-20min is handled with high-speed shearing emulsion machine,
Rotating speed is 8000-12000r/min, is then handled with high pressure microjet Ultra-Micro Grinding Equipment in 25 DEG C, processing pressure is
80-120MPa, number of processes are 2-4 times, obtain paste serous material.
4. the preparation method of small water turtle wine according to claim 1, it is characterised in that：Mixing described in step 4) is blent,
It is the extract liquor for obtaining upper step, with 53-60 ° of rice spirit according to 1:The weight ratio of 4-5 carries out mixing and obtains small water turtle
Wine stoste stands 6-12 months, then the rice spirit with 30-36 ° after the filtering of small water turtle wine stoste is pressed 1：The weight ratio of 2-4
It carries out mixing to blend, that is, small water turtle wine is made.
5. the small water turtle wine that method any one of claim 1-4 obtains.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711440514.9A CN108060047A (en) | 2017-12-27 | 2017-12-27 | Small water turtle wine and preparation method thereof |
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| CN201711440514.9A CN108060047A (en) | 2017-12-27 | 2017-12-27 | Small water turtle wine and preparation method thereof |
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ID=62140268
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1265922A (en) * | 2000-01-27 | 2000-09-13 | 华南理工大学 | Process for preparing calcium carboxymethyl cellulose |
| CN105595334A (en) * | 2015-12-29 | 2016-05-25 | 江南大学 | Maca composite tablet and preparing method thereof |
| CN106190719A (en) * | 2016-07-08 | 2016-12-07 | 柯湘 | A kind of Testudinis wine and preparation method thereof |
-
2017
- 2017-12-27 CN CN201711440514.9A patent/CN108060047A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1265922A (en) * | 2000-01-27 | 2000-09-13 | 华南理工大学 | Process for preparing calcium carboxymethyl cellulose |
| CN105595334A (en) * | 2015-12-29 | 2016-05-25 | 江南大学 | Maca composite tablet and preparing method thereof |
| CN106190719A (en) * | 2016-07-08 | 2016-12-07 | 柯湘 | A kind of Testudinis wine and preparation method thereof |
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Application publication date: 20180522 |