CN107617003A - A kind of cure scapulohumeral periarthritis rhizoma atractylodis dip and preparation method thereof - Google Patents

A kind of cure scapulohumeral periarthritis rhizoma atractylodis dip and preparation method thereof Download PDF

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CN107617003A
CN107617003A CN201710727788.XA CN201710727788A CN107617003A CN 107617003 A CN107617003 A CN 107617003A CN 201710727788 A CN201710727788 A CN 201710727788A CN 107617003 A CN107617003 A CN 107617003A
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parts
raw material
rhizoma atractylodis
scapulohumeral periarthritis
chinese herbal
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廖艳卿
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Abstract

The invention discloses a kind of cure scapulohumeral periarthritis rhizoma atractylodis dip, and it is made up of the herbal raw material of following parts by weight:20~30 parts of rhizoma atractylodis, 10~20 parts of folium artemisiae argyi, 15~25 parts of turpentine, 10~15 parts of Impatientis, 5~10 parts of notopterygium root, 15~20 parts of ramulus mori, 5~10 parts of vomiting nut, 10~15 parts of lycopodium calvatum, 10~15 parts of lopseed, 9~16 parts of the root of Chinese clematis, 10~15 parts of reticulate millettia, 5~10 parts of Ligusticum wallichii.The invention also discloses the preparation method of cure scapulohumeral periarthritis rhizoma atractylodis dip, is crushed by herbal raw material, ultrasound adverse current is extracted, is concentrated under reduced pressure and filtered homogeneous and is made up of master operation.Herbal raw material source of the present invention is wide, and cheap, scientific formulation is reasonable, and preparation technology is simple, and extraction Chinese herbal medicine functional components are high, product safety environmental protection, cure scapulohumeral periarthritis significant effect without any side effects to human body.

Description

A kind of cure scapulohumeral periarthritis rhizoma atractylodis dip and preparation method thereof
Technical field
The invention discloses a kind of dipping, more particularly to a kind of cure scapulohumeral periarthritis rhizoma atractylodis dip and preparation method thereof, category Traditional Chinese medicine field.
Background technology
It is a kind of damaging, regression of shoulder joint and its surrounding tissue it is well known that periarthritis of shoulderjoint abbreviation scapulohumeral periarthritis Venereal disease becomes.Pathogenic factor often causes because of supraspinatus tendinitis, bicipital muscle of arm inflammation, subacromial bursitis etc., can also make because of trauma disorders Shoulder is fixed for a long time, caused by chronic strain or endocrine disturbance.The traditional Chinese medical science think due to wound, strain lesion, liver-kidney deficiency, Muscles and bones lose support, wind-cold damp pathogen takes advantage of empty invasion, is detained between omoplate muscles and bones, cause channels and collaterals to be jammed, qi and blood coagulates puckery, with the passing of time muscles contracture And form this disease.Its it is clinical from the beginning of when show as shoulder arthralgia, can be dull pain, lancinating pain, night aggravates, or even pain is awake, It can not be lain on one's side to Ipsilateral.Shoulder can cause severe pain, and can be radiated to neck or ancon when being pulled.The state of an illness further adds During weight, show as shoulder joint to all directions limitation of activity, with abduction, outward turning and after to stretch obstacle most obvious.
Scapulohumeral periarthritis for a long time, influences the normal life and work of patient, brought much to patient as chronic disease Trouble, and scapulohumeral periarthritis belongs to outer disease, it then follows tcm syndrome differentiation and treatment principle, outer disease should use and control mode outside, so in taking Medicine is obviously ineffective to control scapulohumeral periarthritis, and the medicine symptomatic treatments such as antipyretic analgesic are mainly applied come cure scapulohumeral periarthritis by Western medicine, Cure the symptoms, not the disease.On the whole, there is the shortcomings that scapulohumeral periarthritis obstinate, therefore, scapulohumeral periarthritis in existing scapulohumeral periarthritis medicine for treatment Greatly pain and spirit, financial burden are brought to patient.
Dipping has original effect to human body, with a history of thousands of years in China, since ancient times always by medical field weight Depending on.Dipping method is one of external therapy, i.e., a variety of with decoction or a kind of method containing decoction water washing bath whole body or part, its form It is various.In general, medicine acts on whole body fleshy exterior, part, affected part to the dipping mechanism of action, and through absorbing, circulation channels and collaterals blood vessels are interior Up to internal organs, from outward appearance to inner essence, thus effect is produced.Dipping bathing, can play dredging the channel, activate blood circulation and disperse blood clots, wind dispelling cold dispelling, heat-clearing solution Poison, swelling and pain relieving, negative and positive are adjusted, coordinates internal organs, current qi and blood, moisten the health maintenance effects such as foster whole body.Dipping avoids medicine to spleen The stimulation of stomach and the infringement to liver, effective ingredient is absorbed by skin to play effect, be the various chronic diseases of preventing and treating Disease and the Perfected process of health care.
Chinese herbal medicine is the rarity of Chinese traditional culture, proves that a variety of Chinese herbal medicines have in practice and enhances metabolism, changes Kind blood circulation, expelling wind and clearing away cold, promoting blood circulation and removing obstruction in channels, dispersing swelling and dissipating binds, expelling pathogenic factors from muscles and skin dehumidifying, strengthening the muscles and bones, strengthen the body resistance to consolidate the constitution and other effects, therefore, Chinese herbal medicine is applied to expelling wind and clearing away cold, it is very heavy to ensure that living safety has for improving national life quality for cure scapulohumeral periarthritis The meaning wanted, but Chinese herbal medicine scapulohumeral periarthritis dipping at present not yet realizes scale and industrialization in application, and subject matter is Chinese herbal medicine The drawbacks such as compatibility is unreasonable, functional component recovery rate is low, be difficult to industrialized production, effect is not notable, therefore develop new control Scapulohumeral periarthritis dipping is treated to have important practical significance.
The content of the invention
It is an object of the invention to the above mentioned problem according to existing for existing cure scapulohumeral periarthritis product, exploitation cure scapulohumeral periarthritis are grey Art dip, people is passed through dipping to promote body metabolism, improve body blood and circulate, expelling wind and clearing away cold, promoting blood circulation and removing obstruction in channels, Dispersing swelling and dissipating binds, expelling pathogenic factors from muscles and skin dehumidifying, strengthening the muscles and bones, strengthen the body resistance to consolidate the constitution, the scapulohumeral periarthritis cause of disease dispelled from root, with reach cure scapulohumeral periarthritis it Effect.
To achieve these goals, the present invention uses following technical scheme:
A kind of cure scapulohumeral periarthritis rhizoma atractylodis dip, is made up of the herbal raw material of following parts by weight:20~30 parts of rhizoma atractylodis, folium artemisiae argyi 10 ~20 parts, 15~25 parts of turpentine, 10~15 parts of Impatientis, 5~10 parts of notopterygium root, 15~20 parts of ramulus mori, 5~10 parts of vomiting nut, stretch 10~15 parts of muscle grass, 10~15 parts of lopseed, 9~16 parts of the root of Chinese clematis, 10~15 parts of reticulate millettia, 5~10 parts of Ligusticum wallichii.
The preparation method of cure scapulohumeral periarthritis rhizoma atractylodis dip of the present invention, comprises the following steps:
(1)Stock:The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion;
(2)Feedstock treating:Herbal raw material is cleaned up, at 70~90 DEG C, after air blast drying, pulverizer crushes, and crosses 50 ~100 mesh sieves, mix, obtain composite Chinese herbal raw material;
(3)Ultrasonic adverse current is extracted:By step(2)Gained composite Chinese herbal raw material, 4~6 times of 50~60% ethanol are added, are put into In ultrasonic continuous countercurrent extractor, under the effect of 600 ~ 1000 W ultrasonic assistants, after adverse current extracts 30 ~ 45 min, excessively 120 ~ 180 mesh filter clothes obtain water extract;Filter residue adds 2 ~ 4 times of 50~60% ethanol, carries out ultrasonic continuous countercurrent extraction in the same way, Filter to get filtrate, it is extracts of Chinese herbal medicine to merge extract solution twice;
(4)It is concentrated under reduced pressure:By step(3)The extracts of Chinese herbal medicine of gained at 60~70 DEG C of temperature, vacuum -0.06~- It is evaporated under reduced pressure under 0.085 MPa, reclaims the ethanol in extracts of Chinese herbal medicine to without alcohol taste, obtain removal ethanol Chinese herbal medicine and carry Take liquid;
(5)Filtering:By step(4)Gained extracts of Chinese herbal medicine, impurity and insoluble matter therein are filtered to remove through diatom filter Produce cure scapulohumeral periarthritis rhizoma atractylodis dip.
The present invention provides a kind of cure scapulohumeral periarthritis rhizoma atractylodis dip, the characteristic of each Chinese herbal medicine in combined formulation, using Chinese medical discrimination Theory is developed, and scientific formulation is reasonable, is acted synergistically between each component, proves the present invention to various wind-cold-dampness arthralgias by long-term use Disease, including scapulohumeral periarthritis, pain in the back, skelagia, cervical spondylopathy, femoral head disease, spinal canal stenosis and osteoproliferation have the effect of good to cure Do not recur afterwards.Advantage of the invention is that:(1)Product is not required to by body absorption using medicine during dipping, and drug effect is directly made For affected part, safety and environmental protection, mild in medicine property and, it is without any side effects to human body;(2)Product has pleasant Chinese herbal medicine delicate fragrance, makes This product need to be only taken by 1 with convenient, during use:300~600 ratios are called in heating bath water, can carry out immersion bathing;(3)With Medical bathing powder merely compare by addition, and the present invention uses raw material crushing, the extraction of ultrasound adverse current, filtering homogeneous to have for main preparation section Effect ground improves Chinese herbal medicine functional components, and cure scapulohumeral periarthritis effect is notable;(4)Raw material sources are wide in the present invention, cheap, raw Production. art is simple, is adapted to large-scale production.
Embodiment
Below by embodiment, the present invention will be further described.In the present invention, if not refering in particular to, Suo Youbai Point ratio is unit of weight, and all devices and raw material are commercially available or the industry is commonly used, in following embodiments Method, it is this area conventional method unless otherwise instructed.
Embodiment 1
A kind of cure scapulohumeral periarthritis rhizoma atractylodis dip, is made up of the herbal raw material of following parts by weight:Rhizoma atractylodis, folium artemisiae argyi, turpentine, phoenix are celestial Grass, notopterygium root, ramulus mori, vomiting nut, lycopodium calvatum, lopseed, the root of Chinese clematis, reticulate millettia and Ligusticum wallichii.The tool of each component in herbal raw material Body proportioning is as shown in table 1.
The preparation method of cure scapulohumeral periarthritis rhizoma atractylodis dip of the present invention, comprises the following steps:
(1)Stock:The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion;
(2)Feedstock treating:Herbal raw material is cleaned up, at 80 DEG C, after air blast drying, pulverizer crushes, and crosses 80 mesh Sieve, mix, obtain composite Chinese herbal raw material;
(3)Ultrasonic adverse current is extracted:By step(2)Gained composite Chinese herbal raw material, 4 times of 60% ethanol is added, be put into ultrasonic continuous In countercurrent extraction machine, under the effect of 900 W ultrasonic assistants, after adverse current extracts 35 min, cross 140 mesh filter clothes and obtain water extract; Filter residue adds 3 times of 55% ethanol, carries out ultrasonic continuous countercurrent extraction in the same way, filters to get filtrate, and merges extract solution twice and is For extracts of Chinese herbal medicine;
(4)It is concentrated under reduced pressure:By step(3)The extracts of Chinese herbal medicine of gained enters at 62 DEG C of temperature under the MPa of vacuum -0.06 Row is evaporated under reduced pressure, and is reclaimed the ethanol in extracts of Chinese herbal medicine to without alcohol taste, is obtained removing ethanol extracts of Chinese herbal medicine;
(5)Filtering:By step(4)Gained extracts of Chinese herbal medicine, impurity and insoluble matter therein are filtered to remove through diatom filter Produce cure scapulohumeral periarthritis rhizoma atractylodis dip.
Embodiment 2
A kind of cure scapulohumeral periarthritis rhizoma atractylodis dip, is made up of the herbal raw material of following parts by weight:Rhizoma atractylodis, folium artemisiae argyi, turpentine, phoenix are celestial Grass, notopterygium root, ramulus mori, vomiting nut, lycopodium calvatum, lopseed, the root of Chinese clematis, reticulate millettia and Ligusticum wallichii.The tool of each component in herbal raw material Body proportioning is as shown in table 1.
The preparation method of cure scapulohumeral periarthritis rhizoma atractylodis dip of the present invention, comprises the following steps:
(1)Stock:The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion;
(2)Feedstock treating:Herbal raw material is cleaned up, at 85 DEG C, after air blast drying, pulverizer crushes, and crosses 90 mesh Sieve, mix, obtain composite Chinese herbal raw material;
(3)Ultrasonic adverse current is extracted:By step(2)Gained composite Chinese herbal raw material, 5 times of 55% ethanol is added, be put into ultrasonic continuous In countercurrent extraction machine, under the effect of 800 W ultrasonic assistants, after adverse current extracts 40 min, cross 160 mesh filter clothes and obtain water extract; Filter residue adds 2 times of 50% ethanol, carries out ultrasonic continuous countercurrent extraction in the same way, filters to get filtrate, and merges extract solution twice and is For extracts of Chinese herbal medicine;
(4)It is concentrated under reduced pressure:By step(3)The extracts of Chinese herbal medicine of gained enters at 65 DEG C of temperature under the MPa of vacuum -0.07 Row is evaporated under reduced pressure, and is reclaimed the ethanol in extracts of Chinese herbal medicine to without alcohol taste, is obtained removing ethanol extracts of Chinese herbal medicine;
(5)Filtering:By step(4)Gained extracts of Chinese herbal medicine, impurity and insoluble matter therein are filtered to remove through diatom filter Produce cure scapulohumeral periarthritis rhizoma atractylodis dip.
Embodiment 3
A kind of cure scapulohumeral periarthritis rhizoma atractylodis dip, is made up of the herbal raw material of following parts by weight:Rhizoma atractylodis, folium artemisiae argyi, turpentine, phoenix are celestial Grass, notopterygium root, ramulus mori, vomiting nut, lycopodium calvatum, lopseed, the root of Chinese clematis, reticulate millettia and Ligusticum wallichii.The tool of each component in herbal raw material Body proportioning is as shown in table 1.
The preparation method of cure scapulohumeral periarthritis rhizoma atractylodis dip of the present invention, comprises the following steps:
(1)Stock:The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion;
(2)Feedstock treating:Herbal raw material is cleaned up, at 75 DEG C, after air blast drying, pulverizer crushes, and crosses 60 mesh Sieve, mix, obtain composite Chinese herbal raw material;
(3)Ultrasonic adverse current is extracted:By step(2)Gained composite Chinese herbal raw material, 6 times of 50% ethanol is added, be put into ultrasonic continuous In countercurrent extraction machine, under the effect of 700 W ultrasonic assistants, after adverse current extracts 45 min, cross 180 mesh filter clothes and obtain water extract; Filter residue adds 4 times of 60% ethanol, carries out ultrasonic continuous countercurrent extraction in the same way, filters to get filtrate, and merges extract solution twice and is For extracts of Chinese herbal medicine;
(4)It is concentrated under reduced pressure:By step(3)The extracts of Chinese herbal medicine of gained enters at 68 DEG C of temperature under the MPa of vacuum -0.08 Row is evaporated under reduced pressure, and is reclaimed the ethanol in extracts of Chinese herbal medicine to without alcohol taste, is obtained removing ethanol extracts of Chinese herbal medicine;
(5)Filtering:By step(4)Gained extracts of Chinese herbal medicine, impurity and insoluble matter therein are filtered to remove through diatom filter Produce cure scapulohumeral periarthritis rhizoma atractylodis dip.
The composition and ratio of each embodiment herbal raw material of table 1.
Sequence number Component Embodiment 1 Embodiment 2 Embodiment 3
1 Rhizoma atractylodis(Part) 23 26 29
2 Folium artemisiae argyi(Part) 18 15 13
3 Turpentine(Part) 21 23 19
4 Impatientis(Part) 14 13 11
5 Notopterygium root(Part) 6 8 10
6 Ramulus mori(Part) 19 17 15
7 Vomiting nut(Part) 8 9 5
8 Lycopodium calvatum(Part) 13 12 11
9 Lopseed(Part) 14 11 13
10 The root of Chinese clematis(Part) 13 14 11
11 Reticulate millettia(Part) 11 13 15
12 Ligusticum wallichii(Part) 6 8 10
13 Summation(Part) 166 169 162
Although to reach illustration purpose, described above is the preferred embodiments of the present invention, is not intended to limit the invention, to the greatest extent The present invention is described in detail with reference to the foregoing embodiments for pipe, and for those skilled in the art, it still can be with The technical scheme recorded to foregoing embodiments is modified, or carries out equivalent substitution to which part technical characteristic.It is all Within the spirit and principles in the present invention, any modification, equivalent substitution and improvements made etc., the protection of the present invention should be included in Within the scope of.

Claims (2)

1. a kind of cure scapulohumeral periarthritis rhizoma atractylodis dip, it is characterised in that be made up of the herbal raw material of following parts by weight:Rhizoma atractylodis 20 ~30 parts, 10~20 parts of folium artemisiae argyi, 15~25 parts of turpentine, 10~15 parts of Impatientis, 5~10 parts of notopterygium root, 15~20 parts of ramulus mori, Strychnos nux-vomica 5~10 parts of son, 10~15 parts of lycopodium calvatum, 10~15 parts of lopseed, 9~16 parts of the root of Chinese clematis, 10~15 parts of reticulate millettia and Ligusticum wallichii 5~ 10 parts.
2. a kind of preparation method of cure scapulohumeral periarthritis rhizoma atractylodis dip as claimed in claim 1, it is characterised in that including following Step:
(1)Stock:The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion;
(2)Feedstock treating:Herbal raw material is cleaned up, at 70~90 DEG C, after air blast drying, pulverizer crushes, and crosses 50 ~100 mesh sieves, mix, obtain composite Chinese herbal raw material;
(3)Ultrasonic adverse current is extracted:By step(2)Gained composite Chinese herbal raw material, 4~6 times of 50~60% ethanol are added, are put into In ultrasonic continuous countercurrent extractor, under the effect of 600 ~ 1000 W ultrasonic assistants, after adverse current extracts 30 ~ 45 min, excessively 120 ~ 180 mesh filter clothes obtain water extract;Filter residue adds 2 ~ 4 times of 50~60% ethanol, carries out ultrasonic continuous countercurrent extraction in the same way, Filter to get filtrate, it is extracts of Chinese herbal medicine to merge extract solution twice;
(4)It is concentrated under reduced pressure:By step(3)The extracts of Chinese herbal medicine of gained at 60~70 DEG C of temperature, vacuum -0.06~- It is evaporated under reduced pressure under 0.085 MPa, reclaims the ethanol in extracts of Chinese herbal medicine to without alcohol taste, obtain removal ethanol Chinese herbal medicine and carry Take liquid;
(5)Filtering:By step(4)Gained extracts of Chinese herbal medicine, impurity and insoluble matter therein are filtered to remove through diatom filter Produce cure scapulohumeral periarthritis rhizoma atractylodis dip.
CN201710727788.XA 2017-08-23 2017-08-23 A kind of cure scapulohumeral periarthritis rhizoma atractylodis dip and preparation method thereof Pending CN107617003A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108837056A (en) * 2018-07-27 2018-11-20 山东今古医疗科技有限公司 For treating the nano traditional Chinese medicine liposome aqueogel and preparation method of skeletal joint disease
CN110025675A (en) * 2019-03-29 2019-07-19 陕西盘龙药业集团股份有限公司 A kind of swelling and pain relieving Traditional Chinese medicinal spray and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108837056A (en) * 2018-07-27 2018-11-20 山东今古医疗科技有限公司 For treating the nano traditional Chinese medicine liposome aqueogel and preparation method of skeletal joint disease
CN110025675A (en) * 2019-03-29 2019-07-19 陕西盘龙药业集团股份有限公司 A kind of swelling and pain relieving Traditional Chinese medicinal spray and preparation method thereof
CN110025675B (en) * 2019-03-29 2021-08-10 陕西盘龙药业集团股份有限公司 Traditional Chinese medicine spray for relieving swelling and pain and preparation method thereof

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