CN107746298A - The preparation method of high-dispersion nano organic fertilizer - Google Patents
The preparation method of high-dispersion nano organic fertilizer Download PDFInfo
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- CN107746298A CN107746298A CN201711241130.4A CN201711241130A CN107746298A CN 107746298 A CN107746298 A CN 107746298A CN 201711241130 A CN201711241130 A CN 201711241130A CN 107746298 A CN107746298 A CN 107746298A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F5/00—Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
- C05F5/006—Waste from chemical processing of material, e.g. diestillation, roasting, cooking
- C05F5/008—Waste from biochemical processing of material, e.g. fermentation, breweries
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
Abstract
A kind of preparation method of high-dispersion nano organic fertilizer provided by the invention, including such as：Medical stone surface is polished using sand paper, adds the roughness of coated abrasive surface, the load point provided for nanoparticulate particles；Using medical stone as carrier, nanometer particle load thereon, is being effectively increased the dispersion effect of nanoparticle, reunion is being avoided, improves the utilization rate of nano-particle；First compound high-temperature sterilization can swim the harmful levels of pathogens that can effectively reduce its carrying, reduce the illness rate of plant, and low temperature quickly cools down, and reduces the generation of harmful levels of pathogens in cooling procedure；Lan Gen, folium isatidis, Pudilan, the Radix Astragali and corydlis bungeana addition can effectively play the killing to the harmful levels of pathogens in soil, first extract simultaneously, prepare resulting mixture, ensure that the synergy of above-mentioned Chinese medicine, it is avoided to be disperseed in stirring, so as to cause bactericidal effect to reduce.
Description
Technical field
The present invention relates to a kind of composite nano powder, more particularly to a kind of preparation method of high-dispersion nano organic fertilizer.
Background technology
With the continuous development of agricultural, fertilizer has become the indispensable material of modern agriculture.Nano material is a kind of
Emerging material, it can effectively deposit into absorption of the root system of plant to nutriment, deposit into promotion plant growth.And can also have
The property of the improvement soil of effect, can effectively prevent the generation for the phenomenon that soil moves back fertile and several piece, so nano material is extensive
It is applied in fertilizer, but due to nano material particle diameter very little, easily reunites, cause its function reduction or forfeiture.
The content of the invention
It is an object of the invention to solve at least the above, and provide the advantages of at least will be described later.
It is a still further object of the present invention to provide a kind of preparation method of high-dispersion nano organic fertilizer, it can effectively be prevented
Nanoclusters particle agglomeration.
In order to realize according to object of the present invention and further advantage, there is provided a kind of system of high-dispersion nano organic fertilizer
Preparation Method, comprise the following steps：
(1) medical stone granule that particle diameter is 2-3cm is chosen, is polished its surface using sand paper；By starch, sesbania gum and
Water is proportionally 1:1:3 mixing, obtain mixed glue solution；
Mixed glue solution is sprayed into medical stone surface, the wherein dosage of mixed glue solution is the 5%-10% of medical stone quality,
Obtain loading particle；
(2) it is 1 according to mass ratio by nano-particle and ethylene glycol:50-70 is mixed, and in water bath sonicator 30-50min, is obtained
Nanometer suspension；
Nano-particle is made up of nano-sized carbon and nano-tourmaline；
Nanometer suspension is sprayed on load particle, is loaded with the medical stone of nano-particle；
Wherein, the dosage of nanometer suspension is the 1-5% of load granular mass；
(3) medical stone of load nano particle is dried into 1-2h in the case where temperature is 150-200 DEG C, then in temperature 200-
1-2h is dried at 300 DEG C；
(4) it is 1 in mass ratio by stalk and vinasse:3 mixing, it is equal to be dried to its water content at being then 100 DEG C in temperature
Less than 10%, the particle that particle diameter is 2mm then is being ground into, is obtaining the first hybrid particles；
(5) it is 1000 according to quality by the first hybrid particles, zymophyte and syrup:1：It is 40- in temperature after 200 mixing
At 50 DEG C, compost fermentation 8-10 days, the first compound is obtained：
(6) the first compound is sterilized into 1-2h in the case where temperature is 150-200 DEG C；Then in the environment of -20 DEG C of temperature,
It is cooled to room temperature；
(7) it is 10 according to mass ratio by Radix Isatidis, folium isatidis, Pudilan, the Radix Astragali and corydlis bungeana:5:7:0.5:2, in temperature
At 60-70 DEG C, to dry 2-3h, the particle that particle diameter is 2-4cm is then ground into, obtains the second hybrid particles, by the second mixing
Particle is 1 according to mass ratio with absolute ethyl alcohol:20 mixing, at 90 DEG C of temperature, refluxing extraction 1h, then filter, obtain solid
Filter residue and filtrate；
The liquid in filtrate is removed using the method for vacuum rotary steam, obtains purifying solid, will purify solid in temperature is 50
DEG C baking oven in, dry 2-3 days；
Solid filter residue is dried 2-3 days in the baking oven that temperature is 70 DEG C；
Solid filter residue after drying and purification solid are mixed, obtain the second compound；
(8) by the first compound after step (6) processing, the second compound, barnyard manure, humus and dry through step (3)
The medical stone for being loaded with nano-particle after dry is 1 according to mass ratio:0.6:2:0.5:0.1 mixing, obtaining high-dispersion nano has
Machine fertilizer.
Preferably, in the preparation method of described high-dispersion nano organic fertilizer, in the step (2), by nano-particle
With ethylene glycol according to mass ratio be 1:50-70 is mixed, and in the case where bath temperature is 40-50 DEG C, water bath sonicator 45min, obtains nanometer
Suspension.
Preferably, in the preparation method of described high-dispersion nano organic fertilizer, in the step (3), nanometer will be loaded
The medical stone of particle dries 2h at being 180 DEG C in temperature, then dries 1.5h at 250 DEG C of temperature.
Preferably, in the preparation method of described high-dispersion nano organic fertilizer, in the step (2), nano-particle by
Mass ratio is 3:2 nano-sized carbon and nano-tourmaline composition.
Preferably, in the preparation method of described high-dispersion nano organic fertilizer, in the step (6), by the first mixing
Material sterilizes 1h in the case where temperature is 180 DEG C；Then in the environment of -20 DEG C of temperature, it is cooled to room temperature.
The present invention comprises at least following beneficial effect：
A kind of preparation method of high-dispersion nano organic fertilizer provided by the invention, comprises the following steps：Selection particle diameter is 2-
3cm medical stone granule, polished its surface using sand paper；It is proportionally 1 by starch, sesbania gum and water:1:3 mixing,
Obtain mixed glue solution；Mixed glue solution is sprayed into medical stone surface, the wherein dosage of mixed glue solution is the 5%- of medical stone quality
10%, obtain loading particle；According to mass ratio it is 1 by nano-particle and ethylene glycol:50-70 is mixed, in water bath sonicator 30-
50min, obtain a nanometer suspension；Nano-particle is made up of nano-sized carbon and nano-tourmaline；Nanometer suspension is sprayed on load
On particle, wherein, the dosage of nanometer suspension is the 1-5% of load granular mass；By the medical stone of load nano particle in temperature
Spend to dry 1-2h at 150-200 DEG C, then dry 1-2h at 200-300 DEG C of temperature；It is in mass ratio by stalk and vinasse
1:3 mixing, it is dried to its water content at being then 100 DEG C in temperature and is respectively less than 10%, be then ground into that particle diameter is 2mm
Grain, obtains the first hybrid particles；By the first hybrid particles, zymophyte and syrup according to quality be 1000:1：After 200 mixing,
Temperature is at 40-50 DEG C, compost fermentation 8-10 days, obtains the first compound：By the first compound temperature be 150-200 DEG C
Under, sterilize 1-2h；Then in the environment of -20 DEG C of temperature, it is cooled to room temperature；By Radix Isatidis, folium isatidis, Pudilan, the Radix Astragali and
Corydlis bungeana is 10 according to mass ratio:5:7:0.5:2, in the case where temperature is 60-70 DEG C, 2-3h is dried, it is 2- to be then ground into particle diameter
4cm particle, the second hybrid particles are obtained, according to mass ratio be 1 by the second hybrid particles and absolute ethyl alcohol:20 mixing, in temperature
At 90 DEG C of degree, refluxing extraction 1h, then filter, obtain solid filter residue and filtrate；Removed using the method for vacuum rotary steam in filtrate
Liquid, obtain purifying solid, solid will be purified in temperature is 50 DEG C of baking oven, dried 2-3 days；Solid filter residue is in temperature
In 70 DEG C of baking oven, dry 2-3 days；Solid filter residue after drying and purification solid are mixed, obtain the second compound；By first
Compound, the second compound, barnyard manure, humus and to be loaded with the medical stone of nano-particle according to mass ratio be 1:0.6:2:0.5:
0.1 mixing, obtains high-dispersion nano organic fertilizer.First, the present invention polishes on medical stone surface using sand paper, adds sand paper table
The roughness in face, the load point provided for nanoparticulate particles；Second, using medical stone as carrier, nanometer particle load is existed
Thereon, the dispersion effect of nanoparticle is effectively increased, avoids reunion, improves the utilization rate of nano-particle；Adopt simultaneously
Be compounded to form mixed glue solution with starch and sesbania gum, can effectively make nano-particle being fixed on medical stone surface, prevent its
Come off in follow-up technique, and starch and sesbania gum are nontoxic, can be rapidly degraded in soil, be also used as plant
Nutrient uses；3rd, the first compound high-temperature sterilization can swim the harmful levels of pathogens that can effectively reduce its carrying, reduce the trouble of plant
Sick rate, and low temperature quickly cools down, and reduces the generation of harmful levels of pathogens in cooling procedure；4th, Lan Gen, folium isatidis, Pudilan,
The addition of the Radix Astragali and corydlis bungeana can effectively play the killing to the harmful levels of pathogens in soil, while first extract, and be prepared into mixing
Thing, the synergy of above-mentioned Chinese medicine is ensure that, avoid it from being disperseed in stirring, so as to cause bactericidal effect to reduce；5th, adopt
Plant root can be effectively promoted to nutrient and water as nano particle, wherein nano-particle by the use of nano-particle and nano-tourmaline
The absorption divided, while nano-particle can effectively improve the water conservation and fertilizer-preserving ability of soil, and nanometer electricity with nano-tourmaline
Anion is formed in the air that gas stone can be around it, anion can not only effectively play a part of sterilization, itself and can have
The raising vegetative function of effect.
Further advantage, target and the feature of the present invention embodies part by following explanation, and part will also be by this
The research and practice of invention and be understood by the person skilled in the art.
Embodiment
With reference to embodiment, the present invention is described in further detail, to make those skilled in the art with reference to specification
Word can be implemented according to this.
It should be appreciated that such as " having ", "comprising" and " comprising " term used herein do not allot one or more
The presence or addition of individual other elements or its combination.
Embodiment 1
A kind of preparation method of high-dispersion nano organic fertilizer, comprises the following steps：
(1) medical stone granule that particle diameter is 3cm is chosen, is polished its surface using sand paper；By starch, sesbania gum and water
It is proportionally 1:1:3 mixing, obtain mixed glue solution；
Mixed glue solution is sprayed into medical stone surface, the wherein dosage of mixed glue solution is the 7% of medical stone quality, is born
Carry particle；
(2) it is 1 according to mass ratio by nano-particle and ethylene glycol:55 mixing, in the case where bath temperature is 45 DEG C, water bath sonicator
45min, obtain a nanometer suspension；
Nano-particle is 3 by mass ratio:2 nano-sized carbon and nano-tourmaline composition；
Nanometer suspension is sprayed on load particle, is loaded with the medical stone of nano-particle；
Wherein, the dosage of nanometer suspension is the 3% of load granular mass；
(3) by the medical stone of load nano particle be 180 DEG C in temperature at dry 2h, then dried at 250 DEG C of temperature
1.5h；
(4) it is 1 in mass ratio by stalk and vinasse:3 mixing, it is equal to be dried to its water content at being then 100 DEG C in temperature
Less than 10%, the particle that particle diameter is 2mm then is being ground into, is obtaining the first hybrid particles；
(5) it is 1000 according to quality by the first hybrid particles, zymophyte and syrup:1：It it is 50 DEG C in temperature after 200 mixing
Under, compost fermentation 10 days, obtain the first compound：
(6) the first compound is sterilized into 1h in the case where temperature is 180 DEG C；Then in the environment of -20 DEG C of temperature, it is cooled to
Room temperature；
(7) it is 10 according to mass ratio by Radix Isatidis, folium isatidis, Pudilan, the Radix Astragali and corydlis bungeana:5:7:0.5:2, in temperature
At 60 DEG C, to dry 2h, the particle that particle diameter is 4cm is then ground into, the second hybrid particles are obtained, by the second hybrid particles and nothing
Water-ethanol is 1 according to mass ratio:20 mixing, at 90 DEG C of temperature, refluxing extraction 1h, then filter, obtain solid filter residue and filter
Liquid；
The liquid in filtrate is removed using the method for vacuum rotary steam, obtains purifying solid, will purify solid in temperature is 50
DEG C baking oven in, dry 3 days；
Solid filter residue is dried 3 days in the baking oven that temperature is 70 DEG C；
Solid filter residue after drying and purification solid are mixed, obtain the second compound；
(8) by the first compound after step (6) processing, the second compound, barnyard manure, humus and dry through step (3)
The medical stone for being loaded with nano-particle after dry is 1 according to mass ratio:0.6:2:0.5:0.1 mixing, obtaining high-dispersion nano has
Machine fertilizer.
Embodiment 2
A kind of preparation method of high-dispersion nano organic fertilizer, comprises the following steps：
(1) medical stone granule that particle diameter is 2cm is chosen, is polished its surface using sand paper；By starch, sesbania gum and water
It is proportionally 1:1:3 mixing, obtain mixed glue solution；
Mixed glue solution is sprayed into medical stone surface, the wherein dosage of mixed glue solution is the 10% of medical stone quality, is obtained
Load particle；
(2) it is 1 according to mass ratio by nano-particle and ethylene glycol:50 mixing, in the case where bath temperature is 50 DEG C, water bath sonicator
50min, obtain a nanometer suspension；
Nano-particle is 5 by mass ratio:2 nano-sized carbon and nano-tourmaline composition；
Nanometer suspension is sprayed on load particle, is loaded with the medical stone of nano-particle；Wherein, nanometer suspension
Dosage is the 1% of load granular mass；
(3) by the medical stone of load nano particle be 150 DEG C in temperature at dry 1h, then dried at 200 DEG C of temperature
2h；
(4) it is 1 in mass ratio by stalk and vinasse:3 mixing, it is equal to be dried to its water content at being then 100 DEG C in temperature
Less than 10%, the particle that particle diameter is 2mm then is being ground into, is obtaining the first hybrid particles；
(5) it is 1000 according to quality by the first hybrid particles, zymophyte and syrup:1：It it is 50 DEG C in temperature after 200 mixing
Under, compost fermentation 10 days, obtain the first compound：
(6) the first compound is sterilized into 1h in the case where temperature is 150 DEG C；Then in the environment of -20 DEG C of temperature, it is cooled to
Room temperature；
(7) it is 10 according to mass ratio by Radix Isatidis, folium isatidis, Pudilan, the Radix Astragali and corydlis bungeana:5:7:0.5:2, in temperature
At 70 DEG C, to dry 2h, the particle that particle diameter is 2cm is then ground into, the second hybrid particles are obtained, by the second hybrid particles and nothing
Water-ethanol is 1 according to mass ratio:20 mixing, at 90 DEG C of temperature, refluxing extraction 1h, then filter, obtain solid filter residue and filter
Liquid；
The liquid in filtrate is removed using the method for vacuum rotary steam, obtains purifying solid, will purify solid in temperature is 50
DEG C baking oven in, dry 2 days；
Solid filter residue is dried 3 days in the baking oven that temperature is 70 DEG C；
Solid filter residue after drying and purification solid are mixed, obtain the second compound；
(8) by the first compound after step (6) processing, the second compound, barnyard manure, humus and dry through step (3)
The medical stone for being loaded with nano-particle after dry is 1 according to mass ratio:0.6:2:0.5:0.1 mixing, obtaining high-dispersion nano has
Machine fertilizer.
Embodiment 3
A kind of preparation method of high-dispersion nano organic fertilizer, comprises the following steps：
(1) medical stone granule that particle diameter is 2cm is chosen, is polished its surface using sand paper；By starch, sesbania gum and water
It is proportionally 1:1:3 mixing, obtain mixed glue solution；
Mixed glue solution is sprayed into medical stone surface, the wherein dosage of mixed glue solution is the 10% of medical stone quality, is obtained
Load particle；
(2) it is 1 according to mass ratio by nano-particle and ethylene glycol:70 mixing, in the case where bath temperature is 40 DEG C, water bath sonicator
30min, obtain a nanometer suspension；
Nano-particle is 2 by mass ratio:4 nano-sized carbon and nano-tourmaline composition；
Nanometer suspension is sprayed on load particle, is loaded with the medical stone of nano-particle；Wherein, nanometer suspension
Dosage is the 5% of load granular mass；
(3) by the medical stone of load nano particle be 200 DEG C in temperature at dry 2h, then dried at 300 DEG C of temperature
2h；
(4) it is 1 in mass ratio by stalk and vinasse:3 mixing, it is equal to be dried to its water content at being then 100 DEG C in temperature
Less than 10%, the particle that particle diameter is 2mm then is being ground into, is obtaining the first hybrid particles；
(5) it is 1000 according to quality by the first hybrid particles, zymophyte and syrup:1：It it is 50 DEG C in temperature after 200 mixing
Under, compost fermentation 8 days, obtain the first compound：
(6) the first compound is sterilized into 2h in the case where temperature is 170 DEG C；Then in the environment of -20 DEG C of temperature, it is cooled to
Room temperature；
(7) it is 10 according to mass ratio by Radix Isatidis, folium isatidis, Pudilan, the Radix Astragali and corydlis bungeana:5:7:0.5:2, in temperature
At 70 DEG C, to dry 3h, the particle that particle diameter is 4cm is then ground into, the second hybrid particles are obtained, by the second hybrid particles and nothing
Water-ethanol is 1 according to mass ratio:20 mixing, at 90 DEG C of temperature, refluxing extraction 1h, then filter, obtain solid filter residue and filter
Liquid；
The liquid in filtrate is removed using the method for vacuum rotary steam, obtains purifying solid, will purify solid in temperature is 50
DEG C baking oven in, dry 3 days；
Solid filter residue is dried 3 days in the baking oven that temperature is 70 DEG C；
Solid filter residue after drying and purification solid are mixed, obtain the second compound；
(8) by the first compound after step (6) processing, the second compound, barnyard manure, humus and dry through step (3)
The medical stone for being loaded with nano-particle after dry is 1 according to mass ratio:0.6:2:0.5:0.1 mixing, obtaining high-dispersion nano has
Machine fertilizer.
Embodiment 4
A kind of preparation method of high-dispersion nano organic fertilizer, comprises the following steps：
(1) medical stone granule that particle diameter is 3cm is chosen, is polished its surface using sand paper；By starch, sesbania gum and water
It is proportionally 1:1:3 mixing, obtain mixed glue solution；
Mixed glue solution is sprayed into medical stone surface, the wherein dosage of mixed glue solution is the 5% of medical stone quality, is born
Carry particle；
(2) it is 1 according to mass ratio by nano-particle and ethylene glycol:65 mixing, in the case where bath temperature is 50 DEG C, water bath sonicator
50min, obtain a nanometer suspension；
Nano-particle is 2 by mass ratio:7 nano-sized carbon and nano-tourmaline composition；
Nanometer suspension is sprayed on load particle, is loaded with the medical stone of nano-particle；Wherein, nanometer suspension
Dosage is the 2% of load granular mass；
(3) by the medical stone of load nano particle be 200 DEG C in temperature at dry 2h, then dried at 300 DEG C of temperature
2h；
(4) it is 1 in mass ratio by stalk and vinasse:3 mixing, it is equal to be dried to its water content at being then 100 DEG C in temperature
Less than 10%, the particle that particle diameter is 2mm then is being ground into, is obtaining the first hybrid particles；
(5) it is 1000 according to quality by the first hybrid particles, zymophyte and syrup:1：It it is 50 DEG C in temperature after 200 mixing
Under, compost fermentation 8 days, obtain the first compound：
(6) the first compound is sterilized into 2h in the case where temperature is 170 DEG C；Then in the environment of -20 DEG C of temperature, it is cooled to
Room temperature；
(7) it is 10 according to mass ratio by Radix Isatidis, folium isatidis, Pudilan, the Radix Astragali and corydlis bungeana:5:7:0.5:2, in temperature
At 70 DEG C, to dry 3h, the particle that particle diameter is 4cm is then ground into, the second hybrid particles are obtained, by the second hybrid particles and nothing
Water-ethanol is 1 according to mass ratio:20 mixing, at 90 DEG C of temperature, refluxing extraction 1h, then filter, obtain solid filter residue and filter
Liquid；
The liquid in filtrate is removed using the method for vacuum rotary steam, obtains purifying solid, will purify solid in temperature is 50
DEG C baking oven in, dry 3 days；
Solid filter residue is dried 3 days in the baking oven that temperature is 70 DEG C；
Solid filter residue after drying and purification solid are mixed, obtain the second compound；
(8) by the first compound after step (6) processing, the second compound, barnyard manure, humus and dry through step (3)
The medical stone for being loaded with nano-particle after dry is 1 according to mass ratio:0.6:2:0.5:0.1 mixing, obtaining high-dispersion nano has
Machine fertilizer.
Compliance test result
5 mu of selection has been planted corn trials field and tested, and every mu of corn field is as a group；
Blank group, any chemical fertilizer is not applied；Test group 1, high-dispersion nano prepared by every mu of embodiment 1 for applying 8 kilograms
Organic fertilizer；Test group 2, high-dispersion nano organic fertilizer prepared by every mu of embodiment 2 for applying 8 kilograms；Test group 3, every mu applies 8
Kilogram embodiment 3 prepare high-dispersion nano organic fertilizer；Test group 4, high score prepared by every mu of embodiment 4 for applying 8 kilograms
Dissipate nanometer organic fertilizer.
Corn trials field is normally watered weeding, until corn is ripe, contrast test group 1-4 and blank group corn yield,
Test group 1-4 is shown in Table 1 compared to the effect of increasing production of blank group.
Table 1
| Test group 1 | Test group 2 | Test group 3 | Test group 4 | |
| Effect of increasing production | 57% | 51% | 51% | 54% |
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed
With it can be applied to various suitable the field of the invention completely, can be easily for those skilled in the art
Other modification is realized, therefore under the universal limited without departing substantially from claim and equivalency range, it is of the invention and unlimited
In specific details.
Claims (5)
1. a kind of preparation method of high-dispersion nano organic fertilizer, it is characterised in that comprise the following steps：
(1) medical stone granule that particle diameter is 2-3cm is chosen, is polished its surface using sand paper；Starch, sesbania gum and water are pressed
It is 1 according to ratio:1:3 mixing, obtain mixed glue solution；
Mixed glue solution is sprayed into medical stone surface, the wherein dosage of mixed glue solution is the 5%-10% of medical stone quality, is obtained
Load particle；
(2) it is 1 according to mass ratio by nano-particle and ethylene glycol:50-70 is mixed, and in water bath sonicator 30-50min, obtains nanometer
Suspension；
Nano-particle is made up of nano-sized carbon and nano-tourmaline；
Nanometer suspension is sprayed on load particle, obtains being loaded with the medical stone of nano-particle；
Wherein, the dosage of nanometer suspension is the 1-5% of load granular mass；
(3) by the medical stone of load nano particle be 150-200 DEG C in temperature at dry 1-2h, then in 200-300 DEG C of temperature
Lower drying 1-2h；
(4) it is 1 in mass ratio by stalk and vinasse:3 mixing, it is dried to its water content at being then 100 DEG C in temperature and is respectively less than
10%, the particle that particle diameter is 2mm then is being ground into, is obtaining the first hybrid particles；
(5) it is 1000 according to quality by the first hybrid particles, zymophyte and syrup:1：It it is 40-50 DEG C in temperature after 200 mixing
Under, compost fermentation 8-10 days, obtain the first compound：
(6) the first compound is sterilized into 1-2h in the case where temperature is 150-200 DEG C；Then in the environment of -20 DEG C of temperature, cooling
To room temperature；
(7) it is 10 according to mass ratio by Radix Isatidis, folium isatidis, Pudilan, the Radix Astragali and corydlis bungeana:5:7:0.5:2, be in temperature
At 60-70 DEG C, 2-3h is dried, the particle that particle diameter is 2-4cm is then ground into, obtains the second hybrid particles, by the second mixing
Grain is 1 according to mass ratio with absolute ethyl alcohol:20 mixing, at 90 DEG C of temperature, refluxing extraction 1h, are then filtered, and obtain solid filter
Slag and filtrate；
The liquid in filtrate is removed using the method for vacuum rotary steam, obtains purifying solid, will purify solid in temperature is 50 DEG C
In baking oven, dry 2-3 days；
Solid filter residue is dried 2-3 days in the baking oven that temperature is 70 DEG C；
Solid filter residue after drying and purification solid are mixed, obtain the second compound；
(8) by through step (6) processing after the first compound, the second compound, barnyard manure, humus and through step (3) dry after
The medical stone for being loaded with nano-particle according to mass ratio be 1:0.6:2:0.5:0.1 mixing, obtains high-dispersion nano organic fertilizer.
2. the preparation method of high-dispersion nano organic fertilizer according to claim 1, it is characterised in that in the step (2),
According to mass ratio it is 1 by nano-particle and ethylene glycol:50-70 is mixed, in the case where bath temperature is 40-50 DEG C, water bath sonicator
45min, obtain a nanometer suspension.
3. the preparation method of high-dispersion nano organic fertilizer according to claim 1, it is characterised in that in the step (3),
2h is dried at being 180 DEG C in temperature by the medical stone of load nano particle, then dries 1.5h at 250 DEG C of temperature.
4. the preparation method of high-dispersion nano organic fertilizer according to claim 1, it is characterised in that in the step (2),
Nano-particle is 3 by mass ratio:2 nano-sized carbon and nano-tourmaline composition.
5. the preparation method of high-dispersion nano organic fertilizer according to claim 1, it is characterised in that in the step (6),
By the first compound in the case where temperature is 180 DEG C, 1h is sterilized；Then in the environment of -20 DEG C of temperature, it is cooled to room temperature.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108617376A (en) * | 2018-03-30 | 2018-10-09 | 靖西市秀美边城农业科技有限公司 | A kind of cultural method of tea place interplanting green manure |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1290677A (en) * | 2000-08-04 | 2001-04-11 | 李树春 | Chinese medicinal stone coated urea |
| CN104781215A (en) * | 2012-10-24 | 2015-07-15 | 特姆龙韩国有限公司 | Plant growth enhancer |
| AU2015101436A4 (en) * | 2015-10-06 | 2015-11-12 | Zhiqiang Wang | A novel soil amendment for immobilization of contaminates in cropland and soil quality improvement of sandy, acidic, saline and alkaline land |
| CN105085037A (en) * | 2015-08-12 | 2015-11-25 | 天长市翔净蔬菜种植发展有限公司 | Slow release fertilizer special for melon and preparation method thereof |
| CN106187618A (en) * | 2016-07-21 | 2016-12-07 | 广西宁明百事康生物工程有限公司 | The preparation method that Sorghum vulgare Pers. is fertile |
| CN106187619A (en) * | 2016-07-21 | 2016-12-07 | 广西宁明百事康生物工程有限公司 | The preparation method that Oryza sativa L. is fertile |
| CN106892753A (en) * | 2017-03-21 | 2017-06-27 | 广西宁明百事康生物工程有限公司 | The preparation method of corn fertilizer |
-
2017
- 2017-11-30 CN CN201711241130.4A patent/CN107746298A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1290677A (en) * | 2000-08-04 | 2001-04-11 | 李树春 | Chinese medicinal stone coated urea |
| CN104781215A (en) * | 2012-10-24 | 2015-07-15 | 特姆龙韩国有限公司 | Plant growth enhancer |
| CN105085037A (en) * | 2015-08-12 | 2015-11-25 | 天长市翔净蔬菜种植发展有限公司 | Slow release fertilizer special for melon and preparation method thereof |
| AU2015101436A4 (en) * | 2015-10-06 | 2015-11-12 | Zhiqiang Wang | A novel soil amendment for immobilization of contaminates in cropland and soil quality improvement of sandy, acidic, saline and alkaline land |
| CN106187618A (en) * | 2016-07-21 | 2016-12-07 | 广西宁明百事康生物工程有限公司 | The preparation method that Sorghum vulgare Pers. is fertile |
| CN106187619A (en) * | 2016-07-21 | 2016-12-07 | 广西宁明百事康生物工程有限公司 | The preparation method that Oryza sativa L. is fertile |
| CN106892753A (en) * | 2017-03-21 | 2017-06-27 | 广西宁明百事康生物工程有限公司 | The preparation method of corn fertilizer |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108617376A (en) * | 2018-03-30 | 2018-10-09 | 靖西市秀美边城农业科技有限公司 | A kind of cultural method of tea place interplanting green manure |
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