CN107714548A - A kind of plant sun frost and preparation method thereof - Google Patents
A kind of plant sun frost and preparation method thereof Download PDFInfo
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- CN107714548A CN107714548A CN201711075625.4A CN201711075625A CN107714548A CN 107714548 A CN107714548 A CN 107714548A CN 201711075625 A CN201711075625 A CN 201711075625A CN 107714548 A CN107714548 A CN 107714548A
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- extract
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- black nightshade
- plant sun
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- Animal Behavior & Ethology (AREA)
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- Biotechnology (AREA)
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- Epidemiology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of plant sun frost and preparation method thereof, it is made up of the component of following percetage by weight：Herba Eupatorii extract 1%~3%, black nightshade extract is 1%~3%, Cacumen Platycladi extract 1%~3%, dimethicone is 0.5%~1%, and stearic acid sorbitol ester and sucrose cocoate are 3%~5%, and glycerine is 3%~5%, polyethylene glycol 400 is 2%~3%, sodium carboxymethylcellulose is 0.3%~0.4%, and methyl hydroxybenzoate is 0.15%~0.2%, and surplus is deionized water.Present invention employs Herba Eupatorii extract, black nightshade extract and Cacumen Platycladi extract three combination are as sun-proof active material.Three, which combines, produces synergy, can play and protect the skin from ultraviolet irradiation, anti-sunlight function is notable.
Description
Technical field
The present invention relates to a kind of cosmetics, particularly a kind of plant sun frost and preparation method thereof.
Technical background
It is sun-proof to refer to prevent the purpose of skin is by tanned, sunburn to reach to take certain methods ultraviolet to obstruct or absorb
Line.Sun-proof method：Smear sunscreen product, using sunproof clothes and other items, edible sun-proof food etc..Sunscreen product, which is divided into physics, to be prevented
Solarization, chemical sunscreen, biology are sun-proof etc..
The utilization rate more and more higher of sun-proof class cosmetics, but conventional sun care preparations is substantially and made in the market
With chemical sun, side effect of the chemical sun to skin enjoys query always.Some natural plants not only have protection
The ability of ultraviolet, also has the effect of after-sun concurrently, and enjoys consumer to like.
The content of the invention
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of sun-proof result it is good plant sun frost and its
Preparation method.
To achieve these goals, the present invention adopts the following technical scheme that：
A kind of plant sun frost, is made up of the component of following percetage by weight：
Herba Eupatorii extract 1%~3%, black nightshade extract are 1%~3%, Cacumen Platycladi extract 1%~3%, dimethyl
Silicone oil is 0.5%~1%, and stearic acid sorbitol ester and sucrose cocoate are 3%~5%, and glycerine is 3%~5%, is gathered
Ethylene glycol 400 is 2%~3%, and sodium carboxymethylcellulose is 0.3%~0.4%, and methyl hydroxybenzoate is 0.15%~0.2%,
Surplus is deionized water.
In above-mentioned plant sun frost, as preferable, it is made up of the component of following percetage by weight：
Herba Eupatorii extract 2%, black nightshade extract 2%, Cacumen Platycladi extract 2%, dimethicone 0.8% are stearic
Sour sorbitol ester and sucrose cocoate are 4%, glycerine 4%, polyethylene glycol 400 3%, and sodium carboxymethylcellulose is
0.4%, methyl hydroxybenzoate 0.2%, surplus is deionized water.
The preparation method of above-mentioned plant sun frost, comprises the following steps：
Step 1
After eupatorium, black nightshade and cacumen biotae are crushed respectively cross 20 mesh sieves, by obtained eupatorium crushed material, black nightshade crushed material and
Cacumen biotae crushed material is mixed to get mixed powder and minced, and Vltrasonic device ultrasonic extraction, mistake are used after mincing middle addition ethanol to mixed powder
Extract solution is obtained after filter；
Step 2
Extract solution is well mixed with other components, is heated to 90 DEG C, maintains 20min sterilizings；Then 70 DEG C are cooled to,
Emulsification pretreatment 15min is used under 1500r/min；It is slowly stirred after emulsification and is cooled to 40 DEG C of dischargings, obtains plant sun frost, then pass through
Conventional cosmetics quality and safe and healthy detection, packed after qualified.
In the preparation method of above-mentioned plant sun frost, the ethanol is that the ethanol that mass percent concentration is 50% is molten
Liquid, it is 5 that mixed powder, which minces with the solid-liquid ratio of ethanol,：1, g/L.
In the preparation method of above-mentioned plant sun frost, the supersonic frequency of the ultrasonic extraction is 30kHz, temperature 40
DEG C, ultrasonic time 30min.
Compared with prior art, the present invention has the advantages that：
1. the plant sun frost of the present invention, its composition of raw materials uses plant, green, and skin will not be caused to stimulate
Property injury, the problems such as being also not in heavy-metal residual, hormone residues；
2. the present invention combines Herba Eupatorii extract, black nightshade extract and Cacumen Platycladi extract three as sun-proof active matter
Matter, while ultrasonic extraction process of arranging in pairs or groups, rational Ingredient Amount and technological parameter so that not only active component can be effective by three
Extract, and restrict the effect of be not in mutual between three kinds of plants, the side effect such as effect is offset；
3. the present invention is had found by studying, the active component in various plants source is combined with each other, many skills can be faced
Art difficulty, such as it is possible that light stabilization, thermostabilization equistability problem during the mixing of each active components of plants, it is also possible to occur
Each composition interacting in terms of performance, effect；Therefore, the present invention is according to the drug effect of each plant, active ingredient in formula
The factors such as matter, the rational extraction process of amount body collocation, both ensure that the abundant release of each effective ingredients in plant, and can overcomes difference
Adverse effect between plant between drug effect；
4. the plant sun frost of the present invention, which can play, protects the skin from ultraviolet irradiation injury, anti-sunlight function is notable.
Embodiment
Embodiment 1：
Herba Eupatorii extract 2%, black nightshade extract 2%, Cacumen Platycladi extract 2%, dimethicone 0.8% are stearic
Sour sorbitol ester and sucrose cocoate are 4%, glycerine 4%, polyethylene glycol 400 3%, and sodium carboxymethylcellulose is
0.4%, methyl hydroxybenzoate 0.2%, surplus is deionized water.Unit is mass percent.By eupatorium, black nightshade and cacumen biotae point
Not Fen Sui after cross 20 mesh sieves, obtained eupatorium crushed material, black nightshade crushed material and cacumen biotae crushed material are mixed to get co-grinding
Thing, Vltrasonic device ultrasonic extraction is used after mincing middle addition ethanol to mixed powder, extract solution is obtained after filtering；Ethanol is quality percentage
Specific concentration is 50% ethanol solution, and it is 5 that mixed powder, which minces with the solid-liquid ratio of ethanol,：1(g/L).The supersonic frequency of ultrasonic extraction
For 30kHz, temperature is 40 DEG C, ultrasonic time 30min.Extract solution is well mixed with other components, is heated to 90 DEG C, dimension
Hold 20min sterilizings；Then 70 DEG C are cooled to, emulsification pretreatment 15min is used under 1500r/min；It is slowly stirred and is cooled to after emulsification
40 DEG C of dischargings, plant sun frost is obtained, then by conventional cosmetics quality and safe and healthy detection, packed after qualified.
Embodiment 2：
Herba Eupatorii extract 1%, black nightshade extract 3%, Cacumen Platycladi extract 1%, dimethicone 0.5% are stearic
Sour sorbitol ester and sucrose cocoate are 3%, glycerine 3%, polyethylene glycol 400 3%, and sodium carboxymethylcellulose is
0.4%, methyl hydroxybenzoate 0.2%, surplus is deionized water.Unit is mass percent.By eupatorium, black nightshade and cacumen biotae point
Not Fen Sui after cross 20 mesh sieves, obtained eupatorium crushed material, black nightshade crushed material and cacumen biotae crushed material are mixed to get co-grinding
Thing, Vltrasonic device ultrasonic extraction is used after mincing middle addition ethanol to mixed powder, extract solution is obtained after filtering；Ethanol is quality percentage
Specific concentration is 50% ethanol solution, and it is 5 that mixed powder, which minces with the solid-liquid ratio of ethanol,：1(g/L).The supersonic frequency of ultrasonic extraction
For 30kHz, temperature is 40 DEG C, ultrasonic time 30min.Extract solution is well mixed with other components, is heated to 90 DEG C, dimension
Hold 20min sterilizings；Then 70 DEG C are cooled to, emulsification pretreatment 15min is used under 1500r/min；It is slowly stirred and is cooled to after emulsification
40 DEG C of dischargings, plant sun frost is obtained, then by conventional cosmetics quality and safe and healthy detection, packed after qualified.
Embodiment 3：
Herba Eupatorii extract 3%, black nightshade extract 2%, Cacumen Platycladi extract 3%, dimethicone 1%, stearic acid
Sorbitol ester and sucrose cocoate are 5%, glycerine 5%, polyethylene glycol 400 3%, and sodium carboxymethylcellulose is
0.4%, methyl hydroxybenzoate 0.2%, surplus is deionized water.Unit is mass percent.By eupatorium, black nightshade and cacumen biotae point
Not Fen Sui after cross 20 mesh sieves, obtained eupatorium crushed material, black nightshade crushed material and cacumen biotae crushed material are mixed to get co-grinding
Thing, Vltrasonic device ultrasonic extraction is used after mincing middle addition ethanol to mixed powder, extract solution is obtained after filtering；Ethanol is quality percentage
Specific concentration is 50% ethanol solution, and it is 5 that mixed powder, which minces with the solid-liquid ratio of ethanol,：1(g/L).The supersonic frequency of ultrasonic extraction
For 30kHz, temperature is 40 DEG C, ultrasonic time 30min.Extract solution is well mixed with other components, is heated to 90 DEG C, dimension
Hold 20min sterilizings；Then 70 DEG C are cooled to, emulsification pretreatment 15min is used under 1500r/min；It is slowly stirred and is cooled to after emulsification
40 DEG C of dischargings, plant sun frost is obtained, then by conventional cosmetics quality and safe and healthy detection, packed after qualified.
The embodiment 1-3 of embodiment 4 sun-proof experiment
Experimental principle：Ultraviolet is light of the wavelength in 200~400nm, and skin can be directly shone into one by ultraviolet irradiation
Fixed injury, test whether ultraviolet can be stopped and be absorbed.
Experimental method：Last layer medical adhesive tape, simulation human body skin top layer, blank are pasted on the shiny surface of quartz colorimetric utensil
What is not smeared in group, and 20mg plant suns frost is weighed in experimental group and is uniformly smeared, room temperature 30min, is put into ultraviolet suction
Its absorbance is measured in light photometer, selectes 200~400nm of wavelength.
Evaluate absorbance calculation formula：
(1)Ai=(A280i+A290i+A300i+A310i+A320i)/5
Experimental result：
Grasped by the evaluation method of sun care preparations UVB areas sun-proof result, determination sample UVB (280nm~
320nm) the ultraviolet light absorption angle value in area, the size of the absorbance of comparative sample evaluate protection of the sample to UVB section ultraviolets
Effect, its evaluation criterion are as shown in table 1.The absorbance of different wave length is determined respectively.Long wave is evaluated by critical wavelength method
During ultraviolet protection level, the critical wavelength λ of sample is foundCBetween 376~378nm, critical wavelength is more than 370nm, belongs to
Wide spectrum sun-proof result.Embodiment 1-3 belongs to the rank of complete protectiving ultraviolet irradiation.
The UVB sections sun-proof result of table 1 is evaluated
The UV absorption of the embodiment 1-3 suncreams of table 2
| Wavelength/nm | Absorbance (embodiment 1) | Absorbance (embodiment 2) | Absorbance (embodiment 3) |
| 290 | 1.87 | 1.81 | 1.92 |
| 300 | 2.16 | 2.22 | 2.35 |
| 310 | 2.16 | 2.08 | 2.21 |
| 320 | 1.98 | 2.02 | 1.98 |
| 330 | 1.67 | 1.86 | 1.72 |
Claims (5)
1. a kind of plant sun frost, it is characterised in that be made up of the component of following percetage by weight：
Herba Eupatorii extract 1%~3%, black nightshade extract be 1%~3%, Cacumen Platycladi extract 1%~3%, dimethicone be 0.5%~
1%, stearic acid sorbitol ester and sucrose cocoate are 3%~5%, and glycerine is 3%~5%, and polyethylene glycol 400 is 2%~3%, carboxylic
Sodium carboxymethylcellulose pyce is 0.3%~0.4%, and methyl hydroxybenzoate is 0.15%~0.2%, and surplus is deionized water.
2. plant sun frost as claimed in claim 1, it is characterised in that be made up of the component of following percetage by weight：
Herba Eupatorii extract 2%, black nightshade extract 2%, Cacumen Platycladi extract 2%, dimethicone 0.8%, stearic acid sorbierite
Ester and sucrose cocoate are 4%, glycerine 4%, polyethylene glycol 400 3%, sodium carboxymethylcellulose 0.4%, Metagin
Ester is 0.2%, and surplus is deionized water.
3. a kind of preparation method of the plant sun frost of claim 1 or 2, it is characterised in that the preparation method includes following step
Suddenly：
Step 1
20 mesh sieves are crossed after eupatorium, black nightshade and cacumen biotae are crushed respectively, by obtained eupatorium crushed material, black nightshade crushed material and arbor-vitae
Leaf crushed material is mixed to get mixed powder and minced, and Vltrasonic device ultrasonic extraction is used after mincing middle addition ethanol to mixed powder, after filtering
Obtain extract solution；
Step 2
Extract solution is well mixed with other components, is heated to 90 DEG C, maintains 20min sterilizings；Then 70 DEG C are cooled to,
Emulsification pretreatment 15min is used under 1500r/min；It is slowly stirred after emulsification and is cooled to 40 DEG C of dischargings, obtains plant sun frost, then pass through
Conventional cosmetics quality and safe and healthy detection, packed after qualified.
4. the preparation method of plant sun frost according to claim 3, it is characterised in that the ethanol is that mass percent is dense
The ethanol solution for 50% is spent, it is 5 that mixed powder, which minces with the solid-liquid ratio of ethanol,：1, g/L.
5. the preparation method of plant sun frost according to claim 3, it is characterised in that the supersonic frequency of the ultrasonic extraction
For 30kHz, temperature is 40 DEG C, ultrasonic time 30min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201711075625.4A CN107714548A (en) | 2017-11-06 | 2017-11-06 | A kind of plant sun frost and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711075625.4A CN107714548A (en) | 2017-11-06 | 2017-11-06 | A kind of plant sun frost and preparation method thereof |
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| CN107714548A true CN107714548A (en) | 2018-02-23 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109953922A (en) * | 2019-04-16 | 2019-07-02 | 中国热带农业科学院南亚热带作物研究所 | A kind of Queensland nut peel extract and its preparation method and application |
-
2017
- 2017-11-06 CN CN201711075625.4A patent/CN107714548A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109953922A (en) * | 2019-04-16 | 2019-07-02 | 中国热带农业科学院南亚热带作物研究所 | A kind of Queensland nut peel extract and its preparation method and application |
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Application publication date: 20180223 |