CN107904110A - A kind of small water turtle health liquor and preparation method thereof - Google Patents
A kind of small water turtle health liquor and preparation method thereof Download PDFInfo
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- CN107904110A CN107904110A CN201711440880.4A CN201711440880A CN107904110A CN 107904110 A CN107904110 A CN 107904110A CN 201711440880 A CN201711440880 A CN 201711440880A CN 107904110 A CN107904110 A CN 107904110A
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/12—Materials from mammals; Compositions comprising non-specified tissues or cells; Compositions comprising non-embryonic stem cells; Genetically modified cells
- A61K35/32—Bones; Osteocytes; Osteoblasts; Tendons; Tenocytes; Teeth; Odontoblasts; Cartilage; Chondrocytes; Synovial membrane
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/58—Reptiles
- A61K35/586—Turtles; Tortoises, e.g. terrapins
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/06—Fungi, e.g. yeasts
- A61K36/07—Basidiomycota, e.g. Cryptococcus
- A61K36/076—Poria
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/25—Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
- A61K36/258—Panax (ginseng)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
- A61K36/815—Lycium (desert-thorn)
Abstract
The invention discloses a kind of small water turtle health liquor and preparation method thereof, 1) Feedstock treating；2) hydrolyze；3) Subcritical Water Extraction：The material that upper step obtains is concentrated into raw material weight, it is placed in extraction kettle, adds sodium carboxymethylcellulose, deionized deoxygenated water is injected in kettle, extracted, 150 160 DEG C of extraction temperature, 5 8MPa of pressure, 10 15min of extraction time, extraction terminates, pressure release, extract are flowed into collecting tank and are cooled to room temperature, and obtain extract；4) mix, blend, small water turtle health liquor is made.
Description
Technical field
The present invention relates to health liquor technical field, and in particular to a kind of preparation method of small water turtle health liquor, and use
The pearl wine that this method obtains.
Background technology
It has often been said that " prolonged illness is how empty ".Sick deep chronic disease with the passing of time, often leads to the loss of human body gas, blood, yin, yang,
As soon as and its when forming all non-one days, it, which is treated, recovers also to be difficult to morning and evening to make contributions, and accomplishes in one move, is typically necessary a process.
Traditional Chinese medicine thinks " pathogen usually intruding into collateral in protracted disease ".Various chronic deficient diseases, are usually present that different degrees of qi and blood is not smooth, passages through which vital energy circulates is not smooth,
Treatment needs assistant with medicine promoting blood circulation and removing obstruction in channels to heighten the effect of a treatment often.And the main compatibility of help medicinal liquor has blood-enrich, enriching yin temperature
The tonic food of sun, therefore it is relatively beneficial to the treatment of chronic disease.Personal qi and blood, is valued for logical tune.Though if obtaining help, and it cannot flow
It is logical, then the profit of help is can not receive, the evil of anti-raw stasis.
Alcoholic strength temperature, acrid flavour and bitter sweet have a warm promoting blood circulation, the surname dissipate efficacy of a drug, warm stomach, and dispersing wind and cold of dispelling rouses oneself yang-energy, eliminates
Fatigue etc. acts on.Responsible drinking, can be added to the fun with happy feelings, but cross drink then unrest, and excessive drinking then consumes vigour, even loses one's life.Doctor
Why hobby wine, be to take its benefaction medicine gesture up in the property of internal organs, four limbs bones of the body collectively, therefore have saying for " length that wine is hundred medicines "
Method.By the Chinese medicine to keep fit and healthy and wine " molten " in the medicinal liquor of one, not only preparation is convenient, pharmacological property is stable, safely and effectively, Er Qieyin
It is a kind of good semi-polarity organic solvent for alcohol, the various active ingredients of Chinese medicine are all soluble in wherein, and wine assisting drug, wine help
Medicine gesture and give full play to its effect, improve curative effect.In fact, wine is a kind of best solvent, many to be difficult to other processing methods
The medicine that its active ingredient is separated out, can be extracted by means of this characteristic of wine mostly, and can give full play to its prevention
Disease, the drug effect promoted longevity, here it is medicinal liquor after where cause of many decades without subtracting its glamour.
Help medicinal liquor is not only widely used in the prevention of various chronic deficient diseases, moreover it is possible to which anti-aging, promote longevity.Modern age
Research has shown that many of China's traditional Chinese medicine help medicine has effects that premature senescence resistance, promotes longevity.Such as：The fruit of Chinese wolfberry, energy
Reduce blood glucose, cholesterol；The fleece-flower root, can reduce cholesterol, prevent artery sclerosis；The bark of eucommia, can reduce the absorption of cholesterol, centering
Pivot nervous system has adjustment effect；Angelica sinensis, can anti-anemia action, can prevent hepatic glycogen from reducing, increase coronary blood flow；Glutinous rehmannia,
Energy Li Shui, blood pressure lowering；Radix astragali, there is anticancer, can improve immune function, antifatigue, expands blood vessel, improves skin blood and follows
Ring, reduces blood pressure；Ginseng, can promote protein to synthesize, and reduce blood glucose, strengthen hematopoiesis function, improve immune function, antifatigue energy
Power, suppresses the generation that high courage consolidates mass formed by blood stasis.Help medicinal liquor made of these medicines is selected, frequent appropriate drink-service, has anti-aging and prolong
The effect that year lengthens one's life.
Small water turtle (scientific name：Cyclemys trifasciata), one kind of Testudinidae, is called Cuora trifasciata, disconnected plate tortoise, red
Tripe tortoise, golden head tortoise etc., belong to rare tortoise kind, belong to Reptilia Chelonia Testudinidae, are that one kind views and admires tortoise.Meat flavour is delicious, has very high
Edible and medicinal value, be the terrapin that development prospect is had an optimistic view of.Like the cloudy place covered of selection to inhabit, there is gregarious habit,
Annual winter wants hibernation.Wild small water turtle is extremely rare, in great demand on international, domestic market.Because having feeding habits wide, disease-resistant
The features such as power and Hunger tolerance are strong, viability is strong, artificial feeding is convenient, has considerable economic value.In addition, small water turtle also has pole
High medical value, is traditional Chinese medicine, is one of the exporting of Chinese tradition.Move in water, mainly using earthworm as
Food, also eats fish, shrimp, insect and some plant foods in river in addition.World's distribution of small water turtle is very narrow, main
It is distributed in subtropical countries and the areas such as Chinese Guangdong, Guangxi, Fujian, Hainan, Hong Kong, Macao and north and south portion of Vietnam.
China national two level lays special stress on protecting animal；Hong-Kong fishman administration was classified as protection animal varieties in 2004；Arranged
Enter《Endangered species of wild fauna and flora international trade pact》Two classes protect species；World Conservation Union's pole danger species.Artificial breeding
The mode of small water turtle has two kinds, and one kind is to imitate wild cultivation, exactly copies ingest feature and the growth and development rule of wild small water turtle
Rule cultivation small water turtle, the small water turtle that this mode cultivates can keep that wild small water turtle disease resistance is strong, long lifespan, laying period length
The advantages of, it is the first choice that kind is made in artificial breeding.Another kind is commercialization cultivation, by heating cultivation or cold water culture but to gold
Money tortoise largely feeds food, allows small water turtle fast-growth fast-ripenin, and the small water turtle disease resistance that this mode cultivates is low, the service life
Short, laying period is short not to lay eggs even, is generally used for edible and medicinal.
Modern times using edible small water turtle as disease preventing and treating, improve constitution, antifatigue diet trend.In China, three lines close
Shell small water turtle is favored be subject to south China and Hong Kong, Macao, Taiwan area and Southeast Asia and Overseas Chinese, except because there is higher nourishing
Outside nutrition, labor illness hectic fever due to yin, chronic cough spitting of blood, bloody flux, hemorrhoid blood, arthralgia and myalgia etc. can be controlled.Small water turtle is particularly suitable for tumor patients,
Postoperative rehabilitation person；Hepatopathy, nephrotic, weak, frequent flu, insomniac；The rheumatic bones such as woman puerperal fever headache, scapulohumeral periarthritis
Bitterly, tatanic spondylitis of lumbar vertebra patient；Chronic gastritis, chronic pharyngitis, chronic stomatocace, rhinitis chronic patient and overstrain one's nerves etc.
Sub-health population, to adjust function of human body, improves the immunity of the human body and anti-fatigue ability.The clinical application of binding of pathological, gold
Money tortoise has the special efficacy for keeping human body yin-yang balancing.The content of small water turtle active factors is higher, active factors and various members
Element, which combines, forms one strong fresh combatants, can cure cell and lose extremely, decrease of platelet, and suppresses growth of cancer cells, reaches
Cancer-resisting, the effect for eliminating tumour.Promote blood circulation of human body, while also promote human body cell growth.
The content of the invention
It is an object of the invention to provide a kind of small water turtle health liquor and preparation method thereof, product of the present invention is drunk, can be had
Effect improves calcium absorptivity.
The present invention is achieved through the following technical solutions:
A kind of preparation method of small water turtle health liquor, includes the following steps：
1) Feedstock treating：Small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat；
2) hydrolyze：In the material that upward step obtains, pure water is added, mixture ph is adjusted, pressure is maintained after boiling
Hydrolysis, boils the moisture for maintaining to notice that supplement loses in press process, is adjusted after the completion of hydrolysis and increases pH；
3) Subcritical Water Extraction：The material that upper step obtains is concentrated into raw material weight, is placed in extraction kettle, adds carboxylic first
Base sodium cellulosate, deionized deoxygenated water is injected in kettle, is extracted, 150-160 DEG C of extraction temperature, pressure 5-8MPa, is extracted
Time 10-15min, extraction terminate, pressure release, and extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) mix, blend：The extract that upper step is obtained, with 53-60 ° of medicinal liquor according to 1:The weight ratio of 4-5 is mixed
Close and obtain small water turtle health liquor stoste, stand, then the white wine after the filtering of small water turtle health liquor stoste with 30-36 ° is pressed 1：2-4's
Weight ratio carries out mixing and blends, that is, small water turtle health liquor is made.
Small water turtle described in step 1) of the present invention, preferably Qiezhou stone small water turtle.
Hydrolysis described in step 2), in the material that preferably upward step obtains, adds the pure water of 8-10 times of weight, adjusts
Mixture pH to 1.8-2.5, maintains pressure 0.1Mpa hydrolysis 8-10h after boiling, boil and maintain to notice that supplement is lost in press process
The moisture gone, adjusts after the completion of hydrolysis and increases pH to 6.0-6.5.
Mixing described in step 4), blend, the extract for preferably obtaining upper step, with 53-60 ° of medicinal liquor according to 1:4-5
Weight ratio carry out mixing and obtain small water turtle health liquor stoste, stand 6-12 months, then after small water turtle health liquor stoste is filtered
Rice spirit with 30-36 ° presses 1：The weight ratio of 2-4 carries out mixing and blends, that is, small water turtle health liquor is made.
Medicinal liquor described in step 4), is after the raw materials such as pilose antler, ginseng, matrimony vine, Poria cocos are mixed with arbitrary proportion, adds 8-
Soak 6-12 months, obtain, to improve the mouthfeel of small water turtle health liquor in 53-60 ° of rice spirit of 10 times of weight.
Another single tortoise effect of steeping in wine is bad
The invention further relates to the small water turtle health liquor obtained using preparation method of the present invention.
Compared to the prior art, the advantage of the invention is that：
1st, the prior art, the processing to small water turtle tortoise plastron directly crush after usually dry or are according to Chinese medicine tortoiseshell
Modern conventional concocting method, the method quenched using sand stir-fry wine, or the preparation method using vinegar tortoiseshell, such processing method, and
The effect of small water turtle cannot be played.Inventor is by comparing, the small water turtle health liquor that method using the present invention obtains,
Immersion obtains wine after being substantially better than conventional immersion or hydrolysis, and the product calcium absorptivity that the present invention obtains is higher, the absorptivity of calcium
The wine that the prior art obtains is all remarkably higher than in two kinds of calcium intake levels.
2nd, for the present invention when carrying out Subcritical Water Extraction, it is to close that a certain amount of sodium carboxymethylcellulose is added in material
Key, can be to Ca in solution2+Parcel is formed, prevents it from producing precipitation, blocks extraction equipment pipeline, meanwhile, Ca2+It is abundant, it is beneficial to
The absorption in later stage.
Embodiment
With embodiment, the present invention will be described below, but the invention is not limited in these embodiments.
Embodiment 1
A kind of preparation method of small water turtle health liquor, includes the following steps：
1) Feedstock treating：Small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat；
2) hydrolyze：In the material that upward step obtains, the pure water of 8 times of weight is added, mixture pH to 1.8 is adjusted, boils
Pressure 0.1Mpa hydrolysis 8h are maintained after boiling, boil the moisture for maintaining to notice that supplement loses in press process, adjusts and increases after the completion of hydrolysis
PH to 6.0-6.5；
3) Subcritical Water Extraction：The material that upper step obtains is concentrated into raw material weight, is placed in extraction kettle, adds carboxylic first
Base sodium cellulosate, deionized deoxygenated water is injected in kettle, is extracted, 150-160 DEG C of extraction temperature, pressure 5-8MPa, is extracted
Time 10-15min, extraction terminate, pressure release, and extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) mix, blend：The extract that upper step is obtained, (medicinal liquor, is by pilose antler, ginseng, Chinese holly with 53-60 ° of medicinal liquor
The raw materials such as Qi, Poria cocos are with 1:1:2:After the mixing of 2 part by weight, add and 12 are soaked in 53-60 ° of rice spirit of 8 times of weight
Month, obtain) according to 1:4 weight ratio carries out mixing and obtains small water turtle health liquor stoste, stands 6 months, then by small water turtle health care
Rice spirit after the filtering of wine stoste with 30-36 ° presses 1：3 weight ratio carries out mixing and blends, that is, small water turtle health liquor is made.
Embodiment 2
A kind of preparation method of small water turtle health liquor, includes the following steps：
1) Feedstock treating：Small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat；
2) hydrolyze：In the material that upward step obtains, the pure water of 10 times of weight is added, mixture pH to 2.5 is adjusted, boils
Pressure 0.1Mpa hydrolysis 10h are maintained after boiling, boil the moisture for maintaining to notice that supplement loses in press process, adjusts and increases after the completion of hydrolysis
PH to 6.0-6.5；
3) Subcritical Water Extraction：The material that upper step obtains is concentrated into raw material weight, is placed in extraction kettle, adds carboxylic first
Base sodium cellulosate, deionized deoxygenated water is injected in kettle, is extracted, 150-160 DEG C of extraction temperature, pressure 5-8MPa, is extracted
Time 10-15min, extraction terminate, pressure release, and extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) mix, blend：The extract that upper step is obtained, (medicinal liquor, is by pilose antler, ginseng, Chinese holly with 53-60 ° of medicinal liquor
The raw materials such as Qi, Poria cocos are with 1:1:2:After the mixing of 2 part by weight, add and 12 are soaked in 53-60 ° of rice spirit of 8 times of weight
Month, obtain) according to 1:5 weight ratio carries out mixing and obtains small water turtle health liquor stoste, stands 9 months, then by small water turtle health care
Rice spirit after the filtering of wine stoste with 30-36 ° presses 1：4 weight ratio carries out mixing and blends, that is, small water turtle health liquor is made.
Embodiment 3
A kind of preparation method of small water turtle health liquor, includes the following steps：
1) Feedstock treating：Qiezhou stone small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat；
2) hydrolyze：In the material that upward step obtains, the pure water of 8 times of weight is added, mixture pH to 2.0 is adjusted, boils
Pressure 0.1Mpa hydrolysis 8h are maintained after boiling, boil the moisture for maintaining to notice that supplement loses in press process, adjusts and increases after the completion of hydrolysis
PH to 6.0-6.5；
3) Subcritical Water Extraction：The material that upper step obtains is concentrated into raw material weight, is placed in extraction kettle, adds carboxylic first
Base sodium cellulosate, deionized deoxygenated water is injected in kettle, is extracted, 150-160 DEG C of extraction temperature, pressure 5-8MPa, is extracted
Time 10-15min, extraction terminate, pressure release, and extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) mix, blend：The extract that upper step is obtained, (medicinal liquor, is by pilose antler, ginseng, Chinese holly with 53-60 ° of medicinal liquor
The raw materials such as Qi, Poria cocos are with 1:1:2:After the mixing of 2 part by weight, add and 12 are soaked in 53-60 ° of rice spirit of 8 times of weight
Month, obtain) according to 1:4 weight ratio carries out mixing and obtains small water turtle health liquor stoste, stands 12 months, then by small water turtle health care
Rice spirit after the filtering of wine stoste with 30-36 ° presses 1：2 weight ratio carries out mixing and blends, that is, small water turtle health liquor is made.
Comparative example 1：
Method, in Subcritical Water Extraction, does not add sodium carboxymethylcellulose with embodiment 3.
Comparative example 2：
1) Feedstock treating：Small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat, is crushed；
2) (medicinal liquor, is with 1 by raw materials such as pilose antler, ginseng, matrimony vine, Poria cocos with 53-60 ° of medicinal liquor:1:2:2 part by weight mix
After conjunction, add in 53-60 ° of rice spirit of 8 times of weight and soak 12 months, obtain) according to 1:4 weight ratio carries out mixing and obtains
Take small water turtle health liquor stoste, stand 12 months, then the rice spirit after small water turtle health liquor stoste is filtered with 30-36 °
By 1：2 weight ratio carries out mixing and blends, and obtains.
Comparative example 3：
1) Feedstock treating：Qiezhou stone small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat；
2) hydrolyze：In the material that upward step obtains, the pure water of 8 times of weight is added, mixture pH to 2.0 is adjusted, boils
Pressure 0.1Mpa hydrolysis 8h are maintained after boiling, boil the moisture for maintaining to notice that supplement loses in press process, adjusts and increases after the completion of hydrolysis
PH to 6.0-6.5；
3) mix, blend：The hydrolyzate that upper step is obtained, (medicinal liquor, is by pilose antler, ginseng, Chinese holly with 53-60 ° of medicinal liquor
The raw materials such as Qi, Poria cocos are with 1:1:2:After the mixing of 2 part by weight, add and 12 are soaked in 53-60 ° of rice spirit of 8 times of weight
Month, obtain) according to 1:4 weight ratio carries out mixing and obtains small water turtle health liquor stoste, stands 12 months, then by small water turtle health care
Rice spirit after the filtering of wine stoste with 30-36 ° presses 1：2 weight ratio carries out mixing and blends, and obtains.
Experimental example：
Calcium uptake is tested
Experimental method：
1st, material：The wine that embodiment 3 and comparative example obtain.
2nd, it is grouped：Everyone 50mL/d of the food ration of wine, by adult's 60kg batheroom scales, can convert as 0.83mL/kgBw, sample
Product are given in a manner of oral gavage.Embodiment 3 presses 5,10 times of the daily recommended amounts of human body, comparative example according to health food design flow
5 times of the daily recommended amounts of human body are pressed according to health food design flow, totally 5 groups.
3rd, after rat adaptability feeds 6d, 5 groups are randomly divided into by weight, every group 8, per 4, cage, after feeding 8 weeks, in succession
The metabolism of 3d, claims the food-intake of 3d, excrement weight, and excrement is milled after drying, is surveyed after digestion with atomic absorption spectrophotometer
Calcium content in feed and excrement.
Experiment feed formula, low calcium basal feed formula use semisynthetic feed formula.It is real with increase bone substance density improving function
Proved recipe method：That is casein：Edible bone powder 20.0%, 16.0%, corn flour 33.3%, analysis for soybean powder 15.0%, sucrose 5.5%, jade
Rice bran oil 4.0%, cellulose 2.0%, DL- METHIONINE 0.2%, choline chloride 0.2%, AIN-93G salt-mixtures 2.6%, AIN-93G
Mixed vitamin 1.0%.
Data processing：With the one-way analysis of variance in SPSS statistical packages, the comparison between each group is carried out, is examined with LSD
Test, carry out group and comparison among groups.
4th, interpretation of result
Calcium metabolism is tested：
The apparent absorptivity of calcium=(intake calcium-excrement calcium)/intake calcium × 100%
Can be with the high dose group effect of 3 groups of embodiment is best, its low dose group, and the apparent absorptivity of calcium is high from upper table
In the comparative example group of matched doses, through statistical test P ＜ 0.05.At the same time we according to calcium uptake experimental result judgement mark
Standard, if the absorptivity of given the test agent calcium is all remarkably higher than phase same level calcium carbonate in two kinds of calcium intake levels, can be determined that
Given the test agent is " calcium absorptivity is higher ".
Claims (6)
1. a kind of preparation method of small water turtle health liquor, it is characterised in that include the following steps：
1) Feedstock treating：Small water turtle is taken, after gutting, is cleaned up, retains turtle shell, tortoise meat；
2) hydrolyze：In the material that upward step obtains, pure water is added, adjusts mixture ph, pressure hydrolysis is maintained after boiling,
The moisture for maintaining to notice that supplement loses in press process is boiled, is adjusted after the completion of hydrolysis and increases pH；
3) Subcritical Water Extraction：The material that upper step obtains is concentrated into raw material weight, is placed in extraction kettle, it is fine to add carboxymethyl
The plain sodium of dimension, deionized deoxygenated water is injected in kettle, is extracted, 150-160 DEG C of extraction temperature, pressure 5-8MPa, extraction time
10-15min, extraction terminate, pressure release, and extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) mix, blend：The extract that upper step is obtained, with 53-60 ° of medicinal liquor according to 1:The weight ratio of 4-5 carries out mixing and obtains
Small water turtle health liquor stoste is taken, is stood, then the white wine after the filtering of small water turtle health liquor stoste with 30-36 ° is pressed 1：The weight of 2-4
Blent than carrying out mixing, that is, small water turtle health liquor is made.
A kind of 2. preparation method of small water turtle health liquor according to claim 1, it is characterised in that：Gold described in step 1)
Money tortoise, is Qiezhou stone small water turtle.
A kind of 3. preparation method of small water turtle health liquor according to claim 1, it is characterised in that：Water described in step 2)
Solution, is the pure water that 8-10 times of weight is added in the material that upward step obtains, mixture pH to 1.8-2.5 is adjusted, after boiling
Pressure 0.1Mpa hydrolysis 8-10h are maintained, boil the moisture for maintaining to notice that supplement loses in press process, is adjusted after the completion of hydrolysis and increases pH
To 6.0-6.5.
A kind of 4. preparation method of small water turtle health liquor according to claim 1, it is characterised in that：It is mixed described in step 4)
Close, blend, be the extract for obtaining upper step, with 53-60 ° of medicinal liquor according to 1:The weight ratio of 4-5 carries out mixing and obtains money
Tortoise health liquor stoste, stands 6-12 months, then the rice spirit after the filtering of small water turtle health liquor stoste with 30-36 ° is pressed 1：
The weight ratio of 2-4 carries out mixing and blends, that is, small water turtle health liquor is made.
A kind of 5. preparation method of small water turtle health liquor according to claim 1, it is characterised in that：Medicine described in step 4)
Wine, is after being mixed pilose antler, ginseng, matrimony vine, Poria cocos with arbitrary proportion, added in 53-60 ° of rice spirit of 8-10 times of weight
Immersion obtains for 6-12 months.
6. the small water turtle health liquor that method any one of claim 1-5 obtains.
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| 赵健等: "亚临界水萃取技术及其在肉品检测中的应用", 《肉类研究》 * |
| 赵健等: "亚临界水萃取技术及其在食品方面的应用", 《食品工业科技》 * |
| 高盈娴等: "龟板水提物缓释微球的制备及其特性", 《药学进展》 * |
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