CN108043774A - A kind of equipment for solving ICP atomizers and blocking - Google Patents

A kind of equipment for solving ICP atomizers and blocking Download PDF

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Publication number
CN108043774A
CN108043774A CN201711030853.XA CN201711030853A CN108043774A CN 108043774 A CN108043774 A CN 108043774A CN 201711030853 A CN201711030853 A CN 201711030853A CN 108043774 A CN108043774 A CN 108043774A
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CN
China
Prior art keywords
cleaning
liquid
pipe
liquid zone
atomizer body
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201711030853.XA
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Chinese (zh)
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CN108043774B (en
Inventor
夏辉
杨悦锁
宋晓明
赵传起
高翠萍
温玉娟
刘晓璐
杨新瑶
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Shenyang University
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Shenyang University
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Application filed by Shenyang University filed Critical Shenyang University
Priority to CN201711030853.XA priority Critical patent/CN108043774B/en
Priority to CN202110212218.3A priority patent/CN112892950B/en
Publication of CN108043774A publication Critical patent/CN108043774A/en
Application granted granted Critical
Publication of CN108043774B publication Critical patent/CN108043774B/en
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B15/00Details of spraying plant or spraying apparatus not otherwise provided for; Accessories
    • B05B15/50Arrangements for cleaning; Arrangements for preventing deposits, drying-out or blockage; Arrangements for detecting improper discharge caused by the presence of foreign matter

Abstract

The present invention proposes a kind of equipment for solving ICP atomizers and blocking,Including babinet,Atomizer body,Power set,Cleaning cylinder and reservoir,The first bearing is equipped in babinet,Atomizer body is fixed on the first holder top,Inlet tube is connected on the inlet of atomizer body,Reservoir is divided into cleaning liquid zone by partition plate,Neutralize liquid zone and colour developing liquid zone,Clean liquid zone,It neutralizes in liquid zone and colour developing liquid zone and fills cleaning solution respectively,Neutralizer and developing solution,Clean liquid zone,It neutralizes and is respectively equipped with cleaning liquid pipe on liquid zone and colour developing liquid zone,Neutralize liquid pipe and colour developing liquid pipe,Clean liquid pipe,It neutralizes liquid pipe and colour developing liquid pipe is connected to by four-way valve on inlet tube,Support plate is equipped in cleaning cylinder,Support plate is equipped with test board,The present invention carries out the viscous wall of cleaning atomizer body by cleaning silk rotation,It is cleaned simultaneously by cleaning solution,Cleaning performance is good,The effect of atomizer body can be tested,It is easy to operate.

Description

A kind of equipment for solving ICP atomizers and blocking
Technical field
The present invention relates to Environmental Chemistry testing field, more particularly, to a kind of equipment for solving ICP atomizers and blocking.
Background technology
ICP atomizers generally refer to inductive coupling plasma emission spectrograph (ICP-AES), full spectrum direct-reading plasma Sampling system in the high sensitivity large-scale instrument such as body emission spectrometer (ICAP) and Inductively coupled plasma mass spectrometry instrument (ICP-MS) Gadget, ICP atomizers are consumptive materials, and instrument company does not also guarantee to keep in good repair, and the market price of ICP atomizers is generally 4000-30000 Member differs, and price is relatively expensive, and replacement frequency is very fast, therefore ICP atomizers become the serious burden of analysis measuring unit.
ICP atomizers are double-layer structure, and outer tube is carrier gas access, and inner tube is sample cell, mainly by prepare liquid quality sample mist Change a kind of device of analysis, it is main to be used cooperatively with fog chamber, when side wall is passed through the power gas such as argon gas, will aqueous solution enter atomization Device, and uniform small mist pearl is formed at nozzle, enter wherein intercepting a part of mist pearl in instrument, so as to complete test job, Therefore the atomization quantity of atomizer and atomizing effect directly affect the accuracy of test result.
Processing salinity incrustation at present, we, which invent, provides a kind of precision instrument atomizer incrustation detergent (application number: 2015110187536) the various incrustation in ICP atomizers, can be removed, achieve good removal effect, but for In the case that grain blocks or incrustation is thicker, effect is general, our present Normal practice is exactly to be inserted into some hard lousiness In ICP atomizers, left and right is disclosed, and carries out physics dredging, and effect is not ideal.
The content of the invention
The present invention proposes that a kind of equipment for solving the problem of that ICP atomizers block solves to propose in background technology.
The technical proposal of the invention is realized in this way:
A kind of equipment for solving ICP atomizers and blocking, including babinet, atomizer body, power set, cleaning cylinder and liquid storage Slot, the babinet is interior to be equipped with the first bearing, and the atomizer body is fixed on the first holder top, is set below first bearing Have idler wheel, inlet tube be connected on the inlet of the atomizer body, be connected on the air inlet of the atomizer body into Tracheae, the input terminal of the air inlet pipe are connected on compressor argon bottle, the reservoir by partition plate be divided into cleaning liquid zone, in With liquid zone and colour developing liquid zone, described clean in liquid zone, neutralization liquid zone and colour developing liquid zone fills cleaning solution, neutralizer and colour developing respectively Liquid, the cleaning liquid zone neutralize to be respectively equipped on liquid zone and colour developing liquid zone and clean liquid pipe, neutralization liquid pipe and colour developing liquid pipe, described Cleaning liquid pipe, neutralization liquid pipe and colour developing liquid pipe are connected to by four-way valve on inlet tube, and the cleaning cylinder is arranged on atomizer sheet On the left of body, fixed frame is equipped with below the cleaning cylinder, the fixed frame is bolted on babinet, is set in the cleaning cylinder There is support plate, the support plate is equipped with test board.
The power set include servomotor, speed reducer and the second bearing, and the speed reducer is bolted on the On two bearings, the servomotor is connected on speed reducer, and the speed reducer output shaft is connected with ball screw by shaft coupling, The ball screw is equipped with nut, is welded with connecting rod on the nut, the connecting rod other end is connected to the first bearing On, the ball screw front end is equipped with band silk blind cover, and cleaning silk is fixed in the band silk blind cover, and the cleaning silk can be put into In atomizer body nozzle.
The ball screw is respectively equipped with front limited block and rear limited block on rear side of going forward.
Waste liquid cylinder is equipped with below the cleaning cylinder, the cleaning cylinder lower end is connected with drain pipe and liquid back pipe, the drain Pipe and the upper end of liquid back pipe are equipped with switch valve, and the drain pipe other end is connected in waste liquid cylinder, the liquid back pipe it is another End is connected in the cleaning liquid zone of reservoir.
Peephole is connected at the nozzle of the atomizer body, the peephole is detachable apparatus.
The test board is divided into two sections of the left and right with arc groove, and two sections of the left and right arc groove of the test board is when being closed Circular hole.
The babinet upper end hinge, which is handed over, upper cover plate, and handle is equipped at left and right sides of the babinet.
Above-mentioned technical proposal is employed, beneficial effects of the present invention are:
1st, the present invention carries out the viscous wall of cleaning atomizer body by cleaning silk rotation, and nut drives connecting rod movement The first bearing and atomizer body is driven to move, cleaning silk is enable to clean in atomizer nozzle everywhere, cleaning performance is good;
2nd, the present invention can also be understood atomizer body simultaneously by cleaning solution and be cleaned, and dual cleaning, cleaning performance is good, together When cleaning solution can be recycled, reduce cleaning cost;
3rd, the present invention sets the cleaning situation that atomizer body interior can be checked by peephole, easy to use, while can be with The effect of atomizer body is tested, it is easy to operate.
Description of the drawings
It in order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing There is attached drawing needed in technology description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this Some embodiments of invention, for those of ordinary skill in the art, without having to pay creative labor, may be used also To obtain other attached drawings according to these attached drawings.
Fig. 1 is the structural diagram of the present invention;
Fig. 2 is enlarged drawing at A on Fig. 1;
Structure diagram when Fig. 3 separates for test board and when being closed;
Wherein:1- reservoirs;2- cleans liquid zone;In 3- and liquid zone;4- colour developings liquid zone;5- colour developing liquid pipes;In 6- and liquid pipe; 7- cleans liquid pipe;8- four-way valves;9- air inlet pipe;10- inlet tubes;11- babinets;12- atomizer bodies;13- cleaning cylinders;14- is clear Wash silk;15- test boards;16- upper cover plates;17- servomotors;18- handles;19- speed reducers;20- connecting rods;The second bearings of 21-; 22- support plates;23- fixed frames;24- waste liquid cylinders;25- drain pipes;26- liquid back pipes;The first bearings of 27-;28- peepholes;29- band silks Blind cover;30- ball screws;31- front limited blocks;32- nuts;Limited block after 33-;34- arc grooves.
Specific embodiment
Below in conjunction with the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, those of ordinary skill in the art are obtained every other without creative efforts Embodiment belongs to the scope of protection of the invention.
As shown in Figs. 1-3:
A kind of equipment for solving ICP atomizers and blocking, including babinet 11, atomizer body 12, power set, cleaning cylinder 13 With reservoir 1, the babinet 11 is interior to be equipped with the first bearing 27, and the atomizer body 12 is fixed on 27 top of the first bearing, institute It states 27 lower section of the first bearing and is equipped with idler wheel, inlet tube 10, the atomizer are connected on the inlet of the atomizer body 12 Air inlet pipe 9 is connected on the air inlet of body 12, the input terminal of the air inlet pipe 9 is connected on compressor argon bottle, the storage Liquid bath 1 is divided into cleaning liquid zone 2 by partition plate, neutralizes liquid zone 3 and colour developing liquid zone 4, and the cleaning liquid zone 2 neutralizes liquid zone 3 and colour developing Cleaning solution, neutralizer and developing solution are filled in liquid zone 4 respectively, the cleaning liquid zone 2 is neutralized on liquid zone 3 and colour developing liquid zone 4 respectively Equipped with cleaning liquid pipe 7, liquid pipe 6 and colour developing liquid pipe 5 are neutralized, the cleaning liquid pipe 7, neutralization liquid pipe 6 and colour developing liquid pipe 5 pass through four-way Valve 8 is connected on inlet tube 10, and the cleaning cylinder 13 is arranged on 12 left side of atomizer body, and 13 lower section of cleaning cylinder is equipped with solid Determine frame 23, the fixed frame 23 is bolted on babinet 11, and support plate 22, the support plate 22 are equipped in the cleaning cylinder 13 It is equipped with test board 15.
The power set include servomotor 17,19 and second bearing 21 of speed reducer, and the speed reducer 19 passes through bolt It is fixed on the second bearing 21, the servomotor 17 is connected on speed reducer 19, and 19 output shaft of speed reducer passes through shaft coupling Device is connected with ball screw 30, and the ball screw 30 is equipped with nut 32, connecting rod 20 is welded on the nut 32, described 20 other end of connecting rod is connected on the first bearing 27, and 30 front end of ball screw is equipped with band silk blind cover 29, the band silk Cleaning silk 14 is fixed in blind cover 29, the cleaning silk 14 can be put into 12 nozzle of atomizer body, be rotated by cleaning silk 14 The viscous wall of cleaning atomizer body 12 is carried out, and nut 32 drives the movement of connecting rod 20 to drive the first bearing 27 and atomizer sheet Body 12 moves, and cleaning silk 14 is enable to clean atomizer body 12 everywhere, and cleaning performance is good, the ball screw 30 go forward rear side point Not She You front limited block 31 and rear limited block 33, limit nut 32 moving range, avoid atomizer body 12 move excessively with Cleaning cylinder 13 collides, and 13 lower section of cleaning cylinder is equipped with waste liquid cylinder 24, and 13 lower end of cleaning cylinder is connected with drain pipe 25 With liquid back pipe 26, the upper end of the drain pipe 25 and liquid back pipe 26 is equipped with switch valve, and 25 other end of drain pipe is connected to In waste liquid cylinder 24, the other end of the liquid back pipe 26 is connected in the cleaning liquid zone 2 of reservoir 1, can be recycled cleaning solution, Pollution of the waste liquid to cleaning solution is avoided simultaneously, peephole 28, the observation are connected at the nozzle of the atomizer body 12 Mirror 28 is detachable apparatus, and the cleaning situation inside atomizer body 12, easy to use, the survey can be checked by peephole 28 Test plate (panel) 15 is divided to for two sections of the left and right with arc groove 34, is circular hole when two sections of the left and right arc groove 34 of the test board 15 is closed, It is easily installed, the circular hole that the arc groove 34 on test board 15 forms can make ball screw 30 by the way that 11 upper end of the babinet hinge is handed over There is upper cover plate 16,11 left and right sides of babinet is equipped with handle 18, conveniently moving.
Operation principle:
First, test mode:Servomotor 17 and speed reducer 19 are closed, test board 15 is mounted on support plate 22, control four Port valve 8 connects inlet tube 10 with colour developing liquid pipe 5, starts atomizer body 12, developing solution is injected on test board 15, is passed through Observation test board 15 on color change determine whether atomizer body 12 is good, then control four-way valve 8 by inlet tube 10 with It neutralizes liquid pipe 6 to connect, starts atomizer body 12, neutralizer is injected on test board 15, neutralize the color on test board 15, Wait is tested next time, and during test mode, the switch valve on liquid back pipe 26 is closed, and the switch valve on drain pipe 25 is opened so that Developing solution and neutralizer are drained into waste liquid cylinder 24;
2nd, state is cleaned:Start servomotor 17 and speed reducer 19, servomotor 17 is first allowed to rotate forward, ball screw 30 It rotates forward, cleaning silk 14 also rotates forward the viscous wall for carrying out cleaning atomizer body 12, while under the action of nut 32, drives second Seat 21 moves, and making atomizer body 12, when servomotor 17 inverts, ball screw 30 also inverts, cleaning away from speed reducer 19 Silk 14 also inverts the viscous wall for carrying out cleaning atomizer body 12, and similarly atomizer body 12 is close under the action of nut 32 slows down Machine 19, in cleaning process, control four-way valve 8 connects inlet tube 10 with cleaning liquid pipe 7, passes through pair of cleaning solution and cleaning silk 14 Under recast is used, cleaning performance is good, while the switch valve on liquid back pipe 26 is opened, and the switch valve on drain pipe 25 is closed so that clear Washing lotion can be back to the cleaning liquid zone 2 of reservoir 1, recycle cleaning liquid energy, after cleanings is waited to carry out a flow, observation Mirror 28 is mounted on atomizer body 12, checks in 12 nozzle of atomizer body whether clean up by peephole 28, several Only, peephole 28 is removed, is tested, if unclean, removes peephole 28, continues cleaning until cleaning up.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention With within principle, any modifications, equivalent replacements and improvements are made should all be included in the protection scope of the present invention god.

Claims (7)

1. a kind of equipment for solving ICP atomizers and blocking, including babinet (11), atomizer body (12), power set, cleaning cylinder (13) and reservoir (1), it is characterised in that:The first bearing (27), the atomizer body (12) are equipped in the babinet (11) The first bearing (27) top is fixed on, idler wheel, the feed liquor of the atomizer body (12) are equipped with below first bearing (27) Inlet tube (10) is connected on mouthful, air inlet pipe (9), the air inlet pipe are connected on the air inlet of the atomizer body (12) (9) input terminal is connected on compressor argon bottle, and the reservoir (1) is divided into cleaning liquid zone (2) by partition plate, neutralizes liquid zone (3) and colour developing liquid zone (4), cleaning liquid zone (2), neutralize liquid zone (3) and colour developing liquid zone (4) it is interior fill respectively cleaning solution, in With liquid and developing solution, it is described cleaning liquid zone (2), neutralize liquid zone (3) and colour developing liquid zone (4) on be respectively equipped with clean liquid pipe (7), in With liquid pipe (6) and colour developing liquid pipe (5), the cleaning liquid pipe (7), neutralization liquid pipe (6) and colour developing liquid pipe (5) pass through four-way valve (8) It is connected on inlet tube (10), the cleaning cylinder (13) is arranged on the left of atomizer body (12), below the cleaning cylinder (13) Equipped with fixed frame (23), the fixed frame (23) is bolted on babinet (11), and branch is equipped in the cleaning cylinder (13) Plate (22), the support plate (22) are equipped with test board (15).
A kind of 2. equipment for solving ICP atomizers and blocking according to claim 1, which is characterized in that the power set Including servomotor (17), speed reducer (19) and the second bearing (21), the speed reducer (19) is bolted on second On seat (21), the servomotor (17) is connected on speed reducer (19), and speed reducer (19) output shaft is connected by shaft coupling Ball screw (30) is connected to, the ball screw (30) is equipped with nut (32), connecting rod is welded on the nut (32) (20), connecting rod (20) other end is connected on the first bearing (27), and ball screw (30) front end is equipped with band silk Blind cover (29), cleaning silk (14) is fixed on the band silk blind cover (29), and the cleaning silk (14) can be put into atomizer body (12) in nozzle.
A kind of 3. equipment for solving ICP atomizers and blocking according to claim 2, which is characterized in that the ball screw (30) front limited block (31) and rear limited block (33) are respectively equipped on rear side of going forward.
A kind of 4. equipment for solving ICP atomizers and blocking according to claim 1, which is characterized in that the cleaning cylinder (13) lower section is equipped with waste liquid cylinder (24), and cleaning cylinder (13) lower end is connected with drain pipe (25) and liquid back pipe (26), the row The upper end of liquid pipe (25) and liquid back pipe (26) is equipped with switch valve, and drain pipe (25) other end is connected to waste liquid cylinder (24) In, the other end of the liquid back pipe (26) is connected in the cleaning liquid zone (2) of reservoir (1).
A kind of 5. equipment for solving ICP atomizers and blocking according to claim 1, which is characterized in that the atomizer sheet Peephole (28) is connected at the nozzle of body (12), the peephole (28) is detachable apparatus.
A kind of 6. equipment for solving ICP atomizers and blocking according to claim 1, which is characterized in that the test board (15) it is divided into two sections of the left and right with arc groove (34), is circle when two sections of the left and right arc groove (34) of the test board (15) is closed Hole.
A kind of 7. equipment for solving ICP atomizers and blocking according to claim 1, which is characterized in that the babinet (11) Upper end hinge, which is handed over, upper cover plate (16), and handle (18) is equipped at left and right sides of the babinet (11).
CN201711030853.XA 2017-10-28 2017-10-28 Equipment for solving blockage of ICP atomizer Active CN108043774B (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN201711030853.XA CN108043774B (en) 2017-10-28 2017-10-28 Equipment for solving blockage of ICP atomizer
CN202110212218.3A CN112892950B (en) 2017-10-28 2017-10-28 ICP atomizer blocks up clean system and contains its equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711030853.XA CN108043774B (en) 2017-10-28 2017-10-28 Equipment for solving blockage of ICP atomizer

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CN108043774B CN108043774B (en) 2021-01-01

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CN106363000A (en) * 2016-11-22 2017-02-01 赵靖宇 Test tube cleaning and drying device for chemical tests
CN206095947U (en) * 2016-10-11 2017-04-12 云南环绿环境检测技术有限公司 Inductively coupled plasma emmission spectrum appearance

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CN204842381U (en) * 2015-07-16 2015-12-09 赵明洋 Full -automatic drilling rod internal thread belt cleaning device
CN205587394U (en) * 2016-05-03 2016-09-21 李姗姗 Tube cleaning device for biological teaching
CN105921759B (en) * 2016-06-14 2017-12-19 江苏威拉里新材料科技有限公司 A kind of device dredged open atomizer and blocked up
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Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE507611C2 (en) * 1997-07-03 1998-06-29 Drester Ab Method and apparatus for washing spray guns
CN1367063A (en) * 2001-01-24 2002-09-04 日本电气株式会社 Cleaner for cleaning capillary tube of wire welding equipment
CN101314154A (en) * 2008-07-01 2008-12-03 攀钢集团研究院有限公司 Method for removing obstruction of atomizer
GB2502483A (en) * 2010-09-20 2013-11-27 Ali Waqar Majeed Cleaning device
CN202199458U (en) * 2011-08-03 2012-04-25 周国富 Novel intelligent atomizer
CN103801475A (en) * 2014-03-03 2014-05-21 攀钢集团攀枝花钢铁研究院有限公司 Method for cleaning gas channel branch pipe of atomizer
CN203991539U (en) * 2014-06-19 2014-12-10 中芯国际集成电路制造(北京)有限公司 Eliminate the device that capillary stops up
CN104028524A (en) * 2014-06-28 2014-09-10 井贵富 Test tube washing device
CN206095947U (en) * 2016-10-11 2017-04-12 云南环绿环境检测技术有限公司 Inductively coupled plasma emmission spectrum appearance
CN106363000A (en) * 2016-11-22 2017-02-01 赵靖宇 Test tube cleaning and drying device for chemical tests

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CN108043774B (en) 2021-01-01
CN112892950B (en) 2022-12-06
CN112892950A (en) 2021-06-04

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