CN107669597A - A kind of dendrobium candidum after-sun condensation - Google Patents
A kind of dendrobium candidum after-sun condensation Download PDFInfo
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- CN107669597A CN107669597A CN201711144421.1A CN201711144421A CN107669597A CN 107669597 A CN107669597 A CN 107669597A CN 201711144421 A CN201711144421 A CN 201711144421A CN 107669597 A CN107669597 A CN 107669597A
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- dendrobium candidum
- essential oil
- passion fruit
- fruit seed
- parts
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- 241000026010 Dendrobium candidum Species 0.000 title claims abstract description 130
- 238000009833 condensation Methods 0.000 title claims abstract description 21
- 230000005494 condensation Effects 0.000 title claims abstract description 21
- 239000000341 volatile oil Substances 0.000 claims abstract description 67
- 244000288157 Passiflora edulis Species 0.000 claims abstract description 63
- 235000000370 Passiflora edulis Nutrition 0.000 claims abstract description 63
- 239000000284 extract Substances 0.000 claims abstract description 59
- 244000276331 Citrus maxima Species 0.000 claims abstract description 56
- 235000001759 Citrus maxima Nutrition 0.000 claims abstract description 56
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 38
- 239000002994 raw material Substances 0.000 claims abstract description 13
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims abstract description 12
- 229920002385 Sodium hyaluronate Polymers 0.000 claims abstract description 12
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- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims abstract description 12
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- 238000002360 preparation method Methods 0.000 claims description 21
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- CIWBSHSKHKDKBQ-DUZGATOHSA-N D-isoascorbic acid Chemical compound OC[C@@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-DUZGATOHSA-N 0.000 claims description 15
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- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 15
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- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 5
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- SVTBMSDMJJWYQN-UHFFFAOYSA-N 2-methylpentane-2,4-diol Chemical compound CC(O)CC(C)(C)O SVTBMSDMJJWYQN-UHFFFAOYSA-N 0.000 claims description 4
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 4
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- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims description 3
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- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 2
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 2
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims description 2
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- 230000037394 skin elasticity Effects 0.000 abstract description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 10
- 235000005979 Citrus limon Nutrition 0.000 description 5
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- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 4
- 108091005804 Peptidases Proteins 0.000 description 4
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- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 3
- HEVGGTGPGPKZHF-UHFFFAOYSA-N 1-(1,2-dimethyl-3-methylidenecyclopentyl)-4-methylbenzene Chemical compound CC1C(=C)CCC1(C)C1=CC=C(C)C=C1 HEVGGTGPGPKZHF-UHFFFAOYSA-N 0.000 description 2
- 241001523681 Dendrobium Species 0.000 description 2
- 240000004638 Dendrobium nobile Species 0.000 description 2
- 229930013930 alkaloid Natural products 0.000 description 2
- 229930002875 chlorophyll Natural products 0.000 description 2
- 235000019804 chlorophyll Nutrition 0.000 description 2
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 2
- 239000006210 lotion Substances 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
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- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 1
- QCVGEOXPDFCNHA-UHFFFAOYSA-N 5,5-dimethyl-2,4-dioxo-1,3-oxazolidine-3-carboxamide Chemical compound CC1(C)OC(=O)N(C(N)=O)C1=O QCVGEOXPDFCNHA-UHFFFAOYSA-N 0.000 description 1
- 244000144730 Amygdalus persica Species 0.000 description 1
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- 102000008186 Collagen Human genes 0.000 description 1
- 108010035532 Collagen Proteins 0.000 description 1
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
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- 235000015459 Lycium barbarum Nutrition 0.000 description 1
- 208000003351 Melanosis Diseases 0.000 description 1
- 235000006040 Prunus persica var persica Nutrition 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
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- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
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- 235000006708 antioxidants Nutrition 0.000 description 1
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- 230000009286 beneficial effect Effects 0.000 description 1
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- 238000004821 distillation Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 235000014103 egg white Nutrition 0.000 description 1
- 210000000969 egg white Anatomy 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229940087305 limonene Drugs 0.000 description 1
- 235000001510 limonene Nutrition 0.000 description 1
- -1 linoleic acid, vitamin Chemical class 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
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- 239000002932 luster Substances 0.000 description 1
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- 230000037303 wrinkles Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/004—Aftersun preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a kind of dendrobium candidum after-sun condensation, it is made up of the raw material of following parts by weight：0.2 ~ 0.9 part of dendrobium candidum extract solution, 0.2 ~ 0.8 part of passion fruit seed essential oil, 0.1 ~ 0.3 part of Essential Oil From Citrus Grandis Peel, 0.1 ~ 0.5 part of Sodium Hyaluronate, 0.5 ~ 1.0 part of trehalose, 0.1 ~ 0.3 part of lecithin, 5 ~ 20 parts of NMF, 0.5 ~ 2.5 part of gel-type vehicle, 95 ~ 120 parts of water.The present invention can play quick moisturizing moisturizing, keep the effects such as skin elasticity, resistance free radical, injury that is anti-aging, reducing ultraviolet using dendrobium candidum extract solution, passion fruit seed essential oil, Essential Oil From Citrus Grandis Peel as main composition.
Description
Technical field
The present invention relates to skin care field, especially a kind of dendrobium candidum after-sun condensation.
Background technology
Hot summer, protect, how to be repaired after solarization and very important, because the purple in sunlight before not only carrying out solarization
Outside line can take away the large quantity of moisture in skin, if skin moisturizing and repair after shining are not paid attention to, it is possible that skin
The rubescent, symptom such as generate heat, itch, for a long time in this way, phenomena such as there is also blackening and freckle, color spot and wrinkle, makes face
Skin ageing speed is accelerated.
Dendrobium candidum is the traditional Chinese medicine health care product praised highly in recent years for people, is especially suitable for woman's maintenance.Dendrobium candidum is medicinal
With a long history, medicinal ingredient was not only abundant but also balanced, and simply because its is rare, ancient times only have royal noble just to enjoy, and ordinary big
Crowd can seldom touch.The effect of stem of noble dendrobium beautifying face and moistering lotion is mentioned, it is foremost to be no more than empress's Wu Tse-tien.Historical records, Wu Ze
My god " after the year of cycle of sixty years, her hair remains unchanged shiny black lubrication, is imbued with gloss, skin still peach and cream, high resilience ", and she
Beauty treatment, which is driven in side, just the stem of noble dendrobium.And dendrobium candidum passes through modern study and clinical verification, there is taste in nine large effects of dendrobium candidum
Yin-nourishing essence, strengthen the spleen and stomach, protect liver cholagogic, nourish skin the effect of, have remarkable effect to women cosmetology.
But at present by dendrobium candidum be used for after-sun skin care item there is not been reported.
The content of the invention
The invention provides a kind of dendrobium candidum after-sun condensation, with dendrobium candidum extract solution, passion fruit seed essential oil, shaddock
Peel essential oil is main composition, can play quick moisturizing moisturizing, keep skin elasticity, resistance free radical, anti-aging, reduction purple
Injury of outside line etc. acts on.
To achieve the above object, the technical scheme is that：
A kind of dendrobium candidum after-sun condensation, is made up of the raw material of following parts by weight：0.2 ~ 0.9 part of dendrobium candidum extract solution,
0.2 ~ 0.8 part of passion fruit seed essential oil, 0.1 ~ 0.3 part of Essential Oil From Citrus Grandis Peel, 0.1 ~ 0.5 part of Sodium Hyaluronate, 0.5 ~ 1.0 part of trehalose,
0.1 ~ 0.3 part of lecithin, 5 ~ 20 parts of NMF, 0.5 ~ 2.5 part of gel-type vehicle, 95 ~ 120 parts of water.
Preferably, it is made up of the raw material of following parts by weight：0.5 ~ 0.8 part of dendrobium candidum extract solution, passion fruit seed essential oil 0.3
~ 0.6 part, 0.1 ~ 0.3 part of Essential Oil From Citrus Grandis Peel, 0.2 ~ 0.3 part of Sodium Hyaluronate, 0.6 ~ 0.8 part of trehalose, 0.1 ~ 0.3 part of lecithin,
12 ~ 18 parts of NMF, 0.7 ~ 1.5 part of gel-type vehicle, 95 ~ 120 parts of water.
Preferably, it is made up of the raw material of following parts by weight：0.7 part of dendrobium candidum extract solution, 0.5 part of passion fruit seed essential oil,
0.2 part of Essential Oil From Citrus Grandis Peel, 0.3 part of Sodium Hyaluronate, 0.7 part of trehalose, 0.2 part of lecithin, 15 parts of NMF, 1 part of gel-type vehicle,
100 parts of water.
Preferably, the preparation method of the dendrobium candidum extract solution comprises the following steps：
S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the fresh bar of dendrobium candidum is half-and-half splitted, and section, obtains dendrobium candidum piece, fresh leaf is cut into
2 ~ 5mm segment；
S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum
Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.01~0.05:0.01 ~ 0.05, soak time is 20 ~ 30min, is taken out after immersion
Dendrobium candidum piece；
S1-3. the water of dendrobium candidum piece, fresh leaf and 7 ~ 10 times of weight is added in flash extracter, 10 ~ 20min is extracted, obtains
Dendrobium candidum crude extract；
S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；
S1-5. take precipitation to add the ethanol solution that 6 ~ 8 times of volume fractions are 60 ~ 80%, add ethanol solution weight 0.03 ~
0.05% citric acid, 1 ~ 2h of soak extraction obtain alcohol extract, alcohol extract recovery ethanol, be concentrated under reduced pressure into relative density for 1.1 ~
1.2, obtain concentrate；
S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
It is furthermore preferred that in the step S1-1, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 1 ~ 3:3~10.
Preferably, the preparation method of the passion fruit seed essential oil comprises the following steps：
S2-1. passion fruit seed is taken, cleans, dries, is crushed；
S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure
For 25 ~ 29Mpa, extraction temperature is 40 ~ 45 DEG C, CO2Flow is 30 ~ 35L/h, extracts 2 ~ 3h；Carried from what extraction kettle stayed
The CO of passion fruit seed essential oil2Fluid enters separating still, is separated in the case where pressure is 6 ~ 8MPa, temperature is 30 ~ 35 DEG C, obtains passion fruit seed
Crude oil；
S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 1 ~ 2h；Filtered after the completion of standing, obtain passion fruit seed essence
Oil.
Preferably, the preparation method of the Essential Oil From Citrus Grandis Peel comprises the following steps：
S3-1. shaddock ped is dried in the shade, crushes, add the complex enzyme of dry shaddock ped weight 0.02 ~ 0.05%, and added water and soak 2 ~ 4h, leaching
Filtered after the completion of bubble；
S3-2. the shaddock ped after filtering is distilled with steam distillation to obtain Essential Oil From Citrus Grandis Peel.
It is furthermore preferred that the complex enzyme is made up of the component of following parts by weight：0.5 ~ 1 part of pectase, 4 ~ 6 parts of amylase,
2 ~ 3 parts of cellulase, proteinase-10 .5 ~ 1.2 part.
Preferably, the NMF is glycerine, propane diols, glycerine, butanediol, hexylene glycol, xylitol and D-sorbite
One or both of more than.
Preferably, described adhesive is in carbomer, hydroxypropyl methylcellulose, sodium carboxymethylcellulose and glycan substrate
It is one or more kinds of.
The present invention has advantages below：
（1）Using dendrobium candidum extract solution, passion fruit seed essential oil, Essential Oil From Citrus Grandis Peel as main composition, dendrobium candidum contains the present invention
There are the nutritional ingredients such as dendrobium polysaccharide, alkaloid, can play a part of repairing impaired skin, coordinating yin and yang and beautifying face and moistering lotion；Hundred
Fragrant fruit seed essential oil contains the Multiple components such as linoleic acid, vitamin F, mineral matter, linoleic acid, chlorophyll, can resist freedom
Base, injury that is anti-aging, reducing ultraviolet, the collagen in protection skin, prevention melanin deposition, and it is strong with penetration
The characteristics of, it may also help in other beneficiating ingredients and penetrate into skin；In Essential Oil From Citrus Grandis Peel containing limonene and laurene etc. into
Point, there is the effect such as anti-oxidant, anti-inflammatory, above-mentioned three kinds of composition immixtures, skin, quick moisturizing can be rapidly permeated into, reach and repair
Skin is damaged again, reduces uv damage, prevention melanin deposition and other effects.
（2）Further dendrobium candidum fresh leaf is also used by the present invention, and dendrobium candidum leaf is equally containing dendrobium polysaccharide, life
The nutritional ingredients such as alkaloids, with dendrobium candidum stalk compounding use, the viscosity of dendrobium candidum extract solution can be reduced, is more beneficial for effectively
The extraction of composition, and the cost of facial mask can also be substantially reduced.
（3）The present invention also carries out having carried out color protection and fresh-keeping place to dendrobium candidum using arabo-ascorbic acid and sodium acid carbonate
Reason, can preferably retain the chlorophyll content in dendrobium candidum, and dendrobium candidum extract solution is preserved preferable color and luster, avoid
Jaundice, the generation of browning phenomenon.
（4）The extraction of dendrobium candidum and passion fruit seed essential oil all employ low temperature extraction mode so that dendrobium candidum and
Beneficiating ingredient in passion fruit seed is not subjected to the destruction of high temperature, substantially increases extraction efficiency, so as to improve the shield of the present invention
Skin effect.
（5）Essential Oil From Citrus Grandis Peel has carried out enzymolysis processing in advance, then using steam distillation, the distillation that can accelerate functional component is fast
Degree, greatly improves extraction efficiency.
（6）Raw material of the present invention is natural, does not add chemicals, natural no stimulation, and adds passion fruit seed essential oil and make to have
Faster, skin absorbs more preferably, and long-term use can effectively improve skin quality for the infiltration of effect composition.
Embodiment
Below with reference to specific embodiment, the invention will be further described, but protection scope of the present invention be not limited to it is following
Embodiment.
Embodiment 1
A kind of dendrobium candidum after-sun condensation, is made up of the raw material of following parts by weight：0.7 part of dendrobium candidum extract solution, hundred perfume
0.5 part of fruit seed essential oil, 0.2 part of Essential Oil From Citrus Grandis Peel, 0.3 part of Sodium Hyaluronate, 0.7 part of trehalose, 0.2 part of lecithin, 10 parts of glycerine,
5 parts of propane diols, 1 part of carbomer, 100 parts of water.
Wherein, the preparation method of dendrobium candidum extract solution comprises the following steps：
S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 1:3, the fresh bar pair of dendrobium candidum
Partly split, cut into slices, obtain dendrobium candidum piece, fresh leaf is cut into 2 ~ 5mm segment；
S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum
Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.03:0.02, soak time 25min, dendrobium candidum piece is taken out after immersion；
S1-3. the water of dendrobium candidum piece, fresh leaf and 8 times of weight is added in flash extracter, 15min is extracted, obtains iron sheet stone
Dry measure used in former times crude extract；
S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；
S1-5. take precipitation to add the ethanol solution that 7 times of volume fractions are 70%, add the lemon of ethanol solution weight 0.04%
Acid, soak extraction 2h, alcohol extract is obtained, alcohol extract recovery ethanol, it is 1.1 ~ 1.2 to be concentrated under reduced pressure into relative density, obtains concentrate；
S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
The preparation method of passion fruit seed essential oil comprises the following steps：
S2-1. passion fruit seed is taken, cleans, dries, is crushed；
S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure
For 26Mpa, extraction temperature is 42 DEG C, CO2Flow is 32L/h, extracts 3h；Passion fruit seed essential oil is carried from what extraction kettle stayed
CO2Fluid enters separating still, is separated in the case where pressure is 7MPa, temperature is 33 DEG C, obtains passion fruit seed crude oil；
S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 1.5h；Filtered after the completion of standing, obtain passion fruit seed essence
Oil.
The preparation method of Essential Oil From Citrus Grandis Peel comprises the following steps：
S3-1. shaddock ped is dried in the shade, crushes, add the complex enzyme of dry shaddock ped weight 0.04%, and add water immersion 3h, water is with no mistake
Shaddock ped is defined, and is filtered after the completion of immersion；
S3-2. the shaddock ped after filtering is distilled with steam distillation to obtain Essential Oil From Citrus Grandis Peel.
Wherein, complex enzyme is made up of the component of following parts by weight：0.8 part of pectase, 5 parts of amylase, cellulase 2.5
Part, 1 part of protease.
Embodiment 2
A kind of dendrobium candidum after-sun condensation, is made up of the raw material of following parts by weight：0.5 part of dendrobium candidum extract solution, hundred perfume
0.3 part of fruit seed essential oil, 0.1 part of Essential Oil From Citrus Grandis Peel, 0.2 part of Sodium Hyaluronate, 0.6 part of trehalose, 0.1 part of lecithin, 6 parts of glycerine,
6 parts of butanediol, 0.7 part of carbomer, 95 parts of water.
Wherein, the preparation method of dendrobium candidum extract solution comprises the following steps：
S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 1:6, the fresh bar pair of dendrobium candidum
Partly split, cut into slices, obtain dendrobium candidum piece, fresh leaf is cut into 2 ~ 5mm segment；
S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum
Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.01:0.05, soak time 25min, dendrobium candidum piece is taken out after immersion；
S1-3. the water of dendrobium candidum piece, fresh leaf and 7 times of weight is added in flash extracter, 10min is extracted, obtains iron sheet stone
Dry measure used in former times crude extract；
S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；
S1-5. take precipitation to add the ethanol solution that 8 times of volume fractions are 60%, add the lemon of ethanol solution weight 0.03%
Acid, soak extraction 2h, alcohol extract is obtained, alcohol extract recovery ethanol, it is 1.1 ~ 1.2 to be concentrated under reduced pressure into relative density, obtains concentrate；
S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
The preparation method of passion fruit seed essential oil comprises the following steps：
S2-1. passion fruit seed is taken, cleans, dries, is crushed；
S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure
For 25Mpa, extraction temperature is 45 DEG C, CO2Flow is 35L/h, extracts 2h；Passion fruit seed essential oil is carried from what extraction kettle stayed
CO2Fluid enters separating still, is separated in the case where pressure is 8MPa, temperature is 35 DEG C, obtains passion fruit seed crude oil；
S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 2h；Filtered after the completion of standing, obtain passion fruit seed essential oil.
The preparation method of Essential Oil From Citrus Grandis Peel comprises the following steps：
S3-1. shaddock ped is dried in the shade, crushes, add the complex enzyme of dry shaddock ped weight 0.02%, and add water immersion 3h, water is with no mistake
Shaddock ped is defined, and is filtered after the completion of immersion；
S3-2. the shaddock ped after filtering is distilled with steam distillation to obtain Essential Oil From Citrus Grandis Peel.
Wherein, complex enzyme is made up of the component of following parts by weight：0.5 part of pectase, 6 parts of amylase, 3 parts of cellulase,
1.2 parts of protease.
Embodiment 3
A kind of dendrobium candidum after-sun condensation, is made up of the raw material of following parts by weight：0.8 part of dendrobium candidum extract solution, hundred perfume
0.6 part of fruit seed essential oil, 0.3 part of Essential Oil From Citrus Grandis Peel, 0.3 part of Sodium Hyaluronate, 0.8 part of trehalose, 0.3 part of lecithin, 10 parts of glycerine,
8 parts of D-sorbite, 1.5 parts of sodium carboxymethylcellulose, 120 parts of water.
Wherein, the preparation method of dendrobium candidum extract solution comprises the following steps：
S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 2:7, the fresh bar pair of dendrobium candidum
Partly split, cut into slices, obtain dendrobium candidum piece, fresh leaf is cut into 2 ~ 5mm segment；
S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum
Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.05:0.01, soak time 20min, dendrobium candidum piece is taken out after immersion；
S1-3. the water of dendrobium candidum piece, fresh leaf and 7 times of weight is added in flash extracter, 12min is extracted, obtains iron sheet stone
Dry measure used in former times crude extract；
S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；
S1-5. take precipitation to add the ethanol solution that 6 times of volume fractions are 80%, add the lemon of ethanol solution weight 0.05%
Acid, soak extraction 2h, alcohol extract is obtained, alcohol extract recovery ethanol, it is 1.1 ~ 1.2 to be concentrated under reduced pressure into relative density, obtains concentrate；
S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
The preparation method of passion fruit seed essential oil comprises the following steps：
S2-1. passion fruit seed is taken, cleans, dries, is crushed；
S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure
For 29Mpa, extraction temperature is 45 DEG C, CO2Flow is 30L/h, extracts 2h；Passion fruit seed essential oil is carried from what extraction kettle stayed
CO2Fluid enters separating still, is separated in the case where pressure is 8MPa, temperature is 35 DEG C, obtains passion fruit seed crude oil；
S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 2h；Filtered after the completion of standing, obtain passion fruit seed essential oil.
The preparation method of Essential Oil From Citrus Grandis Peel comprises the following steps：
S3-1. shaddock ped is dried in the shade, crushes, add the complex enzyme of dry shaddock ped weight 0.05%, and add water immersion 3h, water is with no mistake
Shaddock ped is defined, and is filtered after the completion of immersion；
S3-2. the shaddock ped after filtering is distilled with steam distillation to obtain Essential Oil From Citrus Grandis Peel.
Wherein, complex enzyme is made up of the component of following parts by weight：1 part of pectase, 4 parts of amylase, 2 parts of cellulase, egg
White 0.5 part of enzyme.
Embodiment 4
A kind of dendrobium candidum after-sun condensation, is made up of the raw material of following parts by weight：0.2 part of dendrobium candidum extract solution, hundred perfume
0.2 part of fruit seed essential oil, 0.1 part of Essential Oil From Citrus Grandis Peel, 0.1 part of Sodium Hyaluronate, 0.5 part of trehalose, 0.1 part of lecithin, 5 parts of glycerine,
0.5 part of carbomer, 95 parts of water.
Wherein, the preparation method of dendrobium candidum extract solution comprises the following steps：
S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 1:9, the fresh bar pair of dendrobium candidum
Partly split, cut into slices, obtain dendrobium candidum piece, fresh leaf is cut into 2 ~ 5mm segment；
S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum
Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.03:0.03, soak time 20min, dendrobium candidum piece is taken out after immersion；
S1-3. the water of dendrobium candidum piece, fresh leaf and 7 times of weight is added in flash extracter, 12min is extracted, obtains iron sheet stone
Dry measure used in former times crude extract；
S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；
S1-5. take precipitation to add the ethanol solution that 7 times of volume fractions are 80%, add the lemon of ethanol solution weight 0.03%
Acid, soak extraction 1h, alcohol extract is obtained, alcohol extract recovery ethanol, it is 1.1 ~ 1.2 to be concentrated under reduced pressure into relative density, obtains concentrate；
S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
The preparation method of passion fruit seed essential oil comprises the following steps：
S2-1. passion fruit seed is taken, cleans, dries, is crushed；
S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure
For 29Mpa, extraction temperature is 40 DEG C, CO2Flow is 35L/h, extracts 3h；Passion fruit seed essential oil is carried from what extraction kettle stayed
CO2Fluid enters separating still, is separated in the case where pressure is 8MPa, temperature is 30 DEG C, obtains passion fruit seed crude oil；
S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 2h；Filtered after the completion of standing, obtain passion fruit seed essential oil.
The preparation method of Essential Oil From Citrus Grandis Peel comprises the following steps：
S3-1. shaddock ped is dried in the shade, crushes, add the complex enzyme of dry shaddock ped weight 0.03%, and add water immersion 3h, water is with no mistake
Shaddock ped is defined, and is filtered after the completion of immersion；
S3-2. the shaddock ped after filtering is distilled with steam distillation to obtain Essential Oil From Citrus Grandis Peel.
Wherein, complex enzyme is made up of the component of following parts by weight：0.9 part of pectase, 4.5 parts of amylase, cellulase 2.5
Part, 1 part of protease.
Embodiment 5
A kind of dendrobium candidum after-sun condensation, is made up of the raw material of following parts by weight：2 parts of dendrobium candidum extract solution, passion fruit
1 part of seed essential oil, 0.5 part of tea tree ethereal oil, 0.5 part of Sodium Hyaluronate, 0.8 part of lecithin, 5 parts of glycerine, 14 parts of propane diols, xylitol
1 part, 0.03 part of sodium carboxymethylcellulose, 120 parts of water.
Wherein, the preparation method of dendrobium candidum extract solution comprises the following steps：
S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 1:3, the fresh bar pair of dendrobium candidum
Partly split, cut into slices, obtain dendrobium candidum piece, fresh leaf is cut into 2 ~ 5mm segment；
S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum
Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.03:0.03, soak time 20min, dendrobium candidum piece is taken out after immersion；
S1-3. the water of dendrobium candidum piece, fresh leaf and 7 times of weight is added in flash extracter, 12min is extracted, obtains iron sheet stone
Dry measure used in former times crude extract；
S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；
S1-5. take precipitation to add the ethanol solution that 7 times of volume fractions are 80%, add the lemon of ethanol solution weight 0.03%
Acid, soak extraction 2h, alcohol extract is obtained, alcohol extract recovery ethanol, it is 1.1 ~ 1.2 to be concentrated under reduced pressure into relative density, obtains concentrate；
S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
The preparation method of passion fruit seed essential oil comprises the following steps：
S2-1. passion fruit seed is taken, cleans, dries, is crushed；
S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure
For 29Mpa, extraction temperature is 40 DEG C, CO2Flow is 35L/h, extracts 3h；Passion fruit seed essential oil is carried from what extraction kettle stayed
CO2Fluid enters separating still, is separated in the case where pressure is 8MPa, temperature is 35 DEG C, obtains passion fruit seed crude oil；
S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 2h；Filtered after the completion of standing, obtain passion fruit seed essential oil.
The preparation method of Essential Oil From Citrus Grandis Peel comprises the following steps：
S3-1. shaddock ped is dried in the shade, crushes, add the complex enzyme of dry shaddock ped weight 0.05%, and add water immersion 3h, water is with no mistake
Shaddock ped is defined, and is filtered after the completion of immersion；
S3-2. the shaddock ped after filtering is distilled with steam distillation to obtain Essential Oil From Citrus Grandis Peel.
Wherein, complex enzyme is made up of the component of following parts by weight：0.9 part of pectase, 5 parts of amylase, cellulase 2.5
Part, 1 part of protease.
The tester of the product skin sunburn of above-described embodiment 1 ~ 5 is taken to use.
Tester's screening criteria：Skin is tanned severely on the face, has rubescent and decortication phenomenon, and rubescent or decortication area accounts for face
More than the 20% of area.
Application method uses on the face for the product of above-described embodiment is coated in tester, daily sooner or later using once, connects
It is continuous to use two days.
Tester totally 100, it is randomly divided into 5 groups, every group 20.
Using effect judges：
It is effective：Without rubefaction or decortication phenomenon.
Effectively：Rubefaction phenomenon and decortication phenomenon weaken.
It is invalid：Rubefaction and decortication phenomenon are unchanged.
Test result：
| Group | It is effective | Effectively | It is invalid | It is efficient |
| Embodiment 1 | 18 | 2 | 0 | 100% |
| Embodiment 2 | 15 | 5 | 0 | 100% |
| Embodiment 3 | 16 | 4 | 0 | 100% |
| Embodiment 4 | 10 | 9 | 1 | 95% |
| Embodiment 5 | 15 | 4 | 1 | 95% |
Claims (10)
- A kind of 1. dendrobium candidum after-sun condensation, it is characterised in that：It is made up of the raw material of following parts by weight：0.2 ~ 0.9 part of dendrobium candidum extract solution, 0.2 ~ 0.8 part of passion fruit seed essential oil, shaddock ped 0.1 ~ 0.3 part of essential oil, 0.1 ~ 0.5 part of Sodium Hyaluronate, 0.5 ~ 1.0 part of trehalose, 0.1 ~ 0.3 part of lecithin, NMF 5 ~ 20 Part, 0.5 ~ 2.5 part of gel-type vehicle, 95 ~ 120 parts of water.
- 2. dendrobium candidum after-sun condensation according to claim 1, it is characterised in that：It is made up of the raw material of following parts by weight：0.5 ~ 0.8 part of dendrobium candidum extract solution, 0.3 ~ 0.6 part of passion fruit seed essential oil, shaddock ped 0.1 ~ 0.3 part of essential oil, 0.2 ~ 0.3 part of Sodium Hyaluronate, 0.6 ~ 0.8 part of trehalose, 0.1 ~ 0.3 part of lecithin, NMF 12 ~ 18 Part, 0.7 ~ 1.5 part of gel-type vehicle, 95 ~ 120 parts of water.
- 3. dendrobium candidum after-sun condensation according to claim 1, it is characterised in that：It is made up of the raw material of following parts by weight：0.7 part of dendrobium candidum extract solution, 0.5 part of passion fruit seed essential oil, Essential Oil From Citrus Grandis Peel 0.2 Part, 0.3 part of Sodium Hyaluronate, 0.7 part of trehalose, 0.2 part of lecithin, 15 parts of NMF, 1 part of gel-type vehicle, 100 parts of water.
- 4. the dendrobium candidum after-sun condensation according to any one of claim 1 ~ 3, it is characterised in that：The preparation method of the dendrobium candidum extract solution comprises the following steps：S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the fresh bar of dendrobium candidum is half-and-half splitted, and section, obtains dendrobium candidum piece, fresh leaf is cut into 2 ~ 5mm segment；S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.01~0.05:0.01 ~ 0.05, soak time is 20 ~ 30min, is taken out after immersion Dendrobium candidum piece；S1-3. the water of dendrobium candidum piece, fresh leaf and 7 ~ 10 times of weight is added in flash extracter, 10 ~ 20min is extracted, obtains Dendrobium candidum crude extract；S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；S1-5. take precipitation to add the ethanol solution that 6 ~ 8 times of volume fractions are 60 ~ 80%, add ethanol solution weight 0.03 ~ 0.05% citric acid, 1 ~ 2h of soak extraction obtain alcohol extract, alcohol extract recovery ethanol, be concentrated under reduced pressure into relative density for 1.1 ~ 1.2, obtain concentrate；S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
- 5. the dendrobium candidum after-sun condensation according to any one of claim 1 ~ 3, it is characterised in that：The preparation method of the passion fruit seed essential oil comprises the following steps：S2-1. passion fruit seed is taken, cleans, dries, is crushed；S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure For 25 ~ 29Mpa, extraction temperature is 40 ~ 45 DEG C, CO2Flow is 30 ~ 35L/h, extracts 2 ~ 3h；Carried from what extraction kettle stayed The CO of passion fruit seed essential oil2Fluid enters separating still, is separated in the case where pressure is 6 ~ 8MPa, temperature is 30 ~ 35 DEG C, obtains passion fruit seed Crude oil；S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 1 ~ 2h；Filtered after the completion of standing, obtain passion fruit seed essence Oil.
- 6. the dendrobium candidum after-sun condensation according to any one of claim 1 ~ 3, it is characterised in that：The preparation method of the Essential Oil From Citrus Grandis Peel comprises the following steps：S3-1. shaddock ped is dried in the shade, crushes, add the complex enzyme of dry shaddock ped weight 0.02 ~ 0.05%, and added water and soak 2 ~ 4h, leaching Filtered after the completion of bubble；S3-2. the shaddock ped after filtering is distilled with steam distillation to obtain Essential Oil From Citrus Grandis Peel.
- 7. the dendrobium candidum after-sun condensation according to any one of claim 6, it is characterised in that：The complex enzyme is made up of the component of following parts by weight：0.5 ~ 1 part of pectase, 4 ~ 6 parts of amylase, 2 ~ 3 parts of cellulase, Proteinase-10 .5 ~ 1.2 part.
- 8. the dendrobium candidum after-sun condensation according to any one of claim 1 ~ 3, it is characterised in that：The NMF is one kind or two in glycerine, propane diols, glycerine, butanediol, hexylene glycol, xylitol and D-sorbite More than kind.
- 9. the dendrobium candidum after-sun condensation according to any one of claim 1 ~ 3, it is characterised in that：Described adhesive is one or both of carbomer, hydroxypropyl methylcellulose, sodium carboxymethylcellulose and glycan substrate More than.
- 10. dendrobium candidum after-sun condensation according to claim 4, it is characterised in that：In the step S1-1, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 1 ~ 3:3~10.
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| CN109125133A (en) * | 2018-10-24 | 2019-01-04 | 西安惟颐生物科技有限公司 | Female chest maintains compound essential oil |
| CN110613635A (en) * | 2019-11-11 | 2019-12-27 | 高振军 | Hand cream containing passion fruit essential oil and preparation method |
| CN111437236A (en) * | 2020-04-26 | 2020-07-24 | 华南农业大学 | Dendrobium extract, preparation method and application thereof |
| CN111481454A (en) * | 2020-04-10 | 2020-08-04 | 蚌埠天泽家用化学品有限公司 | Preparation method of nourishing anti-cracking hand cream |
| CN112245376A (en) * | 2020-11-27 | 2021-01-22 | 泰州医药城国科化物生物医药科技有限公司 | Preparation method of antioxidant dendrobium extract, dendrobium antioxidant essence and preparation method thereof |
| CN114469806A (en) * | 2022-01-27 | 2022-05-13 | 露乐健康科技股份有限公司 | Composition for relieving after-sun skin and application thereof |
| CN114796075A (en) * | 2022-05-10 | 2022-07-29 | 浙江森宇有限公司 | Compound containing dendrobium officinale flowers and application of compound in skin care products |
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2017
- 2017-11-17 CN CN201711144421.1A patent/CN107669597B/en not_active Expired - Fee Related
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| CN114848566A (en) * | 2022-05-16 | 2022-08-05 | 江南大学 | Preparation method and application of dendrobium officinale extract for resisting skin photoaging |
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