CN107827544A - A kind of production method of the comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition - Google Patents
A kind of production method of the comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition Download PDFInfo
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- CN107827544A CN107827544A CN201711017351.3A CN201711017351A CN107827544A CN 107827544 A CN107827544 A CN 107827544A CN 201711017351 A CN201711017351 A CN 201711017351A CN 107827544 A CN107827544 A CN 107827544A
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- brown alga
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
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- Pest Control & Pesticides (AREA)
- Fertilizers (AREA)
Abstract
A kind of comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition, it is characterised in that first using complex enzyme zymohydrolysis brown alga, obtain brown alga enzymolysis liquid；Secondly by brown alga enzymolysis liquid biofermentation, obtain brown alga zymotic fluid and then prepare iron, calcium, copper chelate by chelating agent of glycine；Finally using brown alga zymotic fluid as base fluid, the N P and K needed for crop is added, iron, calcium, copper chelate and other auxiliary agents, is mixed evenly, obtain a kind of comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition.The bio-organic liquid fertilizer material of the present invention, using brown alga zymotic fluid as base fluid, it is rich in microbial bacterial agent and mycoprotein, nutrition is comprehensive, is easy to crop absorption, not only promotes crop growth, increasing both production and income, improving quality, and crop root microbial population is can effectively improve, be advantageous to improve crop anti-adversity.
Description
Technical field
The invention belongs to fertilizer field, and in particular to a kind of comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition
Production method.
Background technology
Foliage dressing is the important supplement of soil application technology.The traditional approach of soil root fertilizer has been broken in foliage dressing,
Can be described as most flexibly, most easily fertilization mode.But in recent years, most foliar fertilizer effective contents of domestic production are low, battalion
Foster effect is single, element utilization rate is not high, effect is not sufficiently stable.Foliar fertilizer is not high in technological content high, to be finally embodied in whether
It can make in peasant's increasing both production and income, this requires that foliar fertilizer provides more nutritional ingredient as far as possible, to there is higher multielement micro-fertilizer, foot
The hard water resistance humic acid of Available Amino Acids and high activity enough measured, will also there is appropriate nitrogen, phosphorus, potassium certainly, but so more
Composition compounding also want together it is soluble in water without go out precipitation, it goes without saying that be need it is high-tech.Therefore, concentration is developed
The composite multifunction type foliar fertilizer high, nutrition is complete, utilization rate is high is extremely urgent.
The content of the invention
It is an object of the invention to provide a kind of comprehensive brown alga fermentation liquid-based biological-organic liquid of the high nutrition of utilization rate
The production method of fertilizer.
To achieve these goals, the present invention adopts the following technical scheme that：
A kind of comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition, it is characterised in that first using complex enzyme zymohydrolysis
Brown alga, obtain brown alga enzymolysis liquid；Secondly by brown alga enzymolysis liquid biofermentation, brown alga zymotic fluid is obtained and then using glycine as chelating
Agent prepares iron, calcium, copper chelate；Finally using brown alga zymotic fluid as base fluid, the N P and K needed for crop, iron, calcium, copper chelating are added
Thing and other auxiliary agents, are mixed evenly, and obtain a kind of comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition.
The comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of described nutrition, it is characterised in that it is by following steps
It is prepared：
（1）Fresh brown alga is added in grinding pot, is 1 by material-water ratio:0.25 adds deionized water, with 250-300r/min's
Rotating speed grinds 1.5-2h, and homogenate is made, 0-5 DEG C of temperature refrigeration, obtains brown alga slurries；Brown alga slurries are added to enzymolysis container
In, the pH of regulation system is 5.8-6.2, adds complex enzyme by quality 0.4-0.5%, is placed in 48-55 DEG C of thermostat water bath,
Enzyme digestion reaction 70-80h is shaken, is centrifuged with 2000-2500r/min rotating speed, stays supernatant；
（2）By step（1）The supernatant of gained is added in fermentation tank, adds 0.15-0.2% bacillus subtilis and lichens
Bacillus is with 1.5-2：The microbial inoculum of 1 mass ratio mixing, the pH of regulation system is 6-6.5,40 DEG C of fermentation 48h, with 4000-
4500r/min rotating speed centrifugation, stays supernatant；
（3）Glycine and hydroxylamine hydrochloride agent are added in mortar, frerrous chloride, calcium chloride and copper sulphate are added after grinding uniformly,
Continue to grind 30-40min, obtained product is put into vacuum drying chamber and dried, recrystallized after drying with absolute ethyl alcohol, ethanol
Washing 2-3 times, is then dried in vacuo, obtains chelate again；
（4）Take step（2）The supernatant of gained is added in agitator tank, adds urea, potassium dihydrogen phosphate, potassium nitrate, mixing
After stirring, the pH of regulation system is 3-4, adds chelate, boric acid and ammonium molybdate, and rise temperature continues to 40-50 DEG C
Stirring reduces temperature to room temperature, adds neopelex and compound sodium nitrophenolate, continue magnetic agitation 15- to dissolving
20min, obtain the comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition.
The preparation method of the comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of described nutrition, it is characterised in that step
Suddenly（1）Middle complex enzyme is cellulase, pectase, protease, and its mass ratio is 2-2.5：1.2-1.5：1.
The preparation method of the comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of described nutrition, it is characterised in that step
Suddenly（3）Middle glycine, hydroxylamine hydrochloride agent, frerrous chloride, the mass ratio of calcium chloride and copper sulphate are 1：0.08-0.1：0.25-
0.3：0.2-0.22：0.15-0.18.
The preparation method of the comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of described nutrition, it is characterised in that step
Suddenly（3）Middle step（2）Supernatant, urea, potassium dihydrogen phosphate, potassium nitrate, chelate, boric acid, ammonium molybdate, the dodecyl of gained
The mass ratio of benzene sulfonic acid sodium salt and compound sodium nitrophenolate is 1：0.22-0.25：0.15-0.18：0.12-0.15：0.06-0.08：0.03-
0.04：0.02-0.03：0.02-0.03：0.008-0.01.
Using above-mentioned technical scheme, beneficial effects of the present invention are：
The present invention uses complex enzyme zymohydrolysis brown alga, obtains brown alga enzymolysis liquid；Again by brown alga enzymolysis liquid biofermentation, brown alga hair is obtained
Zymotic fluid, using brown alga zymotic fluid as bio-organic liquid fertilizer material base fluid, using microbial inoculum by the soluble protein in brown alga enzymolysis liquid, peptide
The nitrogen sources such as class, amino acids and glucide transform into mycoprotein, are on the one hand easy to the preservation of bio-organic liquid fertilizer material
Be not easy corruption, on the other hand can effectively keep the N nutrients in bio-organic liquid fertilizer material again, improve biological-organic liquid
The quality of fertilizer.The present invention prepares iron, calcium, copper chelate by chelating agent of glycine；Its chelation percent is high, and chelate is stable, adds
Enter into bio-organic liquid fertilizer material, improve the antagonism between nutrient and be more beneficial for crop absorption.The present invention's
Bio-organic liquid fertilizer material, using brown alga zymotic fluid as base fluid, it is rich in microbial bacterial agent and mycoprotein, and nutrition is comprehensive, is easy to
Crop absorbs, and not only promotes crop growth, increasing both production and income, improving quality, and can effectively improve crop root microorganism
Population, be advantageous to improve crop anti-adversity.
Embodiment
The comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition of the present embodiment, it is characterised in that it is by as follows
Step is prepared：
（1）Fresh brown alga is added in grinding pot, is 1 by material-water ratio:0.25 adds deionized water, with 300r/min rotating speed
2h is ground, homogenate is made, 5 DEG C of temperature refrigerations, obtains brown alga slurries；Brown alga slurries are added in enzymolysis container, regulation system
PH be 6, by quality 0.5% add complex enzyme, be placed in 50 DEG C of thermostat water bath, shake enzyme digestion reaction 72h, with 2500r/
Min rotating speed centrifugation, stays supernatant；
（2）By step（1）The supernatant of gained is added in fermentation tank, adds 0.2% bacillus subtilis and lichens gemma bar
Bacterium is with 2：The microbial inoculum of 1 mass ratio mixing, the pH of regulation system are 6.2,40 DEG C of fermentation 48h, with 4000r/min rotating speed from
The heart, stay supernatant；
（3）Glycine and hydroxylamine hydrochloride agent are added in mortar, frerrous chloride, calcium chloride and copper sulphate are added after grinding uniformly,
Continue to grind 40min, obtained product is put into vacuum drying chamber and dried, recrystallized after drying with absolute ethyl alcohol, ethanol is washed
Wash 3 times, be then dried in vacuo again, obtain chelate；
（4）Take step（2）The supernatant of gained is added in agitator tank, adds urea, potassium dihydrogen phosphate, potassium nitrate, mixing
After stirring, the pH of regulation system is 4, adds chelate, boric acid and ammonium molybdate, and rise temperature continues to stir to 50 DEG C
To dissolving, temperature is reduced to room temperature, neopelex and compound sodium nitrophenolate is added, continues magnetic agitation 20min, obtain
The comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition.
The step of the present embodiment（1）Middle complex enzyme is cellulase, pectase, protease, and its mass ratio is 2.5：1.5：
1。
The step of the present embodiment（3）Middle glycine, hydroxylamine hydrochloride agent, frerrous chloride, the mass ratio of calcium chloride and copper sulphate
For 1：0.08：0.3：0.22：0.18.
The step of the present embodiment（3）Middle step（2）The supernatant of gained, urea, potassium dihydrogen phosphate, potassium nitrate, chelate,
Boric acid, ammonium molybdate, the mass ratio of neopelex and compound sodium nitrophenolate are 1：0.25：0.18：0.15：0.08：0.04：
0.03：0.03：0.01.
Claims (5)
1. a kind of comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition, it is characterised in that first using complex enzyme enzyme
Brown alga is solved, obtains brown alga enzymolysis liquid；Secondly by brown alga enzymolysis liquid biofermentation, brown alga zymotic fluid is obtained and then using glycine as chela
Mixture prepares iron, calcium, copper chelate；Finally using brown alga zymotic fluid as base fluid, the N P and K needed for crop, iron, calcium, copper chela are added
Compound and other auxiliary agents, are mixed evenly, and obtain a kind of comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition.
2. the comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition according to claims 1, it is characterised in that
It is prepared by following steps：
（1）Fresh brown alga is added in grinding pot, is 1 by material-water ratio:0.25 adds deionized water, with 250-300r/min's
Rotating speed grinds 1.5-2h, and homogenate is made, 0-5 DEG C of temperature refrigeration, obtains brown alga slurries；Brown alga slurries are added to enzymolysis container
In, the pH of regulation system is 5.8-6.2, adds complex enzyme by quality 0.4-0.5%, is placed in 48-55 DEG C of thermostat water bath,
Enzyme digestion reaction 70-80h is shaken, is centrifuged with 2000-2500r/min rotating speed, stays supernatant；
（2）By step（1）The supernatant of gained is added in fermentation tank, adds 0.15-0.2% bacillus subtilis and lichens
Bacillus is with 1.5-2：The microbial inoculum of 1 mass ratio mixing, the pH of regulation system is 6-6.5,40 DEG C of fermentation 48h, with 4000-
4500r/min rotating speed centrifugation, stays supernatant；
（3）Glycine and hydroxylamine hydrochloride agent are added in mortar, frerrous chloride, calcium chloride and copper sulphate are added after grinding uniformly,
Continue to grind 30-40min, obtained product is put into vacuum drying chamber and dried, recrystallized after drying with absolute ethyl alcohol, ethanol
Washing 2-3 times, is then dried in vacuo, obtains chelate again；
（4）Take step（2）The supernatant of gained is added in agitator tank, adds urea, potassium dihydrogen phosphate, potassium nitrate, mixing
After stirring, the pH of regulation system is 3-4, adds chelate, boric acid and ammonium molybdate, and rise temperature continues to 40-50 DEG C
Stirring reduces temperature to room temperature, adds neopelex and compound sodium nitrophenolate, continue magnetic agitation 15- to dissolving
20min, obtain the comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition.
3. the preparation method of the comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition according to claims 2,
Characterized in that, step（1）Middle complex enzyme is cellulase, pectase, protease, and its mass ratio is 2-2.5：1.2-1.5：1.
4. the preparation method of the comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition according to claims 2,
Characterized in that, step（3）Middle glycine, hydroxylamine hydrochloride agent, frerrous chloride, the mass ratio of calcium chloride and copper sulphate are 1：
0.08-0.1：0.25-0.3：0.2-0.22：0.15-0.18.
5. the preparation method of the comprehensive brown alga fermentation liquid-based bio-organic liquid fertilizer material of nutrition according to claims 2,
Characterized in that, step（3）Middle step（2）Supernatant, urea, potassium dihydrogen phosphate, potassium nitrate, chelate, boric acid, the molybdenum of gained
The mass ratio of sour ammonium, neopelex and compound sodium nitrophenolate is 1：0.22-0.25：0.15-0.18：0.12-0.15：
0.06-0.08：0.03-0.04：0.02-0.03：0.02-0.03：0.008-0.01.
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Cited By (3)
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| CN108424252A (en) * | 2018-05-09 | 2018-08-21 | 天津市辰圣海洋生物技术有限公司 | A kind of preparation method of compound marine alga fertilizer |
| CN112573973A (en) * | 2020-12-25 | 2021-03-30 | 海城市盛世鸿翔有机肥制造有限公司 | Seaweed enzymolysis seedling raising fertilizer, and preparation method and application thereof |
| IT201900019412A1 (en) * | 2019-10-21 | 2021-04-21 | Bict Srl | HYDROLYZED TO PROMOTE VEGETABLE GROWTH, BIOSTIMULATION AND BIOCONTROL, AND ITS USE IN AGRICULTURE |
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| IT201900019412A1 (en) * | 2019-10-21 | 2021-04-21 | Bict Srl | HYDROLYZED TO PROMOTE VEGETABLE GROWTH, BIOSTIMULATION AND BIOCONTROL, AND ITS USE IN AGRICULTURE |
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