CN107751527A - The preparation method and Chinese herbal medicine candy of a kind of pharynx-clearing throat-benefiting Chinese herbal medicine candy - Google Patents
The preparation method and Chinese herbal medicine candy of a kind of pharynx-clearing throat-benefiting Chinese herbal medicine candy Download PDFInfo
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- CN107751527A CN107751527A CN201711003695.9A CN201711003695A CN107751527A CN 107751527 A CN107751527 A CN 107751527A CN 201711003695 A CN201711003695 A CN 201711003695A CN 107751527 A CN107751527 A CN 107751527A
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- chinese herbal
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- 235000009508 confectionery Nutrition 0.000 title claims abstract description 48
- 241000411851 herbal medicine Species 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 31
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 41
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 39
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 24
- 239000000284 extract Substances 0.000 claims abstract description 21
- 239000000843 powder Substances 0.000 claims abstract description 21
- 239000000706 filtrate Substances 0.000 claims abstract description 18
- 244000185386 Thladiantha grosvenorii Species 0.000 claims abstract description 17
- 235000011171 Thladiantha grosvenorii Nutrition 0.000 claims abstract description 17
- 238000001802 infusion Methods 0.000 claims abstract description 17
- 241000205585 Aquilegia canadensis Species 0.000 claims abstract description 14
- 235000007516 Chrysanthemum Nutrition 0.000 claims abstract description 14
- 238000002137 ultrasound extraction Methods 0.000 claims abstract description 14
- 240000000249 Morus alba Species 0.000 claims abstract description 13
- 235000008708 Morus alba Nutrition 0.000 claims abstract description 13
- 235000006753 Platycodon grandiflorum Nutrition 0.000 claims abstract description 13
- 240000003582 Platycodon grandiflorus Species 0.000 claims abstract description 13
- MYSWGUAQZAJSOK-UHFFFAOYSA-N ciprofloxacin Chemical compound C12=CC(N3CCNCC3)=C(F)C=C2C(=O)C(C(=O)O)=CN1C1CC1 MYSWGUAQZAJSOK-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000008103 glucose Substances 0.000 claims abstract description 13
- 235000021552 granulated sugar Nutrition 0.000 claims abstract description 13
- 239000006188 syrup Substances 0.000 claims abstract description 13
- 235000020357 syrup Nutrition 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims abstract description 9
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims abstract description 9
- 235000005187 Taraxacum officinale ssp. officinale Nutrition 0.000 claims abstract description 9
- 229940041616 menthol Drugs 0.000 claims abstract description 9
- 238000002390 rotary evaporation Methods 0.000 claims abstract description 9
- 238000001914 filtration Methods 0.000 claims abstract description 8
- 238000004806 packaging method and process Methods 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 4
- 238000001816 cooling Methods 0.000 claims abstract description 3
- 244000189548 Chrysanthemum x morifolium Species 0.000 claims abstract 2
- 240000001949 Taraxacum officinale Species 0.000 claims abstract 2
- 239000000203 mixture Substances 0.000 claims description 14
- 239000002994 raw material Substances 0.000 claims description 12
- TWCMVXMQHSVIOJ-UHFFFAOYSA-N Aglycone of yadanzioside D Natural products COC(=O)C12OCC34C(CC5C(=CC(O)C(O)C5(C)C3C(O)C1O)C)OC(=O)C(OC(=O)C)C24 TWCMVXMQHSVIOJ-UHFFFAOYSA-N 0.000 claims description 11
- PLMKQQMDOMTZGG-UHFFFAOYSA-N Astrantiagenin E-methylester Natural products CC12CCC(O)C(C)(CO)C1CCC1(C)C2CC=C2C3CC(C)(C)CCC3(C(=O)OC)CCC21C PLMKQQMDOMTZGG-UHFFFAOYSA-N 0.000 claims description 11
- PFOARMALXZGCHY-UHFFFAOYSA-N homoegonol Natural products C1=C(OC)C(OC)=CC=C1C1=CC2=CC(CCCO)=CC(OC)=C2O1 PFOARMALXZGCHY-UHFFFAOYSA-N 0.000 claims description 11
- VTAJIXDZFCRWBR-UHFFFAOYSA-N Licoricesaponin B2 Natural products C1C(C2C(C3(CCC4(C)CCC(C)(CC4C3=CC2)C(O)=O)C)(C)CC2)(C)C2C(C)(C)CC1OC1OC(C(O)=O)C(O)C(O)C1OC1OC(C(O)=O)C(O)C(O)C1O VTAJIXDZFCRWBR-UHFFFAOYSA-N 0.000 claims description 8
- LPLVUJXQOOQHMX-UHFFFAOYSA-N glycyrrhetinic acid glycoside Natural products C1CC(C2C(C3(CCC4(C)CCC(C)(CC4C3=CC2=O)C(O)=O)C)(C)CC2)(C)C2C(C)(C)C1OC1OC(C(O)=O)C(O)C(O)C1OC1OC(C(O)=O)C(O)C(O)C1O LPLVUJXQOOQHMX-UHFFFAOYSA-N 0.000 claims description 8
- 239000001685 glycyrrhizic acid Substances 0.000 claims description 8
- 229960004949 glycyrrhizic acid Drugs 0.000 claims description 8
- UYRUBYNTXSDKQT-UHFFFAOYSA-N glycyrrhizic acid Natural products CC1(C)C(CCC2(C)C1CCC3(C)C2C(=O)C=C4C5CC(C)(CCC5(C)CCC34C)C(=O)O)OC6OC(C(O)C(O)C6OC7OC(O)C(O)C(O)C7C(=O)O)C(=O)O UYRUBYNTXSDKQT-UHFFFAOYSA-N 0.000 claims description 8
- 235000019410 glycyrrhizin Nutrition 0.000 claims description 8
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 3
- 241000723353 Chrysanthemum Species 0.000 description 12
- 239000003814 drug Substances 0.000 description 10
- 235000019441 ethanol Nutrition 0.000 description 10
- 241000245665 Taraxacum Species 0.000 description 7
- 238000001704 evaporation Methods 0.000 description 6
- 230000008020 evaporation Effects 0.000 description 6
- 210000003800 pharynx Anatomy 0.000 description 6
- 150000003254 radicals Chemical class 0.000 description 5
- 244000246386 Mentha pulegium Species 0.000 description 4
- 235000016257 Mentha pulegium Nutrition 0.000 description 4
- 235000004357 Mentha x piperita Nutrition 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 235000001050 hortel pimenta Nutrition 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 3
- 230000031700 light absorption Effects 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 230000003026 anti-oxygenic effect Effects 0.000 description 2
- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 2
- 239000000852 hydrogen donor Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 210000000214 mouth Anatomy 0.000 description 2
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical group [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
- 244000012254 Canarium album Species 0.000 description 1
- 235000009103 Canarium album Nutrition 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- -1 DPPH radicals Chemical class 0.000 description 1
- 241000825107 Hierochloe Species 0.000 description 1
- 235000015466 Hierochloe odorata Nutrition 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 235000021282 Sterculia Nutrition 0.000 description 1
- 240000001058 Sterculia urens Species 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 238000003915 air pollution Methods 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 238000006701 autoxidation reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 208000020670 canker sore Diseases 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000000378 dietary effect Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 239000012458 free base Substances 0.000 description 1
- 230000012010 growth Effects 0.000 description 1
- 230000007773 growth pattern Effects 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 239000007937 lozenge Substances 0.000 description 1
- 210000002200 mouth mucosa Anatomy 0.000 description 1
- KNMNNEPMKDJBDW-UHFFFAOYSA-N n-[2-(3,4-dimethoxyphenyl)ethyl]-1-(2,6-dimethylphenoxy)propan-2-amine;hydrochloride Chemical compound Cl.C1=C(OC)C(OC)=CC=C1CCNC(C)COC1=C(C)C=CC=C1C KNMNNEPMKDJBDW-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 235000017709 saponins Nutrition 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000011888 snacks Nutrition 0.000 description 1
- 229940059107 sterculia Drugs 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 235000000346 sugar Nutrition 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/48—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/364—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/42—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds characterised by the carbohydrates used, e.g. polysaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Food Science & Technology (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Nutrition Science (AREA)
- Medicines Containing Plant Substances (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention discloses a kind of preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy and Chinese herbal medicine candy, wherein, method includes drying honeysuckle, chrysanthemum, mulberry leaf, dandelion, radix glycyrrhizae, Exocarpium Citri Rubrum, Momordica grosvenori, balloonflower root and dark plum, it is ground into powder, add ethanol solution, ultrasonic extraction, filtering, takes filtrate rotary evaporation to medicinal extract；White granulated sugar and glucose syrup are mixed in water, heats, infusion, obtains liquid glucose, the medicinal extract, menthol, citric acid is added after liquid glucose cooling, stirs, be cooled and shaped, packaging.
Description
Technical field
The invention belongs to health food processing technique field, and in particular to a kind of preparation side of pharynx-clearing throat-benefiting Chinese herbal medicine candy
Method and Chinese herbal medicine candy.
Background technology
Due to air pollution, reason, more and more modern times such as dietary structure is unreasonable, work and rest is irregular, operating pressure is big
People has suffered from sphagitis.The main performance of sphagitis is that pharyngeal pain, drying, foreign body sensation and pharynx are itched.Sphagitis can not only influence
People exchange with the external world, notably more influence the quality of work and life.It is used to treat therefore, some also occurs again and again in the market
The medicine and health products of sphagitis, throat piece are one kind that wherein usage amount is maximum, are divided into two kinds of Western medicine and Chinese medicine.Western medicine composition
Throat piece, its main component is iodine or quaternary ammonium salt surface active agent, for example Dobell etc., this kind of medicine contain iodine molecule,
Also very big to the excitant of oral mucosa although activity is big, sterilizing power is strong, long-term use can suppress inside oral cavity and throat
Normal flora growth, upset internal environment of oral cavity, cause local flora to lack of proper care, so as to induce the diseases such as canker sore occur.In
Medicine class throat lozenge is based on traditional Chinese medicine ingredients, wherein with the sterculia seed, honeysuckle, Chinese olive, dark plum, chrysanthemum, the Momordica grosvenori application frequency most
It is more.Compared with Western medicine, traditional Chinese medicine ingredients have the advantages that low toxicity, Small side effects, therapeutic effect are good.
One of confectionery industry Two Mainstays snacks industry traditional as China, is always maintained at quick growth pattern.
In recent years, because increasing people suffers from pharyngolaryngitis, the market that pharynx-clearing throat-benefiting candy occupies incrementally increases.City at present
Pharynx-clearing throat-benefiting candy on field, its Chinese herbal medicine is added in the form of powder or water extract medicinal extract entirely, and the work(of Chinese herbal medicine
It is mostly the materials such as polyphenol, flavones, saponin(e to imitate composition, and solubility of these materials in water is limited, causes the clearing of in the market
The effect of throat benefiting sugar fruit, is smaller.
The content of the invention
The purpose of this part is to summarize some aspects of embodiments of the invention and briefly introduce some preferably to implement
Example.It may do a little simplified or be omitted to avoid making our department in this part and the description of the present application summary and denomination of invention
Point, the purpose of specification digest and denomination of invention obscure, and this simplification or omit and cannot be used for limiting the scope of the present invention.
In view of the preparation method of above-mentioned and/or existing pharynx-clearing throat-benefiting Chinese herbal medicine candy and the technological gap of Chinese herbal medicine candy,
Propose the present invention.
Therefore, one of purpose of the invention is that solve deficiency of the prior art, there is provided a kind of pharynx-clearing throat-benefiting medium-height grass
The preparation method of medicine candy.
In order to solve the above technical problems, the invention provides following technical scheme：A kind of pharynx-clearing throat-benefiting Chinese herbal medicine candy
Preparation method, including,
In terms of mass parts, composition of raw materials includes,
Honeysuckle, chrysanthemum, mulberry leaf, dandelion, radix glycyrrhizae, Exocarpium Citri Rubrum, Momordica grosvenori, balloonflower root and dark plum are dried, are ground into powder,
Ethanol solution is added, ultrasonic extraction, filtering, takes filtrate rotary evaporation to medicinal extract；White granulated sugar and glucose syrup are mixed in water,
Heating, infusion, obtains liquid glucose, adds the medicinal extract, menthol, citric acid after liquid glucose cooling, stirs, is cooled and shaped,
Packaging.
As a kind of preferred scheme of the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy of the present invention, wherein：The baking
Dry, its drying temperature is 30~40 DEG C.
As a kind of preferred scheme of the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy of the present invention, wherein：The second
Alcoholic solution is 75~80% ethanol solutions, and its addition is that every gram of powder adds 8~15ml ethanol solutions.
As a kind of preferred scheme of the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy of the present invention, wherein：It is described super
Sound extracts, and its ultrasonic extraction frequency is 50~55kHz, and extraction time is 25min~40min.
As a kind of preferred scheme of the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy of the present invention, wherein：The rotation
Turn evaporation, its temperature is 35~50 DEG C, and rotating speed is 60~120rpm, below pressure 399.9pa.
As a kind of preferred scheme of the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy of the present invention, wherein：It is described to add
Heat, its heating-up temperature are 65~70 DEG C.
As a kind of preferred scheme of the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy of the present invention, wherein：It is described to endure
Boil, its infusion temperature is 130~145 DEG C, and the infusion time is 20~40min.
As a kind of preferred scheme of the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy of the present invention, wherein：It is described sweet
Grass, wherein the quality containing glycyrrhizic acid is 3~4mg/g.
As a kind of preferred scheme of the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy of the present invention, wherein：Sieve
Chinese fruit, wherein the quality containing Momordia grosvenori aglycone is 10~11mg/g.
It is a further object to provide a kind of Chinese herbal medicine candy.
In order to solve the above technical problems, the invention provides following technical scheme：The Chinese herbal medicine candy is hard candy.
Beneficial effect possessed by the present invention：
Preparation method provided by the invention, extraction time is short, efficiency high, and functional component contains in the Chinese herbal medicine candy prepared
Amount is high, Chinese herbal medicine candy excellent.
Embodiment
In order to facilitate the understanding of the purposes, features and advantages of the present invention, with reference to specific embodiment pair
The embodiment of the present invention is described in detail.
Many details are elaborated in the following description to facilitate a thorough understanding of the present invention, still the present invention can be with
It is different from other manner described here using other to implement, those skilled in the art can be without prejudice to intension of the present invention
In the case of do similar popularization, therefore the present invention is not limited by following public specific embodiment.
Secondly, " one embodiment " or " embodiment " referred to herein refers to may be included at least one realization side of the present invention
Special characteristic, structure or characteristic in formula." in one embodiment " that different places occur in this manual not refers both to
Same embodiment, nor the single or selective embodiment mutually exclusive with other embodiment.
Embodiment 1
Composition of raw materials：50 parts of white granulated sugar, 45 parts of glucose syrup, 2 parts of honeysuckle, 1 part of chrysanthemum, 1 part of peppermint, 1 part of citric acid,
3 parts of radix glycyrrhizae (glycyrrhizic acid content 3.58mg/g), 5 parts of Momordica grosvenori (Momordia grosvenori aglycone content is 10.64mg/g), 4 parts of balloonflower root, Pu Gong
1 part of English, 1 part of mulberry leaf, 4 parts of dark plum, 3 parts of Exocarpium Citri Rubrum.
Preparation method：
(1) honeysuckle, chrysanthemum, mulberry leaf, dandelion, radix glycyrrhizae, Exocarpium Citri Rubrum, Momordica grosvenori, balloonflower root and dark plum are dried at 40 DEG C,
It is ground into powder and weighs herbal powder by composition of raw materials, adding 15ml by every gram of herbal powder adds 80% ethanol solution,
Ultrasonic extraction 25min, ultrasonic extraction frequency 53kHz, then filtering, take filtrate, collect filter residue.Again two are repeated by aforesaid operations
It is secondary, merge filtrate three times, abandon filter residue.
(2) it is 40 DEG C, rotating speed 60rpm by above-mentioned filtrate rotary evaporation to medicinal extract, rotating evaporation temperature, pressure is
350pa。
(3) weigh white granulated sugar and glucose syrup adds water, heat and dissolved at 70 DEG C, and infusion is carried out at 140 DEG C
25min。
(4) treat that liquid glucose cools down after infusion, add each Chinese herbal medicine medicinal extract and menthol, citric acid, stir.
(5) cool down, be shaped to hard candy, packaging.
Embodiment 2
Composition of raw materials：55 parts of white granulated sugar, 50 parts of glucose syrup, 3 parts of honeysuckle, 2 parts of chrysanthemum, 2 parts of peppermint, 2 parts of citric acid,
4 parts of radix glycyrrhizae (glycyrrhizic acid content 3.58mg/g), 6 parts of Momordica grosvenori (Momordia grosvenori aglycone content is 10.64mg/g), 5 parts of balloonflower root, Pu Gong
2 parts of English, 2 parts of mulberry leaf, 5 parts of dark plum, 4 parts of Exocarpium Citri Rubrum.
Preparation method：
(1) honeysuckle, chrysanthemum, mulberry leaf, dandelion, radix glycyrrhizae, Exocarpium Citri Rubrum, Momordica grosvenori, balloonflower root and dark plum are dried at 40 DEG C,
It is ground into powder and weighs herbal powder by composition of raw materials, adding 8ml by every gram of herbal powder adds 80% ethanol solution, surpasses
Sound extracts 40min, ultrasonic extraction frequency 53kHz, then filtering, takes filtrate, collects filter residue.It is repeated twice again by aforesaid operations,
Merge filtrate three times, abandon filter residue.
(2) it is 40 DEG C, rotating speed 60rpm by above-mentioned filtrate rotary evaporation to medicinal extract, rotating evaporation temperature, pressure is
350pa。
(3) weigh white granulated sugar and glucose syrup adds water, heat and dissolved at 70 DEG C, and infusion is carried out at 140 DEG C
25min。
(4) treat that liquid glucose cools down after infusion, add each Chinese herbal medicine medicinal extract and menthol, citric acid, stir.
(5) cool down, be shaped to hard candy, packaging.
Embodiment 3
Composition of raw materials：50 parts of white granulated sugar, 45 parts of glucose syrup, 2 parts of honeysuckle, 1 part of chrysanthemum, 1 part of peppermint, 1 part of citric acid,
3 parts of radix glycyrrhizae (glycyrrhizic acid content 3.58mg/g), 5 parts of Momordica grosvenori (Momordia grosvenori aglycone content is 10.64mg/g), 4 parts of balloonflower root, Pu Gong
1 part of English, 1 part of mulberry leaf, 4 parts of dark plum, 3 parts of Exocarpium Citri Rubrum.
Preparation method：
(1) honeysuckle, chrysanthemum, mulberry leaf, dandelion, radix glycyrrhizae, Exocarpium Citri Rubrum, Momordica grosvenori, balloonflower root and dark plum are dried at 40 DEG C,
It is ground into powder and weighs herbal powder by composition of raw materials, adding 8ml by every gram of herbal powder adds 80% ethanol solution, surpasses
Sound extracts 30min, ultrasonic extraction frequency 53kHz, then filtering, takes filtrate, collects filter residue.It is repeated twice again by aforesaid operations,
Merge filtrate three times, abandon filter residue.
(2) it is 40 DEG C, rotating speed 100rpm by above-mentioned filtrate rotary evaporation to medicinal extract, rotating evaporation temperature, pressure is
350pa。
(3) weigh white granulated sugar and glucose syrup adds water, heat and dissolved at 70 DEG C, and infusion is carried out at 140 DEG C
25min。
(4) treat that liquid glucose cools down after infusion, add each Chinese herbal medicine medicinal extract and menthol, citric acid, stir.
(5) cool down, be shaped to hard candy, packaging.
Embodiment 4
Composition of raw materials：50 parts of white granulated sugar, 45 parts of glucose syrup, 3 parts of honeysuckle, 1 part of chrysanthemum, 2 parts of menthol, citric acid 1
Part, 4 parts of radix glycyrrhizae (glycyrrhizic acid content 3.89mg/g), 6 parts of Momordica grosvenori (Momordia grosvenori aglycone content is 10.03mg/g), 4 parts of balloonflower root,
1 part of dandelion, 1 part of mulberry leaf, 4 parts of dark plum, 4 parts of Exocarpium Citri Rubrum.
Preparation method：
(1) honeysuckle, chrysanthemum, mulberry leaf, dandelion, radix glycyrrhizae, Exocarpium Citri Rubrum, Momordica grosvenori, balloonflower root and dark plum are dried at 40 DEG C,
It is ground into powder and weighs herbal powder by composition of raw materials, adding 10ml by every gram of herbal powder adds 80% ethanol solution,
Ultrasonic extraction 30min, ultrasonic extraction frequency 53kHz, then filtering, take filtrate, collect filter residue.Again two are repeated by aforesaid operations
It is secondary, merge filtrate three times, abandon filter residue.
(2) it is 40 DEG C, rotating speed 60rpm by above-mentioned filtrate rotary evaporation to medicinal extract, rotating evaporation temperature, pressure is
350pa。
(3) weigh white granulated sugar and glucose syrup adds water, heat and dissolved at 70 DEG C, and infusion is carried out at 130 DEG C
25min。
(4) treat that liquid glucose cools down after infusion, add each Chinese herbal medicine medicinal extract and menthol, citric acid, stir.
(5) cool down, be shaped to hard candy, packaging.
Embodiment 5
Composition of raw materials：50 parts of white granulated sugar, 45 parts of glucose syrup, 2 parts of honeysuckle, 1 part of chrysanthemum, 1 part of peppermint, 1 part of citric acid,
3 parts of radix glycyrrhizae (glycyrrhizic acid content 3.89mg/g), 5 parts of Momordica grosvenori (Momordia grosvenori aglycone content is 10.03mg/g), 4 parts of balloonflower root, Pu Gong
1 part of English, 1 part of mulberry leaf, 4 parts of dark plum, 3 parts of Exocarpium Citri Rubrum.
Preparation method：
(1) honeysuckle, chrysanthemum, mulberry leaf, dandelion, radix glycyrrhizae, Exocarpium Citri Rubrum, Momordica grosvenori, balloonflower root and dark plum are dried at 40 DEG C,
It is ground into powder and weighs herbal powder by composition of raw materials, adding 15ml by every gram of herbal powder adds 80% ethanol solution,
Ultrasonic extraction 30min, ultrasonic extraction frequency 53kHz, then filtering, take filtrate, collect filter residue.Again two are repeated by aforesaid operations
It is secondary, merge filtrate three times, abandon filter residue.
(2) it is 40 DEG C, rotating speed 60rpm by above-mentioned filtrate rotary evaporation to medicinal extract, rotating evaporation temperature, pressure is
350pa。
(3) weigh white granulated sugar and glucose syrup adds water, heat and dissolved at 70 DEG C, and infusion is carried out at 140 DEG C
25min。
(4) treat that liquid glucose cools down after infusion, add each Chinese herbal medicine medicinal extract and menthol, citric acid, stir.
(5) cool down, be shaped to hard candy, packaging.
Embodiment 6
Obtained product in embodiment 1~5, after measured, there is obvious pharynx-clearing throat-benefiting effect.
Obtained product in embodiment 1~5 is subjected to DPPH radicals scavenging measure again, takes commercially available Chinese herbal medicine candy conduct
Sample 6,10g is respectively taken, diluted with absolute ethyl alcohol prepare 30ml solution respectively；0.2ml samples are taken, take 2.8ml 0.1mmol/L
DDPH ethanol solutions, the well mixed 30min that places in the dark under 517nm after surveying light absorption value.
Sample oxidation resistance clearance rate, is calculated according to equation below：
Clearance rate (%)=(Ai-Aj)/Ai × 100%
Wherein, Ai is the DPPH light absorption values for adding blank ethanol, and Aj is the reacted DPPH light absorption values of sample-adding product.
Final result, such as following table：
It has been investigated that the active ingredient in Momordica grosvenori is Momordia grosvenori aglycone, according to Momordica grosvenori addition in this formula, arhat
When Momordia grosvenori aglycone content is 10~11mg/g in fruit, Momordia grosvenori aglycone reacts most strong with ultra-oxygen anion free radical, can effectively hinder
The initiation chain reaction of disconnected free radical, hydrogen is supplied free radical by it, itself is changed into free radical, and caused free radical is stable because of it
Property reduces the transmission speed of autoxidation chain reaction, and antioxidation is preferably played as free base absorbant；It is another
Aspect, Radix Glycyrrhizae acid have certain reproducibility, and it is used as hydrogen donor again, can reduce oxidized free radical, originally match somebody with somebody
Under Fang Chengfen, the content of Radix Glycyrrhizae acid is 3~4mg/g, and now the mass ratio of glycyrrhizic acid and Momordia grosvenori aglycone can mutually promote
The result entered enables the antioxygenic property of obtained Chinese herbal medicine candy to strengthen to maximum.When the two content ratio is not in this scope
When, antioxygenic property improves and unobvious, or even has weakened, and pushes away that to trace it to its cause be that reduction has been contained in the presence of a large amount of hydrogen donors
The progress of reaction.
It should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although with reference to preferable
The present invention is described in detail embodiment, it will be understood by those within the art that, can be to the technology of the present invention
Scheme is modified or equivalent substitution, and without departing from the spirit and scope of technical solution of the present invention, it all should cover in this hair
Among bright right.
Claims (10)
- A kind of 1. preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy, it is characterised in that：Including,In terms of mass parts, composition of raw materials includes,Honeysuckle, chrysanthemum, mulberry leaf, dandelion, radix glycyrrhizae, Exocarpium Citri Rubrum, Momordica grosvenori, balloonflower root and dark plum are dried, are ground into powder, is added Ethanol solution, ultrasonic extraction, filtering, filtrate rotary evaporation is taken to medicinal extract；White granulated sugar and glucose syrup are mixed in water, heats, infusion, obtains liquid glucose, after liquid glucose cooling described in addition Medicinal extract, menthol, citric acid, stir, be cooled and shaped, packaging.
- 2. the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy according to claim 1, it is characterised in that：The drying, it dries Dry temperature is 30~40 DEG C.
- 3. the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy according to claim 1, it is characterised in that：The ethanol solution is 75~80% ethanol solutions, its addition are that every gram of powder adds 8~15ml ethanol solutions.
- 4. the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy according to claim 1, it is characterised in that：The ultrasonic extraction, Its ultrasonic extraction frequency is 50~55kHz, and extraction time is 25min~40min.
- 5. the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy according to claim 1, it is characterised in that：The rotary evaporation, Its temperature is 35~50 DEG C, and rotating speed is 60~120rpm, below pressure 399.9pa.
- 6. the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy according to claim 1, it is characterised in that：The heating, it adds Hot temperature is 65~70 DEG C.
- 7. the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy according to claim 1, it is characterised in that：The infusion, it is endured Temperature is boiled as 130~145 DEG C, the infusion time is 20~40min.
- 8. the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy according to claim 1, it is characterised in that：The radix glycyrrhizae, wherein Quality containing glycyrrhizic acid is 3~4mg/g.
- 9. the preparation method of pharynx-clearing throat-benefiting Chinese herbal medicine candy according to claim 1, it is characterised in that：The Momordica grosvenori, its In the quality containing Momordia grosvenori aglycone be 10~11mg/g.
- 10. Chinese herbal medicine candy made of a kind of preparation method of the Chinese herbal medicine candy of pharynx-clearing throat-benefiting according to claim 1, it is special Sign is：The Chinese herbal medicine candy is hard candy.
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| CN109198133A (en) * | 2018-11-15 | 2019-01-15 | 江西草珊瑚保健科技有限公司 | A kind of candy for removing halitosis |
| CN112889989A (en) * | 2021-02-20 | 2021-06-04 | 重庆海王生物工程有限公司 | Throat-moistening and cough-relieving lollipop and preparation method thereof |
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