CN107916463A - 一种新型抗菌袜 - Google Patents

一种新型抗菌袜 Download PDF

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CN107916463A
CN107916463A CN201610885984.5A CN201610885984A CN107916463A CN 107916463 A CN107916463 A CN 107916463A CN 201610885984 A CN201610885984 A CN 201610885984A CN 107916463 A CN107916463 A CN 107916463A
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copper
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虞剑
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Hangzhou Fish Non Fish Textile Co Ltd
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    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
    • D01F6/90—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyamides
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00—General methods for the manufacture of artificial filaments or the like
    • D01F1/02—Addition of substances to the spinning solution or to the melt
    • D01F1/10—Other agents for modifying properties
    • D01F1/103—Agents inhibiting growth of microorganisms
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
    • D01F2/06—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from viscose
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04C—BRAIDING OR MANUFACTURE OF LACE, INCLUDING BOBBIN-NET OR CARBONISED LACE; BRAIDING MACHINES; BRAID; LACE
    • D04C1/00—Braid or lace, e.g. pillow-lace; Processes for the manufacture thereof
    • D04C1/02—Braid or lace, e.g. pillow-lace; Processes for the manufacture thereof made from particular materials
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04C—BRAIDING OR MANUFACTURE OF LACE, INCLUDING BOBBIN-NET OR CARBONISED LACE; BRAIDING MACHINES; BRAID; LACE
    • D04C1/00—Braid or lace, e.g. pillow-lace; Processes for the manufacture thereof
    • D04C1/06—Braid or lace serving particular purposes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
    • D06M10/04—Physical treatment combined with treatment with chemical compounds or elements
    • D06M10/06—Inorganic compounds or elements
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/34—Polyamides
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
    • D10B2201/20—Cellulose-derived artificial fibres
    • D10B2201/22—Cellulose-derived artificial fibres made from cellulose solutions
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
    • D10B2201/20—Cellulose-derived artificial fibres
    • D10B2201/22—Cellulose-derived artificial fibres made from cellulose solutions
    • D10B2201/24—Viscose
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
    • D10B2201/20—Cellulose-derived artificial fibres
    • D10B2201/28—Cellulose esters or ethers, e.g. cellulose acetate
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/02—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyamides
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/10—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyurethanes
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2401/00—Physical properties
    • D10B2401/06—Load-responsive characteristics
    • D10B2401/061—Load-responsive characteristics elastic
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    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2401/00—Physical properties
    • D10B2401/13—Physical properties anti-allergenic or anti-bacterial
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    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2501/00—Wearing apparel
    • D10B2501/02—Underwear
    • D10B2501/021—Hosiery; Panti-hose

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
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  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Artificial Filaments (AREA)
  • Socks And Pantyhose (AREA)

Abstract

一种新型抗菌袜采用再生纤维素纤维、锦纶铜纤维和氨纶结合，是袜子具备良好的抗菌吸汗效果，并且袜子内加入氨纶是袜子的定型与回弹效果更加理想，而袜子内的锦纶同纤维采用高声波技术安全环保，袜子抗菌性能超过洗涤50次的国家最高标准，吸湿性能也能超过洗涤10的国家最高标准。

Description

一种新型抗菌袜
技术领域
本发明涉及抗菌袜领域，具体涉及一种新型抗菌袜，具备良好的抗菌吸汗效果。
背景技术
袜子是人们生活中不可缺少的生活用品，起着保护脚和美化脚的作用。袜子生产是我国针织工业的一个重要组成部分。袜子要求穿着舒适，具有良好的透气性。如果穿着透气性能不好的袜子，脚部会感到闷热、潮湿、非常难受，还容易滋生细菌，诱发脚气、脚藓等脚部疾病。
已知国内注册105696112A一种铜离子抗菌袜，按照以下步骤进行制备 ：将硝酸银、硝酸铜和硝酸铈配置成溶液 A 加入壳聚糖，恒温搅拌得到铜离子抗菌剂 ；将铜离子抗菌剂、山梨酸、聚酯、纳米二氧化钛、纳米氧化锌、茶多酚、β- 环糊精挤出造粒得到铜离子抗菌母粒 ；将铜离子抗菌母粒与锦纶切片纺丝得到铜离子抗菌锦纶纤维 ；将铜离子抗菌锦纶纤维与精梳棉混合编织得到所述铜离子抗菌袜，所述铜离子抗菌袜中，铜离子抗菌锦纶纤维的含量为12-20％，精梳棉的含量为80-88％，该抗菌袜主要由铜离子抗菌锦纶纤维和精梳棉组成，在日常使用中，袜子再洗涤后袜子内的铜离子抗菌锦纶纤维损耗严重，抗菌效果流失较快，增加使用成本。
本发明内容
为解决现有技术不足，本发明提供了一种新型抗菌袜，采用高频超声波技术，有效提高抗菌袜使用寿命，延长抗菌效果。
一种新型抗菌袜，包括再生纤维素纤维、锦纶铜纤维和氨纶，所述锦纶铜纤维包括铜离子抗菌母粒与锦纶，所述锦纶铜纤维制备方法与现有技术相同为：
1、将硝酸银、硝酸铜和硝酸铈加入100重量份水中配置成溶液A，其中，溶液A中，硝酸银的浓度为1 .5-2 .5mmol/L，硝酸铜的浓度为0 .2-0 .4mmol/L，硝酸铈的浓度为0 .1-0.5mmol/L，然后加入0 .8-1 .5重量份壳聚糖，在40-55℃下恒温搅拌3-4 .5h，经抽滤、干燥、研磨得到铜离子抗菌剂；
2、按重量份将5-20份铜离子抗菌剂、0 .5-3份山梨酸、30-50份聚酯、2-10份纳米二氧化钛、3-10份纳米氧化锌、2-8份茶多酚、3-10份β-环糊精加入双螺杆挤出机中挤出造粒得到铜离子抗菌母粒；
3、将铜离子抗菌母粒与锦纶切片纺丝得到锦纶铜纤维；
所述再生纤维素纤维制备方法与现有技术相同为：
采用碱溶液法制备纺丝液并升温至 10-30℃；然后向其中加入纳米纤维素并分散均匀，所述纳米纤维素质量相当于所述纺丝液中纤维素原料质量的 0.01-5％，所述纳米纤维素长度≤ 5μm，长径比≥ 50，然后进行湿法纺丝得到初生纤维素纤维，再将所述初生纤维素纤维制备成再生纤维素纤维；
最后将再生纤维素纤维、锦纶铜纤维和氨纶通过编织工艺制成袜子，其特征在于，其中再生纤维素纤维含42.5％，锦纶铜纤维含49.5％，氨纶含8％。
进一步的，所述再生纤维素纤维包括粘胶纤维，醋酸纤维和铜铵纤维中的任意一种。
进一步的，所述锦纶铜纤维制备方法包括：通过高频超声波技术将含铜离子矿物质和亲水活性矿物质结合，再通过整理法制成锦纶铜纤维素。
进一步的，所述后整理法为采用抗菌液对纤维进行浸渍或浸轧，通过高温焙烘或其他方法将抗菌剂固定在纤维上的方法。
本发明对比现有技术所具有的增益效果是：
本发明一种新型抗菌袜采用再生纤维素纤维、锦纶铜纤维和氨纶结合，是袜子具备良好的抗菌吸汗效果，并且袜子内加入氨纶是袜子的定型与回弹效果更加理想，而袜子内的锦纶同纤维采用高声波技术安全环保，袜子抗菌性能超过洗涤50次的国家最高标准，吸湿性能也能超过洗涤10的国家最高标准。
具体实施方式
本发明提出的一种新型抗菌袜；
锦纶铜离子纤维素制备方法：
1、将硝酸银、硝酸铜和硝酸铈加入100重量份水中配置成溶液A，其中，溶液A中，硝酸银的浓度为1 .5mmol/L，硝酸铜的浓度为0 .4mmol/L，硝酸铈的浓度为0 .1mmol/L，然后加入1 .5重量份壳聚糖，在40℃下恒温搅拌4 .5h，经抽滤、干燥、研磨得到铜离子抗菌剂；
2、按重量份将5份铜离子抗菌剂、3份山梨酸、30份聚酯、10份纳米二氧化钛、3份纳米氧化锌、8份茶多酚、3份β-环糊精加入双螺杆挤出机中挤出造粒得到铜离子抗菌母粒；
3、将铜离子抗菌母粒与锦纶切片纺丝得到铜离子抗菌锦纶纤维；
再生纤维素纤维制备方法：
采用碱溶液法制备纺丝液并升温至 10-30℃；然后向其中加入纳米纤维素并分散均匀，所述纳米纤维素质量相当于所述纺丝液中纤维素原料质量的 0.01-5％，所述纳米纤维素长度≤ 5μm，长径比≥ 50，然后进行湿法纺丝得到初生纤维素纤维，再将所述初生纤维素纤维制备成再生纤维素纤维；
采用编织机将含再生纤维素纤维42.5％，锦纶铜纤维49.5％，氨纶含8％编织。
其中锦纶铜离子纤维素的制备方法还包括：通过高频超声波技术将含铜离子矿物质和亲水活性矿物质结合，再通过整理法制成锦纶铜纤维素。
众所周知，抗菌袜内包含抗菌分子，而洗涤后抗菌分子容易丢失，洗涤数次之后抗菌性能大大降低，本发明采用超声波技术与后整理法技术，提高了铜离子纤维素与锦纶之间的牢固性，增加使用寿命，在不妨碍抗菌抑菌效果的同时，更加耐用，降低使用成本，使用次数超国家最高标准。

Claims (4)

1.一种新型抗菌袜，包括再生纤维素纤维、锦纶铜纤维和氨纶，所述锦纶铜纤维包括铜离子抗菌母粒与锦纶，所述锦纶铜纤维制备方法与现有技术相同为：
1）、将硝酸银、硝酸铜和硝酸铈加入100重量份水中配置成溶液A，其中，溶液A中，硝酸银的浓度为1 .5-2 .5mmol/L，硝酸铜的浓度为0 .2-0 .4mmol/L，硝酸铈的浓度为0 .1-0.5mmol/L，然后加入0 .8-1 .5重量份壳聚糖，在40-55℃下恒温搅拌3-4 .5h，经抽滤、干燥、研磨得到铜离子抗菌剂；
2）、按重量份将5-20份铜离子抗菌剂、0 .5-3份山梨酸、30-50份聚酯、2-10份纳米二氧化钛、3-10份纳米氧化锌、2-8份茶多酚、3-10份β-环糊精加入双螺杆挤出机中挤出造粒得到铜离子抗菌母粒；
3）、将铜离子抗菌母粒与锦纶切片纺丝得到锦纶铜纤维；
所述再生纤维素纤维制备方法与现有技术相同为：
采用碱溶液法制备纺丝液并升温至 10-30℃；然后向其中加入纳米纤维素并分散均匀，所述纳米纤维素质量相当于所述纺丝液中纤维素原料质量的 0.01-5％，所述纳米纤维素长度≤ 5μm，长径比≥ 50，然后进行湿法纺丝得到初生纤维素纤维，再将所述初生纤维素纤维制备成再生纤维素纤维；
最后将再生纤维素纤维、锦纶铜纤维和氨纶通过编织工艺制成袜子，其特征在于，其中再生纤维素纤维含42.5％，锦纶铜纤维含49.5％，氨纶含8％。
2.进一步的，所述再生纤维素纤维包括粘胶纤维，醋酸纤维和铜铵纤维中的任意一种。
3.根据权利要求1所述一种新型抗菌袜，其特征在于所述锦纶铜纤维制备方法包括：通过高频超声波技术将含铜离子矿物质和亲水活性矿物质结合，再通过整理法制成锦纶铜纤维素。
4.根据权利要求1所述一种新型抗菌袜，其特征在于所述后整理法为采用抗菌液对纤维进行浸渍或浸轧，通过高温焙烘或其他方法将抗菌剂固定在纤维上的方法。
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109957868A (zh) * 2019-04-03 2019-07-02 广州哥伦布科技发展有限公司 一种抗菌面料、其制备方法及其应用
CN111172615A (zh) * 2020-01-20 2020-05-19 天津科技大学 一种湿法纺丝制备的阻燃性纳米纤维素复合纤维及其制备工艺
WO2021126132A1 (en) * 2019-12-18 2021-06-24 Bony Teksti̇l İşletmeleri̇ Sanayi̇ Ve Ti̇caret Anoni̇m Şi̇rketi̇ A sock structure with cellulosic acetate sustainable content
CN113403726A (zh) * 2021-07-07 2021-09-17 杭州宽明纺织有限公司 一种抗菌功能面料及其生产工艺

Citations (2)

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