CN107811939A - A kind of dendrobium candidum facial mask - Google Patents
A kind of dendrobium candidum facial mask Download PDFInfo
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- CN107811939A CN107811939A CN201711143995.7A CN201711143995A CN107811939A CN 107811939 A CN107811939 A CN 107811939A CN 201711143995 A CN201711143995 A CN 201711143995A CN 107811939 A CN107811939 A CN 107811939A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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Abstract
The invention provides a kind of dendrobium candidum facial mask, it is made up of the raw material of following parts by weight：0.5 ~ 2 part of dendrobium candidum extract solution, 0.2 ~ 1 part of passion fruit seed essential oil, 0.1 ~ 0.5 part of tea tree ethereal oil, 0.1 ~ 0.5 part of Sodium Hyaluronate, 0.2 ~ 0.8 part of lecithin, 5 ~ 20 parts of NMF, 0.01 ~ 0.03 part of adhesive, 95 ~ 120 parts of water.The dendrobium candidum extract solution that the present invention is extracted using dendrobium candidum stalk and fresh leaf, is mixed with passion fruit seed essential oil, tea tree ethereal oil, can be played and be removed the effect such as acne, Whitening, spot, moisturizing moisturizing.
Description
Technical field
The present invention relates to skin care field, especially a kind of dendrobium candidum facial mask.
Background technology
Dendrobium candidum is the traditional Chinese medicine health care product praised highly in recent years for people, is especially suitable for woman's maintenance.Dendrobium candidum is medicinal
With a long history, medicinal ingredient was not only abundant but also balanced, and simply because its is rare, ancient times only have royal noble just to enjoy, and ordinary big
Crowd can seldom touch.The effect of stem of noble dendrobium beautifying face and moistering lotion is mentioned, it is foremost to be no more than empress's Wu Tse-tien.Historical records, Wu Ze
My god " after the year of cycle of sixty years, her hair remains unchanged shiny black lubrication, is imbued with gloss, skin still peach and cream, high resilience ", and she
Beauty treatment, which is driven in side, just the stem of noble dendrobium.
And dendrobium candidum passes through modern study and clinical verification, there are nourishing essence, help in nine large effects of dendrobium candidum
Taste, protect liver cholagogic, the effect of skin is nourished, have remarkable effect to women cosmetology.But current being made of dendrobium candidum
Cosmetic mostly be to be processed again after maple bucket is made in dendrobium candidum, its process can nutritious loss, and also only be utilization
The stalk of dendrobium candidum, and the leaf of dendrobium candidum is not utilized more.
The content of the invention
The invention provides a kind of dendrobium candidum facial mask, the dendrobium candidum extracted using dendrobium candidum stalk and fresh leaf is extracted
Liquid, mixed with passion fruit seed essential oil, tea tree ethereal oil, can play and remove the effect such as acne, Whitening, spot, moisturizing moisturizing.
To achieve the above object, the technical scheme is that：
A kind of dendrobium candidum facial mask, is made up of the raw material of following parts by weight：0.5 ~ 2 part of dendrobium candidum extract solution, passion fruit seed essence
Oil 0.2 ~ 1 part, 0.1 ~ 0.5 part of tea tree ethereal oil, 0.1 ~ 0.5 part of Sodium Hyaluronate, 0.2 ~ 0.8 part of lecithin, 5 ~ 20 parts of NMF,
0.01 ~ 0.03 part of adhesive, 95 ~ 120 parts of water.
Preferably, it is made up of the raw material of following parts by weight：0.8 ~ 1.6 part of dendrobium candidum extract solution, passion fruit seed essential oil 0.4
~ 0.9 part, it is 0.2 ~ 0.4 part of tea tree ethereal oil, 0.2 ~ 0.4 part of Sodium Hyaluronate, 0.3 ~ 0.7 part of lecithin, 10 ~ 15 parts of NMF, viscous
0.01 ~ 0.03 part of mixture, 95 ~ 120 parts of water.
It is furthermore preferred that it is made up of the raw material of following parts by weight：1.2 parts of dendrobium candidum extract solution, passion fruit seed essential oil 0.8
Part, 0.2 part of tea tree ethereal oil, 0.3 part of Sodium Hyaluronate, 0.5 part of lecithin, 13 parts of NMF, 0.02 part of adhesive, 100 parts of water.
Preferably, the preparation method of the dendrobium candidum extract solution comprises the following steps：
S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the fresh bar of dendrobium candidum is half-and-half splitted, and section, obtains dendrobium candidum piece, fresh leaf is cut into
2 ~ 5mm segment；
S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum
Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.01~0.05:0.01 ~ 0.05, soak time is 20 ~ 30min, is taken out after immersion
Dendrobium candidum piece；
S1-3. the water of dendrobium candidum piece, fresh leaf and 7 ~ 10 times of weight is added in flash extracter, 10 ~ 20min is extracted, obtains
Dendrobium candidum crude extract；
S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；
S1-5. take precipitation to add the ethanol solution that 6 ~ 8 times of volume fractions are 60 ~ 80%, add ethanol solution weight 0.03 ~
0.05% citric acid, 1 ~ 2h of soak extraction obtain alcohol extract, alcohol extract recovery ethanol, be concentrated under reduced pressure into relative density for 1.1 ~
1.2, obtain concentrate；
S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
Preferably, the preparation method of the passion fruit seed essential oil comprises the following steps：
S2-1. passion fruit seed is taken, cleans, dries, is crushed；
S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure
For 25 ~ 29Mpa, extraction temperature is 40 ~ 45 DEG C, CO2Flow is 30 ~ 35L/h, extracts 2 ~ 3h；Carried from what extraction kettle stayed
The CO of passion fruit seed essential oil2Fluid enters separating still, is separated in the case where pressure is 6 ~ 8MPa, temperature is 30 ~ 35 DEG C, obtains passion fruit seed
Crude oil；
S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 1 ~ 2h；Filtered after the completion of standing, obtain passion fruit seed essence
Oil.
Preferably, the NMF is glycerine, propane diols, glycerine, butanediol, hexylene glycol, xylitol and D-sorbite
One or both of more than.
Preferably, described adhesive is in sodium carboxymethylcellulose, hydroxyethyl cellulose, xanthans, carragheen and pectin
One or more.
Preferably, in the step S1-1, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 1 ~ 3:3~10.
The present invention has advantages below：
（1）Fully the fresh leaf of dendrobium candidum is also used by the present invention, and dendrobium candidum leaf is equally containing dendrobium polysaccharide, alkaloid
Etc. nutritional ingredient, it may have the effect of coordinating yin and yang, moistening lung and production of body fluid, beautifying face and moistering lotion, with dendrobium candidum stalk compounding use, can drop
The viscosity of low dendrobium candidum extract solution, the extraction of active ingredient is more beneficial for, and the cost of facial mask can also be substantially reduced.
（2）The present invention is also added into passion fruit seed essential oil and tea tree ethereal oil, and passion fruit seed essential oil contains linoleic acid, vitamin
F, the Multiple components such as mineral matter, linoleic acid, chlorophyll, can resist free radical, it is anti-aging, reduce ultraviolet injury,
Protect skin in collagen, prevention melanin deposition, and with penetration it is strong the characteristics of, may also help in other beneficial into
Divide and penetrate into skin；Tea tree ethereal oil contain Meng's ethene, dipentene, limonene, cineol, sesame oil brain and anisoxide etc. into
Point, there is the effects such as significant anti-inflammatory, regulation skin oil and fat secretion, dendrobium candidum extract solution, passion fruit seed essential oil and tea tree essence
Oil synergy, the speed that dendrobium candidum beneficiating ingredient penetrates into skin, and the water oil of comprehensive adjustment skin can be greatly improved
Balance, play and remove the effects such as acne, Whitening, spot, moisturizing moisturizing, holding elasticity of skin.
（3）The present invention also carries out having carried out color protection and fresh-keeping place to dendrobium candidum using arabo-ascorbic acid and sodium acid carbonate
Reason, can preferably retain the chlorophyll content in dendrobium candidum, and dendrobium candidum extract solution is preserved preferable color and luster, avoid
Jaundice, the generation of browning phenomenon.
（4）The extraction of dendrobium candidum and passion fruit seed essential oil all employ low temperature extraction mode so that dendrobium candidum and
Beneficiating ingredient in passion fruit seed is not subjected to the destruction of high temperature, substantially increases extraction efficiency, so as to improve the shield of the present invention
Skin effect.
（5）Raw material of the present invention is natural, does not add chemicals, natural no stimulation, and adds passion fruit seed essential oil and make to have
Faster, skin absorbs more preferably, and long-term use can effectively improve skin quality for the infiltration of effect composition.
Embodiment
Below with reference to specific embodiment, the invention will be further described, but protection scope of the present invention be not limited to it is following
Embodiment.
Embodiment 1
A kind of dendrobium candidum facial mask, is made up of the raw material of following parts by weight：1.2 parts of dendrobium candidum extract solution, passion fruit seed essential oil
0.8 part, 0.2 part of tea tree ethereal oil, 0.3 part of Sodium Hyaluronate, 0.5 part of lecithin, 6 parts of glycerine, 7 parts of propane diols, xanthans 0.02
Part, 100 parts of water.
Wherein, the preparation method of dendrobium candidum extract solution comprises the following steps：
S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 1:3, the fresh bar pair of dendrobium candidum
Partly split, cut into slices, obtain dendrobium candidum piece, fresh leaf is cut into 2 ~ 5mm segment；
S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum
Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.03:0.02, soak time 25min, dendrobium candidum piece is taken out after immersion；
S1-3. the water of dendrobium candidum piece, fresh leaf and 8 times of weight is added in flash extracter, 15min is extracted, obtains iron sheet stone
Dry measure used in former times crude extract；
S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；
S1-5. take precipitation to add the ethanol solution that 7 times of volume fractions are 70%, add the lemon of ethanol solution weight 0.04%
Acid, soak extraction 2h, alcohol extract is obtained, alcohol extract recovery ethanol, it is 1.1 ~ 1.2 to be concentrated under reduced pressure into relative density, obtains concentrate；
S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
The preparation method of passion fruit seed essential oil comprises the following steps：
S2-1. passion fruit seed is taken, cleans, dries, is crushed；
S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure
For 26Mpa, extraction temperature is 42 DEG C, CO2Flow is 32L/h, extracts 3h；Passion fruit seed essential oil is carried from what extraction kettle stayed
CO2Fluid enters separating still, is separated in the case where pressure is 7MPa, temperature is 33 DEG C, obtains passion fruit seed crude oil；
S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 1.5h；Filtered after the completion of standing, obtain passion fruit seed essence
Oil.
Embodiment 2
A kind of dendrobium candidum facial mask, is made up of the raw material of following parts by weight：0.8 part of dendrobium candidum extract solution, passion fruit seed essential oil
0.4 part, 0.2 part of tea tree ethereal oil, 0.2 part of Sodium Hyaluronate, 0.3 part of lecithin, 6 parts of glycerine, 4 parts of glycerine, hydroxy ethyl fiber
Plain 0.01 part, 95 parts of water.
Wherein, the preparation method of dendrobium candidum extract solution comprises the following steps：
S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 1:6, the fresh bar pair of dendrobium candidum
Partly split, cut into slices, obtain dendrobium candidum piece, fresh leaf is cut into 2 ~ 5mm segment；
S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum
Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.01:0.05, soak time 25min, dendrobium candidum piece is taken out after immersion；
S1-3. the water of dendrobium candidum piece, fresh leaf and 7 times of weight is added in flash extracter, 10min is extracted, obtains iron sheet stone
Dry measure used in former times crude extract；
S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；
S1-5. take precipitation to add the ethanol solution that 8 times of volume fractions are 60%, add the lemon of ethanol solution weight 0.03%
Acid, soak extraction 2h, alcohol extract is obtained, alcohol extract recovery ethanol, it is 1.1 ~ 1.2 to be concentrated under reduced pressure into relative density, obtains concentrate；
S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
The preparation method of passion fruit seed essential oil comprises the following steps：
S2-1. passion fruit seed is taken, cleans, dries, is crushed；
S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure
For 25Mpa, extraction temperature is 45 DEG C, CO2Flow is 35L/h, extracts 2h；Passion fruit seed essential oil is carried from what extraction kettle stayed
CO2Fluid enters separating still, is separated in the case where pressure is 8MPa, temperature is 35 DEG C, obtains passion fruit seed crude oil；
S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 2h；Filtered after the completion of standing, obtain passion fruit seed essential oil.
Embodiment 3
A kind of dendrobium candidum facial mask, is made up of the raw material of following parts by weight：1.6 parts of dendrobium candidum extract solution, passion fruit seed essential oil
0.9 part, 0.4 part of tea tree ethereal oil, 0.4 part of Sodium Hyaluronate, 0.7 part of lecithin, 6 parts of glycerine, 9 parts of D-sorbite, ethoxy it is fine
Dimension plain 0.03 part, 120 parts of water.
Wherein, the preparation method of dendrobium candidum extract solution comprises the following steps：
S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 2:7, the fresh bar pair of dendrobium candidum
Partly split, cut into slices, obtain dendrobium candidum piece, fresh leaf is cut into 2 ~ 5mm segment；
S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum
Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.05:0.01, soak time 20min, dendrobium candidum piece is taken out after immersion；
S1-3. the water of dendrobium candidum piece, fresh leaf and 7 times of weight is added in flash extracter, 12min is extracted, obtains iron sheet stone
Dry measure used in former times crude extract；
S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；
S1-5. take precipitation to add the ethanol solution that 6 times of volume fractions are 80%, add the lemon of ethanol solution weight 0.05%
Acid, soak extraction 2h, alcohol extract is obtained, alcohol extract recovery ethanol, it is 1.1 ~ 1.2 to be concentrated under reduced pressure into relative density, obtains concentrate；
S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
The preparation method of passion fruit seed essential oil comprises the following steps：
S2-1. passion fruit seed is taken, cleans, dries, is crushed；
S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure
For 29Mpa, extraction temperature is 45 DEG C, CO2Flow is 30L/h, extracts 2h；Passion fruit seed essential oil is carried from what extraction kettle stayed
CO2Fluid enters separating still, is separated in the case where pressure is 8MPa, temperature is 35 DEG C, obtains passion fruit seed crude oil；
S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 2h；Filtered after the completion of standing, obtain passion fruit seed essential oil.
Embodiment 4
A kind of dendrobium candidum facial mask, is made up of the raw material of following parts by weight：0.5 part of dendrobium candidum extract solution, passion fruit seed essential oil
0.2 part, 0.1 part of tea tree ethereal oil, 0.1 part of Sodium Hyaluronate, 0.2 part of lecithin, 5 parts of glycerine, 0.01 part of carragheen, 95 parts of water.
Wherein, the preparation method of dendrobium candidum extract solution comprises the following steps：
S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 1:9, the fresh bar pair of dendrobium candidum
Partly split, cut into slices, obtain dendrobium candidum piece, fresh leaf is cut into 2 ~ 5mm segment；
S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum
Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.03:0.03, soak time 20min, dendrobium candidum piece is taken out after immersion；
S1-3. the water of dendrobium candidum piece, fresh leaf and 7 times of weight is added in flash extracter, 12min is extracted, obtains iron sheet stone
Dry measure used in former times crude extract；
S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；
S1-5. take precipitation to add the ethanol solution that 7 times of volume fractions are 80%, add the lemon of ethanol solution weight 0.03%
Acid, soak extraction 1h, alcohol extract is obtained, alcohol extract recovery ethanol, it is 1.1 ~ 1.2 to be concentrated under reduced pressure into relative density, obtains concentrate；
S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
The preparation method of passion fruit seed essential oil comprises the following steps：
S2-1. passion fruit seed is taken, cleans, dries, is crushed；
S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure
For 29Mpa, extraction temperature is 40 DEG C, CO2Flow is 35L/h, extracts 3h；Passion fruit seed essential oil is carried from what extraction kettle stayed
CO2Fluid enters separating still, is separated in the case where pressure is 8MPa, temperature is 30 DEG C, obtains passion fruit seed crude oil；
S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 2h；Filtered after the completion of standing, obtain passion fruit seed essential oil.
Embodiment 5
A kind of dendrobium candidum facial mask, is made up of the raw material of following parts by weight：2 parts of dendrobium candidum extract solution, passion fruit seed essential oil 1
Part, 0.5 part of tea tree ethereal oil, 0.5 part of Sodium Hyaluronate, 0.8 part of lecithin, 5 parts of glycerine, 14 parts of propane diols, 1 part of xylitol, carboxylic
0.03 part of sodium carboxymethylcellulose pyce, 120 parts of water.
Wherein, the preparation method of dendrobium candidum extract solution comprises the following steps：
S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 1:3, the fresh bar pair of dendrobium candidum
Partly split, cut into slices, obtain dendrobium candidum piece, fresh leaf is cut into 2 ~ 5mm segment；
S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum
Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.03:0.03, soak time 20min, dendrobium candidum piece is taken out after immersion；
S1-3. the water of dendrobium candidum piece, fresh leaf and 7 times of weight is added in flash extracter, 12min is extracted, obtains iron sheet stone
Dry measure used in former times crude extract；
S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；
S1-5. take precipitation to add the ethanol solution that 7 times of volume fractions are 80%, add the lemon of ethanol solution weight 0.03%
Acid, soak extraction 2h, alcohol extract is obtained, alcohol extract recovery ethanol, it is 1.1 ~ 1.2 to be concentrated under reduced pressure into relative density, obtains concentrate；
S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
The preparation method of passion fruit seed essential oil comprises the following steps：
S2-1. passion fruit seed is taken, cleans, dries, is crushed；
S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure
For 29Mpa, extraction temperature is 40 DEG C, CO2Flow is 35L/h, extracts 3h；Passion fruit seed essential oil is carried from what extraction kettle stayed
CO2Fluid enters separating still, is separated in the case where pressure is 8MPa, temperature is 35 DEG C, obtains passion fruit seed crude oil；
S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 2h；Filtered after the completion of standing, obtain passion fruit seed essential oil.
The product of above-described embodiment 1 ~ 5 is taken to be used to carbuncled tester on the face.
Tester's screening criteria：There are obvious acne on the face, and acne area accounts for more than the 20% of face area.
Then application method is sealed and used to tester, tester every 2 for face paper is soaked in aforesaid liquid
Day use 1 time, apply for 1 time and to observe using effect after 15 ~ 20min on the face, two weeks.
Tester totally 100, it is randomly divided into 5 groups, every group 20.
Using effect judges：
It is effective：Acne are wholly absent, and former acne growth site is without vestige.
Effectively：Acne disappear, but acne growth site has vestige, or acne diminish.
It is invalid：Acne are unchanged.
Test result：
| Group | It is effective | Effectively | It is invalid | It is efficient |
| Embodiment 1 | 13 | 6 | 1 | 95% |
| Embodiment 2 | 10 | 7 | 3 | 85% |
| Embodiment 3 | 10 | 8 | 2 | 90% |
| Embodiment 4 | 6 | 8 | 6 | 70% |
| Embodiment 5 | 10 | 4 | 6 | 70% |
After use, there is 85% tester to feed back skin ratio and use preceding water profit, glossy, bright before ratio of skin tone, using effect
Preferably.Summary test data is visible, and the dendrobium candidum facial mask of the present embodiment, which has, preferably removes acne, moisturizing moisturizing etc.
Effect.
Claims (8)
- A kind of 1. dendrobium candidum facial mask, it is characterised in that：It is made up of the raw material of following parts by weight：0.5 ~ 2 part of dendrobium candidum extract solution, 0.2 ~ 1 part of passion fruit seed essential oil, tea tree ethereal oil 0.1 ~ 0.5 part, 0.1 ~ 0.5 part of Sodium Hyaluronate, 0.2 ~ 0.8 part of lecithin, 5 ~ 20 parts of NMF, 0.01 ~ 0.03 part of adhesive, 95 ~ 120 parts of water.
- 2. dendrobium candidum facial mask according to claim 1, it is characterised in that：It is made up of the raw material of following parts by weight：0.8 ~ 1.6 part of dendrobium candidum extract solution, 0.4 ~ 0.9 part of passion fruit seed essential oil, tea tree 0.2 ~ 0.4 part of essential oil, 0.2 ~ 0.4 part of Sodium Hyaluronate, 0.3 ~ 0.7 part of lecithin, 10 ~ 15 parts of NMF, adhesive 0.01 ~ 0.03 part, 95 ~ 120 parts of water.
- 3. dendrobium candidum facial mask according to claim 1, it is characterised in that：It is made up of the raw material of following parts by weight：1.2 parts of dendrobium candidum extract solution, 0.8 part of passion fruit seed essential oil, tea tree ethereal oil 0.2 Part, 0.3 part of Sodium Hyaluronate, 0.5 part of lecithin, 13 parts of NMF, 0.02 part of adhesive, 100 parts of water.
- 4. the dendrobium candidum facial mask according to any one of claim 1 ~ 3, it is characterised in that：The preparation method of the dendrobium candidum extract solution comprises the following steps：S1-1. the fresh bar of dendrobium candidum and fresh leaf are taken, the fresh bar of dendrobium candidum is half-and-half splitted, and section, obtains dendrobium candidum piece, fresh leaf is cut into 2 ~ 5mm segment；S1-2. dendrobium candidum piece and fresh leaf add arabo-ascorbic acid, sodium acid carbonate and water immersion, by weight, dendrobium candidum Piece:Arabo-ascorbic acid:Sodium acid carbonate=100:0.01~0.05:0.01 ~ 0.05, soak time is 20 ~ 30min, is taken out after immersion Dendrobium candidum piece；S1-3. the water of dendrobium candidum piece, fresh leaf and 7 ~ 10 times of weight is added in flash extracter, 10 ~ 20min is extracted, obtains Dendrobium candidum crude extract；S1-4. dendrobium candidum crude extract centrifuges, and separates supernatant and precipitation；S1-5. take precipitation to add the ethanol solution that 6 ~ 8 times of volume fractions are 60 ~ 80%, add ethanol solution weight 0.03 ~ 0.05% citric acid, 1 ~ 2h of soak extraction obtain alcohol extract, alcohol extract recovery ethanol, be concentrated under reduced pressure into relative density for 1.1 ~ 1.2, obtain concentrate；S1-6. merge supernatant and concentrate, obtain dendrobium candidum extract solution.
- 5. the dendrobium candidum facial mask according to any one of claim 1 ~ 3, it is characterised in that：The preparation method of the passion fruit seed essential oil comprises the following steps：S2-1. passion fruit seed is taken, cleans, dries, is crushed；S2-2. the passion fruit seed of crushing is fitted into supercritical extraction reactor and uses supercritical CO2Carry out supercritical extract, extracting pressure For 25 ~ 29Mpa, extraction temperature is 40 ~ 45 DEG C, CO2Flow is 30 ~ 35L/h, extracts 2 ~ 3h；Carried from what extraction kettle stayed The CO of passion fruit seed essential oil2Fluid enters separating still, is separated in the case where pressure is 6 ~ 8MPa, temperature is 30 ~ 35 DEG C, obtains passion fruit seed Crude oil；S2-3. passion fruit seed crude oil is added into activated carbon, stirring, stands 1 ~ 2h；Filtered after the completion of standing, obtain passion fruit seed essence Oil.
- 6. the dendrobium candidum facial mask according to any one of claim 1 ~ 3, it is characterised in that：The NMF is one kind or two in glycerine, propane diols, glycerine, butanediol, hexylene glycol, xylitol and D-sorbite More than kind.
- 7. the dendrobium candidum facial mask according to any one of claim 1 ~ 3, it is characterised in that：Described adhesive is one or both of sodium carboxymethylcellulose, hydroxyethyl cellulose, xanthans, carragheen and pectin More than.
- 8. dendrobium candidum facial mask according to claim 4, it is characterised in that：In the step S1-1, the weight ratio of the fresh bar of dendrobium candidum and fresh leaf is 1 ~ 3:3~10.
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| CN201711143995.7A CN107811939A (en) | 2017-11-17 | 2017-11-17 | A kind of dendrobium candidum facial mask |
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| CN108938520A (en) * | 2018-09-06 | 2018-12-07 | 湖南中新创生物科技有限公司 | A kind of dendrobium candidum facial mask and preparation method thereof |
| CN109953927A (en) * | 2019-04-16 | 2019-07-02 | 山东中医药大学 | A kind of Novel facial mask that capableing of beautifying face and moistering lotion and drug and preparation method |
| EP3552600A1 (en) * | 2018-04-12 | 2019-10-16 | Shanghai Traditional Chinese Medicine Co., Ltd. | Composition containing dendrobium candidum extract and preparation method and use thereof |
| CN114796075A (en) * | 2022-05-10 | 2022-07-29 | 浙江森宇有限公司 | Compound containing dendrobium officinale flowers and application of compound in skin care products |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| EP3552600A1 (en) * | 2018-04-12 | 2019-10-16 | Shanghai Traditional Chinese Medicine Co., Ltd. | Composition containing dendrobium candidum extract and preparation method and use thereof |
| CN108464960A (en) * | 2018-04-17 | 2018-08-31 | 凯瑞欧（天津）生物技术有限公司 | A kind of dendrobium candidum beauty-care gel |
| CN108938520A (en) * | 2018-09-06 | 2018-12-07 | 湖南中新创生物科技有限公司 | A kind of dendrobium candidum facial mask and preparation method thereof |
| CN109953927A (en) * | 2019-04-16 | 2019-07-02 | 山东中医药大学 | A kind of Novel facial mask that capableing of beautifying face and moistering lotion and drug and preparation method |
| CN114796075A (en) * | 2022-05-10 | 2022-07-29 | 浙江森宇有限公司 | Compound containing dendrobium officinale flowers and application of compound in skin care products |
| CN114796075B (en) * | 2022-05-10 | 2023-10-20 | 浙江森宇有限公司 | Dendrobium officinale flower-containing compound and application thereof in skin care products |
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Application publication date: 20180320 |