CN107709346B - 用于分离银胶菊的异戊二烯组分的方法 - Google Patents

用于分离银胶菊的异戊二烯组分的方法 Download PDF

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CN107709346B
CN107709346B CN201680036396.2A CN201680036396A CN107709346B CN 107709346 B CN107709346 B CN 107709346B CN 201680036396 A CN201680036396 A CN 201680036396A CN 107709346 B CN107709346 B CN 107709346B
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argentatin
polar solvent
polar
citrullin
obtaining
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CN107709346A (zh
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C·奎尔茨
D·德尔彼尔德
M·卡尔达拉罗
G·吉洛提
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Versalis SpA
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Versalis SpA
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09F—NATURAL RESINS; FRENCH POLISH; DRYING-OILS; OIL DRYING AGENTS, i.e. SICCATIVES; TURPENTINE
    • C09F1/00—Obtaining purification, or chemical modification of natural resins, e.g. oleo-resins
    • C09F1/04—Chemical modification, e.g. esterification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
    • C07C29/095—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of esters of organic acids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0018—Evaporation of components of the mixture to be separated
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/005—Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/14—Preparation of carboxylic acid esters from carboxylic acid halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/56—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07J—STEROIDS
    • C07J53/00—Steroids in which the cyclopenta(a)hydrophenanthrene skeleton has been modified by condensation with a carbocyclic rings or by formation of an additional ring by means of a direct link between two ring carbon atoms, including carboxyclic rings fused to the cyclopenta(a)hydrophenanthrene skeleton are included in this class
    • C07J53/002—Carbocyclic rings fused
    • C07J53/004—3 membered carbocyclic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07J—STEROIDS
    • C07J71/00—Steroids in which the cyclopenta(a)hydrophenanthrene skeleton is condensed with a heterocyclic ring
    • C07J71/0005—Oxygen-containing hetero ring
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08C—TREATMENT OR CHEMICAL MODIFICATION OF RUBBERS
    • C08C1/00—Treatment of rubber latex
    • C08C1/02—Chemical or physical treatment of rubber latex before or during concentration
    • C08C1/04—Purifying; Deproteinising
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/02—Systems containing two condensed rings the rings having only two atoms in common
    • C07C2602/14—All rings being cycloaliphatic
    • C07C2602/32—All rings being cycloaliphatic the ring system containing at least eleven carbon atoms

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Steroid Compounds (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • External Artificial Organs (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
CN201680036396.2A 2015-07-31 2016-07-29 用于分离银胶菊的异戊二烯组分的方法 Active CN107709346B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
ITUB2015A002746A ITUB20152746A1 (it) 2015-07-31 2015-07-31 Metodo per la separazione dei costituenti isoprenici del guayule.
IT102015000040937 2015-07-31
PCT/IB2016/054578 WO2017021852A1 (en) 2015-07-31 2016-07-29 Method for the separation of the isoprenic constituents of guayule

Publications (2)

Publication Number Publication Date
CN107709346A CN107709346A (zh) 2018-02-16
CN107709346B true CN107709346B (zh) 2020-11-03

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US (1) US10570312B2 (https=)
EP (1) EP3328874B1 (https=)
JP (1) JP6776326B2 (https=)
CN (1) CN107709346B (https=)
BR (1) BR112017026757B1 (https=)
CY (1) CY1122620T1 (https=)
DK (1) DK3328874T3 (https=)
ES (1) ES2770005T3 (https=)
HR (1) HRP20200135T1 (https=)
HU (1) HUE048056T2 (https=)
IT (1) ITUB20152746A1 (https=)
LT (1) LT3328874T (https=)
MX (1) MX2018001048A (https=)
MY (1) MY185910A (https=)
PL (1) PL3328874T3 (https=)
PT (1) PT3328874T (https=)
RS (1) RS59889B1 (https=)
RU (1) RU2704821C2 (https=)
SI (1) SI3328874T1 (https=)
SM (1) SMT202000066T1 (https=)
WO (1) WO2017021852A1 (https=)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ITUB20159400A1 (it) * 2015-12-14 2017-06-14 Versalis Spa Procedimento per l?estrazione di lattice, resina e gomma da piante di guayule.
CN109096112B (zh) * 2018-09-20 2021-06-18 上海诗丹德标准技术服务有限公司 款冬酮的制备方法
MX2023007210A (es) * 2020-12-17 2023-08-21 Bridgestone Corp Extraccion de resina de guayule.
WO2022133477A1 (en) * 2020-12-18 2022-06-23 Bridgestone Corporation Modified guayule resin product and related processes
EP4288443A1 (en) * 2021-02-08 2023-12-13 Bridgestone Corporation Modified guayule resin product and related processes
CN117443077B (zh) * 2023-10-27 2024-03-15 临沂广辰化工有限公司 一种菊酸乙酯提纯加工装置及方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4739038A (en) * 1987-01-30 1988-04-19 The Firestone Tire & Rubber Company Process for the controlled partition of guayule resin

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090099309A1 (en) * 2007-10-16 2009-04-16 Yulex Corporation Guayule resin multipolymer
CN107074986B (zh) * 2014-10-22 2018-12-28 维尔萨利斯股份公司 用于加工和利用银胶菊植物的集成工艺

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4739038A (en) * 1987-01-30 1988-04-19 The Firestone Tire & Rubber Company Process for the controlled partition of guayule resin

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
Concise Multigram Purification of Guayulin A from Guayule;Jerome H. Zoeller et al.;《J. Agric. Food Chem.》;19940831;第42卷(第8期);第1648页 Figure 1 *
Insect Growth Regulatory Activity of Some Extracts and Compounds from Parthenium argentatum on Fall Armyworm Spodoptera frugiperda;Carlos L. Céspedes et al.;《Z. Naturforsch.》;20011231;第56C卷;第95页最后一段,第96页倒数第1段和第97页第1段 *
Triterpenes in Parthenium argentatum, structures of argentatins C and D;Romo de Vivar, A. et al.;《Phytochemistry》;19901231;第29卷(第3期);第917页右分栏第2段 *

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WO2017021852A1 (en) 2017-02-09
RS59889B1 (sr) 2020-03-31
JP2018522890A (ja) 2018-08-16
RU2018105348A3 (https=) 2019-08-29
US20180171178A1 (en) 2018-06-21
JP6776326B2 (ja) 2020-10-28
LT3328874T (lt) 2020-04-10
RU2018105348A (ru) 2019-08-29
CY1122620T1 (el) 2021-03-12
HUE048056T2 (hu) 2020-05-28
SMT202000066T1 (it) 2020-07-08
BR112017026757A2 (pt) 2018-08-21
EP3328874A1 (en) 2018-06-06
HRP20200135T1 (hr) 2020-08-21
US10570312B2 (en) 2020-02-25
MY185910A (en) 2021-06-14
BR112017026757B1 (pt) 2021-09-28
CN107709346A (zh) 2018-02-16
ITUB20152746A1 (it) 2017-01-31
EP3328874B1 (en) 2019-11-06
RU2704821C2 (ru) 2019-10-31
DK3328874T3 (da) 2020-02-10
PL3328874T3 (pl) 2020-07-27
SI3328874T1 (sl) 2020-04-30
ES2770005T3 (es) 2020-06-30
PT3328874T (pt) 2020-02-10
MX2018001048A (es) 2018-06-07

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