CN107935783A - A kind of microelement type water-soluble fertilizer containing amino-acid liquid and its production technology - Google Patents
A kind of microelement type water-soluble fertilizer containing amino-acid liquid and its production technology Download PDFInfo
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- CN107935783A CN107935783A CN201711400892.4A CN201711400892A CN107935783A CN 107935783 A CN107935783 A CN 107935783A CN 201711400892 A CN201711400892 A CN 201711400892A CN 107935783 A CN107935783 A CN 107935783A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C3/00—Fertilisers containing other salts of ammonia or ammonia itself, e.g. gas liquor
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- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
- C05F17/50—Treatments combining two or more different biological or biochemical treatments, e.g. anaerobic and aerobic treatment or vermicomposting and aerobic treatment
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
- C05G5/23—Solutions
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
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Abstract
The present invention provides a kind of microelement type water-soluble fertilizer containing amino-acid liquid, it includes following component：Cottonseed Meal, corncob, wheat bran, edible mushroom bran, silkworm chrysalis, cicada slough, discarded animal skin, ferrous sulfate heptahydrate, cupric sulfate pentahydrate, white vitriol, manganese sulfate monohydrate, ten water Boratexes, ammonium molybdate tetrahydrate, composite bacteria agent A and B, wormcast, citric acid, pH adjusting agent and water.Its production technology uses modern biotechnology inoculating compound bacterium agent A and B, the production technology fermented using two-stage aerobic, animal protein contained by contained vegetable protein in agricultural wastes, edible mushroom bran and discarded animal skin is decomposed into small molecule free amino acid and natural active matter and nutritional ingredient, full-scope safeguards are provided for plant health growth, by being chelated with micro- component, microelement type water-soluble fertilizer containing amino-acid liquid is prepared.The present invention takes full advantage of agricultural wastes, edible mushroom bran and discarded animal skin, realizes resource reutilization, environment friendly and pollution-free.
Description
Technical field
It is specifically a kind of to be suitable for rice and wheat, beans, greengrocery, water the present invention relates to agrochemical technical field
The microelement type water-soluble fertilizer containing amino-acid liquid and its production technology of fruit, greenweed, nursery stock class etc..
Background technology
Fertilizer is applied in modern agricultural production has become the weight for promoting plant growth, increase yield and improvement plant quality
Want one of measure.Current fertilizer widely used on the market is mainly inorganic fertilizer.Inorganic fertilizer is mineral matter fertilizer, also crying
Fertilizer is learned, its component is simple, and active constituent content is high, scattered, is easily absorbed and used by plants, is referred to as " quick-acting fertilizer ".However,
With people's long period it is a large amount of it is unreasonable apply inorganic fertilizer, SOIL CARBON AND NITROGEN is out of proportion, in being manured into soil for many years
Fertilizer only has small part to be utilized by this season plant absorption, the fertilizer of remaining 70-80% is by soil fixing, formation phosphate, nitrate
Precipitation residual, destroys the crumb structure of soil, causes the soil hardening of getting worse, and fertilizer effective rate of utilization is low, cultivation
Property be deteriorated, strongly limit further improving for plant products and quality.On the other hand, the required trace element of plant growth
It is present in more in the form of EDTA Chelating states in fertilizer, used chelating agent EDETATE SODIUM energy activating soil heavy metal, promotes root
It is that the excess of heavy metal is absorbed, in addition, EDETATE SODIUM no biotoxicity itself, but its heavy metal chelate formed has
Bio-toxicity, easily biological-degradable, is not unfavorable for the sustainable development of agricultural production.
Amino acid fertilizer is increasingly widely recognized as a kind of new-type fertilizer be subject to people, and research shows, amino acid pair
The effect of soil and plant is as follows：
1st, amino acid inherently plant nutrient agent, the nutrition contribution to plant are not only to provide nitrogen source, can also mitigate plant weight
The toxic action of metal ion, the physiological metabolism on plant produce immeasurable influence；
2nd, amino acid can increase the content of plant chlorophyll, have unique facilitation to the photosynthesis of plant, can increase
The content of VC and sugar, significantly improve plant quality；
3rd, amino acid can supplement various nutrients required in plant, can adjust various nutrients assimilation ratio and
Equilibrium state in plant, so as to play the role of adjusting plant normal growth.
4th, with the trace element needed for plant chelatropic reaction can occur for amino acid, and generation solubility is good, is easily inhaled by plant
The chelate of receipts.
Agricultural wastes refer to the organic matter being dropped in whole agricultural production process, and research shows, contains in organic matter
There is the plant nutrient such as abundant vegetable protein and nitrogen, phosphorus, potassium, important adjustment effect is played in farmland ecosystem, is had
Very high recycle value.Edible mushroom bran is the waste residue after culturing edible fungus, wherein containing substantial amounts of crude fibre, lignin and
Mycelium（Include abundant vegetable protein, amino acid, carbohydrate, vitamin and trace element）Deng nutriment.If
These discarded edible mushroom chaffs cannot be dealt carefully with, on the one hand, contained nutriment can be made to be discarded for a long time, it is impossible to obtain effectively
Utilization, very unfortunately, on the other hand, eat mushroom bran metabolism caused by some toxin, dirt can be caused to agroecological environment
Dye, very big hidden danger is brought to edible fungus culturing afterwards.In addition, greatly developing with various regions aquaculture, raiser is to discarded
Animal skin is arbitrarily stacked, and is made wherein serious comprising the loss of a large amount of animal proteins.Therefore, if to agricultural wastes, edible mushroom
Processing is hydrolyzed in contained vegetable protein or animal protein in health and discarded animal skin, is separated into free amino acid, adds
Add trace element that trace element is made and contain Amino acid liquid fertilizer, will exert far reaching influence to modern agriculture.
The content of the invention
The technical assignment of the present invention is in view of the deficiencies of the prior art, there is provided a kind of microelement type water containing amino-acid liquid
Molten fertilizer and its production technology.
The technical solution adopted by the present invention to solve the technical problems is：
A kind of microelement type water-soluble fertilizer containing amino-acid liquid, is 1 liter of calculating by the liquid water-soluble fertilizer total amount, it is formulated
Middle raw material composition and each component mass fraction are as follows：30-60 grams of Cottonseed Meal, 75-90 grams of corncob, 45-60 grams of wheat bran, edible mushroom
100-120 grams of chaff, 10-20 grams of silkworm chrysalis, 30-50 grams of cicada slough, discarded 40-80 grams of animal skin, 13-21 grams of ferrous sulfate heptahydrate,
18-27 grams of cupric sulfate pentahydrate, 16-24 grams of white vitriol, 23-32 grams of manganese sulfate monohydrate, ten 0-25 grams of water Boratexes, four water molybdenums
Sour 0-10 grams of ammonium, composite bacteria agent A 2-3 gram, composite bacteria agent B 4-6 gram, 8-10 grams of wormcast, 4-6 grams of citric acid, pH adjusting agent
1-5 grams, surplus is water；
Wherein composite bacteria agent A is Aspergillus flavus and unwrapping wire styreptomyces globispotus strain in mass ratio 1:0.8-1.5 is combined, composite bacteria agent
B is photosynthetic bacteria, saccharomycete, bacillus azotobacter 0.5-0. 8 in mass ratio：1：1-1.2 it is combined.
Preferably, it is 1 liter of calculating by the liquid water-soluble fertilizer total amount, raw material composition and each component mass parts during it is formulated
Number is as follows：45-50 grams of Cottonseed Meal, 80-84 grams of corncob, 45-52 grams of wheat bran, edible 105-110 grams of mushroom bran, 12-16 grams of silkworm chrysalis,
40-50 grams of cicada slough, discarded 60-75 grams of animal skin, 18-21 grams of ferrous sulfate heptahydrate, 16-18 grams of cupric sulfate pentahydrate, seven water sulphur
Sour 23-25 grams of zinc, 22-25 grams of manganese sulfate monohydrate, ten 10-25 grams of water Boratexes, 5-10 grams of ammonium molybdate tetrahydrate, composite bacteria agent A 2-
2.5 grams, composite bacteria agent B 4-5 gram, 8-9 grams of wormcast, 4-5 grams of citric acid, 2-4 grams of pH adjusting agent, surplus is water；
Wherein composite bacteria agent A is Aspergillus flavus and unwrapping wire styreptomyces globispotus strain in mass ratio 1:1 is combined, and composite bacteria agent B is light
Close bacterium, saccharomycete, bacillus azotobacter in mass ratio 0.6：1：1.2 it is combined.
The pH adjusting agent is sodium hydroxide, the one or more in potassium hydroxide, disodium hydrogen phosphate.
2nd, the present invention also provides a kind of production technology of microelement type water-soluble fertilizer containing amino-acid liquid, including following work
Skill step：
1）Cottonseed Meal, corncob, wheat bran and edible mushroom bran are used into ultra-fine pulverizer disintegrating respectively, are ground into 40-80 mesh fine powders, is mixed
Close uniformly, obtain mixing fine powders A；
2）Step 1）Gained mixing fine powders A carbon-nitrogen ratios add suitable quantity of water and stir to water content 40-60%, prepare between 20-30
One grade fermemtation culture medium, controls pH value 6.8-7.5, and one grade fermemtation culture medium is inoculated with by yellow bent after 121 DEG C sterilize 15 minutes
The composite bacteria agent A that mould and unwrapping wire styreptomyces globispotus strain are formed, carries out level-one aerobic fermentation, and fermentation temperature is controlled at 30-37 DEG C, hair
One grade fermemtation liquid was made at 2-4 days in ferment time control；
3）By silkworm chrysalis, cicada slough, discarded animal skin after degreasing, drying, crushed using superfine technique, be ground into 40-80
Mesh fine powder, is uniformly mixed, obtains mixing fine powders B；
4）Step 3）Gained mixing fine powders B carbon-nitrogen ratios add suitable quantity of water and stir to water content 40-60%, prepare between 20-30
Second order fermentation culture medium, controls pH value 6.8-7.5, and second order fermentation culture medium coordinates after 121 DEG C sterilize 15 minutes and adds earthworm
Earthworm excrement, with step 2）Gained one grade fermemtation liquid is mixed, and prepares second order fermentation culture medium, inoculation photosynthetic bacteria, saccharomycete, fixed nitrogen
The composite bacteria agent B that bacillus is formed, carries out two level aerobic fermentation, at 28-41 DEG C, fermentation time control exists for fermentation temperature control
3-7 days, second order fermentation liquid is made, free amino acid nitrogen content reaches 20-25% in second order fermentation liquid, and effective total viable count is
107-109CFU/L；
5）Stop fermentation, centrifuge, collect filtrate, degerming removal of impurities, sequentially adds ferrous sulfate heptahydrate, white vitriol, one
Water manganese sulfate, cupric sulfate pentahydrate, add citric acid and fully chelate, control the chelatropic reaction time for 0.6-1.5 it is small when, pH is
7.0-9.0, temperature is 70-80 DEG C, after chelatropic reaction, it is filling, sterilize, pack it is above-mentioned that microelement type contains aminoacids solution
Body water-soluble fertilizer product.
The level-one aerobic fermentation process degrades the cell wall structure contained by one grade fermemtation culture medium, discharges intracellular
Inclusion, two level aerobic fermentation process further divide the cell wall structure after degraded and cell inclusion and second order fermentation culture medium
Solve as small molecule free amino acid.
Microelement type water-soluble fertilizer containing the amino-acid liquid technical target of the product produced according to above-mentioned processing step is such as
Under：The g/L of amino acid content >=100, the g/L of copper+iron+manganese+zinc >=20.
The present invention a kind of microelement type water-soluble fertilizer containing amino-acid liquid and its production technology compared with prior art,
Caused beneficial effect is,
1st, the present invention utilizes modern biotechnology inoculating compound bacterium agent A and composite bacteria agent B, the production work fermented using two-stage aerobic
Skill, small molecule free amine group is decomposed into by animal protein contained by vegetable protein contained by one grade fermemtation culture medium and secondary medium
Acid, wherein level-one aerobic fermentation process refer to degrade the cell wall structure contained by one grade fermemtation culture medium, discharge intracellular
Inclusion, two level aerobic fermentation process refer to the cell wall structure after degraded and cell inclusion and second order fermentation culture medium into one
Step be decomposed into small molecule free amino acid, by with trace element（Copper, iron, manganese, zinc, can also compound boron, molybdenum etc.）Chelating, prepares
Microelement type water-soluble fertilizer containing amino-acid liquid, microelement type water-soluble fertilizer containing the amino-acid liquid product technology produced
Index is as follows：The g/L of amino acid content >=100, the g/L of copper+iron+manganese+zinc >=20；As a result of inoculating compound bacterium agent A respectively
The technique that two-stage aerobic fermentation is carried out with composite bacteria agent B, whole process do not have high temperature and pressure and chemical reagent, thus to greatest extent
Ground is extracted natural active matter and the nutrition of available to plant contained in one grade fermemtation culture medium and second order fermentation culture medium
Component, can strengthen the anti-adversity abilities such as the drought resisting of plant, cold-resistant, disease and insect resistance；
2nd, the nutriment of the invention by adding suitable proportion in agricultural wastes, edible mushroom bran and discarded animal skin,
Microelement type water-soluble fertilizer containing amino-acid liquid is fermented into, further explores the condition of composite bacteria agent symbiosis, it is ensured that fertilizer
Material ideal effect after use, this can not only improve the cyclic utilization rate of waste resource, turn waste into wealth, and can save into
This, exerts far reaching influence modern agriculture；
3rd, the present invention makes produced fertilizer be easier to be absorbed by plants using sodium citrate, free amino acid as association complex
Utilize, the heavy metal chelate formed is readily biodegradable, and eco-toxicity is low, environment friendly and pollution-free；
4th, the microelement type water-soluble fertilizer containing amino-acid liquid produced using the present invention can reduce a few kiloton tradition inorganic fertilizer
Expect usage amount, compounding application wormcast, can further improve soil aggregate structure, be conducive to water conservation, fertilizer conservation, ventilation and promote root
System's development, comfortable growing environment is provided for plant, is improved for Ecological Environment and is provided technical support.
Embodiment
With reference to embodiment to the present invention a kind of microelement type water-soluble fertilizer containing amino-acid liquid and its
Production technology is described in detail below.
Embodiment one
A kind of microelement type water-soluble fertilizer containing amino-acid liquid, is 1 liter of calculating by the liquid water-soluble fertilizer total amount, it is formulated
Middle raw material composition and each component mass fraction are as follows：30 grams of Cottonseed Meal, 75 grams of corncob, 45 grams of wheat bran, edible 100 grams of mushroom bran,
15 grams of silkworm chrysalis, 32 grams of cicada slough, discarded 65 grams of animal skin, 15 grams of ferrous sulfate heptahydrate, 20 grams of cupric sulfate pentahydrate, white vitriol
32 grams, 20 grams of manganese sulfate monohydrate, 2 grams of composite bacteria agent A, 4 grams of composite bacteria agent B, 9 grams of wormcast, 5 grams of citric acid, sodium hydroxide 1
Gram, surplus is water.Wherein composite bacteria agent A is Aspergillus flavus and unwrapping wire styreptomyces globispotus strain in mass ratio 1:0.8 is combined, compound
Microbial inoculum B is photosynthetic bacteria, saccharomycete, bacillus azotobacter in mass ratio 0.5：1：:1 is combined.
A kind of production technology of microelement type water-soluble fertilizer containing amino-acid liquid, comprises the technical steps that：
1）Cottonseed Meal, corncob, wheat bran and edible mushroom bran are used into ultra-fine pulverizer disintegrating respectively, are ground into 40 mesh fine powders, is mixed
Uniformly, mixing fine powders A is obtained；
2）Step 1）Gained mixing fine powders A carbon-nitrogen ratios are 25, add suitable quantity of water and stir to water content 40%, prepare one grade fermemtation training
Base is supported, control pH values 6.8, one grade fermemtation culture medium is inoculated with by Aspergillus flavus and unwrapping wire ball spore after 121 DEG C sterilize 15 minutes
The composite bacteria agent A that streptomycete is formed, carries out level-one aerobic fermentation, and at 30 DEG C, fermentation time was controlled at 2 days for fermentation temperature control,
One grade fermemtation liquid is made；Above-mentioned level-one aerobic fermentation process degrades the cell wall structure contained by one grade fermemtation culture medium, release
Go out cell inclusion；
3）By silkworm chrysalis, cicada slough, discarded animal skin after degreasing, drying, crushed using superfine technique, it is thin to be ground into 40 mesh
Powder, is uniformly mixed, obtains mixing fine powders B；
4）Step 3）Gained mixing fine powders B carbon-nitrogen ratios are 20, add suitable quantity of water and stir to water content 40%, prepare second order fermentation training
Base, control pH values 6.8 are supported, second order fermentation culture medium coordinates after 121 DEG C sterilize 15 minutes and adds wormcast, with step 2）
Gained one grade fermemtation liquid is mixed, and prepares second order fermentation culture medium, and inoculation photosynthetic bacteria, saccharomycete, bacillus azotobacter are formed
Composite bacteria agent B, carry out two level aerobic fermentation, at 28 DEG C, fermentation time was controlled at 3 days for fermentation temperature control, and two level hair is made
Zymotic fluid, free amino acid nitrogen content reaches 20% in second order fermentation liquid, and effective total viable count is 5 × 107CFU/L；Above-mentioned two level
Aerobic fermentation process is further broken into small point to the cell wall structure after degraded and cell inclusion and second order fermentation culture medium
Sub- free amino acid；
5）Stop fermentation, centrifuge, collect filtrate, degerming removal of impurities, sequentially adds ferrous sulfate heptahydrate, white vitriol, one
Water manganese sulfate, cupric sulfate pentahydrate, add citric acid and fully chelate, control the chelatropic reaction time for 0.6 it is small when, pH 7, temperature
It is filling, sterilize, pack above-mentioned microelement type water-soluble fertilizer containing amino-acid liquid product after chelatropic reaction for 70 DEG C.
Embodiment two
A kind of microelement type water-soluble fertilizer containing amino-acid liquid, is 1 liter of calculating by the liquid water-soluble fertilizer total amount, it is formulated
Middle raw material composition and each component mass fraction are as follows：45 grams of Cottonseed Meal, 84 grams of corncob, 52 grams of wheat bran, edible 110 grams of mushroom bran,
14 grams of silkworm chrysalis, 40 grams of cicada slough, discarded 60 grams of animal skin, 21 grams of ferrous sulfate heptahydrate, 18 grams of cupric sulfate pentahydrate, white vitriol
25 grams, 25 grams of ten water Boratex, 25 grams of manganese sulfate monohydrate, 10 grams of ammonium molybdate tetrahydrate, 2.5 grams of composite bacteria agent A, composite bacteria agent B 5
Gram, 8 grams of wormcast, 4 grams of citric acid, 2 grams of potassium hydroxide, surplus is water.Wherein composite bacteria agent A is Aspergillus flavus and unwrapping wire ball spore
Streptomycete in mass ratio 1:1 is combined, and composite bacteria agent B is photosynthetic bacteria, saccharomycete, bacillus azotobacter in mass ratio 0.6：1：
1.2 it is combined.
A kind of production technology of microelement type water-soluble fertilizer containing amino-acid liquid, comprises the technical steps that：
1）Cottonseed Meal, corncob, wheat bran and edible mushroom bran are used into ultra-fine pulverizer disintegrating respectively, are ground into 60 mesh fine powders, is mixed
Uniformly, mixing fine powders A is obtained；
2）Step 1）Gained mixing fine powders A carbon-nitrogen ratios are 25, add suitable quantity of water and stir to water content 50%, prepare one grade fermemtation training
Base is supported, control pH values 7.0, one grade fermemtation culture medium is inoculated with by Aspergillus flavus and unwrapping wire ball spore after 121 DEG C sterilize 15 minutes
The composite bacteria agent A that streptomycete is formed, carries out level-one aerobic fermentation, and at 35 DEG C, fermentation time was controlled at 3 days for fermentation temperature control,
One grade fermemtation liquid is made；
3）By silkworm chrysalis, cicada slough, discarded animal skin after degreasing, drying, crushed using superfine technique, it is thin to be ground into 60 mesh
Powder, is uniformly mixed, obtains mixing fine powders B；
4）Step 3）Gained mixing fine powders B carbon nitrogen is 24, adds suitable quantity of water and stirs to water content 50%, prepares second order fermentation culture
Base, control pH values 7.0, second order fermentation culture medium coordinate after 121 DEG C sterilize 15 minutes and add wormcast, with step 2）Institute
Obtain one grade fermemtation liquid to be mixed, prepare second order fermentation culture medium, inoculation photosynthetic bacteria, saccharomycete, bacillus azotobacter are formed
Composite bacteria agent B, carries out two level aerobic fermentation, at 37 DEG C, fermentation time was controlled at 4 days for fermentation temperature control, and second order fermentation is made
Liquid, free amino acid nitrogen content reaches 22.5% in second order fermentation liquid, and effective total viable count is 2.7 × 108CFU/L；
5）Stop fermentation, centrifuge, collect filtrate, degerming removal of impurities, sequentially adds ferrous sulfate heptahydrate, white vitriol, one
Water manganese sulfate, cupric sulfate pentahydrate, add citric acid and fully chelate, control the chelatropic reaction time for 1 it is small when, pH 8.0, temperature
It is filling, sterilize, pack above-mentioned microelement type water-soluble fertilizer containing amino-acid liquid product after chelatropic reaction for 75 DEG C.
Embodiment three
A kind of microelement type water-soluble fertilizer containing amino-acid liquid, is 1 liter of calculating by the liquid water-soluble fertilizer total amount, it is formulated
Middle raw material composition and each component mass fraction are as follows：60 grams of Cottonseed Meal, 90 grams of corncob, 60 grams of wheat bran, edible 120 grams of mushroom bran,
20 grams of silkworm chrysalis, 30 grams of cicada slough, discarded 40 grams of animal skin, 13 grams of ferrous sulfate heptahydrate, 24 grams of cupric sulfate pentahydrate, white vitriol
30 grams, 5 grams of ten water Boratex, 18 grams of manganese sulfate monohydrate, 3 grams of composite bacteria agent A, 6 grams of composite bacteria agent B, 8 grams of wormcast, lemon
6 grams of acid, 2 grams of potassium hydroxide, 3 grams of disodium hydrogen phosphate, surplus is water.Wherein composite bacteria agent A is Aspergillus flavus and unwrapping wire ball spore chain
Mould in mass ratio 1:1 is combined, and composite bacteria agent B is photosynthetic bacteria, saccharomycete, bacillus azotobacter in mass ratio 0.6：1：
1.1 it is combined.
A kind of production technology of microelement type water-soluble fertilizer containing amino-acid liquid, comprises the technical steps that：
1）Cottonseed Meal, corncob, wheat bran and edible mushroom bran are used into ultra-fine pulverizer disintegrating respectively, are ground into 60 mesh fine powders, is mixed
Uniformly, mixing fine powders A is obtained；
2）Step 1）Gained mixing fine powders A carbon-nitrogen ratios are 27, add suitable quantity of water and stir to water content 60%, prepare one grade fermemtation training
Base is supported, control pH values 7.5, one grade fermemtation culture medium is inoculated with by Aspergillus flavus and unwrapping wire ball spore after 121 DEG C sterilize 15 minutes
The composite bacteria agent A that streptomycete is formed, carries out level-one aerobic fermentation, and at 37 DEG C, fermentation time was controlled at 4 days for fermentation temperature control,
One grade fermemtation liquid is made；
3）By silkworm chrysalis, cicada slough, discarded animal skin after degreasing, drying, crushed using superfine technique, it is thin to be ground into 60 mesh
Powder, is uniformly mixed, obtains mixing fine powders B；
4）Step 3）Gained mixing fine powders B carbon-nitrogen ratios are 25, add suitable quantity of water and stir to water content 60%, prepare second order fermentation training
Base, control pH values 7.5 are supported, second order fermentation culture medium coordinates after 121 DEG C sterilize 15 minutes and adds wormcast, with step 2）
Gained one grade fermemtation liquid is mixed, and prepares second order fermentation culture medium, and inoculation photosynthetic bacteria, saccharomycete, bacillus azotobacter are formed
Composite bacteria agent B, carry out two level aerobic fermentation, at 41 DEG C, fermentation time was controlled at 5 days for fermentation temperature control, and two level hair is made
Zymotic fluid, free amino acid nitrogen content reaches 25% in second order fermentation liquid, and effective total viable count is 5 × 108CFU/L；
5）Stop fermentation, centrifuge, collect filtrate, degerming removal of impurities, sequentially adds ferrous sulfate heptahydrate, white vitriol, one
Water manganese sulfate, cupric sulfate pentahydrate, add citric acid and fully chelate, control the chelatropic reaction time for 1.5 it is small when, pH 9.0, temperature
Spend for 80 DEG C, it is filling, sterilize, pack above-mentioned microelement type water-soluble fertilizer containing amino-acid liquid and produce after chelatropic reaction
Product.
Example IV
A kind of microelement type water-soluble fertilizer containing amino-acid liquid, is 1 liter of calculating by the liquid water-soluble fertilizer total amount, it is formulated
Middle raw material composition and each component mass fraction are as follows：50 grams of Cottonseed Meal, 80 grams of corncob, 45 grams of wheat bran, edible 105 grams of mushroom bran,
16 grams of silkworm chrysalis, 50 grams of cicada slough, discarded 75 grams of animal skin, 18 grams of ferrous sulfate heptahydrate, 17 grams of cupric sulfate pentahydrate, white vitriol
23 grams, 10 grams of ten water Boratex, 22 grams of manganese sulfate monohydrate, 8 grams of ammonium molybdate tetrahydrate, 2 grams of composite bacteria agent A, composite bacteria agent B 4.5
Gram, 9 grams of wormcast, 4.5 grams of citric acid, 2 grams of sodium hydroxide, 2 grams of disodium hydrogen phosphate, surplus be water.Wherein composite bacteria agent A is Huang
Aspergillus and unwrapping wire styreptomyces globispotus strain in mass ratio 1:1 is combined, and composite bacteria agent B is photosynthetic bacteria, saccharomycete, fixed nitrogen gemma bar
Bacterium in mass ratio 0.6：1：1.2 it is combined.
A kind of production technology of microelement type water-soluble fertilizer containing amino-acid liquid, comprises the technical steps that：
1）Cottonseed Meal, corncob, wheat bran and edible mushroom bran are used into ultra-fine pulverizer disintegrating respectively, are ground into 80 mesh fine powders, is mixed
Uniformly, mixing fine powders A is obtained；
2）Step 1）Gained mixing fine powders A carbon-nitrogen ratios are 20, add suitable quantity of water and stir to water content 60%, prepare one grade fermemtation training
Base is supported, control pH values 6.8, one grade fermemtation culture medium is inoculated with by Aspergillus flavus and unwrapping wire ball spore after 121 DEG C sterilize 15 minutes
The composite bacteria agent A that streptomycete is formed, carries out level-one aerobic fermentation, and at 37 DEG C, fermentation time was controlled at 2 days for fermentation temperature control,
One grade fermemtation liquid is made；
3）By silkworm chrysalis, cicada slough, discarded animal skin after degreasing, drying, crushed using superfine technique, it is thin to be ground into 80 mesh
Powder, is uniformly mixed, obtains mixing fine powders B；
4）Step 3）Gained mixing fine powders B carbon-nitrogen ratios are 30, add suitable quantity of water and stir to water content 60%, prepare second order fermentation training
Base, control pH values 7.0 are supported, second order fermentation culture medium coordinates after 121 DEG C sterilize 15 minutes and adds wormcast, with step 2）
Gained one grade fermemtation liquid is mixed, and prepares second order fermentation culture medium, and inoculation photosynthetic bacteria, saccharomycete, bacillus azotobacter are formed
Composite bacteria agent B, carry out two level aerobic fermentation, at 32 DEG C, fermentation time was controlled at 6 days for fermentation temperature control, and two level hair is made
Zymotic fluid, free amino acid nitrogen content reaches 20% in second order fermentation liquid, and effective total viable count is 107CFU/L；
5）Stop fermentation, centrifuge, collect filtrate, degerming removal of impurities, sequentially adds ferrous sulfate heptahydrate, white vitriol, one
Water manganese sulfate, cupric sulfate pentahydrate, add citric acid and fully chelate, control the chelatropic reaction time for 1 it is small when, pH 9.0, temperature
It is filling, sterilize, pack above-mentioned microelement type water-soluble fertilizer containing amino-acid liquid product after chelatropic reaction for 80 DEG C.
Embodiment five
A kind of microelement type water-soluble fertilizer containing amino-acid liquid, is 1 liter of calculating by the liquid water-soluble fertilizer total amount, it is formulated
Middle raw material composition and each component mass fraction are as follows：30 grams of Cottonseed Meal, 75 grams of corncob, 45 grams of wheat bran, edible 112 grams of mushroom bran,
10 grams of silkworm chrysalis, 40 grams of cicada slough, discarded 80 grams of animal skin, 13 grams of ferrous sulfate heptahydrate, 16 grams of cupric sulfate pentahydrate, white vitriol
23 grams, 27 grams of manganese sulfate monohydrate, 6 grams of ammonium molybdate tetrahydrate, 2.5 grams of composite bacteria agent A, 5 grams of composite bacteria agent B, 10 grams of wormcast, lemon
4 grams of lemon acid, 0.5 gram of sodium hydroxide, 0.5 gram of potassium hydroxide, 1 gram of disodium hydrogen phosphate, surplus is water.Wherein composite bacteria agent A is Huang
Aspergillus and unwrapping wire styreptomyces globispotus strain in mass ratio 1:1.5 are combined, and composite bacteria agent B is photosynthetic bacteria, saccharomycete, fixed nitrogen bud
Spore bacillus in mass ratio 0.8：1：1.2 it is combined.
A kind of production technology of microelement type water-soluble fertilizer containing amino-acid liquid, comprises the technical steps that：
1）Cottonseed Meal, corncob, wheat bran and edible mushroom bran are used into ultra-fine pulverizer disintegrating respectively, are ground into 50 mesh fine powders, is mixed
Uniformly, mixing fine powders A is obtained；
2）Step 1）Gained mixing fine powders A carbon-nitrogen ratios are 30, add suitable quantity of water and stir to water content 45%, prepare one grade fermemtation training
Base is supported, control pH values 7.0, one grade fermemtation culture medium is inoculated with by Aspergillus flavus and unwrapping wire ball spore after 121 DEG C sterilize 15 minutes
The composite bacteria agent A that streptomycete is formed, carries out level-one aerobic fermentation, and at 32 DEG C, fermentation time was controlled at 3 days for fermentation temperature control,
One grade fermemtation liquid is made；
3）By silkworm chrysalis, cicada slough, discarded animal skin after degreasing, drying, crushed using superfine technique, it is thin to be ground into 50 mesh
Powder, is uniformly mixed, obtains mixing fine powders B；
4）Step 3）Gained mixing fine powders B carbon-nitrogen ratios are 28, add suitable quantity of water and stir to water content 45%, prepare second order fermentation training
Base, control pH values 7.5 are supported, second order fermentation culture medium coordinates after 121 DEG C sterilize 15 minutes and adds wormcast, with step 2）
Gained one grade fermemtation liquid is mixed, and prepares second order fermentation culture medium, and inoculation photosynthetic bacteria, saccharomycete, bacillus azotobacter are formed
Composite bacteria agent B, carry out two level aerobic fermentation, at 37 DEG C, fermentation time was controlled at 7 days for fermentation temperature control, and two level hair is made
Zymotic fluid, free amino acid nitrogen content reaches 25% in second order fermentation liquid, and effective total viable count is 109CFU/L；
5）Stop fermentation, centrifuge, collect filtrate, degerming removal of impurities, sequentially adds ferrous sulfate heptahydrate, white vitriol, one
Water manganese sulfate, cupric sulfate pentahydrate, add citric acid and fully chelate, control the chelatropic reaction time for 1 it is small when, pH 8.0, temperature
It is filling, sterilize, pack above-mentioned microelement type water-soluble fertilizer containing amino-acid liquid product after chelatropic reaction for 75 DEG C.
Embodiment six
A kind of microelement type water-soluble fertilizer containing amino-acid liquid, is 1 liter of calculating by the liquid water-soluble fertilizer total amount, it is formulated
Middle raw material composition and each component mass fraction are as follows：48 grams of Cottonseed Meal, 82 grams of corncob, 50 grams of wheat bran, edible 107 grams of mushroom bran,
12 grams of silkworm chrysalis, 45 grams of cicada slough, discarded 70 grams of animal skin, 20 grams of ferrous sulfate heptahydrate, 16 grams of cupric sulfate pentahydrate, white vitriol
24 grams, 15 grams of ten water Boratex, 24 grams of manganese sulfate monohydrate, 5 grams of ammonium molybdate tetrahydrate, 2 grams of composite bacteria agent A, 4 grams of composite bacteria agent B,
8.5 grams of wormcast, 5 grams of citric acid, 1 gram of sodium hydroxide, 2 grams of potassium hydroxide, surplus is water.Wherein composite bacteria agent A is aspergillus flavus
Bacterium and unwrapping wire styreptomyces globispotus strain in mass ratio 1:1 is combined, and composite bacteria agent B is photosynthetic bacteria, saccharomycete, bacillus azotobacter are pressed
Mass ratio 0.6：1：1.2 it is combined.
A kind of production technology of microelement type water-soluble fertilizer containing amino-acid liquid, comprises the technical steps that：
1）Cottonseed Meal, corncob, wheat bran and edible mushroom bran are used into ultra-fine pulverizer disintegrating respectively, are ground into 70 mesh fine powders, is mixed
Uniformly, mixing fine powders A is obtained；
2）Step 1）Gained mixing fine powders A carbon-nitrogen ratios are 22, add suitable quantity of water and stir to water content 40%, prepare one grade fermemtation training
Base is supported, control pH values 7.0, one grade fermemtation culture medium is inoculated with by Aspergillus flavus and unwrapping wire ball spore after 121 DEG C sterilize 15 minutes
The composite bacteria agent A that streptomycete is formed, carries out level-one aerobic fermentation, and at 36 DEG C, fermentation time was controlled at 2 days for fermentation temperature control,
One grade fermemtation liquid is made；
3）By silkworm chrysalis, cicada slough, discarded animal skin after degreasing, drying, crushed using superfine technique, it is thin to be ground into 70 mesh
Powder, is uniformly mixed, obtains mixing fine powders B；
4）Step 3）Gained mixing fine powders B carbon-nitrogen ratios are 30, add suitable quantity of water and stir to water content 40%, prepare second order fermentation training
Base, control pH values 7.5 are supported, second order fermentation culture medium coordinates after 121 DEG C sterilize 15 minutes and adds wormcast, with step 2）
Gained one grade fermemtation liquid is mixed, and prepares second order fermentation culture medium, and inoculation photosynthetic bacteria, saccharomycete, bacillus azotobacter are formed
Composite bacteria agent B, carry out two level aerobic fermentation, at 37 DEG C, fermentation time was controlled at 5 days for fermentation temperature control, and two level hair is made
Zymotic fluid, free amino acid nitrogen content reaches 20% in second order fermentation liquid, and effective total viable count is 109CFU/L；
5）Stop fermentation, centrifuge, collect filtrate, degerming removal of impurities, sequentially adds ferrous sulfate heptahydrate, white vitriol, one
Water manganese sulfate, cupric sulfate pentahydrate, add citric acid and fully chelate, control the chelatropic reaction time for 0.6 it is small when, pH 7.0, temperature
Spend for 70 DEG C, it is filling, sterilize, pack above-mentioned microelement type water-soluble fertilizer containing amino-acid liquid and produce after chelatropic reaction
Product.
Field trial example
In order to test a kind of effect of microelement type water-soluble fertilizer containing amino-acid liquid of the present invention in production, the present invention is made
The fertilizer of work is used for the field trial of crop, specifically tests basic condition：
Test soil：Northern brown earth
Test process：A kind of microelement type water-soluble fertilizer containing amino-acid liquid prepared using embodiment one to embodiment six,
Trial crops are sprayed by the way of pouring root, sprinkling irrigation use after diluting 1000-1500 times with clear water.Since seedling stage,
Sprayed every 7-10 days once, the plant difference stage of growth respectively sprays 1 time, suitable for industrial crops such as flowers, fruit tree, vegetables.
Spraying time best results after 4 points in the afternoon.It should not be sprayed when wind, rain, greasy weather or too strong sunlight.Rain after spray, fill spray one
It is secondary.
Result of the test：Crop has obvious effect of increasing production.The crop yield such as citrus, apple, grape, "Hami" melon 20-
28%, fruit growth is accelerated, the maturity period shifts to an earlier date, and color and luster is good, full of nutrition, recovers former fragrance, uniform coloring, and fruit grade carries
Height, disease resistance enhancing.The crop yields such as Jasmine, rose increase 20-25%, make flowers keep pattern bright-coloured, extend flower
Phase.The soil property content of organic matter can be improved at the same time, prevent soil hardening, improve soil aggregate structure, promote root system development, enhancing is planted
The anti-adversity abilities such as the drought resisting of thing, cold-resistant, disease and insect resistance.
Claims (6)
1. a kind of microelement type water-soluble fertilizer containing amino-acid liquid, it is characterised in that be by the liquid water-soluble fertilizer total amount
1 liter of calculating, raw material composition and each component mass fraction are as follows during it is formulated：30-60 grams of Cottonseed Meal, 75-90 grams of corncob, wheat bran
45-60 grams, edible 100-120 grams of mushroom bran, 10-20 grams of silkworm chrysalis, 30-50 grams of cicada slough, discarded 40-80 grams of animal skin, seven water sulphur
Sour 13-21 grams ferrous, 18-27 grams of cupric sulfate pentahydrate, 16-24 grams of white vitriol, 23-32 grams of manganese sulfate monohydrate, ten water boric acid
0-25 grams of sodium, 0-10 grams of ammonium molybdate tetrahydrate, composite bacteria agent A 2-3 gram, composite bacteria agent B 4-6 gram, 8-10 grams of wormcast, citric acid
4-6 grams, 1-5 grams of pH adjusting agent, surplus are water；
Wherein composite bacteria agent A is Aspergillus flavus and unwrapping wire styreptomyces globispotus strain in mass ratio 1:0.8-1.5 is combined, composite bacteria agent
B is photosynthetic bacteria, saccharomycete, bacillus azotobacter 0.5-0. 8 in mass ratio：1：1-1.2 it is combined.
2. a kind of microelement type water-soluble fertilizer containing amino-acid liquid according to claim 1, it is characterised in that by described
Liquid water-soluble fertilizer total amount is 1 liter of calculating, and raw material composition and each component mass fraction are as follows during it is formulated：45-50 grams of Cottonseed Meal,
80-84 grams of corncob, 45-52 grams of wheat bran, edible 105-110 grams of mushroom bran, 12-16 grams of silkworm chrysalis, 40-50 grams of cicada slough, discarded animal
60-75 grams of fur, 18-21 grams of ferrous sulfate heptahydrate, 16-18 grams of cupric sulfate pentahydrate, 23-25 grams of white vitriol, sulfuric acid monohydrate
22-25 grams of manganese, ten 10-25 grams of water Boratexes, 5-10 grams of ammonium molybdate tetrahydrate, composite bacteria agent A 2-2.5 gram, composite bacteria agent B 4-5
Gram, 8-9 grams of wormcast, 4-5 grams of citric acid, 2-4 grams of pH adjusting agent, surplus is water；
Wherein composite bacteria agent A is Aspergillus flavus and unwrapping wire styreptomyces globispotus strain in mass ratio 1:1 is combined, and composite bacteria agent B is light
Close bacterium, saccharomycete, bacillus azotobacter in mass ratio 0.6：1：1.2 it is combined.
A kind of 3. microelement type water-soluble fertilizer containing amino-acid liquid according to claim 1 or 2, it is characterised in that institute
PH adjusting agent is stated as the one or more in sodium hydroxide, potassium hydroxide, disodium hydrogen phosphate.
4. a kind of production technology of microelement type water-soluble fertilizer containing amino-acid liquid, it is characterised in that walked including following technique
Suddenly：
1）Cottonseed Meal, corncob, wheat bran and edible mushroom bran are used into ultra-fine pulverizer disintegrating respectively, are ground into 40-80 mesh fine powders, is mixed
Close uniformly, obtain mixing fine powders A；
2）Step 1）Gained mixing fine powders A carbon-nitrogen ratios add suitable quantity of water and stir to water content 40-60%, prepare between 20-30
One grade fermemtation culture medium, controls pH value 6.8-7.5, and one grade fermemtation culture medium is inoculated with by yellow bent after 121 DEG C sterilize 15 minutes
The composite bacteria agent A that mould and unwrapping wire styreptomyces globispotus strain are formed, carries out level-one aerobic fermentation, and fermentation temperature is controlled at 30-37 DEG C, hair
One grade fermemtation liquid was made at 2-4 days in ferment time control；
3）By silkworm chrysalis, cicada slough, discarded animal skin after degreasing, drying, crushed using superfine technique, be ground into 40-80
Mesh fine powder, is uniformly mixed, obtains mixing fine powders B；
4）Step 3）Gained mixing fine powders B carbon-nitrogen ratios add suitable quantity of water and stir to water content 40-60%, prepare between 20-30
Second order fermentation culture medium, controls pH value 6.8-7.5, and second order fermentation culture medium coordinates after 121 DEG C sterilize 15 minutes and adds earthworm
Earthworm excrement, with step 2）Gained one grade fermemtation liquid is mixed, and prepares second order fermentation culture medium, inoculation photosynthetic bacteria, saccharomycete, fixed nitrogen
The composite bacteria agent B that bacillus is formed, carries out two level aerobic fermentation, at 28-41 DEG C, fermentation time control exists for fermentation temperature control
3-7 days, second order fermentation liquid is made, free amino acid nitrogen content reaches 20-25% in second order fermentation liquid, and effective total viable count is
107-109CFU/L；
5）Stop fermentation, centrifuge, collect filtrate, degerming removal of impurities, sequentially adds ferrous sulfate heptahydrate, white vitriol, one
Water manganese sulfate, cupric sulfate pentahydrate, add citric acid and fully chelate, control the chelatropic reaction time for 0.6-1.5 it is small when, pH is
7.0-9.0, temperature is 70-80 DEG C, after chelatropic reaction, it is filling, sterilize, pack it is above-mentioned that microelement type contains aminoacids solution
Body water-soluble fertilizer product.
5. a kind of production technology of microelement type water-soluble fertilizer containing amino-acid liquid according to claim 4, its feature
It is, the level-one aerobic fermentation process degrades the cell wall structure contained by one grade fermemtation culture medium, discharges cell and includes
Thing, two level aerobic fermentation process further decompose the cell wall structure after degraded and cell inclusion and second order fermentation culture medium
For small molecule free amino acid.
6. a kind of production technology of microelement type water-soluble fertilizer containing amino-acid liquid according to claim 4 or 5, it is special
Sign is that the water-soluble fertilizer product technical indicator of liquid is as follows：The g/L of amino acid content >=100, copper+iron+manganese+zinc >=20
g/L。
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108640719A (en) * | 2018-06-27 | 2018-10-12 | 安徽瑞然生物药肥科技有限公司 | A kind of preparation method of amino acid foliage fertilizer |
| CN108863606A (en) * | 2018-09-03 | 2018-11-23 | 安徽省文胜生物工程股份有限公司 | A kind of preparation method of high-concentration biological bacterium amino acid water-soluble fertilizer |
| CN108947658A (en) * | 2018-07-26 | 2018-12-07 | 陈云 | Amino acid Water soluble fertilizer and preparation method thereof |
| CN110218107A (en) * | 2019-07-01 | 2019-09-10 | 潘凤芝 | A kind of nutrient solution and its production technology containing microelement |
| CN110776350A (en) * | 2018-07-13 | 2020-02-11 | 郑向阳 | Multi-element functional fertilizer |
| CN112390682A (en) * | 2020-11-18 | 2021-02-23 | 苏宇鑫 | Preparation process of water-soluble fertilizer containing biological bacteria |
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2017
- 2017-12-22 CN CN201711400892.4A patent/CN107935783A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108640719A (en) * | 2018-06-27 | 2018-10-12 | 安徽瑞然生物药肥科技有限公司 | A kind of preparation method of amino acid foliage fertilizer |
| CN110776350A (en) * | 2018-07-13 | 2020-02-11 | 郑向阳 | Multi-element functional fertilizer |
| CN108947658A (en) * | 2018-07-26 | 2018-12-07 | 陈云 | Amino acid Water soluble fertilizer and preparation method thereof |
| CN108863606A (en) * | 2018-09-03 | 2018-11-23 | 安徽省文胜生物工程股份有限公司 | A kind of preparation method of high-concentration biological bacterium amino acid water-soluble fertilizer |
| CN110218107A (en) * | 2019-07-01 | 2019-09-10 | 潘凤芝 | A kind of nutrient solution and its production technology containing microelement |
| CN112390682A (en) * | 2020-11-18 | 2021-02-23 | 苏宇鑫 | Preparation process of water-soluble fertilizer containing biological bacteria |
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