CN107417103A - A kind of pottery jade glaze - Google Patents
A kind of pottery jade glaze Download PDFInfo
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- CN107417103A CN107417103A CN201710370474.9A CN201710370474A CN107417103A CN 107417103 A CN107417103 A CN 107417103A CN 201710370474 A CN201710370474 A CN 201710370474A CN 107417103 A CN107417103 A CN 107417103A
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- glaze
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- pottery jade
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Glass Compositions (AREA)
Abstract
A kind of pottery jade glaze, it is prepared by the raw material of following parts by weight：Red 25 30 parts of feldspar, 15 25 parts of melilite, 11 14 parts of calcite, 16 18 parts of quartz, 3.5 4.5 parts of lime stone, 1.5 2 parts of barium sulfate, 0.7 1 parts of zirconium silicate, 1.8 2.2 parts of zinc oxide, 2.3 2.6 parts of tin oxide.The present invention is formulated and controlled burning process compared with prior art, by adjusting, and improves the stability that colour stability is mutually formed with glass, its yield rate is improved by original 30% to more than 80%, saved cost and resource.
Description
Technical field
The present invention relates to a kind of glaze, and in particular to a kind of pottery jade glaze.
Background technology
Pottery is one of five big kiln porcelain of China's Song Dynasty, and using transmutation as god, natural transmutation is the elite institute of pottery art
It is being the distinctive gem of art in Countermeasure In Yuzhou City of Henan Province.Chun glaze is the decoration and protective layer on pottery surface, is to determine the life of pottery glaze colours
Into principal element, its colour generation and quality have much relations with glaze formula and burning process." jade glaze " in pottery is with it
Color such as bluish waves, such as ice are famous rich in jade texture as beautiful, bear the reputation of " an ancient unit of weight kiln jewel ".However, the manufacture difficulty of jade glaze
Greatly, yield rate is very low, and it is unstable to be mainly shown as that glaze colours colour generation is mutually formed with glass, therefore, need to be to conventional formulation and firing
Technique is improved.
The content of the invention
The purpose of the present invention is that to solve the pottery jade glaze that the deficiencies in the prior art provide a kind of high yield rate.
The purpose of the present invention is realized with following technical proposals：
A kind of pottery jade glaze, it is prepared by the raw material of following parts by weight：Red feldspar 25-30 parts, melilite 15-25
Part, calcite 11-14 parts, quartzy 16-18 parts, lime stone 3.5-4.5 parts, barium sulfate 1.5-2 parts, zirconium silicate 0.7-1 parts, oxidation
Zinc 1.8-2.2 parts, tin oxide 2.3-2.6 parts.
It is prepared by the raw material of following parts by weight：Red 27.50 parts of feldspar, 20 parts of melilite, 12.5 parts of calcite,
17 parts of quartz, 4 parts of lime stone, 1.75 parts of barium sulfate, 0.85 part of zirconium silicate, 2 parts of zinc oxide, 2.45 parts of tin oxide.
The preparation method of pottery jade glaze as described above, comprises the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；
（2）Glazing；
（3）Burn till, firing temperature is 1280-1300 DEG C.
Step（2）Middle glazing mode is using leaching glaze.
Step（3）Middle firing process specifically comprises the following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln,
Fired under oxidizing atmosphere, temperature is ramped up 900-950 DEG C in 2.5-3.5h；2. under reducing atmosphere, make temperature in 3-
4.5h is ramped up 1280-1300 DEG C；3. 2-2.5h under reducing atmosphere, is kept under the conditions of 1280-1300 DEG C；4. it is cooled to
Room temperature, it is made.
The present invention uses red feldspar and melilite compared with prior art, in formula, and as primary solvent, calcite is to help
Solvent, quartz can improve the mobility of glaze, and barium sulfate can reduce melt viscosity, increase the gloss of glaze, and zirconium silicate can improve glaze
Heat endurance and chemical stability, also used in this formula as opacifiers, promote glaze paint formed jade texture, zinc oxide
It is toning and toner with tin oxide；Then by controlling burning process, improve colour stability mutually formed with glass it is steady
It is qualitative, its yield rate is improved by original 30% to more than 80%, save cost and resource.
Embodiment
Embodiment 1
A kind of pottery jade glaze, is prepared by the raw material of following parts by weight：Red feldspar 25-30 parts, melilite 15-25 parts, side
Solve stone 11-14 parts, quartzy 16-18 parts, lime stone 3.5-4.5 parts, barium sulfate 1.5-2 parts, zirconium silicate 0.7-1 parts, zinc oxide
1.8-2.2 part, tin oxide 2.3-2.6 parts.
The preparation method of above-mentioned pottery jade glaze, comprises the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；
（2）Using the method glazing of leaching glaze；
（3）Burn till, firing temperature is 1280-1300 DEG C.
Firing process specifically comprises the following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln, under oxidizing atmosphere
Fire, temperature is ramped up 900-950 DEG C in 2.5-3.5h；2. temperature under reducing atmosphere, is set to be ramped up in 3-4.5h
1280-1300℃；3. 2-2.5h under reducing atmosphere, is kept under the conditions of 1280-1300 DEG C；4. being cooled to room temperature, it is made.
For the present invention using melilite, white feldspar as primary solvent, silicon, the content of iron are higher, although glaze paint gloss can be improved,
It is that its iron-holder is higher also easily to cause glaze to precipitate, therefore, it was found that, glaze can be increased by adding lime stone
Suspension, prevents its precipitation, and addition barium sulfate can reduce melt viscosity, further improve glaze mobility；Add zinc oxide and
Tin oxide can improve colour stability, and addition zirconium silicate can improve the stability that glaze glass is mutually formed.Therefore, the present invention is above-mentioned
Under the comprehensive function of raw material, parameter is burnt till by strictly controlling, drastically increases the yield rate of jade glaze.
Embodiment 2
A kind of pottery jade glaze, is prepared by the raw material of following parts by weight：Red 27.5 parts of feldspar, 20 parts of melilite, calcite
12.5 parts, quartz 17 parts, 4 parts of lime stone, 1.75 parts of barium sulfate, 0.85 part of zirconium silicate, 2 parts of zinc oxide, 2.45 parts of tin oxide.
The preparation method of above-mentioned pottery jade glaze, comprises the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；
（2）Using the method glazing of leaching glaze；
（3）Burn till, firing temperature is 1290 DEG C.
Firing process specifically comprises the following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln, under oxidizing atmosphere
Fire, temperature is ramped up 925 DEG C in 3h；2. temperature under reducing atmosphere, is set to be ramped up 1290 DEG C in 225min；3.
Under reducing atmosphere, 135min is kept under the conditions of 1290 DEG C；4. being cooled to room temperature, it is made.
The pottery jade glaze glaze colours obtained using said ratio and method moistens glossy, and in colour-stable, jade texture is strong,
Yield rate reaches more than 83%.
Embodiment 3
A kind of pottery jade glaze, is prepared by the raw material of following parts by weight：Red 27.5 parts of feldspar, 20 parts of melilite, calcite
12.5 parts, quartz 17 parts, 4 parts of lime stone, 1.75 parts of barium sulfate, 0.85 part of zirconium silicate, 2 parts of zinc oxide, 2.45 parts of tin oxide.
The preparation method of above-mentioned pottery jade glaze, comprises the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；
（2）Using the method glazing of leaching glaze；
（3）Burn till, firing temperature is 1280 DEG C.
Firing process specifically comprises the following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln, under oxidizing atmosphere
Fire, temperature is ramped up 950 DEG C in 2.5h；2. temperature under reducing atmosphere, is set to be ramped up 1280 DEG C in 4.5h；3.
Under reducing atmosphere, 2.5h is kept under the conditions of 1280 DEG C；4. being cooled to room temperature, it is made.
The pottery jade glaze glaze colours obtained using said ratio and method moistens glossy, and in colour-stable, jade texture is strong,
Yield rate reaches more than 81%.
Embodiment 4
A kind of pottery jade glaze, is prepared by the raw material of following parts by weight：Red 27.5 parts of feldspar, 20 parts of melilite, calcite
12.5 parts, quartz 17 parts, 4 parts of lime stone, 1.75 parts of barium sulfate, 0.85 part of zirconium silicate, 2 parts of zinc oxide, 2.45 parts of tin oxide.
The preparation method of above-mentioned pottery jade glaze, comprises the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；
（2）Using the method glazing of leaching glaze；
（3）Burn till, firing temperature is 1300 DEG C.
Firing process specifically comprises the following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln, under oxidizing atmosphere
Fire, temperature is ramped up 900 DEG C 3.5；2. temperature under reducing atmosphere, is set to be ramped up 1300 DEG C in 3h；3. also
Under Primordial Qi atmosphere, 2h is kept under the conditions of 1300 DEG C；4. being cooled to room temperature, it is made.
The pottery jade glaze glaze colours obtained using said ratio and method moistens glossy, and in colour-stable, jade texture is strong,
Yield rate reaches more than 80%.
Embodiment 5
A kind of pottery jade glaze, is prepared by the raw material of following parts by weight：Red 25 parts of feldspar, 25 parts of melilite, calcite 12
Part, 18 parts of quartz, 4 parts of lime stone, 1.75 parts of barium sulfate, 0.85 part of zirconium silicate, 2 parts of zinc oxide, 2.45 parts of tin oxide.Specific system
Preparation Method with embodiment 2, the pottery jade glaze glaze colours prepared using said ratio and method moisten it is glossy, in colour-stable,
Jade texture is strong, and yield rate reaches more than 80%.
Comparative example 1
A kind of pottery jade glaze, is prepared by the raw material of following parts by weight：Red 27.5 parts of feldspar, 20 parts of melilite, calcite
12.5 parts, quartz 17 parts, 1.75 parts of barium sulfate, 0.85 part of zirconium silicate, 2 parts of zinc oxide, 2.45 parts of tin oxide.Preparation method is the same as real
Apply example 2.Compared with Example 2, lime stone, the pottery jade glaze jade matter obtained using said ratio and method is not used in this example
Feel weaker, yield rate 30%.
Comparative example 2
A kind of pottery jade glaze, is prepared by the raw material of following parts by weight：Red 27.5 parts of feldspar, 20 parts of melilite, calcite
12.5 parts, quartz 17 parts, 4 parts of lime stone, 1.75 parts of barium sulfate, 2 parts of zinc oxide, 2.45 parts of tin oxide.Preparation method is the same as implementation
Example 2.Compared with Example 2, zirconium silicate is not used in this example, and the pottery jade glaze colour generation obtained using said ratio and method is more
Unstable, beautiful texture is weak, yield rate 45%.
Comparative example 3
A kind of pottery jade glaze, is prepared by the raw material of following parts by weight：Red 40 parts of feldspar, 20 parts of melilite, calcite
12.5 parts, quartz 17 parts, 1 part of lime stone, 1 part of barium sulfate, 0.85 part of zirconium silicate, 2 parts of zinc oxide, 2.45 parts of tin oxide.Prepare
Method is the same as embodiment 2.This example compared with Example 2, adds the dosage of red feldspar, reduces the use of lime stone and barium sulfate
Amount, the pottery jade glaze glaze aberration obtained using said ratio and method, matt, colour generation is unstable, and jade texture is weak, finished product
Rate is 30%.
The formula for the pottery jade glaze that 6-18 of the embodiment of the present invention is provided is shown in Table 1-2.
Claims (5)
- A kind of 1. pottery jade glaze, it is characterised in that：It is prepared by the raw material of following parts by weight：Red feldspar 25-30 parts, Melilite 15-25 parts, calcite 11-14 parts, quartzy 16-18 parts, lime stone 3.5-4.5 parts, barium sulfate 1.5-2 parts, zirconium silicate 0.7-1 parts, zinc oxide 1.8-2.2 parts, tin oxide 2.3-2.6 parts.
- 2. pottery jade glaze as claimed in claim 1, it is characterised in that：It is prepared by the raw material of following parts by weight： Red 27.50 parts of feldspar, 20 parts of melilite, 12.5 parts of calcite, 17 parts of quartz, 4 parts of lime stone, 1.75 parts of barium sulfate, zirconium silicate 0.85 part, 2 parts of zinc oxide, 2.45 parts of tin oxide.
- 3. the preparation method of the pottery jade glaze as described in claim any one of 1-2, it is characterised in that comprise the following steps：(1) add water to mix above-mentioned raw materials, ball milling, obtain glaze slip；(2) glazing；(3) burn till, firing temperature is 1280-1300 DEG C.
- 4. the preparation method of pottery jade glaze as claimed in claim 3, it is characterised in that step（2）Middle glazing mode is using leaching Glaze.
- 5. the preparation method of pottery jade glaze as claimed in claim 3, it is characterised in that step（3）Middle firing process specifically wraps Include following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, makes temperature in 2.5-3.5h It is ramped up 900-950 DEG C；2. under reducing atmosphere, temperature is set to be ramped up 1280-1300 DEG C in 3-4.5h；3. in also Primordial Qi Under atmosphere, 2-2.5h is kept under the conditions of 1280-1300 DEG C；4. being cooled to room temperature, it is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710370474.9A CN107417103A (en) | 2017-05-23 | 2017-05-23 | A kind of pottery jade glaze |
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| CN201710370474.9A CN107417103A (en) | 2017-05-23 | 2017-05-23 | A kind of pottery jade glaze |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111470773A (en) * | 2019-12-20 | 2020-07-31 | 吉林省梓楗新型建材股份有限公司 | Method for one-time sintering of microcrystalline jade |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104341138A (en) * | 2014-08-29 | 2015-02-11 | 福建省德化县腾艺陶瓷有限公司 | Blank, glaze formula and preparation process for preparation of imitated ceramics by utilizing waste porcelain clay |
| CN106242287A (en) * | 2016-08-18 | 2016-12-21 | 温书强 | A kind of red glaze of an ancient unit of weight and preparation method thereof |
-
2017
- 2017-05-23 CN CN201710370474.9A patent/CN107417103A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104341138A (en) * | 2014-08-29 | 2015-02-11 | 福建省德化县腾艺陶瓷有限公司 | Blank, glaze formula and preparation process for preparation of imitated ceramics by utilizing waste porcelain clay |
| CN106242287A (en) * | 2016-08-18 | 2016-12-21 | 温书强 | A kind of red glaze of an ancient unit of weight and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 阎夫立，阎飞，王双华: "《中国钧瓷》", 31 December 2004, 河南科学技术出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111470773A (en) * | 2019-12-20 | 2020-07-31 | 吉林省梓楗新型建材股份有限公司 | Method for one-time sintering of microcrystalline jade |
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Application publication date: 20171201 |