CN107641455A - A kind of automotive upholstery anti-fingerprint UV coating, preparation method and applications - Google Patents
A kind of automotive upholstery anti-fingerprint UV coating, preparation method and applications Download PDFInfo
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- CN107641455A CN107641455A CN201710890266.1A CN201710890266A CN107641455A CN 107641455 A CN107641455 A CN 107641455A CN 201710890266 A CN201710890266 A CN 201710890266A CN 107641455 A CN107641455 A CN 107641455A
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Abstract
The invention provides a kind of automotive upholstery anti-fingerprint UV coating, preparation method and applications, raw material is：9 25 30 parts of official's aliphatic polyurethane acrylic resins；4 15 20 parts of official's aliphatic polyurethane acrylic resins；15 20 parts of anti-fingerprint acrylic resin；184 23 parts of ultraviolet initiator；12 parts of ultraviolet initiator TPO；0.3 0.5 parts of levelling agent；0.3 0.5 parts of anti-fingerprint levelling agent；10 30 parts of ethyl acetate；10 15 parts of butyl acetate.Compared with prior art, automotive trim provided by the invention is excellent with UV coating properties, and coating, which can reach, is fully cured crosslinking, and solvent noresidue is not after-tacked, moreover, good dispersion during spraying, levelability are moderate, thixotropy is moderate, coating uniform, without obvious tangerine peel, without pinprick bubble, free from admixture point is present.Lacquer painting levelling is plentiful, and glossiness is good, anti-fingerprint positive effect.
Description
Technical field
The invention belongs to technical field of paint preparation, and in particular to a kind of automotive upholstery anti-fingerprint UV coating, preparation side
Method and its application.
Background technology
Nowadays with the enhancing of people's environmental consciousness and the development of polymer science, it is desirable to use the cry of environmental protection coating material
The index of coating VOC content, development and application ring are all progressively being tightened up to find competitive advantage by more and more higher, domestic each enterprise
Guarantor's type coating.
UV paint belongs to environment-friendly type coating, has the advantages of curing rate is fast, operating efficiency is high, so automotive trim UV light
The research and development of oily series paint are to comply with market trend, and automotive trim UV gloss oil series paint has pole in the application of automotive upholstery
Its wide prospect.More and more higher especially is required in the touch-screen of high-end automobile middle control, is operated for touch-screen with fingerprint,
Because common UV paint face coat cloth is enough smooth, fingerprint is readily retained on touch-screen.
The content of the invention
The invention provides a kind of automotive upholstery anti-fingerprint UV coating and preparation method thereof, it is for ABS, PC, ABS+
PC plastic rubber substrate has good adhesive force, and the paint film formed has the performances such as solvent resistant, water resistance.
Present invention also offers a kind of automotive upholstery anti-fingerprint UV coating automotive upholstery application.
A kind of automotive upholstery anti-fingerprint UV coating provided by the invention, include the raw material of following parts by weight：
The levelling agent is selected from BYK-333 type levelling agents, and BYK-333 is organosilicon levelling agent, the anti-fingerprint levelling agent
It is fluorine-containing propene acid compound levelling agent selected from Japanese SHIN-ETSU HANTOTAI KY-1203.
The 9 official aliphatic polyurethane acrylic resin is polyurethane acroleic acid oligomer；The 4 official aliphatic poly ammoniacum
Acrylic resin is polyurethane acrylate oligomer.
A kind of preparation method of automotive upholstery anti-fingerprint UV coating provided by the invention, comprises the following steps：
1) under the conditions of lucifuge, by the official's aliphatic polyurethane acrylic resin of 25-30 parts by weight 9, the official's fat of 15-20 weight 4
Fat race polyurethane acroleic acid part resin and 15-20 parts by weight anti-fingerprint crylic acid ester mixtures, are stirred, obtain mixed material A；
2) the 2-3 parts of ultraviolet initiator 184 and purple under agitation, are added into the butyl acetate of 10-15 parts by weight
Outer light trigger TPO 1-2 parts, are stirred, obtain mixed material B；
3) under agitation, mixed material B is added in mixed material A, sequentially adds 0.3-0.5 parts by weight streams
Flat agent and 0.3-0.5 part anti-fingerprint levelling agents, are stirred and evenly mixed；
4) ethyl acetate 10-30 parts by weight are added under agitation, and tune thickening degree to 20-30S, viscosity test condition is
25 DEG C, NK-2 cups, filtering, obtain automotive upholstery anti-fingerprint UV coating.
In above-mentioned preparation process, all stirrings are carried out under the conditions of 300-700 revs/min.
Further, time 8-12min is stirred described in step 1).
It is 12-18min that the time is stirred described in step 2) and step 3).
Filtering described in step 4) refers to that 300 mesh filter.
Preferably, the preparation method comprises the following steps：
1) under the conditions of lucifuge, by the official's aliphatic polyurethane acrylated oligomer of 25-30 parts by weight 9,15-20 parts by weight 4
Official's aliphatic urethane acrylate oligomer and 15-20 parts by weight anti-fingerprint acrylate are under the conditions of 300-700 revs/min
10min is stirred, obtains mixed material A；
2) butyl acetate of 10-15 parts by weight is stirred under the conditions of 300-700 revs/min, added under agitation
The 2-3 parts of ultraviolet initiator 184 and ultraviolet initiator TPO 1-2 parts are added, 15min is stirred, obtains mixed material B；
3) under 300-700 revs/min of stirring condition, material B is slowly added into material A, sequentially adds levelling
Agent BYK-333 0.2-0.5 parts by weight and anti-fingerprint levelling agent KY-1203 0.3-0.5 parts by weight, stir 15min；
4) continue under 300-700 revs/min of stirring condition, add ethyl acetate 10-30 parts by weight, adjust thickening degree extremely
20-30S, viscosity test condition are 25 DEG C, NK-2 cups, the filtering of 300 mesh, obtain automotive upholstery anti-fingerprint UV coating.
Present invention also offers a kind of automotive upholstery anti-fingerprint UV coating automotive upholstery application.
Specifically for ABS, PC or ABS+PC base material.
Specifically the application method of automotive upholstery anti-fingerprint UV coating is：By the automotive upholstery anti-fingerprint UV of above-mentioned preparation
Coating, UV coating curing agents and UV paint thinners are by weight 10:1：:4-5 is mixed, and is sprayed on prime coat, normal temperature levelling
After drying 5-7 minutes, kept for 10 minutes at 60 DEG C, UV solidifications, UV exposure energies are 600-800MJ/cm2。
The UV paint thinners include the raw material of following parts by weight：50 parts of 50 parts of ethyl acetate and butyl acetate；
The UV paint thinners preparation method is：The butyl acetate of parts by weight 50 and the ethyl acetate of parts by weight 50 are mixed
After conjunction stirs 10 minutes.
The UV coating curing agents include the raw material of following parts by weight：25 parts of 75 parts of CN3390 and butyl acetate；
The UV coating curing agents preparation method is：By the butyl acetate of parts by weight 25 and the Degussa of parts by weight 75
After CN3390 is mixed evenly 10 minutes.
In inventive formulation, 9 official's aliphatic polyurethane acrylic resins are used for providing the adhesive force and surface levelling of matrix
Property, 4 official's aliphatic poly ammoniacum acrylate oligomers offer dryness and crosslink density, anti-fingerprint acrylate are used for providing paint film
Water droplet angle, there is provided the anti-fingerprint effect of coating surface, ultraviolet initiator are used for triggering the polymerization of monomer and polyester, levelling agent
The levelability of paint film is provided, anti-fingerprint levelling agent provides paint film smoothness, BYK-333 types levelling agent and KY-1203 levelling agents two
Person makes the levelability of integral system more preferable, more smooth with the use of that can solve UV coating surface anti-fingerprint effect problems.Acetic acid
Ethyl ester and butyl acetate are solvent, give the preferable mobility of paint and solvent release.Drawn by the light of BASF IRGACURE 184
Send out agent 2-3 parts by weight and BASF IRGACURE TPO photoinitiator 1-2 parts by weight composition ultraviolet initiator.Two kinds light-initiated
Agent shares, and can absorb the ultraviolet of ultraviolet region different-waveband so that the solidification of UV coating is more thorough, so as to be carried for paint film
For more preferable surface property.
Preparation method provided by the invention, to improve the functioning efficiency of UV absorbers, whole preparation process need to kept away
Carried out under optical condition, cause preparation system under greenware condition to prevent it from absorbing ultraviolet light in the preparation process of coating
Solidification crosslinking, which occurs, influences the quality of UV coating and the filming performance of paint film；Ultraviolet initiator first must dissolve through butyl acetate
Add afterwards but among reaction system, to ensure that it is uniformly dispersed in system.
Compared with prior art, anti-fingerprint UV paints disclosed by the invention are free of VOC, after hardening
Crosslink density is much higher than hot baking type coating, and coating is in organic solvent each side such as hardness, wear-resisting, acid and alkali-resistance, salt spray resistance, resistance to gasoline
The performance indications in face are very high, and particularly its paint film is plentiful, gloss, surface smoothness, fingerprint resistance are especially prominent, UV paint solidifications
Speed is fast, and production efficiency is high, and curing mechanism belongs to a kind of chain reaction of free radical, and crosslinking curing is completed in moment, set family planning
Production flowing water linear velocity reaches as high as 100m/min, and workpiece is offline to be packed, and the efficiency using UV coating is that traditional drying-type applies
More than 15 times of material；The energy is saved, UV coating solidifies by ultraviolet light, and General Production Lines energy consumption is within 50kW, and energy expenditure is about
For the 1/5 of traditional drying-type heat curing coating.
The paint film obtained using application method provided by the invention has good water resistance, ethyl acetate and butyl acetate
With the use of ensure that the deliquescent of each raw material while improving the drying property of construction again.In automobile prepared by the present invention
The paint film that gadget is formed with anti-fingerprint UV coating, paint film coating, which can reach, is fully cured crosslinking, and solvent noresidue is not after-tacked, and
And good dispersion during spraying, levelability is moderate, and thixotropy is moderate, coating uniform, without obvious tangerine peel, without pinprick bubble, free from admixture
Point is present.Lacquer painting levelling is plentiful, and glossiness is good, and paint film smoothness is good.
Compared with prior art, automotive upholstery anti-fingerprint UV coating properties provided by the invention are excellent, and coating can reach
Crosslinking is fully cured, solvent noresidue is not after-tacked, moreover, good dispersion during spraying, levelability is moderate, and thixotropy is moderate, coating
Uniformly, exist without obvious tangerine peel, without pinprick bubble, free from admixture point.Lacquer painting levelling is plentiful, and glossiness is good, smoothness is good, anti-fingerprint
Significant effect.
Popular VW TL226 are the most stringent standards of automotive upholstery industry, present most of automotive upholstery manufacturers
Equally the performance of paint is detected using VW TL226 standard, automotive upholstery anti-fingerprint UV provided by the invention
Coating is tested by multinomial performance, can fully meet the requirement of TL226 standards.
Embodiment
With specific embodiment 1~5 and comparative example 1~3, the present invention is described in detail below, automobile in each embodiment
The raw material and parts by weight of inside gadget anti-fingerprint UV coating are shown in Table 1, and the preparation method of each embodiment is as follows：
(1) according to the formula of each embodiment in table 1, by 9 official's aliphatic polyurethane acrylic resins, 4 official's aliphatic poly ammonia
Ester acrylic resin and anti-fingerprint acrylate stir 10min under the conditions of 300-700 revs/min, obtain mixed material A；
(2) it is formulated according to table 1, butyl acetate is stirred under the conditions of 300-700 revs/min, added under agitation
The ultraviolet initiators of IRGACURE 184 and IRGACURE TPO ultraviolet initiators, 15min is stirred, obtains mixed material B；
(3) under 300-700 revs/min of stirring condition, mixed material B is slowly added into mixed material A, then successively
Levelling agent BYK-333 and anti-fingerprint levelling agent KY-1203 is added, stirs 15min；
(4) continue under 300-700 revs/min of stirring condition, addition ethyl acetate, tune thickening degree to 20-30S (25 DEG C,
NK-2), 300 mesh filter, and obtain the anti-fingerprint UV coating of automotive upholstery.
The whole preparation process of embodiment 1~5 is carried out under the conditions of lucifuge.
Table 1
The parts by weight of automotive upholstery anti-fingerprint UV coating and raw material are shown in Table 2 in comparative example 1~3, the preparation side of comparative example 1
Method is with embodiment 1, simply without 4 official's aliphatic polyurethane acrylic acid oligomers of addition；The preparation method of comparative example 2 is the same as real
Example 2 is applied, simply wherein only adds a kind of ultraviolet initiator and levelling agent, but adds total amount and does not change；The system of comparative example 3
Preparation Method is with embodiment 3, and simply the addition of part material is different.
Table 2
Anti-fingerprint UV coating, UV curing agent and the UV lacquer diluents that each embodiment and comparative example are obtained are by weight 10：
1：4-5 is allocated, and the UV paint thinners include the raw material of following parts by weight：50 parts of ethyl acetate；50 parts of butyl acetate；It is made
Preparation Method is：After the ethyl acetate of the butyl acetate of parts by weight 50 and parts by weight 50 is mixed evenly into 10 minutes；Will
UV coating after allotment is sprayed on the prime coat of dried automotive upholstery, after normal temperature levelling is dried 5 minutes, 60 DEG C
Kept for 10 minutes, then carry out UV solidifications, UV exposure energies are 600-800MJ/cm2, the paint film coating that each embodiment obtains is equal
It is even, without obvious tangerine peel, without pinprick bubble, free from admixture point is present, and paint film levelling is plentiful, and glossiness is good, smoothness is good, anti-fingerprint shows
Write.
Paint film property is detected, its testing result is as shown in table 3：
Table 3
It is as follows with the testing standard of anti-fingerprint UV coating for automotive upholstery：
1. outward appearance：Evaluation film forming whether there is the surface blemishes such as foaming, orange peel, shrinkage cavity, ripple, prickly heat.
2. Storage period：Whether evaluation paint occurs within the shelf-life thickens, is layered, plays glue, change colour, returns the abnormal feelings such as thick
Condition；
For each performance of above paint film testing standard referring to masses VW TL226 standards.
As can be seen that automotive upholstery anti-fingerprint UV coating prepared by the present invention can comply fully with greatly from above-mentioned table 3
Many VW TL226 standards.
It is above-mentioned to be retouched in detail with reference to what embodiment was carried out to automotive upholstery anti-fingerprint UV coating and its preparation method and application
State, be illustrative rather than limited, several embodiments can be included according to limited scope, therefore do not departing from this
Changing and modifications under invention general plotting, it should belong within protection scope of the present invention.
Claims (9)
- A kind of 1. automotive upholstery anti-fingerprint UV coating, it is characterised in that the automotive upholstery anti-fingerprint UV coating include with The raw material of lower parts by weight：
- 2. automotive upholstery anti-fingerprint UV coating according to claim 1, it is characterised in that the levelling agent is selected from BYK- 333 type levelling agents；The anti-fingerprint levelling agent is selected from Japanese SHIN-ETSU HANTOTAI KY-1203.
- 3. the preparation method of the automotive upholstery anti-fingerprint UV coating described in a kind of claim 1 or 2, it is characterised in that described Preparation method comprises the following steps：1) under the conditions of lucifuge, by the official's aliphatic polyurethane acrylic resin of 25-30 parts by weight 9, the official's aliphatic of 15-20 weight 4 Polyurethane acroleic acid part resin and 15-20 parts by weight anti-fingerprint crylic acid ester mixtures, are stirred, obtain mixed material A；2) the 2-3 parts of ultraviolet initiator 184 and ultraviolet light under agitation, are added into the butyl acetate of 10-15 parts by weight Initiator TPO 1-2 parts, are stirred, obtain mixed material B；3) under agitation, mixed material B is added in mixed material A, sequentially adds 0.3-0.5 parts by weight levelling agents With 0.3-0.5 part anti-fingerprint levelling agents, stir and evenly mix；4) ethyl acetate 10-30 parts by weight are added under agitation, and adjusting thickening degree, viscosity test condition is 25 to 20-30S DEG C, NK-2 cups, filtering, obtain automotive upholstery anti-fingerprint UV coating.
- 4. preparation method according to claim 3, it is characterised in that all stirrings are at 300-700 revs/min in preparation process Carried out under the conditions of clock.
- 5. the preparation method according to claim 3 or 4, it is characterised in that time 8- is stirred described in step 1) 12min。
- 6. preparation method according to claim 3, it is characterised in that be stirred the time described in step 2) and step 3) It is 12-18min.
- 7. a kind of automotive upholstery anti-fingerprint UV coating described in claim 1 is in the application of automotive upholstery.
- 8. application according to claim 7, it is characterised in that for ABS, PC or ABS+PC base material.
- 9. application according to claim 8, it is characterised in that specifically preparation method is：By automotive upholstery anti-fingerprint UV Coating, UV coating curing agents and UV paint thinners are by weight 10:1：:4-5 is mixed, and is sprayed on prime coat, normal temperature levelling After drying 5-7 minutes, kept for 10 minutes at 60 DEG C, UV solidifications, UV exposure energies are 600-800MJ/cm2。
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710890266.1A CN107641455B (en) | 2017-09-27 | 2017-09-27 | Anti-fingerprint UV coating for automotive interior parts, and preparation method and application thereof |
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| CN201710890266.1A CN107641455B (en) | 2017-09-27 | 2017-09-27 | Anti-fingerprint UV coating for automotive interior parts, and preparation method and application thereof |
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| CN107641455B CN107641455B (en) | 2019-12-24 |
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Cited By (1)
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| Publication number | Publication date |
|---|---|
| CN107641455B (en) | 2019-12-24 |
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