CN108056962A - A kind of Brazil's perfume cocoa berry extract and its application in suncream is prepared - Google Patents
A kind of Brazil's perfume cocoa berry extract and its application in suncream is prepared Download PDFInfo
- Publication number
- CN108056962A CN108056962A CN201810029258.2A CN201810029258A CN108056962A CN 108056962 A CN108056962 A CN 108056962A CN 201810029258 A CN201810029258 A CN 201810029258A CN 108056962 A CN108056962 A CN 108056962A
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- China
- Prior art keywords
- berry extract
- brazil
- fragrant
- suncream
- cocoa
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
Abstract
The invention discloses a kind of fragrant cocoa berry extract of Brazil and its preparing the application of suncream.The fragrant cocoa berry extract of Brazil employs mixed type Extraction solvent, and ethyl alcohol, the mass percent of isopropyl alcohol and water are in solvent（20‑30）：（5‑10）：（60‑80）.Compared with prior art, the beneficial effects of the present invention are, Brazil perfume cocoa berry extract has excellent sun-proof result in cosmetics, by using specific mixed type solvent, it and is compounded by specified weight ratio so that the fragrant cocoa berry extract of Brazil extracted has apparent synergistic effect on sun-proof function.
Description
Technical field
The present invention relates to daily cosmetics fields, are specifically related to a kind of fragrant cocoa berry extract of Brazil and its prevent preparing
Shine the application in frost.
Background technology
Skin is the important component of human body, is even more the mark for directly expressing health and aging.Work as skin metabolism
Vigorous, blood circulation is unimpeded, and when full of nutrition, then skin is fine and smooth, smooth, tender, is rich in elasticity, and is less prone to wrinkle and color
Spot.When skin metabolism weakens, poor blood circulation, when nutriment is bad, then skin can become gloomy, aging, and be also easy to produce
Wrinkle and color spot.
Sun-proof research is cosmeceutical, the hot spot of dermatology.Effect of the sun-screening agent in cosmetics is pre- antiultraviolet
To the hurtful important measures of human body.The ultraviolet screener substance applied at present is divided into two classes：Physical barrier agent and chemistry
Absorbent.Chemical absorbent is also known as ultra-violet absorber, is divided into chemical synthesis and natural two kinds of extraction.Chemical synthesis it is ultraviolet
Light absorbers such as cinnamic acid, cinnamate, salicylate, benzophenone derivates etc.；The ultra-violet absorber of natural extract refers to
The natural ultraviolet absorber compounds extracted from plant, such as：Flavone compound, anthraquinone analog compound, plant are more
Phenolic compound and its derivative etc..Due to the ultra-violet absorber of chemical synthesis, there are one in the application of the industries such as cosmetics
Fixed toxic side effect, thus naturally, the research of nontoxic ultra-violet absorber application increasingly get more and more people's extensive concerning.
The fragrant cocoa of Guarana also known as Brazil, botanical term are called Paullinia cupana, are that Sapindaceae rattan shape fills
Wood abounds in Brazilian northern Amazon River basin, is that Brazil is most well-known, and the medicinal plant of rainforest for having history to record very early
Object.Guarana was introduced into China before 10 years, was originally mainly used in the field of health care products such as heart and brain of refreshing oneself, and slowly started to be situated between later
Enter cosmetic industry, nowadays Guarana has become the toiletries of development space maximum.The emergence of Guarana is not accidental, and
It is the needs for having catered to social crowd instantly, with the high speed development of Chinese society, inferior health, physical efficiency loss, the crowd to stay up late
It is more and more, and Guarana cosmetics are exactly a kind of function cosmetics that can supplement skin energy, are hungered and thirst to skin, spot,
Wrinkle can play good reparation effect.
At present, although the plant extracts for the sun-proof aspect enriched in the market there are species, Brazil's perfume cocoa
（PAULLINIA CUPANA）Berry extract, which exists in, have been used in cosmetic material Names Catalogue, but has no related Brazil
Report of the fragrant cocoa berry extract as sunscreen actives.
The content of the invention
In view of the deficienciess of the prior art, the object of the present invention is to provide a kind of fragrant cocoa berry extract of Brazil and its
Prepare the application in suncream.The present invention is realized particular by following technical scheme：
A kind of fragrant cocoa berry extract of Brazil, Extraction solvent is ethyl alcohol, the mixture of isopropyl alcohol and water.
Preferably, ethyl alcohol, the mass ratio of isopropyl alcohol and water are in the Extraction solvent（20-30）：（5-10）：（60-80）.
Preferably, ethyl alcohol, the mass ratio of isopropyl alcohol and water are 30 in the Extraction solvent：10：60.
Preferably, the dosage of the Extraction solvent is the 5-10 times of weight of the fragrant cocoa of Brazil.
Preferably, the preparation method of the fragrant cocoa berry extract of described Brazil is：After Brazilian fragrant cocoa is crushed, 5- is added in
The Extraction solvent of 10 times of weight, impregnate 12-24h, then heating and refluxing extraction 2-3 time, each reflux extracting time be 1-2h, mistake
Filter, dry after the recovered solvent of merging filtrate to get.
The present invention also provides application of the fragrant cocoa berry extract of above-mentioned Brazil in suncream is prepared.
Preferably, weight percent of the fragrant cocoa berry extract of described Brazil in suncream is 1-5%.
Preferably, a kind of suncream is made of the raw material of following weight percent：
Brazilian perfume cocoa berry extract：1-5%
Polysorbate 60：1.5%-3%
Rilanit special：2%-5%
Atoleine：5%-8%
Saualane：1%-2%
Glycerine：3%-5%
1,4- butanediols：1%-2%
Triethanolamine：0.2%-0.3%
Phenoxyethanol：0.01%-0.03%
Essence：0.01%-0.05%
Deionized water：Surplus.
It is highly preferred that a kind of suncream, is made of the raw material of following weight percent：
Brazilian perfume cocoa berry extract：3%
Polysorbate 60：2%
Rilanit special：4%
Atoleine：7%
Saualane：1%
Glycerine：5%
1,4- butanediols：1%
Triethanolamine：0.3%
Phenoxyethanol：0.03%
Essence：0.01%
Deionized water：Surplus.
The preparation method of above-mentioned suncream, comprises the following steps that：
（1）Raw material is divided into following three groups：
Group one：Polysorbate 60, rilanit special, atoleine, saualane；
Group two：Glycerine, 1,4- butanediols, triethanolamine, deionized water；
Group three：Brazilian perfume cocoa berry extract, Phenoxyethanol, essence；
（2）Oil phase pot will be added in after group one all components mixing, and be warming up to 80-90 DEG C, stir evenly, 30 minutes duration；
（3）Water phase pot will be added in after group two all components mixing, and be warming up to 80-90 DEG C, stir evenly, 30 minutes duration；
（4）By step（1）、（2）Liquid be mutually mixed carry out emulsifying, 30 minutes duration, by mixed liquor after emulsification
It is cooled to 45-55 DEG C, three all components of addition group stir evenly, and 30 minutes duration, are finally cooled to room temperature to obtain the final product.
Compared with prior art, the advantageous effect of cosmetics of the present invention is：The fragrant cocoa berry extract of Brazil of the present invention is
The mixed solvent compounded by special ratios extracts to obtain, and ethyl alcohol, the mass ratio of isopropyl alcohol and water are in the Extraction solvent
（20-30）：（5-10）：（60-80）, Brazil perfume cocoa berry extract is in cosmetics with excellent sun-proof result.
Specific embodiment
The present invention is described in further detail with reference to embodiment.
Embodiment 1：
A kind of fragrant cocoa berry extract of Brazil, Extraction solvent is ethyl alcohol, the mixture of isopropyl alcohol and water, second in the Extraction solvent
Alcohol, the mass ratio of isopropyl alcohol and water are 30：10：60, extracting method is：After Brazilian fragrant cocoa is crushed, 8 times of weight of addition
Extraction solvent impregnates for 24 hours, then heating and refluxing extraction 3 times, and each reflux extracting time is 2h, is filtered, and merging filtrate is recovered
After solvent dry to get.
Embodiment 2：
A kind of fragrant cocoa berry extract of Brazil, Extraction solvent is ethyl alcohol, the mixture of isopropyl alcohol and water, second in the Extraction solvent
Alcohol, the mass ratio of isopropyl alcohol and water are 20：10：80, extracting method is：After Brazilian fragrant cocoa is crushed, 5 times of weight of addition
Extraction solvent impregnates 12h, then heating and refluxing extraction 2 times, and each reflux extracting time is 1h, is filtered, merging filtrate is recovered
After solvent dry to get.
Embodiment 3：
A kind of fragrant cocoa berry extract of Brazil, Extraction solvent is ethyl alcohol, the mixture of isopropyl alcohol and water, second in the Extraction solvent
Alcohol, the mass ratio of isopropyl alcohol and water are 30：5：70, extracting method is：After Brazilian fragrant cocoa is crushed, 10 times of weight of addition
Extraction solvent impregnates 18h, then heating and refluxing extraction 3 times, and each reflux extracting time is 2h, is filtered, merging filtrate is recovered
After solvent dry to get.
Comparative example 1：
A kind of fragrant cocoa berry extract of Brazil, Extraction solvent are the mixture of second alcohol and water, second alcohol and water in the Extraction solvent
Mass ratio be 40：60, extracting method is：After Brazilian fragrant cocoa is crushed, the Extraction solvent of 8 times of weight is added in, is impregnated
For 24 hours, then heating and refluxing extraction 3 times, each reflux extracting time are 2h, are filtered, dry after the recovered solvent of merging filtrate, i.e.,
.
Comparative example 2：
A kind of fragrant cocoa berry extract of Brazil, Extraction solvent are the mixture of isopropyl alcohol and water, isopropanol in the Extraction solvent
Mass ratio with water is 40：60, extracting method is：After Brazilian fragrant cocoa is crushed, the Extraction solvent of 8 times of weight, leaching are added in
For 24 hours, then heating and refluxing extraction 3 times, each reflux extracting time is 2h to bubble, is filtered, dry after the recovered solvent of merging filtrate,
To obtain the final product.
Embodiment 4-8：
Raw material weight percentage dosage by being specified in following table 1 prepares suncream, and it is different to respectively obtain sunscreen actives
Suncream.Preparation method is identical, specifically includes following processing step：
（1）Raw material is divided into following three groups：
Group one：Polysorbate 60, rilanit special, atoleine, saualane；
Group two：Glycerine, 1,4- butanediols, triethanolamine, deionized water；
Group three：Brazilian perfume cocoa berry extract, Phenoxyethanol, essence；
（2）Oil phase pot will be added in after group one all components mixing, and be warming up to 85 DEG C, stir evenly, 30 minutes duration；
（3）Water phase pot will be added in after group two all components mixing, and be warming up to 85 DEG C, stir evenly, 30 minutes duration；
（4）By step（1）、（2）Liquid be mutually mixed carry out emulsifying, 30 minutes duration, by mixed liquor after emulsification
It is cooled to 50 DEG C, three all components of addition group stir evenly, and 30 minutes duration, are finally cooled to room temperature to obtain the final product.
Table 1
First, sun-proof result evaluation is carried out using ultraviolet spectrophotometry, sample to be tested is suncream made from embodiment 4-8.
Specific method is as follows：
（1）3M medical air-permeable adhesive tapes are cut into 1cm × 4cm sizes, are pasted onto quartz colorimetric utensil light transmission side surface.
（2）Power on, preheat ultraviolet specrophotometer, set UVB areas Detection wavelength as 285nm, 290nm, 295nm,
300nm, 305nm, 310nm, 315nm and 320nm.
（3）The quartz colorimetric utensil for posting adhesive tape is placed in sample arm and reference light paths, adjusts instrument zero.
（4）Sample to be tested 8mg accurately is weighed, sample is uniformly applied on quartz colorimetric utensil 3M adhesive tapes.Same method system
Standby five parallel samples.
（5）The article colorimetric ware prepared is placed in 35 DEG C of drying boxes, it is 30 minutes dry.
（6）Sample to be tested cuvette is placed in sample arm, another quartz colorimetric utensil for posting adhesive tape is taken to be placed in reference
In light path, the ultraviolet light absorption angle value of UVB areas setting wavelength is measured respectively, then takes the arithmetic average of each measured value.
（7）Five parallel samples of sequentially determining, as above method draws the average of five samples, then calculates five sample averages
Arithmetic average is the absorbance of the test sample.
Evaluation criterion：Absorbance<1.0 ± 0.1, represent the sample without sun-proof result；Absorbance=1.0 ± 0.1, table
Sample product have rudimentary sun-proof result, suitable for winter, morning and evening in spring and autumn and rainy days；Absorbance>1.0, and<2.0 ± 0.2, table
Show that the sample has intermediate sun-proof result, suitable for moderate strength sunlight；Absorbance>2.0, it is advanced anti-to represent that the sample has
Effect is shone, suitable for summer illumination or outdoor activities, tourism etc..As it can be seen that absorbance is bigger, it is better to the protection effect of UVB.
Test result is shown in Table 2.
2 absorbance measurement result of table
2nd, with reference to the Ministry of Public Health《Cosmetics health specification》" sun care preparations SPF (spf value) measure side in (version in 2007)
The relevant regulations of method " carry out sun-proof result evaluation to suncream made from embodiment 4-8, and concrete outcome is shown in Table 3.
3 spf value measurement result of table
Sun protection factor SPF（Sun Protection Factor）It is to measure defence capability of the sunscreen products to sunlight middle-ultraviolet lamp UVB
Detection index, show the height of the sun-proof efficiency that sun-proof articles can play.It is according to the minimum Erythema Dose of skin come
Definite.Rudimentary sunscreen products SPF is SPF2 ~ 6, and middle rank is SPF6 ~ 8, and high sunscreen products are then SPF8 ~ 12, and spf value exists
Product in the range of 12 ~ 30 then belongs to the high-strength or strong sunscreen products of superelevation.
As it can be seen that the fragrant cocoa berry extract of Brazil of the present invention employs specific mixed type solvent, and by specified weight ratio
It is compounded, plays apparent synergistic effect for the sun-proof function of Brazilian fragrant cocoa berry extract, achieve this field skill
The unexpected technique effect of art personnel.
Above-described embodiment is only currently preferred case study on implementation, it is impossible to limit present invention model claimed with this
Enclose, done on the basis of the present invention any unsubstantiality of those skilled in the art and replacing belong to the present invention claims
The scope of protection.
Claims (10)
1. a kind of fragrant cocoa berry extract of Brazil, which is characterized in that Extraction solvent is ethyl alcohol, the mixture of isopropyl alcohol and water.
A kind of 2. fragrant cocoa berry extract of Brazil according to claim 1, which is characterized in that second in the Extraction solvent
Alcohol, the mass ratio of isopropyl alcohol and water are（20-30）：（5-10）：（60-80）.
A kind of 3. fragrant cocoa berry extract of Brazil according to claim 2, which is characterized in that second in the Extraction solvent
Alcohol, the mass ratio of isopropyl alcohol and water are 30：10：60.
A kind of 4. fragrant cocoa berry extract of Brazil according to claim 1-3, which is characterized in that the use of the Extraction solvent
It measures as the 5-10 times of weight of Brazilian fragrant cocoa.
5. the fragrant cocoa berry extract of a kind of Brazil according to claim 4, which is characterized in that the fragrant cocoa of Brazil carries
The preparation method for taking object is：After Brazilian fragrant cocoa is crushed, the Extraction solvent of 5-10 times of weight is added in, impregnates 12-24h, so
Heating and refluxing extraction 2-3 times afterwards, each reflux extracting time are 1-2h, are filtered, dry after the recovered solvent of merging filtrate, i.e.,
.
6. a kind of application of the fragrant cocoa berry extract of Brazil according to claim 1 in suncream is prepared.
7. a kind of application of the fragrant cocoa berry extract of Brazil according to claim 6 in suncream is prepared, feature exist
In the weight percent of the fragrant cocoa berry extract of Brazil is 1-5%.
8. a kind of suncream, which is characterized in that be made of the raw material of following weight percent：
Brazilian perfume cocoa berry extract：1-5%
Polysorbate 60：1.5%-3%
Rilanit special：2%-5%
Atoleine：5%-8%
Saualane：1%-2%
Glycerine：3%-5%
1,4- butanediols：1%-2%
Triethanolamine：0.2%-0.3%
Phenoxyethanol：0.01%-0.03%
Essence：0.01%-0.05%
Deionized water：Surplus.
9. a kind of suncream according to claim 8, which is characterized in that be made of the raw material of following weight percent：
Brazilian perfume cocoa berry extract：3%
Polysorbate 60：2%
Rilanit special：4%
Atoleine：7%
Saualane：1%
Glycerine：5%
1,4- butanediols：1%
Triethanolamine：0.3%
Phenoxyethanol：0.03%
Essence：0.01%
Deionized water：Surplus.
10. the preparation method of a kind of suncream according to claim 8 or claim 9, which is characterized in that walked including following technique
Suddenly：
（1）Raw material is divided into following three groups：
Group one：Polysorbate 60, rilanit special, atoleine, saualane；
Group two：Glycerine, 1,4- butanediols, triethanolamine, deionized water；
Group three：Brazilian perfume cocoa berry extract, Phenoxyethanol, essence；
（2）Oil phase pot will be added in after group one all components mixing, and be warming up to 80-90 DEG C, stir evenly, 30 minutes duration；
（3）Water phase pot will be added in after group two all components mixing, and be warming up to 80-90 DEG C, stir evenly, 30 minutes duration；
（4）By step（1）、（2）Liquid be mutually mixed carry out emulsifying, 30 minutes duration, by mixed liquor after emulsification
It is cooled to 45-55 DEG C, three all components of addition group stir evenly, and 30 minutes duration, are finally cooled to room temperature to obtain the final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810029258.2A CN108056962A (en) | 2018-01-12 | 2018-01-12 | A kind of Brazil's perfume cocoa berry extract and its application in suncream is prepared |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810029258.2A CN108056962A (en) | 2018-01-12 | 2018-01-12 | A kind of Brazil's perfume cocoa berry extract and its application in suncream is prepared |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108056962A true CN108056962A (en) | 2018-05-22 |
Family
ID=62141537
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810029258.2A Pending CN108056962A (en) | 2018-01-12 | 2018-01-12 | A kind of Brazil's perfume cocoa berry extract and its application in suncream is prepared |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08268863A (en) * | 1995-03-31 | 1996-10-15 | Mandamu:Kk | Tyrosinase biosynthesis promotor and hair cosmetic and sun-burn cosmetic |
| CN105813694A (en) * | 2013-10-16 | 2016-07-27 | 传统医疗保健有限公司 | Use of a composition for the pigmentation of hair and hairs |
| CN107049851A (en) * | 2017-02-11 | 2017-08-18 | 佛山文森特知识产权服务有限公司 | A kind of redness relieving mask containing camomile extract |
-
2018
- 2018-01-12 CN CN201810029258.2A patent/CN108056962A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08268863A (en) * | 1995-03-31 | 1996-10-15 | Mandamu:Kk | Tyrosinase biosynthesis promotor and hair cosmetic and sun-burn cosmetic |
| CN105813694A (en) * | 2013-10-16 | 2016-07-27 | 传统医疗保健有限公司 | Use of a composition for the pigmentation of hair and hairs |
| CN107049851A (en) * | 2017-02-11 | 2017-08-18 | 佛山文森特知识产权服务有限公司 | A kind of redness relieving mask containing camomile extract |
Non-Patent Citations (1)
| Title |
|---|
| 王建新主编: "《化妆品植物原料大全》", 30 June 2012, 中国纺织出版社 * |
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| PB01 | Publication | ||
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180522 |
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| RJ01 | Rejection of invention patent application after publication |