CN107550761A - A kind of make-up remover containing chitosan and preparation method thereof - Google Patents
A kind of make-up remover containing chitosan and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of make-up remover containing chitosan and preparation method thereof, the make-up remover by weight percentage, including following material component：Vegetable oil 15% 40%, polyalcohol 5% 20%, chitosan 5% 10%, isopropyl palmitate 10% 20%, solid state wax 2% 10%, polyethylene glycol 2% 8%, preservative 0.05% 0.1%, essence 0.1% 0.3%, water surplus, wherein, polyethylene glycol is not included in the polyalcohol.The invention further particularly discloses a kind of preparation method of the make-up remover containing chitosan simultaneously.The make-up remover containing chitosan as made from such scheme is the compounding mixture being process by various raw materials by rational allocation, its have it is easy to use, be not easy to drip, moisturizing, moisturizing, maintenance, remove blackhead, remove cutin, purify all multiactions such as pore, the metal of absorption residual color make-up.
Description
Technical field
The invention belongs to daily cosmetic field, specifically, is related to a kind of make-up remover containing chitosan and its preparation
Method.
Background technology
With the continuous progress of make-up technique, cosmetics become more and more important in the status of today's society, people for
The requirement of cosmetics also more and more higher.And remove ornaments and formal dress be after making up, a step essential before face cleaning, the pole not in place of removing ornaments and formal dress holds
The skin problems such as easy appearance length is remained silent, small pox.
In market of today, common makeup removing class product has makeup remover and makeup remover.Chinese patent application
(CN105616315A) a kind of makeup remover is disclosed, its component is：Cucumber 15%-20%, aloe 10%-15%, egg
10%-15%, alcohol 10%-15%, glycerine 8%-10%, tomato 8%-10%, Chinese leaf 8%-10%, olive oil
8%-10%.Makeup remover can either cleaning skin, the makeup remover of the enough skin cares of and can is adapted to that face skin is coarse, pore is thick
Greatly, the crowd of complexion yellowing, but the fat content in makeup remover is seldom, facial color make-up is not completely soluble in makeup remover, easily
There is halfway situation of removing ornaments and formal dress, cause skin various problems occur.Chinese patent application (CN201310398425.8) is open
A kind of makeup remover, quality composition are as follows：Vegetable oil 30%-50%, ethylhexyl palmitate the 25%-45%, (ethyl of glycerine three
Caproic acid) ester 5%-10%, emulsifying agent 5%-10%, C15-19 alkane 5%-10%, other 1%-4%.Makeup remover can be completely molten
Color make-up is solved, makes makeup removing thorough, but makeup remover has a mobility, easy sliding drippage during makeup removing, cause inconvenience.
In view of this, it is that those skilled in the art need solve to research and develop a kind of makeup removing class product thorough, easy to use of removing ornaments and formal dress
A problem certainly.
The content of the invention
The present invention is according to above-mentioned technical background, there is provided a kind of make-up remover containing chitosan and preparation method thereof, this is unloaded
Adornment cream not only has and can thoroughly remove the color make-up of residual, action effect easy to use, while also has and remove cutin, purification
Pore etc. acts on.
To solve the above problems, the technical solution adopted in the present invention is：
A kind of make-up remover containing chitosan, by weight percentage, including following material component：Vegetable oil 15%-
40%, polyalcohol 5%-20%, chitosan 5%-10%, isopropyl palmitate 10%-20%, solid state wax 2%-10%, poly- second
Glycol 2%-8%, preservative 0.05%-0.1%, essence 0.1%-0.3%, water surplus, wherein, do not include in the polyalcohol
Polyethylene glycol.
Further, on the basis of above-mentioned technical proposal, the present invention can also do following improvement：
Preferably, a kind of make-up remover containing chitosan, by weight percentage, including following material component：Vegetable oil
20%, polyalcohol 10%, chitosan 7%, isopropyl palmitate 12%, solid state wax 5%, polyethylene glycol 4%, preservative
0.06%, essence 0.1%, water 41.84%.
Preferably, a kind of make-up remover containing chitosan, by weight percentage, including following material component：Vegetable oil
30%, polyalcohol 15%, chitosan 9%, isopropyl palmitate 16%, solid state wax 8%, polyethylene glycol 6%, preservative
0.08%, essence 0.2%, water 15.72%.
Further, heretofore described vegetable oil is by jojoba oil and olive oil by weight 1:1 composition.
Specifically, the composition in jojoba oil includes the mineral such as vitamin E, vitamin C, cetanol, protein, magnesium, calcium
Matter, it has an excellent dissolving blackhead, removes blackhead, purifies the effect of pore, can be with addition, jojoba oil moistness is very high
The careful skin of moisturizing, and cetanol composition therein has good antiphlogistic effects.The factor is moistened containing natural in olive oil,
Can effectively moisturizing skin, and olive oil has stickiness very much, be coated in the loss that skin moisture can be prevented on skin, cleaning face
After reuse olive oil and can effectively nourish skin.Jojoba oil and olive oil cosmetic field all based on oil use,
The present invention is by the two by weight 1:Skin cell aquaporin can be opened after 1 compounding use rapidly, discharge powerful moisturizing, moisten,
Maintenance effect, and have significantly more effect to removing blackhead, purifying pore.
Further, heretofore described chitosan is Chitosan powder, chitosan have excellent biocompatibility and
Film forming, and non-stimulated nontoxic to skin, is applied in the present invention, can make the present invention have good moisture absorption, moisturizing,
Conditioning, the function such as antibacterial, play antiallergic sense to skin and anti-inflammatory produce, it is quick repair substrate fire damage, quick healing of wound,
Repair epidermal barrier, remove cutin, purify the effect such as pore, the metal of absorption residual color make-up.
Further, heretofore described polyalcohol is the one or more in glycerine, butanediol, propane diols, sorbierite.
Wherein, glycerine has very strong hygroscopicity, and the moisture that can be allowed on skin will not distribute very much soon, while can also be appropriate
Aqueous vapor is drawn from air；Butanediol has excellent performance of keeping humidity, good bacteriostasis；Propane diols performance of keeping humidity is gentle,
Clearly, sticky sense is low, and moisture-keeping function is excellent with using effect, and security is good, nonirritant and sensitization；Sorbierite has very
The moisture-keeping function of mitigation, and moisture retention can be also played during low temperature, good frost resistance, the cold-resistant stability of product can be improved, in addition
Sorbierite is to skin without any stimulation.Polyalcohol is set as in glycerine, butanediol, propane diols, sorbierite by the present invention
One or more, the water content of keratoderma can be significantly improved after makeup removing, increase skin elasticity, make skin health fine and smooth
It is dynamic, while can also prevent skin damage and promote damaged skin reparation.
Further, heretofore described solid state wax is by beeswax and Brazil wax by weight 1:1 composition.
Wherein, beeswax is a kind of thickener, stabilizer and film forming agent, and cosmetics can be made more soft and smooth, gentle, plays protection
With the effect for preventing dehydration, while beeswax has very strong tolerance to temperature, is not easy to be influenceed by natural temperature, can make preparation
Cosmetics keep application state, be applied on skin also can stablize play a role；Brazil wax has high gloss, easily
Emulsification, has good Oil keeping, is mainly used as curing agent in the present invention, can increase the stability of cosmetics, and it is viscous to adjust it
Denseness, soft effect is produced during use to skin.The present invention is by solid state wax by beeswax and Brazil wax by weight 1:1 is multiple
With use, the fusing point of make-up remover can be not only improved, also imparts the high glossiness of make-up remover and heat-resistant stability, and it is also
Easily mixed with other dispensings in the present invention such as vegetable oil, isopropyl palmitate etc., reach steady quality, the work that can be deposited for a long time
Use effect.
Further, heretofore described preservative is by nipagin esters and imidazolidinyl urea by weight 1:95 compositions.
Wherein, parabens preservative can broad-spectrum antiseptic, stability is strong, under acid and alkaline case can antibacterial,
Gram-positive and negative bacterium are effective against under high temperature and low temperature, but work can be irritating to the skin if a large amount of uses
With；Imidazolidinyl urea is a most popular kind in formaldehyde donor class preservative, and it has activity well, to golden yellow
The action effect of the bacteriums such as color staphylococcus, Escherichia coli is fine, and can be with all component interworkings in cosmetics.In view of preservative
Excessively can have certain injury to skin, thus the present invention strictly by the percentage by weight of preservative be limited to standard metering it
It is interior and of the invention by preservative nipagin esters and imidazolidinyl urea by weight 1:95 carry out compounding use, are greatly improved
The antiseptic property of make-up remover finished product, the breeding of the microorganism after pollution is killed or suppresses, playing prevents that cosmetics are putrid and deteriorated
Effect, it is ensured that avoid make-up remover from being caused infection by microorganism pollution when in use.
Further, heretofore described essence is lemon extract or Mint Essence.Essence can cover raw material smell,
Assign the pleasurable sensation in terms of product sensory.
The present invention also provides a kind of preparation method of the make-up remover containing chitosan, comprises the following steps：
(1) deionized water of formula ratio, polyalcohol, polyethylene glycol, is taken to add in kettle and be stirred, after stirring again
Progress homogenous disperse emulsification under normal temperature is added into high cut disperse emulsification pot, by emulsification pot after material mixed stability
Temperature rises to 60 DEG C of -80 DEG C of holding 10-15min, obtains solution one；
(2) vegetable oil, solid state wax, isopropyl palmitate, are added into oil cauldron according to formula ratio, then by the temperature in oil cauldron
Degree rises to 70 DEG C -90 DEG C, and stirring is until uniformly, obtain solution two；
(3) temperature residing for solution two in oil cauldron, is down to 50 DEG C -55 DEG C, chitosan, anti-corrosion are added according to formula ratio
Agent, essence, then proceed to stir and gradually cool the temperature to normal temperature, it is to be mixed uniformly after obtain solution three；
(4), mixed in the emulsification pot for adding solution three in step (1) with solution one, continue stirring until material
It is completely dissolved；
(5) after the material in step (4) in emulsification pot, is carried out into deaeration processing, then it is transferred into final packaging, makes
Its natural cooling, obtains make-up remover.
The present invention is the compounding mixture being process by various raw materials by rational allocation, vegetable oil therein and palm
Isopropyl propionate is all grease, and vegetable oil uses as base starting material in the present invention, therefore occupies larger specific gravity, and it can make skin soft
It is soft, lubrication and surface cleaning, friction effect is played on a skin surface, while hydrophobic film is formed, play protection skin, and
External harmful substance invasion and attack can be prevented；Isopropyl palmitate uses as oil carrier, essence solubilizer in the present invention,
And its energy moisturizing, help to eliminate drying, and allow skin to become soft high resilience.In other inventive formulation except with the addition of by
The polyalcohols of one or more compositions in glycerine, butanediol, propane diols, sorbierite reach the action effect of moisturizing moisturizing
Outside, this polyalcohol of polyethylene glycol is also added, polyethylene glycol, which removes, in the present invention has the function that humectant and skin-friendly
Outside effect, it is also act as matrix, plays a part of to adjust the viscosity and fusing point of make-up remover, while it also reduces whole in make-up remover
The excitant of body matrix.
Beneficial effect of the present invention：Present invention employs above-mentioned raw materials and preparation method, removes obtained make-up remover and is provided with
It is easy to use, be not easy to drip, moisturizing, moisturizing, maintenance effect outside, be also provided with dissolving blackhead, remove the effect of blackhead, and
This raw material of chitosan is carried out compounding with other raw materials and mixed by the present invention, obtained make-up remover is also provided with removal cutin,
Purify pore, the effect of the metal of absorption residual color make-up, the defects of overcoming traditional makeup remover and makeup remover.
Embodiment
The principle and feature of the present invention are described with reference to specific embodiment, wherein, illustrated embodiment is served only for
The present invention is explained, is not intended to limit the scope of the present invention.
Embodiment 1：
A kind of make-up remover containing chitosan, including following material component：Vegetable oil 15g, polyalcohol 5g, chitosan 5g,
Isopropyl palmitate 20g, solid state wax 2g, polyethylene glycol 8g, preservative 0.1g, essence 0.1g, water 44.8g.Wherein, the plant
Oil is jojoba oil and olive oil, and the two shared weight ratio is 1:1；The polyalcohol is the mixture of glycerine and butanediol；Institute
It is beeswax and Brazil wax to state solid state wax, and the two shared weight ratio is 1:1；The preservative is nipagin esters and imidazolidinyl
Urea, the two shared weight ratio are 1:95；The chitosan is Chitosan powder；The essence is lemon extract.
A kind of preparation method of above-mentioned make-up remover containing chitosan, comprises the following steps：
(1) deionized water of formula ratio, polyalcohol, polyethylene glycol, is taken to add in kettle and be stirred, after stirring again
Progress homogenous disperse emulsification under normal temperature is added into high cut disperse emulsification pot, by emulsification pot after material mixed stability
Temperature rises to 60 DEG C of -80 DEG C of holding 10min, obtains solution one；
(2) vegetable oil, solid state wax, isopropyl palmitate, are added into oil cauldron according to formula ratio, then by the temperature in oil cauldron
Degree rises to 70 DEG C -90 DEG C, and stirring is until uniformly, obtain solution two；
(3) temperature residing for solution two in oil cauldron, is down to 50 DEG C -55 DEG C, chitosan, anti-corrosion are added according to formula ratio
Agent, essence, then proceed to stir and gradually cool the temperature to normal temperature, it is to be mixed uniformly after obtain solution three；
(4), mixed in the emulsification pot for adding solution three in step (1) with solution one, continue stirring until material
It is completely dissolved；
(5) after the material in step (4) in emulsification pot, is carried out into deaeration processing, then it is transferred into final packaging, makes
Its natural cooling, obtains make-up remover.
Embodiment 2：
A kind of make-up remover containing chitosan, including following material component：Vegetable oil 20g, polyalcohol 8g, chitosan 6g,
Isopropyl palmitate 18g, solid state wax 4g, polyethylene glycol 7g, preservative 0.06g, essence 0.2g, water 36.74g.Wherein, the plant
Thing oil is jojoba oil and olive oil, and the two shared weight ratio is 1:1；The polyalcohol is the mixture of glycerine and propane diols；
The solid state wax is beeswax and Brazil wax, and the two shared weight ratio is 1:1；The preservative is nipagin esters and imidazolidine
Base urea, the two shared weight ratio are 1:95；The chitosan is Chitosan powder；The essence is lemon extract.
A kind of preparation method of above-mentioned make-up remover containing chitosan, comprises the following steps：
(1) deionized water of formula ratio, polyalcohol, polyethylene glycol, is taken to add in kettle and be stirred, after stirring again
Progress homogenous disperse emulsification under normal temperature is added into high cut disperse emulsification pot, by emulsification pot after material mixed stability
Temperature rises to 60 DEG C of -80 DEG C of holding 11min, obtains solution one；
(2) vegetable oil, solid state wax, isopropyl palmitate, are added into oil cauldron according to formula ratio, then by the temperature in oil cauldron
Degree rises to 70 DEG C -90 DEG C, and stirring is until uniformly, obtain solution two；
(3) temperature residing for solution two in oil cauldron, is down to 50 DEG C -55 DEG C, chitosan, anti-corrosion are added according to formula ratio
Agent, essence, then proceed to stir and gradually cool the temperature to normal temperature, it is to be mixed uniformly after obtain solution three；
(4), mixed in the emulsification pot for adding solution three in step (1) with solution one, continue stirring until material
It is completely dissolved；
(5) after the material in step (4) in emulsification pot, is carried out into deaeration processing, then it is transferred into final packaging, makes
Its natural cooling, obtains make-up remover.
Embodiment 3：
A kind of make-up remover containing chitosan, including following material component：Vegetable oil 30g, polyalcohol 15g, chitosan 8g,
Isopropyl palmitate 16g, solid state wax 6g, polyethylene glycol 5g, preservative 0.08g, essence 0.3g, water 19.62g.Wherein, the plant
Thing oil is jojoba oil and olive oil, and the two shared weight ratio is 1:1；The polyalcohol is the mixing of butanediol and propane diols
Thing；The solid state wax is beeswax and Brazil wax, and the two shared weight ratio is 1:1；The preservative is nipagin esters and miaow
Oxazolidinyl urea, the two shared weight ratio are 1:95；The chitosan is Chitosan powder；The essence is Mint Essence.
A kind of preparation method of above-mentioned make-up remover containing chitosan, comprises the following steps：
(1) deionized water of formula ratio, polyalcohol, polyethylene glycol, is taken to add in kettle and be stirred, after stirring again
Progress homogenous disperse emulsification under normal temperature is added into high cut disperse emulsification pot, by emulsification pot after material mixed stability
Temperature rises to 60 DEG C of -80 DEG C of holding 12min, obtains solution one；
(2) vegetable oil, solid state wax, isopropyl palmitate, are added into oil cauldron according to formula ratio, then by the temperature in oil cauldron
Degree rises to 70 DEG C -90 DEG C, and stirring is until uniformly, obtain solution two；
(3) temperature residing for solution two in oil cauldron, is down to 50 DEG C -55 DEG C, chitosan, anti-corrosion are added according to formula ratio
Agent, essence, then proceed to stir and gradually cool the temperature to normal temperature, it is to be mixed uniformly after obtain solution three；
(4), mixed in the emulsification pot for adding solution three in step (1) with solution one, continue stirring until material
It is completely dissolved；
(5) after the material in step (4) in emulsification pot, is carried out into deaeration processing, then it is transferred into final packaging, makes
Its natural cooling, obtains make-up remover.
Embodiment 4：
A kind of make-up remover containing chitosan, including following material component：Vegetable oil 35g, polyalcohol 18g, chitosan 9g,
Isopropyl palmitate 14g, solid state wax 8g, polyethylene glycol 3g, preservative 0.09g, essence 0.1g, water 12.81g.Wherein, the plant
Thing oil is jojoba oil and olive oil, and the two shared weight ratio is 1:1；The polyalcohol is glycerine, propane diols and sorbierite
Mixture；The solid state wax is beeswax and Brazil wax, and the two shared weight ratio is 1:1；The preservative is nipagin esters
And imidazolidinyl urea, the two shared weight ratio are 1:95；The chitosan is Chitosan powder；The essence is Mint Essence.
A kind of preparation method of above-mentioned make-up remover containing chitosan, comprises the following steps：
(1) deionized water of formula ratio, polyalcohol, polyethylene glycol, is taken to add in kettle and be stirred, after stirring again
Progress homogenous disperse emulsification under normal temperature is added into high cut disperse emulsification pot, by emulsification pot after material mixed stability
Temperature rises to 60 DEG C of -80 DEG C of holding 14min, obtains solution one；
(2) vegetable oil, solid state wax, isopropyl palmitate, are added into oil cauldron according to formula ratio, then by the temperature in oil cauldron
Degree rises to 70 DEG C -90 DEG C, and stirring is until uniformly, obtain solution two；
(3) temperature residing for solution two in oil cauldron, is down to 50 DEG C -55 DEG C, chitosan, anti-corrosion are added according to formula ratio
Agent, essence, then proceed to stir and gradually cool the temperature to normal temperature, it is to be mixed uniformly after obtain solution three；
(4), mixed in the emulsification pot for adding solution three in step (1) with solution one, continue stirring until material
It is completely dissolved；
(5) after the material in step (4) in emulsification pot, is carried out into deaeration processing, then it is transferred into final packaging, makes
Its natural cooling, obtains make-up remover.
Embodiment 5：
A kind of make-up remover containing chitosan, including following material component：Vegetable oil 40g, polyalcohol 20g, chitosan
10g, isopropyl palmitate 10g, solid state wax 10g, polyethylene glycol 2g, preservative 0.05g, essence 0.2g, water 7.75g.Wherein, institute
It is jojoba oil and olive oil to state vegetable oil, and the two shared weight ratio is 1:1；The polyalcohol is glycerine, butanediol, propane diols
With the mixture of sorbierite；The solid state wax is beeswax and Brazil wax, and the two shared weight ratio is 1:1；The preservative
For nipagin esters and imidazolidinyl urea, the two shared weight ratio is 1:95；The chitosan is Chitosan powder；The essence is
Mint Essence.
A kind of preparation method of above-mentioned make-up remover containing chitosan, comprises the following steps：
(1) deionized water of formula ratio, polyalcohol, polyethylene glycol, is taken to add in kettle and be stirred, after stirring again
Progress homogenous disperse emulsification under normal temperature is added into high cut disperse emulsification pot, by emulsification pot after material mixed stability
Temperature rises to 60 DEG C of -80 DEG C of holding 15min, obtains solution one；
(2) vegetable oil, solid state wax, isopropyl palmitate, are added into oil cauldron according to formula ratio, then by the temperature in oil cauldron
Degree rises to 70 DEG C -90 DEG C, and stirring is until uniformly, obtain solution two；
(3) temperature residing for solution two in oil cauldron, is down to 50 DEG C -55 DEG C, chitosan, anti-corrosion are added according to formula ratio
Agent, essence, then proceed to stir and gradually cool the temperature to normal temperature, it is to be mixed uniformly after obtain solution three；
(4), mixed in the emulsification pot for adding solution three in step (1) with solution one, continue stirring until material
It is completely dissolved；
(5) after the material in step (4) in emulsification pot, is carried out into deaeration processing, then it is transferred into final packaging, makes
Its natural cooling, obtains make-up remover.
It is below the physical and chemical testing carried out to a kind of make-up remover containing chitosan in embodiment 1-5, its test result
It is as follows：
1. outward appearance：Translucent lotion
2. hardness：It is neither too hard, nor too soft
2.pH values：5.5-6.5
3. heat-resistant stability investigates (48 DEG C × 24h):It is qualified
4. cold-resistant study on the stability (- 15 DEG C × 24h):It is qualified.
Meanwhile in order to prove the security of product of the present invention and effect, tests below is carried out：
First, security test：
1st, microorganism pollution is tested
Microorganism testing is according to European Pharmacopoeia/British Pharmacopoeia/American Pharmacopeia/European Union's cosmetic product and fragrance association guideization
Cosmetic and fragrance association method are carried out.The microbiological indicator of assessment mainly includes：Total number of bacteria, mould and yeast, Pseudomonas aeruginosa,
Staphylococcus aureus, Escherichia coli, salmonella, Candida albicans, clostridium, Enterobacter and Gram-negative
Bacterium and bile tolerant Gram-negative bacteria.
Test result：After testing, the microbiological indicator qualification rate of the make-up remover in embodiment 1-5 is 99.9%.
2nd, the validity test of preservative
The present invention is assessed the stability and preservative efficacy of microorganism, by being prepared to being inoculated with embodiment 1-5
Object bacteria, the change of its micro organism quantity is observed in different times, so that it is determined that whether preservative reaches regulation anti-corrosive antibacterial
Effect.The methods of this test Main Basiss EP (5.1.3)/BP (Appx.XVI C)/USP (51)/COLIPA or CTFA, is carried out.
The object bacteria of inoculation typically has following 5 kinds：Pseudomonas aeruginosa, staphylococcus aureus, Escherichia coli, black-koji mould and Candida albicans
Bacterium.
The time-program(me) of sampling and testing is 0,3,5 and 7 day after inoculation, and the result of sampling is shown, embodiment in the present invention
Make-up remover in 1-5 was at the 7th day, bacterium or mould therein<10cfu/g (ml), illustrate the protective system of the present invention to micro-
Biology has an inhibitory or killing effect of extra-heavy, product production, storage and using when be not easy very much microbial contamination.
2nd, efficacy test：
Comparative example：Common make-up remover, formula are as follows：
Preparation method is：
Mineral oil, cetearyl octanoate, PEG-20 stearins, PEG-10 isostearates are claimed in proportion
It is good, sequentially add in order in agitated kettle, heat to 85 DEG C -90 DEG C, be incubated 10-20 minutes, stirring and dissolving is well mixed,
Then 30 DEG C~31 DEG C are cooled to, adds butanediol, is stirred 5 minutes.
Specific test is as follows：
Test crowd：20~30 years old female volunteers often made up
Test number：60 people
Method of testing：10 people are that a component is 5 test groups and 1 control group, and test group and control group are using identical
Color make-up carry out same face cosmetic, then 5 test groups are carried out using the make-up remover in embodiment 1-5 in the present invention respectively
Makeup removing, 1 control group are removed ornaments and formal dress using the common make-up remover in comparative example, and it is one month to continue usage time.
1st, makeup removing effect
Judgment criteria is：
Very well：Rear face remove ornaments and formal dress without any residual color make-up thing；
It is good：The remaining a small amount of color make-up thing of rear face of removing ornaments and formal dress but performance unobvious；
Typically：Makeup removing rear face nubbin color make-up thing and have a little obvious；
Difference：The obvious remaining a large amount of color make-up things of rear face of removing ornaments and formal dress；
Evaluation result is shown in Table 1
Table 1
It can be apparent from that the color make-up residue of make-up remover of the present invention is substantially fewer than comparative example, and clean power is bright by above-mentioned table 1
It is aobvious higher than comparative example.
2nd, skin is comfortable, glossy effect
Judgment criteria is：
Very well：Removing ornaments and formal dress, rear face is clearly comfortable, and skin is smooth, water profit；
It is good：Removing ornaments and formal dress, rear face is clearly comfortable, and skin surface slightly shows coarse；
Typically：Removing ornaments and formal dress, rear face is dry and astringent, greasy, and skin surface is coarse；
Difference：Rear face of removing ornaments and formal dress is dry and astringent, greasy, coarse, skin problem easily occurs；
Evaluation result is shown in Table 2
Table 2
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Comparative example | |
| Very well | 10 | 9 | 8 | 9 | 8 | 4 |
| It is good | Nothing | 1 | 2 | 1 | 2 | 4 |
| Typically | Nothing | Nothing | Nothing | Nothing | Nothing | 1 |
| Difference | Nothing | Nothing | Nothing | Nothing | Nothing | 1 |
By above-mentioned table 2 can be apparent from the comfortable height of skin of make-up remover of the present invention, glossy effect is good, moisture retention is strong.
3rd, pore cleanser, purification pore effect
Judgment criteria is：
Effectively：Facial blackhead is wholly absent, and pore shrinks obvious；
Typically：Facial blackhead largely disappears, and pore has slight diminution；
It is poor：Facial blackhead is obvious, and pore is thick obvious；
Evaluation result is shown in Table 3
Table 3
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Comparative example | |
| Effectively | 10 | 9 | 10 | 8 | 9 | 2 |
| Typically | Nothing | 1 | Nothing | 2 | 1 | 5 |
| It is poor | Nothing | Nothing | Nothing | Nothing | Nothing | 3 |
Can be apparent from make-up remover of the present invention by above-mentioned table 3 has obvious pore cleanser compared to comparative example, shrinks hair
Hole effect.
In addition, the present invention determines the proportion between each raw material after substantial amounts of experimental verification, such as vegetable oil ratio
Scope is 15%-40%, and the proportion of solid state wax is solid state wax 2%-10%, because, applicants experimentally found that,
When the too high levels of vegetable oil and solid state wax (be higher than total content 50%), the fusing point of the make-up remover can be too high, causes human body
Temperature can not make its thawing, cause use feeling to decline；And when the content of vegetable oil and solid state wax is very few (less than total content
20%) when, the makeup removing ability of make-up remover can significantly decline again.Therefore the species ratio of the invention by rationally limiting oily wax,
Strictly the fusing point of make-up remover is controlled between 30-40 degrees Celsius, make that it is presented in packaging is solid-like, when contact skin
During skin, it can rapidly melt again under the massage of hand and spread out, while the moisture that unhydrated polyalcohol contact skin is a small amount of, produce one
Fixed heat, opens skin pore, more profound cleaning skin and pore dirt, while effectively nourishes skin, improves
Skin water content, reach and remove blackhead, remove the action effects such as cutin, purification pore.
The above embodiments are merely illustrative of the technical scheme of the present invention and are not intended to be limiting thereof；The present invention is not limited to above-mentioned
Preferred embodiment, anyone should learn that the modification made under the enlightenment of the present invention or some technical characteristics are carried out etc.
With replace, it is every with it is of the invention have it is same or similar as technical scheme, belong to protection scope of the present invention.
Claims (10)
- A kind of 1. make-up remover containing chitosan, it is characterised in that by weight percentage, including following material component：Wherein, polyethylene glycol is not included in the polyalcohol.
- A kind of 2. make-up remover containing chitosan according to claim 1, it is characterised in that by weight percentage, bag Include following material component：
- A kind of 3. make-up remover containing chitosan according to claim 1, it is characterised in that by weight percentage, bag Include following material component：
- 4. a kind of make-up remover containing chitosan according to claim 1, it is characterised in that the vegetable oil is by Jojoba Oil and olive oil are by weight 1:1 composition.
- 5. a kind of make-up remover containing chitosan according to claim 1, it is characterised in that the chitosan is chitosan Powder.
- A kind of 6. make-up remover containing chitosan according to claim 1, it is characterised in that the polyalcohol be glycerine, One or more in butanediol, propane diols, sorbierite.
- A kind of 7. make-up remover containing chitosan according to claim 1, it is characterised in that the solid state wax by beeswax and Brazil wax is by weight 1:1 composition.
- 8. a kind of make-up remover containing chitosan according to claim 1, it is characterised in that the preservative is by nipalgin Ester and imidazolidinyl urea are by weight 1:95 compositions.
- 9. a kind of make-up remover containing chitosan according to claim 1, it is characterised in that the essence is lemon extract Or Mint Essence.
- 10. a kind of preparation method of the make-up remover containing chitosan, it is characterised in that comprise the following steps：(1) deionized water, polynary of formula ratio, is weighed according to the make-up remover containing chitosan described in any one of claim 1 to 9 Alcohol, polyethylene glycol are added in kettle and are stirred, and are added into high cut disperse emulsification pot to enter under normal temperature again after stirring Row homogenous disperse is emulsified, and the temperature emulsified in pot is risen into 60 DEG C of -80 DEG C of holding 10-15min after material mixed stability, obtained Solution one；(2) vegetable oil, solid state wax, isopropyl palmitate, are added into oil cauldron according to formula ratio, then by the temperature liter in oil cauldron To 70 DEG C -90 DEG C, stirring is until uniformly, obtain solution two；(3) temperature residing for solution two in oil cauldron, is down to 50 DEG C -55 DEG C, chitosan, preservative, perfume (or spice) are added according to formula ratio Essence, then proceed to stir and gradually cool the temperature to normal temperature, it is to be mixed uniformly after obtain solution three；(4), mixed in the emulsification pot for adding solution three in step (1) with solution one, continue stirring until material is complete Dissolving；(5) after the material in step (4) in emulsification pot, is carried out into deaeration processing, then it is transferred into final packaging, makes it certainly So cooling, obtains make-up remover.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710896780.6A CN107550761A (en) | 2017-09-28 | 2017-09-28 | A kind of make-up remover containing chitosan and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710896780.6A CN107550761A (en) | 2017-09-28 | 2017-09-28 | A kind of make-up remover containing chitosan and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108888574A (en) * | 2018-08-08 | 2018-11-27 | 东莞市白天鹅纸业有限公司 | A kind of paper handkerchief make up remover and preparation method thereof |
| CN108926505A (en) * | 2018-08-17 | 2018-12-04 | 卢莺莺 | A kind of exfoliating skin care scrub cream and preparation method thereof |
| US20220401346A1 (en) * | 2021-06-17 | 2022-12-22 | Mike Jenson Raj | Hair removal admixture with wax, antiseptic, analgesic, moisturizing oil, and chemical depilatory: Hair removal chemical composite/creamy wax. |
-
2017
- 2017-09-28 CN CN201710896780.6A patent/CN107550761A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108888574A (en) * | 2018-08-08 | 2018-11-27 | 东莞市白天鹅纸业有限公司 | A kind of paper handkerchief make up remover and preparation method thereof |
| CN108926505A (en) * | 2018-08-17 | 2018-12-04 | 卢莺莺 | A kind of exfoliating skin care scrub cream and preparation method thereof |
| CN108926505B (en) * | 2018-08-17 | 2021-05-14 | 恒冠湄颜健康产业(广州)有限公司 | Skin-care scrub cream for removing cutin and preparation method thereof |
| US20220401346A1 (en) * | 2021-06-17 | 2022-12-22 | Mike Jenson Raj | Hair removal admixture with wax, antiseptic, analgesic, moisturizing oil, and chemical depilatory: Hair removal chemical composite/creamy wax. |
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Application publication date: 20180109 |