CN107601891A - A kind of porcelain glaze and its preparation application method - Google Patents
A kind of porcelain glaze and its preparation application method Download PDFInfo
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- CN107601891A CN107601891A CN201711066014.3A CN201711066014A CN107601891A CN 107601891 A CN107601891 A CN 107601891A CN 201711066014 A CN201711066014 A CN 201711066014A CN 107601891 A CN107601891 A CN 107601891A
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Abstract
The invention belongs to porcelain field, and in particular to a kind of porcelain glaze and its preparation application method, be made up of the raw material of following parts by weight：Kaolin, potassium feldspar, calcite, quartz, plant ash, fluorite, ox bone ash, alkali stone, frit, bentonite；Frit is made up of the raw material of following parts by weight：Silica, aluminum oxide, boric acid, potassium carbonate, sodium carbonate, application method is prepared to prepare including glaze, the steps such as the firing of liquefied gas kiln, the gloss of the anti-chilling performance of glaze layer of the present invention and increase glaze layer, high abrasion transparent microcrystal fritted glaze, method for cooking is more scientific and effective than traditional firing mode, firing time length, and transmutation effect is good.
Description
Technical field
The invention belongs to porcelain field, and in particular to a kind of porcelain glaze and its preparation application method.
Background technology
Refreshing Hou tradition chun glaze formula is fairly simple, and the introduction of the nineties liquefied gas makes formula gradually diversified, but how
The physical property for improving glaze still seems particularly significant, while under Environmental Protection Situation, liquefied gas kiln is fired into refreshing Hou porcelain
Main flow, but be to heat up too soon the shortcomings that liquefaction, such as it is 9 to 10 small with 20 several hours, liquefied gas with the firing of bavin coal in the past
When can cease fire, so cause firing time short, transmutation effect is general.How to extend the firing time of liquefied gas kiln is to work as
The very puzzled problem of preceding porcelain people.
The content of the invention
The defects of based on prior art, it is an object of the invention to provide a kind of porcelain glaze and its prepare application method.
In order to achieve the above object, the present invention uses following technical scheme：A kind of porcelain glaze, by the original of following parts by weight
Material composition：5-10 parts of kaolin, potassium feldspar 25-30 parts, calcite 5-10 parts, quartzy 10-15 parts, Copper Ores 5-8 parts, vegetation
Grey 3-5 parts, fluorite 5-10 parts, ox bone ash 10-15 parts, alkali stone 3-5 parts, frit 5-10 parts, bentonite 1-2 parts；
The frit is made up of the raw material of following parts by weight：Silica 50-60 parts, aluminum oxide 3-5 parts, boric acid 15-18 parts, carbon
Sour potassium 8-10 parts, sodium carbonate 5-10 parts.
Described porcelain glaze, is made up of the raw material of following parts by weight：8 parts of kaolin, 28 parts of potassium feldspar, 8 parts of calcite,
12 parts of quartz, 6 parts of Copper Ores, 4 parts of plant ash, 8 parts of fluorite, 12 parts of ox bone ash, 4 parts of alkali stone, 7 parts of frit, 1 part of bentonite；
The frit is made up of the raw material of following parts by weight：55 parts of silica, 4 parts of aluminum oxide, 17 parts of boric acid, 9 parts of potassium carbonate,
8 parts of sodium carbonate.
The preparation application method of the frit includes：By the high borosilicate frit, respectively composition is equal according to the proportioning, mixing
After even and sieving, through high temperature（Melting temperature is 1550~1580 DEG C, and soaking time is 2~5 hours）Melt to clarification with
Change, the glass metal being homogenized then is poured into water quenching and makes its fragmentation, drying cullet slag obtains frit.
The preparation application method of described porcelain glaze, including following preparation process：
1）Weigh the kaolin of above-mentioned parts by weight, potassium feldspar, calcite, quartz, Copper Ores, plant ash, firefly respectively by formula ratio
Stone, ox bone ash, alkali stone, frit, bentonite are put into ball mill, and ball milling 35-40 hours, glaze slip fineness was that 10000-hole sieve tails over
0.02~0.05% glaze slip；
2）Using glaze spraying technique by step 1）In glaze be sprayed on molded billet surface；
3）By step 2）In spraying glaze after base substrate be put into liquefied gas kiln, light a fire early stage, first to carrying out dropping force in kiln
Operation make it that pressure is 0.015-0.045MP；
4）By step 3）In liquefied gas kiln in carry out warming temperature, start to boost when temperature reaches 950 DEG C, temperature from
By pressure rise to 0.075-0.13MP in 950 DEG C to 1200 DEG C of temperature-rise period；
5) when step 4）Middle liquefied gas kiln temperature reduces pressure to 0.015-0.02MP again after reaching 1100-1280 DEG C；
6）When liquefied gas kiln temperature reaching 1290-1300 DEG C to carrying out being incubated 2-3 small in kiln；
7）Afterwards to step 6）Carried out in middle liquefied gas kiln only fiery after being warming up to 1310-1300 DEG C；
8）Again liquefied gas kiln is carried out being cooled to 1000-1100 DEG C and be incubated 1-1.5h again；
9）Cooled after insulation, wicket can be slightly opened when dropping to below 200 DEG C makes its rapid cooling, at 100 DEG C or so
Kiln discharge.
Bentonite of the present invention improves the anti-chilling performance of glaze layer and increases the gloss of glaze layer, is main using boric acid, silica
Composition forms low melting point high rigidity glass material；High abrasion transparent microcrystal fritted glaze of the present invention is formed, plant ash is introduced primarily into calcium
The elements such as phosphorus, it is good cosolvent, there is certain suspension to glaze slip, the melting temperature of glaze can be reduced and the high temperature of glaze glues
Degree, while has opaque and the facilitation to chun glaze split-phase, and dosage should control, and fluorite is a kind of mineral, isometric system,
Its main component is calcirm-fluoride, can reduce the melting temperature of glaze, increases the mobility of glaze, while has milkiness effect, can be improved
The glossiness of chun glaze, the suspension of glaze slip being improved, ox bone ash is made of ox bone calcining, can be used as cosolvent, make glaze paint gloss,
Promote liquid phase separation, method for cooking is more scientific and effective than traditional firing mode, firing time length, and transmutation effect is good.
Embodiment
The present invention is described in further details below by embodiment, embodiment is only used for illustrating the present invention, and unlimited
The scope of the present invention processed.
Embodiment 1：A kind of porcelain glaze, is made up of the raw material of following parts by weight：5 parts of kaolin, 25 parts of potassium feldspar, Fang Xie
5 parts of stone, 10 parts of quartz, 5 parts of Copper Ores, 3 parts of plant ash, 5 parts of fluorite, 10 parts of ox bone ash, 3 parts of alkali stone, 5 parts of frit, bentonite 1
Part；Bentonite improves the anti-chilling performance of glaze layer and increases the gloss of glaze layer.
The frit is made up of the raw material of following parts by weight：50 parts of silica, 3 parts of aluminum oxide, 15 parts of boric acid, potassium carbonate
8 parts, 5 parts of sodium carbonate.
The preparation application method of the frit includes：By the high borosilicate frit, respectively composition is equal according to the proportioning, mixing
After even and sieving, through high temperature（Melting temperature is 1550~1580 DEG C, and soaking time is 2~5 hours）Melt to clarification with
Change, the glass metal being homogenized then is poured into water quenching and makes its fragmentation, drying cullet slag obtains frit；With boric acid,
Silica is that main component forms low melting point high rigidity glass material；Form high abrasion transparent microcrystal fritted glaze of the present invention.
The preparation application method of described porcelain glaze, including following preparation process：
1）Weigh the kaolin of above-mentioned parts by weight, potassium feldspar, calcite, quartz, plant ash, fluorite, ox bone respectively by formula ratio
Ash, alkali stone, frit, in bentonite input ball mill, ball milling 35-40 hours, glaze slip fineness be 10000-hole sieve tail over 0.02~
0.05% glaze slip；
2）Using glaze spraying technique by step 1）In glaze be sprayed on molded billet surface；
3）By step 2）In spraying glaze after base substrate be put into liquefied gas kiln, light a fire early stage, first to carrying out dropping force in kiln
Operation make it that pressure is 0.015MP；
4）By step 3）In liquefied gas kiln in carry out warming temperature, start to boost when temperature reaches 950 DEG C, temperature from
By pressure rise to 0.075MP in 950 DEG C to 1200 DEG C of temperature-rise period；
5) when step 4）Middle liquefied gas kiln temperature reduces pressure to 0.015MP again after reaching 1100 DEG C；
6）When liquefied gas kiln temperature reaching 1290 DEG C to carrying out being incubated 2 small in kiln；
7）Afterwards to step 6）Carried out in middle liquefied gas kiln only fiery after being warming up to 1310 DEG C；
8）Again liquefied gas kiln is carried out being cooled to 1000 DEG C and be incubated 1h again；
9）Cooled after insulation, wicket can be slightly opened when dropping to below 200 DEG C makes its rapid cooling, at 100 DEG C or so
Kiln discharge.
Embodiment 2：A kind of porcelain glaze, is made up of the raw material of following parts by weight：8 parts of kaolin, 28 parts of potassium feldspar, Fang Xie
8 parts of stone, 12 parts of quartz, 6 parts of Copper Ores, 4 parts of plant ash, 8 parts of fluorite, 12 parts of ox bone ash, 4 parts of alkali stone, 7 parts of frit, bentonite 1
Part；Bentonite improves the anti-chilling performance of glaze layer and increases the gloss of glaze layer.
The frit is made up of the raw material of following parts by weight：55 parts of silica, 4 parts of aluminum oxide, 17 parts of boric acid, potassium carbonate
9 parts, 8 parts of sodium carbonate.
The preparation application method of the frit includes：By the high borosilicate frit, respectively composition is equal according to the proportioning, mixing
After even and sieving, through high temperature（Melting temperature is 1550~1580 DEG C, and soaking time is 2~5 hours）Melt to clarification with
Change, the glass metal being homogenized then is poured into water quenching and makes its fragmentation, drying cullet slag obtains frit；With boric acid,
Silica is that main component forms low melting point high rigidity glass material；Form high abrasion transparent microcrystal fritted glaze of the present invention.
The preparation application method of described porcelain glaze, including following preparation process：
1）Weigh the kaolin of above-mentioned parts by weight, potassium feldspar, calcite, quartz, plant ash, fluorite, ox bone respectively by formula ratio
Ash, alkali stone, frit, in bentonite input ball mill, ball milling 35-40 hours, glaze slip fineness be 10000-hole sieve tail over 0.02~
0.05% glaze slip；
2）Using glaze spraying technique by step 1）In glaze be sprayed on molded billet surface；
3）By step 2）In spraying glaze after base substrate be put into liquefied gas kiln, light a fire early stage, first to carrying out dropping force in kiln
Operation make it that pressure is 0.02MP；
4）By step 3）In liquefied gas kiln in carry out warming temperature, start to boost when temperature reaches 950 DEG C, temperature from
By pressure rise to 0.1MP in 950 DEG C to 1200 DEG C of temperature-rise period；
5) when step 4）Middle liquefied gas kiln temperature reduces pressure to 0.015MP again after reaching 1270 DEG C；
6）When liquefied gas kiln temperature reaching 1295 DEG C to carrying out being incubated 2.5 small in kiln；
7）Afterwards to step 6）Carried out in middle liquefied gas kiln only fiery after being warming up to 1320 DEG C；
8）Again liquefied gas kiln is carried out being cooled to 1050 DEG C and be incubated 1.3h again；
9）Cooled after insulation, wicket can be slightly opened when dropping to below 200 DEG C makes its rapid cooling, at 100 DEG C or so
Kiln discharge.
Embodiment 3：A kind of porcelain glaze, is made up of the raw material of following parts by weight：10 parts of kaolin, 30 parts of potassium feldspar, side
10 parts of stone is solved, 15 parts of quartz, 8 parts of Copper Ores, 5 parts of plant ash, 10 parts of fluorite, ox bone is grey 15 parts, 5 parts of alkali stone, and 10 parts of frit is swollen
2 parts of profit soil；Bentonite improves the anti-chilling performance of glaze layer and increases the gloss of glaze layer.
The frit is made up of the raw material of following parts by weight：60 parts of silica, 5 parts of aluminum oxide, 18 parts of boric acid, potassium carbonate
10 parts, 10 parts of sodium carbonate.
The preparation application method of the frit includes：By the high borosilicate frit, respectively composition is equal according to the proportioning, mixing
After even and sieving, through high temperature（Melting temperature is 1550~1580 DEG C, and soaking time is 2~5 hours）Melt to clarification with
Change, the glass metal being homogenized then is poured into water quenching and makes its fragmentation, drying cullet slag obtains frit；With boric acid,
Silica is that main component forms low melting point high rigidity glass material；Form high abrasion transparent microcrystal fritted glaze of the present invention.
The preparation application method of described porcelain glaze, including following preparation process：
1）Weigh the kaolin of above-mentioned parts by weight, potassium feldspar, calcite, quartz, plant ash, fluorite, ox bone respectively by formula ratio
Ash, alkali stone, frit, in bentonite input ball mill, ball milling 35-40 hours, glaze slip fineness be 10000-hole sieve tail over 0.02~
0.05% glaze slip；
2）Using glaze spraying technique by step 1）In glaze be sprayed on molded billet surface；
3）By step 2）In spraying glaze after base substrate be put into liquefied gas kiln, light a fire early stage, first to carrying out dropping force in kiln
Operation make it that pressure is 0.045MP；
4）By step 3）In liquefied gas kiln in carry out warming temperature, start to boost when temperature reaches 950 DEG C, temperature from
By pressure rise to 0.13MP in 950 DEG C to 1200 DEG C of temperature-rise period；
5) when step 4）Middle liquefied gas kiln temperature reduces pressure to 0.02MP again after reaching 1280 DEG C；
6）When liquefied gas kiln temperature reaching 1300 DEG C to carrying out being incubated 3 small in kiln；
7）Afterwards to step 6）Stop fire after 1300 DEG C of heating is carried out in middle liquefied gas kiln；
8）Again liquefied gas kiln is carried out being cooled to 1100 DEG C and be incubated 1-1.5h again；
9）Cooled after insulation, wicket can be slightly opened when dropping to below 200 DEG C makes its rapid cooling, at 100 DEG C or so
Kiln discharge.
Claims (4)
1. a kind of porcelain glaze, it is characterised in that be made up of the raw material of following parts by weight：5-10 parts of kaolin, potassium feldspar 25-
30 parts, calcite 5-10 parts, quartzy 10-15 parts, Copper Ores 5-8 parts, plant ash 3-5 parts, fluorite 5-10 parts, ox bone ash 10-15
Part, alkali stone 3-5 parts, frit 5-10 parts, bentonite 1-2 parts；
The frit is made up of the raw material of following parts by weight：Silica 50-60 parts, aluminum oxide 3-5 parts, boric acid 15-18 parts, carbon
Sour potassium 8-10 parts, sodium carbonate 5-10 parts.
2. porcelain glaze according to claim 1, it is characterised in that be made up of the raw material of following parts by weight：Kaolin 8
Part, 28 parts of potassium feldspar, 8 parts of calcite, 12 parts of quartz, 6 parts of Copper Ores, 4 parts of plant ash, 8 parts of fluorite, 12 parts of ox bone ash, alkali stone 4
Part, 7 parts of frit, 1 part of bentonite；
The frit is made up of the raw material of following parts by weight：55 parts of silica, 4 parts of aluminum oxide, 17 parts of boric acid, 9 parts of potassium carbonate,
8 parts of sodium carbonate.
3. porcelain glaze according to claim 2, it is characterised in that：The preparation application method of the frit includes：By institute
Stating high borosilicate frit, respectively composition is according to the proportioning, after being well mixed and sieving, through high temperature（Melting temperature is 1550~1580
DEG C, soaking time is 2~5 hours）Clarification and homogenizing are melted to, the glass metal being homogenized then is poured into water quenching and made
Its fragmentation, drying cullet slag obtain frit.
4. a kind of preparation application method of pottery glaze according to claim 1, it is characterised in that prepare step including following
Suddenly：
1）Weigh the kaolin of above-mentioned parts by weight, potassium feldspar, calcite, Copper Ores, quartz, plant ash, firefly respectively by formula ratio
Stone, ox bone ash, alkali stone, frit, bentonite are put into ball mill, and ball milling 35-40 hours, glaze slip fineness was that 10000-hole sieve tails over
0.02~0.05% glaze slip；
2）Using glaze spraying technique by step 1）In glaze be sprayed on molded billet surface；
3）By step 2）In spraying glaze after base substrate be put into liquefied gas kiln, light a fire early stage, first to carrying out dropping force in kiln
Operation make it that pressure is 0.015-0.045MP；
4）By step 3）In liquefied gas kiln in carry out warming temperature, start to boost when temperature reaches 950 DEG C, temperature from
By pressure rise to 0.075-0.13MP in 950 DEG C to 1200 DEG C of temperature-rise period；
5) when step 4）Middle liquefied gas kiln temperature reduces pressure to 0.015-0.02MP again after reaching 1100-1280 DEG C；
6）When liquefied gas kiln temperature reaching 1290-1300 DEG C to carrying out being incubated 2-3 small in kiln；
7）Afterwards to step 6）Carried out in middle liquefied gas kiln only fiery after being warming up to 1310-1300 DEG C；
8）Again liquefied gas kiln is carried out being cooled to 1000-1100 DEG C and be incubated 1-1.5h again；
9）Cooled after insulation, wicket can be slightly opened when dropping to below 200 DEG C makes its rapid cooling, at 100 DEG C or so
Kiln discharge.
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108530034A (en) * | 2018-06-27 | 2018-09-14 | 福建省德化县陶缘茗陶瓷文化有限公司 | A kind of completely glaze ceramics and preparation method thereof |
| CN108793749A (en) * | 2018-07-26 | 2018-11-13 | 华宁县白塔山建筑陶瓷有限责任公司 | Ceramics colouring pigment and preparation method thereof |
| CN109231956A (en) * | 2018-09-14 | 2019-01-18 | 杨根成 | A kind of ancient customs figure image pottery production method |
| CN112759361A (en) * | 2021-01-06 | 2021-05-07 | 福建省威尔陶瓷股份有限公司 | High-siliceous high-temperature reinforced daily porcelain and preparation method thereof |
| CN113651532A (en) * | 2021-05-08 | 2021-11-16 | 浙江天物文化科技有限公司 | Tianmu mountain raw ore glaze and preparation method thereof |
| CN113754469A (en) * | 2021-09-16 | 2021-12-07 | 丽江永胜瓷业有限责任公司 | Lead dust removing method for ceramic glazing device |
| CN113788617A (en) * | 2021-09-26 | 2021-12-14 | 广东百强陶瓷有限公司 | Super-wear-resistant high-permeability diamond microcrystalline glaze and production process thereof |
| CN114478066A (en) * | 2021-12-30 | 2022-05-13 | 福建省佳美集团公司 | Ceramic glazing method |
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| CN106007669A (en) * | 2016-05-27 | 2016-10-12 | 张晓兵 | Totally closed zero-air-outlet double-layer Jun porcelain heat preserving cup and production method thereof |
| CN106892683A (en) * | 2017-03-10 | 2017-06-27 | 景德镇陶瓷大学 | A kind of architectural pottery high abrasion transparent microcrystal fritted glaze and the preparation method and obtained product of glaze layer |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106007669A (en) * | 2016-05-27 | 2016-10-12 | 张晓兵 | Totally closed zero-air-outlet double-layer Jun porcelain heat preserving cup and production method thereof |
| CN106892683A (en) * | 2017-03-10 | 2017-06-27 | 景德镇陶瓷大学 | A kind of architectural pottery high abrasion transparent microcrystal fritted glaze and the preparation method and obtained product of glaze layer |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108530034A (en) * | 2018-06-27 | 2018-09-14 | 福建省德化县陶缘茗陶瓷文化有限公司 | A kind of completely glaze ceramics and preparation method thereof |
| CN108530034B (en) * | 2018-06-27 | 2020-07-07 | 福建省德化县陶缘茗陶瓷文化有限公司 | Full-glaze ceramic and preparation method thereof |
| CN108793749A (en) * | 2018-07-26 | 2018-11-13 | 华宁县白塔山建筑陶瓷有限责任公司 | Ceramics colouring pigment and preparation method thereof |
| CN109231956A (en) * | 2018-09-14 | 2019-01-18 | 杨根成 | A kind of ancient customs figure image pottery production method |
| CN112759361A (en) * | 2021-01-06 | 2021-05-07 | 福建省威尔陶瓷股份有限公司 | High-siliceous high-temperature reinforced daily porcelain and preparation method thereof |
| CN113651532A (en) * | 2021-05-08 | 2021-11-16 | 浙江天物文化科技有限公司 | Tianmu mountain raw ore glaze and preparation method thereof |
| CN113754469A (en) * | 2021-09-16 | 2021-12-07 | 丽江永胜瓷业有限责任公司 | Lead dust removing method for ceramic glazing device |
| CN113788617A (en) * | 2021-09-26 | 2021-12-14 | 广东百强陶瓷有限公司 | Super-wear-resistant high-permeability diamond microcrystalline glaze and production process thereof |
| CN114478066A (en) * | 2021-12-30 | 2022-05-13 | 福建省佳美集团公司 | Ceramic glazing method |
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