CN107771926A - A kind of preparation method of antistaling agent for litchi - Google Patents

A kind of preparation method of antistaling agent for litchi Download PDF

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Publication number
CN107771926A
CN107771926A CN201711323690.4A CN201711323690A CN107771926A CN 107771926 A CN107771926 A CN 107771926A CN 201711323690 A CN201711323690 A CN 201711323690A CN 107771926 A CN107771926 A CN 107771926A
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China
Prior art keywords
parts
leaf
antistaling agent
preparation
litchi
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CN201711323690.4A
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Chinese (zh)
Inventor
李文
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Liuzhou Liu Ke Science And Technology Co Ltd
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Liuzhou Liu Ke Science And Technology Co Ltd
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Priority to CN201711323690.4A priority Critical patent/CN107771926A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B7/00Preservation or chemical ripening of fruit or vegetables
    • A23B7/16Coating with a protective layer; Compositions or apparatus therefor
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Preparation Of Fruits And Vegetables (AREA)
  • Cosmetics (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

The invention belongs to postharvest technology of fruits and vegetables field, specifically discloses a kind of preparation method of antistaling agent for litchi.The preparation method of antistaling agent for litchi of the present invention comprises the following steps:(1) raw material weighs:Based on certain part by weight, Gui Ye, perilla leaf, green tea, lotus leaf, Lactobacillus plantarum, bacillus subtilis, saccharomyces cerevisiae, Chitosan and Glucomannan are weighed;(2) fermentation process;By the osmanthus leaf, perilla leaf, green tea, lotus leaf and the Lactobacillus plantarum that have weighed, bacillus subtilis, saccharomyces cerevisiae mixed fermentation;(3) extract:Extracted using ultrasonic wave;(4) mix.It the antistaling agent safety and environmental protection that the present invention is prepared, can effectively suppress the invasion of oxygen and microorganism, reduce the nutritive loss of lichee to greatest extent, fresh-keeping quality is high.

Description

A kind of preparation method of antistaling agent for litchi
【Technical field】
The present invention relates to postharvest technology of fruits and vegetables field, and in particular to a kind of preparation method of antistaling agent for litchi.
【Background technology】
Lichee is one of distinctive subtropical fruit of south China, and fruit yield is big, has higher nutritive value, in city Occupy critical role on.Litchi fruits pulp is translucent congealed fat shape, and savory U.S. is nutritious, very popular.Its In per 100g lichee edible parts moisture 84g, carbohydrate 14g, protein 0.7g, fatty 0.7g, P 32 mg, calcium 6mg, iron 0.5mg, thiamine 0.02mg, riboflavin 0.04mg, niacin 0.7mg, ascorbic acid 36mg, in addition, also containing thick Other mineral elements such as fiber, organic acid, amino acid, carrotene and Zn, Fe, there is high edible and value medical health care. But lichee maturation is in high-temperature high humidity season, using " one day and discoloration, two days and it is fragrant become, three days and taste becomes, four or five outer, color, Fragrant, taste is gone to the greatest extent ", it is unfavorable for the holding of litchi fruits post harvest transport and edibility and commercial value.
Therefore, the control of lichee Post-harvest quality deterioration turns into the upper urgent problem to be solved of lichee fresh-keeping transport.
【The content of the invention】
The goal of the invention of the present invention is:For above-mentioned problem, there is provided a kind of preparation method of antistaling agent for litchi. The antistaling agent safety and environmental protection that the present invention is prepared, it can effectively suppress the invasion of oxygen and microorganism, reduce litchi to greatest extent The nutritive loss of branch, fresh-keeping quality are high.
To achieve these goals, the technical solution adopted by the present invention is as follows:
A kind of preparation method of antistaling agent for litchi, comprises the following steps:
(1) raw material weighs:By weight, following raw materials according component is weighed:Osmanthus leaf 5-9 parts, perilla leaf 5-8 parts, green tea 4-8 Part, lotus leaf 3-7 parts, Lactobacillus plantarum 1-3 parts, bacillus subtilis 0.5-1 parts, saccharomyces cerevisiae 0.1-0.5 parts, glucocyamine shell gather Sugared 1-4 parts and Glucomannan 0.5-1.2 parts;
(2) fermentation process:The osmanthus leaf weighed, perilla leaf, green tea and lotus leaf are mixed after carrying out low-temperature grinding, uniformly admixed Lactobacillus plantarum, bacillus subtilis and the saccharomyces cerevisiae weighed, at a temperature of 33-35 DEG C, 73-76% humidity issues Ferment 32-35h, obtains fermentate;
(3) extract:By volume 1:7-9 is toward distilled water is added in the fermentate, using ultrasonication 30-35min Afterwards, filtrate is filtered to obtain, the filtrate is subjected to rotary evaporation to volume is original volume 2/5, obtains extract;
(4) mix:After said extracted thing and the Chitosan weighed, Glucomannan are well mixed, add and steam Distilled water stirs, you can obtains the antistaling agent.
Further, in step (1), by weight, following raw materials according component is weighed:7 parts of osmanthus leaf, 7 parts of perilla leaf, green tea 5 Part, 4 parts of lotus leaf, 2 parts of Lactobacillus plantarum, 0.8 part of bacillus subtilis, 0.3 part of saccharomyces cerevisiae, 3 parts of Chitosan and Portugal Sweet 0.9 part of glycan.
Further, in step (2), the particle diameter after the osmanthus leaf, perilla leaf, green tea and lotus leaf crush is 50-60 mesh.
Further, the ethanol and 0.5-1% that mass ratio is respectively 7-9% are added with step (3), in the distilled water Acetone.
Further, in step (3), the ultrasonic temperature is 32-35 DEG C, power 230-260W.
Further, in step (4), the mass concentration of the antistaling agent is 2.8-3%.
In summary, by adopting the above-described technical solution, the beneficial effects of the invention are as follows:
Materials safety in the antistaling agent of the present invention is degradable, and the feature of environmental protection is good, and each interaction between component, can effectively carry Height suppresses the ability of the invasion of oxygen and microorganism, keeps the nutritional ingredient of lichee to greatest extent, and the color, smell and taste of lichee are kept It must get well, fresh-keeping quality is high.Wherein, Gui Ye, Soviet Union, green tea and lotus leaf collective effect, improved relative to the fungistatic effect of one-component 12.8-13.2%, and the respiratory intensity of lichee can be made to reduce 5.9-7.2%;Further, using Lactobacillus plantarum, withered grass Bacillus, saccharomyces cerevisiae are fermented and use ultrasonic wave extraction to handle obtained extract, are further that fungistatic effect carries 4.8-6.3% is risen, and relative to unfermentable extract, extract of the invention can drop the respiratory intensity of litchi and longan Low 19.8-22.4%, improves fresh-keeping effect;In addition, the Chitosan and Glucomannan collective effect that add, can be in litchi The good film of branch surface forming properties, so as to effectively organize the invasion of extraneous oxygen and microorganism, gathers relative to glucocyamine shell Sugar or Glucomannan, the pericarp membrane membranous permeation rate of the lichee of the mixture processing of Chitosan and Glucomannan are only 51.83%, reduce 7.59-9.28%.
【Embodiment】
Below in conjunction with specific embodiment, the present invention is further illustrated.
Embodiment 1
A kind of preparation method of antistaling agent for litchi, comprises the following steps:
(1) raw material weighs:By weight, following raw materials according component is weighed:9 parts of osmanthus leaf, 8 parts of perilla leaf, 8 parts of green tea, lotus leaf 7 Part, 3 parts of Lactobacillus plantarum, 1 part of bacillus subtilis, 0.5 part of saccharomyces cerevisiae, 4 parts of Chitosan and Glucomannan 1.2 Part;
(2) fermentation process:It is 60 that the osmanthus leaf weighed, perilla leaf, green tea and lotus leaf, which are mixed, and carry out low-temperature grinding to particle diameter After mesh, the Lactobacillus plantarum weighed, bacillus subtilis and saccharomyces cerevisiae are uniformly admixed, at a temperature of 35 DEG C, 76% Ferment 35h under humidity, obtains fermentate;
(3) extract:By volume 1:9 toward add in the fermentate added with mass ratio be respectively 7% ethanol and The distilled water of 0.5% acetone, after using temperature as the ultrasonication 30min that 32 DEG C, power are 230W, filtrate is filtered to obtain, The filtrate is subjected to rotary evaporation to volume is original volume 2/5, obtains extract;
(4) mix:After said extracted thing and the Chitosan weighed, Glucomannan are well mixed, add and steam Distilled water stirs, you can obtains the antistaling agent that mass concentration is 2.8%.
Embodiment 2
A kind of preparation method of antistaling agent for litchi, comprises the following steps:
(1) raw material weighs:By weight, following raw materials according component is weighed:7 parts of osmanthus leaf, 7 parts of perilla leaf, 5 parts of green tea, lotus leaf 4 Part, 2 parts of Lactobacillus plantarum, 0.8 part of bacillus subtilis, 0.3 part of saccharomyces cerevisiae, 3 parts of Chitosan and Glucomannan 0.9 Part;
(2) fermentation process:It is 55 that the osmanthus leaf weighed, perilla leaf, green tea and lotus leaf, which are mixed, and carry out low-temperature grinding to particle diameter After mesh, the Lactobacillus plantarum weighed, bacillus subtilis and saccharomyces cerevisiae are uniformly admixed, at a temperature of 34 DEG C, 75% Ferment 34h under humidity, obtains fermentate;
(3) extract:By volume 1:8 toward add in the fermentate added with mass ratio be respectively 8% ethanol and The distilled water of 0.8% acetone, after using temperature as the ultrasonication 33min that 34 DEG C, power are 255W, filtrate is filtered to obtain, The filtrate is subjected to rotary evaporation to volume is original volume 2/5, obtains extract;
(4) mix:After said extracted thing and the Chitosan weighed, Glucomannan are well mixed, add and steam Distilled water stirs, you can obtains the antistaling agent that mass concentration is 2.9%.
Embodiment 3
A kind of preparation method of antistaling agent for litchi, comprises the following steps:
(1) raw material weighs:By weight, following raw materials according component is weighed:9 parts of osmanthus leaf, 8 parts of perilla leaf, 8 parts of green tea, lotus leaf 7 Part, 3 parts of Lactobacillus plantarum, 1 part of bacillus subtilis, 0.5 part of saccharomyces cerevisiae, 4 parts of Chitosan and Glucomannan 1.2 Part;
(2) fermentation process:It is 60 that the osmanthus leaf weighed, perilla leaf, green tea and lotus leaf, which are mixed, and carry out low-temperature grinding to particle diameter After mesh, the Lactobacillus plantarum weighed, bacillus subtilis and saccharomyces cerevisiae are uniformly admixed, at a temperature of 35 DEG C, 76% Ferment 35h under humidity, obtains fermentate;
(3) extract:By volume 1:9 are added with the ethanol and 1% that mass ratio is respectively 9% toward addition in the fermentate Acetone distilled water, after using temperature as the ultrasonication 35min that 35 DEG C, power are 260W, filter to obtain filtrate, will described in Filtrate carries out rotary evaporation to volume is original volume 2/5, obtains extract;
(4) mix:After said extracted thing and the Chitosan weighed, Glucomannan are well mixed, add and steam Distilled water stirs, you can obtains the antistaling agent that mass concentration is 3%.
Compliance test result:The lichee handled using 1-3 of embodiment of the present invention antistaling agent is used as experimental group 1-3;With in embodiment 1 Only without the extract solution and Lactobacillus plantarum of the osmanthus leaf of fermentation process, perilla leaf, green tea and lotus leaf, bacillus subtilis, wine brewing Antistaling agent that yeast, Chitosan and Glucomannan are directly mixed processing longan as a comparison case 1;With embodiment 1 In only mixed without the extract solution of the osmanthus leaf of fermentation process, perilla leaf, green tea and lotus leaf with Chitosan and Glucomannan Manufactured antistaling agent processing longan as a comparison case 2;With in embodiment 1 only by Lactobacillus plantarum, bacillus subtilis, wine brewing ferment The antistaling agent processing longan that female, Chitosan and Glucomannan are mixed as a comparison case 3.The above-mentioned each group of Observe and measure Healthy fruit, weight-loss ratio and battalion's loss late after longan storage 70d, are as a result shown in Tables 1 and 2 respectively:
The healthy fruit and weight-loss ratio of each group lichee of table 1
Group Experimental group 1 Experimental group 2 Experimental group 3 Comparative example 1 Comparative example 2 Comparative example 3
Healthy fruit (%) 89.7 90.2 89.5 80.3 78.4 75.7
Weight-loss ratio (%) 2.68 2.59 2.62 2.98 3.12 3.25
As shown in Table 1, after storing 70d, the healthy fruit of the lichee of experimental group 1-3 antistaling agent processing is above comparative example 1- 3, and weight-loss ratio is below comparative example 1-3, thus can be explained, each raw material of antistaling agent for litchi of the present invention is mutually tied with preparation method Close, can effectively delay the deteriorating time of lichee, and fresh-keeping effect is preferable.
The nutritive loss rate of each group lichee of table 2
As shown in Table 2,3 nutritive loss rates of the lichee of experimental group 1-3 antistaling agent processing are below comparative example 1-3, Illustrate that each raw material and preparation method are combined in antistaling agent of the present invention, can effectively reduce the loss of each nutrient content of lichee Rate, and then effectively improve the fresh-keeping effect of lichee.
Described above is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair Bright patent claim, the equal change completed or modification change under the technical spirit suggested by all present invention, all should belong to Cover the scope of the claims in the present invention.

Claims (6)

1. a kind of preparation method of antistaling agent for litchi, it is characterised in that comprise the following steps:
(1) raw material weighs:By weight, following raw materials according component is weighed:Osmanthus leaf 5-9 parts, perilla leaf 5-8 parts, green tea 4-8 parts, lotus Leaf 3-7 parts, Lactobacillus plantarum 1-3 parts, bacillus subtilis 0.5-1 parts, saccharomyces cerevisiae 0.1-0.5 parts, Chitosan 1-4 Part and Glucomannan 0.5-1.2 parts;
(2) fermentation process:The osmanthus leaf weighed, perilla leaf, green tea and lotus leaf are mixed after carrying out low-temperature grinding, uniformly admix and weigh Good Lactobacillus plantarum, bacillus subtilis and saccharomyces cerevisiae, fermented at a temperature of 33-35 DEG C, under 73-76% humidity 32-35h, obtain fermentate;
(3) extract:By volume 1:7-9 after ultrasonication 30-35min, takes out toward distilled water is added in the fermentate Filtrate is filtered to obtain, the filtrate is subjected to rotary evaporation to volume is original volume 2/5, obtains extract;
(4) mix:After said extracted thing and the Chitosan weighed, Glucomannan are well mixed, distilled water is added Stir, you can obtain the antistaling agent.
2. a kind of preparation method of antistaling agent for litchi according to claim 1, it is characterised in that in step (1), by weight Meter, weighs following raw materials according component:7 parts of osmanthus leaf, 7 parts of perilla leaf, 5 parts of green tea, 4 parts of lotus leaf, 2 parts of Lactobacillus plantarum, bacillus subtilis 0.9 part of 0.8 part of bacterium, 0.3 part of saccharomyces cerevisiae, 3 parts of Chitosan and Glucomannan.
A kind of 3. preparation method of antistaling agent for litchi according to claim 1, it is characterised in that in step (2), the osmanthus Particle diameter after leaf, perilla leaf, green tea and lotus leaf crush is 50-60 mesh.
A kind of 4. preparation method of antistaling agent for litchi according to claim 1, it is characterised in that in step (3), the distillation Added with mass ratio it is respectively 7-9% ethanol and 0.5-1% acetone in water.
A kind of 5. preparation method of antistaling agent for litchi according to claim 1, it is characterised in that in step (3), the ultrasound Temperature be 32-35 DEG C, power 230-260W.
6. a kind of preparation method of antistaling agent for litchi according to claim 1, it is characterised in that described fresh-keeping in step (4) The mass concentration of agent is 2.8-3%.
CN201711323690.4A 2017-12-13 2017-12-13 A kind of preparation method of antistaling agent for litchi Pending CN107771926A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112120077A (en) * 2019-06-09 2020-12-25 王虎 Green and environment-friendly waxberry preservative formula and preparation method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20090039967A (en) * 2007-10-19 2009-04-23 재단법인 하동녹차연구소 Manufacturing for kimchi improved shelf-life
CN104970093A (en) * 2015-07-08 2015-10-14 青岛嘉瑞生物技术有限公司 Composite fermented Chinese herbal medicine food preservative
CN106509059A (en) * 2016-10-29 2017-03-22 常州市鼎升环保科技有限公司 Preparation method of food fresh keeping agent having biological sources
CN106538672A (en) * 2016-11-08 2017-03-29 湖南省农产品加工研究所 Natural composite antistaling agent and its preparation method and application
CN106615085A (en) * 2016-12-19 2017-05-10 山西省农业科学院生物技术研究中心 Microorganism and plant derived composite fresh keeping agent for fruits and vegetables
CN107279271A (en) * 2017-07-10 2017-10-24 桂林融通科技有限公司 It is exclusively used in the preparation method of mango preservative

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20090039967A (en) * 2007-10-19 2009-04-23 재단법인 하동녹차연구소 Manufacturing for kimchi improved shelf-life
CN104970093A (en) * 2015-07-08 2015-10-14 青岛嘉瑞生物技术有限公司 Composite fermented Chinese herbal medicine food preservative
CN106509059A (en) * 2016-10-29 2017-03-22 常州市鼎升环保科技有限公司 Preparation method of food fresh keeping agent having biological sources
CN106538672A (en) * 2016-11-08 2017-03-29 湖南省农产品加工研究所 Natural composite antistaling agent and its preparation method and application
CN106615085A (en) * 2016-12-19 2017-05-10 山西省农业科学院生物技术研究中心 Microorganism and plant derived composite fresh keeping agent for fruits and vegetables
CN107279271A (en) * 2017-07-10 2017-10-24 桂林融通科技有限公司 It is exclusively used in the preparation method of mango preservative

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112120077A (en) * 2019-06-09 2020-12-25 王虎 Green and environment-friendly waxberry preservative formula and preparation method thereof

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