CN107582774A - One kind treats rheumatalgia pain monkshood dip and preparation method thereof - Google Patents
One kind treats rheumatalgia pain monkshood dip and preparation method thereof Download PDFInfo
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- CN107582774A CN107582774A CN201710727890.XA CN201710727890A CN107582774A CN 107582774 A CN107582774 A CN 107582774A CN 201710727890 A CN201710727890 A CN 201710727890A CN 107582774 A CN107582774 A CN 107582774A
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Abstract
The invention discloses one kind to treat rheumatalgia pain monkshood dip, and it is made up of the herbal raw material of following parts by weight：20~25 parts of 20~30 parts of monkshood, 20~30 parts of radix aconiti agrestis, 15~25 parts of vomiting nut, 10~20 parts of the root of herbaceous peony, 10~20 parts of lopseed, 9~16 parts of asarum, 15~20 parts of Rhizoma Arisaematis (processed), 15~25 parts of the root of Chinese clematis, 5~10 parts of Ramulus Taxilli, 15~25 parts of HERBA EPIMEDII and spina gleditsiae.The invention also discloses the preparation method for the treatment of rheumatalgia pain monkshood dip, enzymolysis is crushed by raw material, wants step to be made based on microbial fermentation, ultrasonic assistant flooding and ultrasonic assistant alcohol extract.Herbal raw material source of the present invention is wide, and cheap, scientific formulation is reasonable, and preparation technology is simple, and extraction Chinese herbal medicine functional components are high, and product safety environmental protection is without any side effects to human body, treats rheumatalgia pain significant effect.
Description
Technical field
The invention discloses a kind of dip, more particularly to one kind to treat rheumatalgia pain monkshood dip and its preparation side
Method, belong to traditional Chinese medicine field.
Background technology
Rheumatic arthritis is a kind of common disease, shows as painful swelling of joints, waist, leg, elbow, joint of lower extremity pain, type master
Have：Rheumatic arthritis, arthralgia are not cured long, arthralgia fever with chilliness, arthralgia local deformation etc., if no
To effective treatment or malpractice, it can not only cause each position arthralgia of the waist-leg of patient very unbearably, lower limb difficulty in walking,
Serious meeting causes quadriplegia, life-long disabilities.Doctor trained in Western medicine uses the medicines such as glucocorticoids, immunodepressant, treatment at present
Effect is undesirable, and toxic side effect, it is impossible to long-term use of.Have been reported that and be simply pulverized and mixed using Chinese herbal medicine or mixing water is fried
Rheumatalgia pain is treated into pill, tablet, decoction etc., but because such preparation method obtains product Chinese herbal medicine functional components
It is low, it is more difficult to it is absorbed and used, and takes Chinese herbal medicine taste and also having for liver are necessarily stimulated and damaged, therefore, should
It is also restrained with effect and application scale.
Dipping has original effect to human body, with a history of thousands of years in China, since ancient times always by medical field weight
Depending on.Dipping method is one of external therapy, i.e., a variety of with decoction or a kind of method containing decoction water washing bath whole body or part, its form
It is various.In general, medicine acts on whole body fleshy exterior, part, affected part to the dipping mechanism of action, and through absorbing, circulation channels and collaterals blood vessels are interior
Up to internal organs, from outward appearance to inner essence, thus effect is produced.Dipping bathing, can play dredging the channel, activate blood circulation and disperse blood clots, wind dispelling cold dispelling, heat-clearing solution
Poison, swelling and pain relieving, negative and positive are adjusted, coordinates internal organs, current qi and blood, moisten the health maintenance effects such as foster whole body.Dipping avoids medicine to spleen
The stimulation of stomach and the infringement to liver, effective ingredient is absorbed by skin to play effect, be the various chronic diseases of preventing and treating
Disease and the Perfected process of health care.
Chinese herbal medicine is the rarity of Chinese traditional culture, proves that a variety of Chinese herbal medicines have in practice and enhances metabolism, changes
Kind blood circulation, the strong kidney of tonifying liver, make inquiries the work(such as active, removing damp-heat, swelling and pain relieving, expelling wind and clearing away cold, expelling pathogenic factors from muscles and skin dehumidifying, strengthening the muscles and bones
Effect, therefore, Chinese herbal medicine dipping is applied to treatment rheumatalgia pain for improving national life quality, ensures that living safety has ten
Divide important meaning, but treatment rheumatalgia pain dipping not yet realizes scale and industrialization, subject matter medium-height grass in application at present
Medicine compatibility is unreasonable, the drawbacks such as functional component recovery rate is low, be difficult to industrialized production, effect is not notable, therefore develops new
Treatment rheumatalgia pain dipping has important practical significance.
The content of the invention
It is an object of the invention to according to it is existing treatment ache of rheumatoid arthritis product and technology existing for above mentioned problem,
Exploitation one kind treats rheumatalgia pain monkshood dip, people is passed through whole body dipping to promote body metabolism, improves body
Blood circulation, makes inquiries active, expelling wind and clearing away cold, expelling pathogenic factors from muscles and skin dehumidifying, the strong kidney of tonifying liver, strengthening the muscles and bones, the cause of disease is dispelled from root, allows people
Puzzlement away from rheumatalgia pain.
To achieve these goals, the present invention uses following technical scheme：
One kind treats rheumatalgia pain monkshood dip, is made up of the herbal raw material of following parts by weight：20~30 parts of monkshood, radix aconiti agrestis
20~30 parts, 15~25 parts of vomiting nut, 10~20 parts of the root of herbaceous peony, 10~20 parts of lopseed, 9~16 parts of asarum, Rhizoma Arisaematis (processed) 15~20
20~25 parts of part, 15~25 parts of the root of Chinese clematis, 5~10 parts of Ramulus Taxilli, 15~25 parts of HERBA EPIMEDII and spina gleditsiae.
The preparation method of present invention treatment rheumatalgia pain monkshood dip, comprises the following steps：
（1）Stock：The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion；
（2）Feedstock treating：Herbal raw material is cleaned up, at 70~85 DEG C, after air blast drying, pulverizer crushes, and crosses 50
~100 mesh sieves, mix, obtain composite Chinese herbal raw material；
（3）Enzymolysis：By step（2）Gained composite Chinese herbal raw material adds water to solid-to-liquid ratio 1：3~5, by 2.0~3.0 g/L, 1.5
~2.5 g/L, 2~4 g/L ratios add non-starch polysaccharide enzyme, carbohydrase, cellulase respectively, in 500 ~ 800 W ultrasonic waves
Under booster action, the min of coordinated enzymatic hydrolysis 45~60 under the conditions of 40~50 DEG C；
（4）Microbial fermentation：To step（3）The Bifidobacterium added in gained Enzymolysis liquid after 3~5% activation（Viable count >=
20000000000/ml）, ferment under anaerobic condition 15~20 h, controls 28~35 DEG C of fermentation temperature；
（5）Ultrasonic assistant flooding：By step（4）Microbial fermentation mixed liquor, 85~95 DEG C are warmed to, in 600 ~ 800 W
Under ultrasonic assistant effect, 45 ~ 60 min are extracted, after extraction terminates, 150 ~ 200 mesh filter clothes is crossed and obtains water extract.Filter residue adds 3 ~ 5
Times pure water, carries out Ultrasonic Wave-Assisted Extraction, filters to get filtrate in the same way, and it is water extract to merge extract solution twice；
（6）Ultrasonic assistant alcohol steep：To step（5）The ethanol that 3~6 times of concentration are 55~65% is added in gained filter residue,
Under the conditions of 600~900 W ultrasonic assistants, 40~60 min, 50~60 DEG C of extraction temperature are extracted；
（7）Centrifugation：Extraction centrifuges solid residue and alcohol extract after terminating；
（8）Concentration distillation：Alcohol extract is concentrated under reduced pressure and is distilled to recover ethanol；
（9）Mixing：By step（5）Water extract and step（8）Reclaim the leaching liquor mixing after ethanol；
（10）Filtering：Mixed liquor is filtered to remove impurity and insoluble matter therein through diatom filter and produces treatment rheumatalgia pain river
Root of three-nerved spicebush body lotion.
The present invention provides one kind and treats rheumatalgia pain monkshood dip, the characteristic of each Chinese herbal medicine in combined formulation, using Syndrome Differentiation of Chinese Medicine
Card theory is developed, and scientific formulation is reasonable, is acted synergistically between each component, proves that the present invention is ached various chill by long-term use
Bitterly, including pain in the back, skelagia, cervical spondylopathy, scapulohumeral periarthritis and femoral head disease, spinal canal stenosis, osteoproliferation have the effect of good.This hair
Bright advantage is：（1）Product is not required to by body absorption using medicine during dipping, and drug effect is directly acted on into affected part, safety
Environmental protection, mild in medicine property and, it is without any side effects to human body；（2）Product has pleasant Chinese herbal medicine delicate fragrance, easy to use, during use
This product only need to be taken by 1：300~600 ratios are called in heating bath water, can carry out immersion bathing；（3）Added merely with medical bathing powder
Compare, compared with medical bathing powder adds merely, the present invention crushes enzymolysis, microbial fermentation, ultrasonic assistant flooding using raw material
With the extraction of ultrasonic assistant alcohol based on want preparation process, improve Chinese herbal medicine functional components, treatment rheumatalgia pain effect is notable；
（4）Raw material sources are wide in the present invention, cheap, and production and processing technology is simple, are adapted to large-scale production.
Embodiment
Below by embodiment, the present invention will be further described.In the present invention, if not refering in particular to, Suo Youbai
Point ratio is unit of weight, and all devices and raw material are commercially available or the industry is commonly used, in following embodiments
Method, it is this area conventional method unless otherwise instructed.
Embodiment 1
One kind treats rheumatalgia pain monkshood dip, is made up of the herbal raw material of following each component：Monkshood, radix aconiti agrestis, vomiting nut,
The root of herbaceous peony, lopseed, asarum, Rhizoma Arisaematis (processed), the root of Chinese clematis, Ramulus Taxilli, HERBA EPIMEDII and spina gleditsiae.Each component is specific in herbal raw material
Proportioning is as shown in table 1.
The preparation method of present invention treatment rheumatalgia pain monkshood dip, comprises the following steps：
（1）Stock：The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion；
（2）Feedstock treating：Herbal raw material is cleaned up, at 82 DEG C, after air blast drying, pulverizer crushes, and crosses 60 mesh
Sieve, mix, obtain composite Chinese herbal raw material；
（3）Enzymolysis：By step（2）Gained composite Chinese herbal raw material adds water to solid-to-liquid ratio 1：4, by 2.5 g/L, 1.8 g/L, 3 g/
L ratios add non-starch polysaccharide enzyme, carbohydrase, cellulase respectively, under the effect of 750 W ultrasonic assistants, in 40 DEG C of conditions
The lower min of coordinated enzymatic hydrolysis 56；
（4）Microbial fermentation：To step（3）The Bifidobacterium added in gained Enzymolysis liquid after 3% activation（Viable count >=200
Hundred million/ml）, ferment under anaerobic condition 20 h, controls 30 DEG C of fermentation temperature；
（5）Ultrasonic assistant flooding：By step（4）Microbial fermentation mixed liquor, 85 DEG C are warmed to, it is auxiliary in 650 W ultrasonic waves
Help under effect, extract 50 min, after extraction terminates, cross 180 mesh filter clothes and obtain water extract.Filter residue adds 5 times of pure water, by same sample prescription
Method carries out Ultrasonic Wave-Assisted Extraction, filters to get filtrate, and it is water extract to merge extract solution twice；
（6）Ultrasonic assistant alcohol steep：To step（5）The ethanol that 5 times of concentration are 58% is added in gained filter residue, in 650 W
Under the conditions of ultrasonic assistant, 50 min, 60 DEG C of extraction temperature are extracted；
（7）Centrifugation：Extraction centrifuges solid residue and alcohol extract after terminating；
（8）Concentration distillation：Alcohol extract is concentrated under reduced pressure and is distilled to recover ethanol；
（9）Mixing：By step（5）Water extract and step（8）Reclaim the leaching liquor mixing after ethanol；
（10）Filtering：Mixed liquor is filtered to remove impurity and insoluble matter therein through diatom filter and produces treatment rheumatalgia pain river
Root of three-nerved spicebush body lotion.
Embodiment 2
One kind treats rheumatalgia pain monkshood dip, is made up of the herbal raw material of following each component：Monkshood, radix aconiti agrestis, vomiting nut,
The root of herbaceous peony, lopseed, asarum, Rhizoma Arisaematis (processed), the root of Chinese clematis, Ramulus Taxilli, HERBA EPIMEDII and spina gleditsiae.Each component is specific in herbal raw material
Proportioning is as shown in table 1.
The preparation method of present invention treatment rheumatalgia pain monkshood dip, comprises the following steps：
（1）Stock：The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion；
（2）Feedstock treating：Herbal raw material is cleaned up, at 78 DEG C, after air blast drying, pulverizer crushes, and crosses 100 mesh
Sieve, mix, obtain composite Chinese herbal raw material；
（3）Enzymolysis：By step（2）Gained composite Chinese herbal raw material adds water to solid-to-liquid ratio 1：3, by 2.2 g/L, 2.0 g/L, 3.5
G/L ratios add non-starch polysaccharide enzyme, carbohydrase, cellulase respectively, under the effect of 650 W ultrasonic assistants, in 43 DEG C of bars
The min of coordinated enzymatic hydrolysis 52 under part；
（4）Microbial fermentation：To step（3）The Bifidobacterium added in gained Enzymolysis liquid after 4% activation（Viable count >=200
Hundred million/ml）, ferment under anaerobic condition 18 h, controls 32 DEG C of fermentation temperature；
（5）Ultrasonic assistant flooding：By step（4）Microbial fermentation mixed liquor, 90 DEG C are warmed to, it is auxiliary in 700 W ultrasonic waves
Help under effect, extract 56 min, after extraction terminates, cross 160 mesh filter clothes and obtain water extract.Filter residue adds 4 times of pure water, by same sample prescription
Method carries out Ultrasonic Wave-Assisted Extraction, filters to get filtrate, and it is water extract to merge extract solution twice；
（6）Ultrasonic assistant alcohol steep：To step（5）The ethanol that 4 times of concentration are 60% is added in gained filter residue, in 750 W
Under the conditions of ultrasonic assistant, 45 min, 55 DEG C of extraction temperature are extracted；
（7）Centrifugation：Extraction centrifuges solid residue and alcohol extract after terminating；
（8）Concentration distillation：Alcohol extract is concentrated under reduced pressure and is distilled to recover ethanol；
（9）Mixing：By step（5）Water extract and step（8）Reclaim the leaching liquor mixing after ethanol；
（10）Filtering：Mixed liquor is filtered to remove impurity and insoluble matter therein through diatom filter and produces treatment rheumatalgia pain river
Root of three-nerved spicebush body lotion.
Embodiment 3
One kind treats rheumatalgia pain monkshood dip, is made up of the herbal raw material of following each component：Monkshood, radix aconiti agrestis, vomiting nut,
The root of herbaceous peony, lopseed, asarum, Rhizoma Arisaematis (processed), the root of Chinese clematis, Ramulus Taxilli, HERBA EPIMEDII and spina gleditsiae.Each component is specific in herbal raw material
Proportioning is as shown in table 1.
The preparation method of present invention treatment rheumatalgia pain monkshood dip, comprises the following steps：
（1）Stock：The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion；
（2）Feedstock treating：Herbal raw material is cleaned up, at 74 DEG C, after air blast drying, pulverizer crushes, and crosses 80 mesh
Sieve, mix, obtain composite Chinese herbal raw material；
（3）Enzymolysis：By step（2）Gained composite Chinese herbal raw material adds water to solid-to-liquid ratio 1：5, by 2.8 g/L, 2.3 g/L, 2.5
G/L ratios add non-starch polysaccharide enzyme, carbohydrase, cellulase respectively, under the effect of 550 W ultrasonic assistants, in 46 DEG C of bars
The min of coordinated enzymatic hydrolysis 48 under part；
（4）Microbial fermentation：To step（3）The Bifidobacterium added in gained Enzymolysis liquid after 5% activation（Viable count >=200
Hundred million/ml）, ferment under anaerobic condition 16 h, controls 34 DEG C of fermentation temperature；
（5）Ultrasonic assistant flooding：By step（4）Microbial fermentation mixed liquor, 95 DEG C are warmed to, it is auxiliary in 750 W ultrasonic waves
Help under effect, extract 46 min, after extraction terminates, cross 200 mesh filter clothes and obtain water extract.Filter residue adds 3 times of pure water, by same sample prescription
Method carries out Ultrasonic Wave-Assisted Extraction, filters to get filtrate, and it is water extract to merge extract solution twice；
（6）Ultrasonic assistant alcohol steep：To step（5）The ethanol that 6 times of concentration are 62% is added in gained filter residue, in 850 W
Under the conditions of ultrasonic assistant, 55min, 50 DEG C of extraction temperature are extracted；
（7）Centrifugation：Extraction centrifuges solid residue and alcohol extract after terminating；
（8）Concentration distillation：Alcohol extract is concentrated under reduced pressure and is distilled to recover ethanol；
（9）Mixing：By step（5）Water extract and step（8）Reclaim the leaching liquor mixing after ethanol；
（10）Filtering：Mixed liquor is filtered to remove impurity and insoluble matter therein through diatom filter and produces treatment rheumatalgia pain river
Root of three-nerved spicebush body lotion.
The composition and ratio of each embodiment herbal raw material of table 1.
| Sequence number | Component | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| 1 | Monkshood（Part） | 23 | 26 | 29 |
| 2 | Radix aconiti agrestis（Part） | 25 | 27 | 21 |
| 3 | Vomiting nut（Part） | 23 | 19 | 16 |
| 4 | The root of herbaceous peony（Part） | 13 | 16 | 19 |
| 5 | Lopseed（Part） | 18 | 16 | 14 |
| 6 | Asarum（Part） | 11 | 13 | 15 |
| 7 | Rhizoma Arisaematis (processed)（Part） | 18 | 16 | 17 |
| 8 | The root of Chinese clematis（Part） | 21 | 18 | 23 |
| 9 | Ramulus Taxilli（Part） | 6 | 9 | 7 |
| 10 | HERBA EPIMEDII（Part） | 17 | 20 | 23 |
| 11 | Spina gleditsiae（Part） | 23 | 21 | 22 |
| 12 | Summation（Part） | 198 | 201 | 206 |
Although to reach illustration purpose, described above is the preferred embodiments of the present invention, is not intended to limit the invention, to the greatest extent
The present invention is described in detail with reference to the foregoing embodiments for pipe, and for those skilled in the art, it still can be with
The technical scheme recorded to foregoing embodiments is modified, or carries out equivalent substitution to which part technical characteristic.It is all
Within the spirit and principles in the present invention, any modification, equivalent substitution and improvements made etc., the protection of the present invention should be included in
Within the scope of.
Claims (2)
1. one kind treats rheumatalgia pain monkshood dip, it is characterised in that is made up of following herbal raw material by weight：River
20~30 parts of crow, 20~30 parts of radix aconiti agrestis, 15~25 parts of vomiting nut, 10~20 parts of the root of herbaceous peony, 10~20 parts of lopseed, asarum 9~16
Part, 15~20 parts of Rhizoma Arisaematis (processed), 15~25 parts of the root of Chinese clematis, 5~10 parts of Ramulus Taxilli, 15~25 parts of HERBA EPIMEDII and spina gleditsiae 20~25
Part.
A kind of 2. preparation method for the treatment of rheumatalgia pain monkshood dip as claimed in claim 1, it is characterised in that including with
Lower step：
（1）Stock：The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion；
（2）Feedstock treating：Herbal raw material is cleaned up, at 70~85 DEG C, after air blast drying, pulverizer crushes, and crosses 50
~100 mesh sieves, mix, obtain composite Chinese herbal raw material；
（3）Enzymolysis：By step（2）Gained composite Chinese herbal raw material adds water to solid-to-liquid ratio 1：3~5, by 2.0~3.0 g/L, 1.5
~2.5 g/L, 2~4 g/L ratios add non-starch polysaccharide enzyme, carbohydrase, cellulase respectively, in 500 ~ 800 W ultrasonic waves
Under booster action, the min of coordinated enzymatic hydrolysis 45~60 under the conditions of 40~50 DEG C；
（4）Microbial fermentation：To step（3）The Bifidobacterium added in gained Enzymolysis liquid after 3~5% activation（Viable count >=
20000000000/ml）, ferment under anaerobic condition 15~20 h, controls 28~35 DEG C of fermentation temperature；
（5）Ultrasonic assistant flooding：By step（4）Microbial fermentation mixed liquor, 85~95 DEG C are warmed to, in 600 ~ 800 W
Under ultrasonic assistant effect, 45 ~ 60 min are extracted, after extraction terminates, 150 ~ 200 mesh filter clothes is crossed and obtains water extract；Filter residue adds 3 ~ 5
Times pure water, carries out Ultrasonic Wave-Assisted Extraction, filters to get filtrate in the same way, and it is water extract to merge extract solution twice；
（6）Ultrasonic assistant alcohol steep：To step（5）The ethanol that 3~6 times of concentration are 55~65% is added in gained filter residue,
Under the conditions of 600~900 W ultrasonic assistants, 40~60 min, 50~60 DEG C of extraction temperature are extracted；
（7）Centrifugation：Extraction centrifuges solid residue and alcohol extract after terminating；
（8）Concentration distillation：Alcohol extract is concentrated under reduced pressure and is distilled to recover ethanol；
（9）Mixing：By step（5）Water extract and step（8）Reclaim the leaching liquor mixing after ethanol；
（10）Filtering：Mixed liquor is filtered to remove impurity and insoluble matter therein through diatom filter and produces treatment rheumatalgia pain river
Root of three-nerved spicebush body lotion.
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| CN201710727890.XA CN107582774A (en) | 2017-08-23 | 2017-08-23 | One kind treats rheumatalgia pain monkshood dip and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113425774A (en) * | 2021-06-25 | 2021-09-24 | 杨建民 | Herbal wrapped moxibustion liquid medicine for treating rheumatic ostealgia and preparation method thereof |
-
2017
- 2017-08-23 CN CN201710727890.XA patent/CN107582774A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113425774A (en) * | 2021-06-25 | 2021-09-24 | 杨建民 | Herbal wrapped moxibustion liquid medicine for treating rheumatic ostealgia and preparation method thereof |
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