CN107984118A - A kind of preparation method of brazing cream - Google Patents

A kind of preparation method of brazing cream Download PDF

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Publication number
CN107984118A
CN107984118A CN201711361450.3A CN201711361450A CN107984118A CN 107984118 A CN107984118 A CN 107984118A CN 201711361450 A CN201711361450 A CN 201711361450A CN 107984118 A CN107984118 A CN 107984118A
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CN
China
Prior art keywords
weight
solder
lotion
brazing
component
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201711361450.3A
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Chinese (zh)
Inventor
莫文剑
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Tong Baorui New Material Co Ltd
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Suzhou Tong Baorui New Material Co Ltd
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Application filed by Suzhou Tong Baorui New Material Co Ltd filed Critical Suzhou Tong Baorui New Material Co Ltd
Priority to CN201711361450.3A priority Critical patent/CN107984118A/en
Publication of CN107984118A publication Critical patent/CN107984118A/en
Withdrawn legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K35/00Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
    • B23K35/40Making wire or rods for soldering or welding

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Cosmetics (AREA)

Abstract

The present invention discloses a kind of preparation method of brazing cream, comprises the following steps:1) solder is weighed and into each component in lotion by suitable proportioning;Lotion and solder are smelted into respectively into each component in lotion and solder by what is weighed again, then weigh each component by appropriate proportioning again;2) solder weighed and brazing flux are added again described into lotion, are stirred 30~45 minutes, stir evenly, obtain brazing cream, to obtain the final product.The method of the present invention does not have fluorine-containing material by using a small amount of brazing flux in the brazing flux used, has used organic substance, has obvious low corrosivity to part;And solder is by the tin of specific proportioning, silver with copper into the fusing point of obtained brazing cream is low, is easy to weld.

Description

A kind of preparation method of brazing cream
Technical field
The present invention relates to a kind of preparation method of brazing cream, belong to technical field of welding materials.
Background technology
As modernization industry automates the development of soldering high efficiency large-scale production, welding workpiece small batch Production, weld shape constantly variation complicate.Traditional filiform, ring-type, strip is substituted to weld with paste-like soldering material-solder paste Connect material and realize that high-efficiency automatic welding production has been trend of the times.China's advanced automation pricker of continuous Introduced From Abroad in recent years Production line is welded, such as flame automatic brazing production line, protective atmosphere meshbeltfurnace brazing lines;It is domestic at the same time also to have many producers certainly Master develops more advanced automation brazing lines, to meet ever-increasing market demand.Welded with traditional Cu alloys Silk, weld-ring are compared with solder strip, are combined using brazing cream and automatic dropping glue equipment, can to complex parts and irregular part into Row automation paint, the part to be welded after application is brazed into continous way soldering oven, so as to fulfill the continuous of whole welding procedure Change and automate.Joint element intensity height, weld seam beauty and corrosion resistance after welding is good.
But brazing flux content is high in current brazing cream, since borofluoride has strong corrosivity at high temperature, for Excessive corrosion and destruction can be caused by weldering part and brazing equipment, postwelding needs to clean part, in welding process Corrosivity volatile matter can also bring a series of problems to working environment and environmental protection.
The content of the invention
It is an object of the invention to provide a kind of preparation method of brazing cream, the brazing cream that this method obtains contains a small amount of Brazing flux, has part obvious low corrosivity, and fusing point is low, is easily assembled to, good fluidity, joint element intensity after welding, and It is small to the harmfulness of environment.
To reach above-mentioned purpose, the present invention provides following technical solution:
On the one hand, the present invention provides a kind of brazing cream, includes each component of following parts by weight:70~85 parts of solder, into 15~22 parts of lotion, and dosage be 5~8 parts of solder quality brazing flux, wherein, the solder by 94~96 weight % tin, 3 The silver of~4 weight % and the copper of 1~1.5 weight % form;The brazing flux in decanedioic acid, succinic acid and laurate at least It is a kind of;It is described to include following component into lotion:The poly- second propylene of 14~16 weight %, the solvent of 65~95 weight %, 2~3 weights Measure the nonionic surface active agent of % and the activator of 0.8~1.1 weight %.
Further, the solder is made of the copper of the tin of 95 weight %, the silver of 4 weight % and 1 weight %.
Further, it is described to include following component into lotion:The poly- second propylene of 15 weight %, the solvent of 81 weight %, 3 weights Measure the nonionic surface active agent of % and the activator of 1 weight %.
Further, the solvent is diethylene glycol monoethyl ether or dipropylene glycol monomethyl ether.
Further, the nonionic surface active agent is fatty glyceride.
Further, the activator is unrighted acid and/or animal oil.
Further, the brazing cream includes each component of following parts by weight:75 parts of solder, into 18 parts of lotion, and Dosage is the brazing flux of 7 parts of solder quality.
On the other hand, the present invention also provides a kind of preparation method of above-mentioned brazing cream, comprise the following steps:
1) solder is weighed and into each component in lotion by suitable proportioning;It will weigh again into each in lotion and solder Component is smelted into lotion and solder respectively, then weighs each component by appropriate proportioning again;
2) solder weighed and brazing flux are added again described into lotion, is stirred 30~45 minutes, stirs evenly, obtain To brazing cream, to obtain the final product.
Further, in step 1), it will weigh into each component in lotion and be smelted into cream at 90~140 DEG C Body.
Further, it will weigh into each component in lotion and be smelted into lotion at 120 DEG C.
Further, in step 1), the solder that will weigh, in crucible, at 1150~1250 DEG C, and in vacuum bar Melting under part.
Further, the melting at 1180 DEG C.
The beneficial effects of the present invention are:By using a small amount of brazing flux, and there is no fluorine-containing material in the brazing flux used, Organic substance has been used, there is obvious low corrosivity to part;And solder by the tin of specific proportioning, silver and copper into, The fusing point of obtained brazing cream is low, is easy to weld;In addition, unrighted acid and animal oil are added in the preparation process of lotion Deng activator, solder and solder and the combination power on organic moiety surface are considerably increased, is conducive to anti-layering and the mistake of brazing cream Pipe, technologic guarantee is provided to automate, mass producing;And by controlling the parameter in preparation method so that system The brazing cream performance obtained is more excellent.
Described above is only the general introduction of technical solution of the present invention, in order to better understand the technological means of the present invention, And can be practiced according to the content of specification, described in detail below with presently preferred embodiments of the present invention as after.
Embodiment
With reference to embodiment, the embodiment of the present invention is described in further detail.Following embodiments are used for Illustrate the present invention, but be not limited to the scope of the present invention.
Embodiment 1
1) each component in solder is weighed by the proportioning of the copper of the tin of 95 weight %, the silver of 4 weight % and 1 weight %, then By each component solder in the solder weighed in crucible, at 1180 DEG C, and solder is smelted under vacuum condition;By 15 weights Measure poly- second propylene, the diethylene glycol monoethyl ether of 81 weight % of %, the fatty glyceride of 3 weight %, and the insatiable hunger of 1 weight % The each component in lotion is weighed into the proportioning of aliphatic acid, lotion is smelted into at 120 DEG C;
2) solder weighed and decanedioic acid are added again described into lotion, is stirred 30 minutes, stirs evenly, obtain Fused materials mixture, obtains brazing cream, to obtain the final product.
By obtained brazing cream, it is mainly used for welding low-carbon steel part, postwelding piece surface noresidue, weld seam is fine and closely woven, and And there is very high weld strength;In addition the corrosion-free phenomenon of part is produced.
Embodiment 2
1) each component in solder is weighed by the proportioning of the copper of the tin of 95 weight %, the silver of 4 weight % and 1 weight %, then By each component solder in the solder weighed in crucible, at 1180 DEG C, and solder is smelted under vacuum condition;By 15 weights Measure the poly- second propylene of %, the diethylene glycol monoethyl ether of 81 weight %, the nonionic surface active agent and 1 weight % of 3 weight % The proportioning of animal oil weigh into each component in lotion, be smelted into lotion at 120 DEG C;
2) solder weighed and succinic acid are added again described into lotion, is stirred 35 minutes, stirs evenly, obtain Fused materials mixture, obtains brazing cream, to obtain the final product.
By obtained brazing cream, it is mainly used for welding low-carbon steel part, postwelding piece surface noresidue, weld seam is fine and closely woven, and And there is very high weld strength;In addition the corrosion-free phenomenon of part is produced.
Embodiment 3
1) each component in solder is weighed by the proportioning of the copper of the tin of 95 weight %, the silver of 4 weight % and 1 weight %, then By each component solder in the solder weighed in crucible, at 1180 DEG C, and solder is smelted under vacuum condition;By 15 weights Measure the poly- second propylene of %, the dipropylene glycol monomethyl ether of 81 weight %, the nonionic surface active agent and 1 weight % of 3 weight % The proportioning of activator (containing unrighted acid and animal oil) weigh into each component in lotion, by it at 120 DEG C It is smelted into lotion;
2) solder weighed and laurate are added again described into lotion, is stirred 45 minutes, stirs evenly, obtain Fused materials mixture, obtains brazing cream, to obtain the final product.
By obtained brazing cream, it is mainly used for welding low-carbon steel part, postwelding piece surface noresidue, weld seam is fine and closely woven, and And there is very high weld strength;In addition the corrosion-free phenomenon of part is produced.
Each technical characteristic of embodiment described above can be combined arbitrarily, to make description succinct, not to above-mentioned reality Apply all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited In contradiction, the scope that this specification is recorded all is considered to be.
Embodiment described above only expresses the several embodiments of the present invention, its description is more specific and detailed, but simultaneously Cannot therefore it be construed as limiting the scope of the patent.It should be pointed out that come for those of ordinary skill in the art Say, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the protection of the present invention Scope.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.

Claims (10)

1. a kind of preparation method of brazing cream, comprises the following steps:
1) solder is weighed and into each component in lotion by suitable proportioning;It will weigh again into each component in lotion and solder Lotion and solder are smelted into respectively, then weigh each component by appropriate proportioning again;Wherein, brazing cream includes following parts by weight Several each components:70~85 parts of solder, the brazing flux into 15~22 parts of lotion, and dosage for 5~8 parts of solder quality, wherein, institute Solder is stated to be made of the copper of the tin of 94~96 weight %, the silver of 3~4 weight % and 1~1.5 weight %;The brazing flux is selected from the last of the ten Heavenly stems At least one of diacid, succinic acid and laurate boric acid;It is described to include following component into lotion:The poly- second of 14~16 weight % The activation of propylene, the solvent of 65~95 weight %, the nonionic surface active agent of 2~3 weight % and 0.8~1.1 weight % Agent;
2) solder weighed and brazing flux are added again described into lotion, is stirred 30~45 minutes, stirs evenly, obtain copper Soldering paste, to obtain the final product.
2. the preparation method of brazing cream according to claim 1, it is characterised in that in step 1), will weigh into cream Each component in body is smelted into lotion at 90~140 DEG C.
3. the preparation method of brazing cream according to claim 2, it is characterised in that will weigh into each component in lotion Lotion is smelted into at 120 DEG C.
4. the preparation method of brazing cream according to any one of claim 1 to 3, it is characterised in that, will in step 1) The solder weighed, in crucible, at 1150~1250 DEG C, and the melting under vacuum condition.
5. the preparation method of brazing cream according to claim 4, it is characterised in that the melting at 1180 DEG C.
6. the preparation method of brazing cream according to any one of claim 1 to 3, the solder by 95 weight % tin, 4 The silver of weight % and the copper of 1 weight % form.
7. the preparation method of brazing cream according to any one of claim 1 to 3, described to include following component into lotion: The activation of the poly- second propylene of 15 weight %, the solvent of 81 weight %, the nonionic surface active agent of 3 weight % and 1 weight % Agent.
8. brazing cream according to claim 7, it is characterised in that the solvent is diethylene glycol monoethyl ether or dipropylene glycol Monomethyl ether.
9. brazing cream according to claim 7, it is characterised in that the nonionic surface active agent is fatty acid glycerine Ester.
10. brazing cream according to claim 7, it is characterised in that the activator is unrighted acid and/or animal Oil.
CN201711361450.3A 2017-12-18 2017-12-18 A kind of preparation method of brazing cream Withdrawn CN107984118A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5527628A (en) * 1993-07-20 1996-06-18 Iowa State University Research Foudation, Inc. Pb-free Sn-Ag-Cu ternary eutectic solder
WO1997009455A1 (en) * 1995-09-01 1997-03-13 Sarnoff Corporation Soldering composition
CN1586795A (en) * 2004-08-31 2005-03-02 广州有色金属研究院 Copper welding paste for automatic brazing and its preparing method
CN103659053A (en) * 2012-09-13 2014-03-26 莫文剑 Copper welding paste for braze welding and preparation method thereof
CN107052616A (en) * 2016-11-30 2017-08-18 安徽华众焊业有限公司 Soldering copper soldering paste

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5527628A (en) * 1993-07-20 1996-06-18 Iowa State University Research Foudation, Inc. Pb-free Sn-Ag-Cu ternary eutectic solder
WO1997009455A1 (en) * 1995-09-01 1997-03-13 Sarnoff Corporation Soldering composition
CN1586795A (en) * 2004-08-31 2005-03-02 广州有色金属研究院 Copper welding paste for automatic brazing and its preparing method
CN103659053A (en) * 2012-09-13 2014-03-26 莫文剑 Copper welding paste for braze welding and preparation method thereof
CN107052616A (en) * 2016-11-30 2017-08-18 安徽华众焊业有限公司 Soldering copper soldering paste

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Application publication date: 20180504