CN107500930A - The method that organic fertilizer is prepared using Momordica grosvenori root tuber - Google Patents
The method that organic fertilizer is prepared using Momordica grosvenori root tuber Download PDFInfo
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- CN107500930A CN107500930A CN201710934179.1A CN201710934179A CN107500930A CN 107500930 A CN107500930 A CN 107500930A CN 201710934179 A CN201710934179 A CN 201710934179A CN 107500930 A CN107500930 A CN 107500930A
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- momordica grosvenori
- residue
- anistree
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/70—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting wettability, e.g. drying agents
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/90—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Soil Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
Abstract
The present invention provides the method that organic fertilizer is prepared using Momordica grosvenori root tuber, and step includes crushing dried fructus momordicae root tuber, rinsed with water, separating coarse starch, aqueous and Momordica grosvenori residue；Aqueous extracts Momordica grosvenori residue and anistree waste residue, filters to obtain filter residue and filtrate；Filter residue carbonizes to obtain activated carbon granule after air-drying；Filtrate adds after potassium dihydrogen phosphate, potassium nitrate and obtains zymotic fluid through fermentation of bacillus subtilis；High temperature is gelatinized after Crude starch adds aqueous, is added acrylic acid, catalyst and crosslinking agent, is reacted to obtain starch gel, then low temperature drying crushes to obtain dry gel particle；Activated carbon granule and dry gel particle are added into zymotic fluid, wind to water content is organic fertilizer below 25%.The present invention uses microbial fermentation, effectively increase the content of organic nitrogen in organic fertilizer, phosphorus, potassium, make full use of cellulose and lignin in Momordica grosvenori and anistree waste residue, it is converted into activated carbon, it is easy to adsorb substantial amounts of organic matter, reach slowly release organic nitrogen, phosphorus, potassium under the influence of gel, turn avoid the loss of nutrient in fertilizer；The vigor of bacillus subtilis is ensure that in whole production process, under conditions of the nutriment and water-keeping gel for having abundance, can continue to keep the propagation of microorganism, to improve the ratio of the beneficial bacterium such as bacillus subtilis in soil.
Description
Technical field
The present invention relates to a kind of method that organic fertilizer is prepared using Momordica grosvenori root tuber, belongs to the technology that fertilizer industry is applied
Field.
Background technology
Momordica grosvenori is the perennial liana of Curcurbitaceae, and the sweet tea glucoside in fruit is 300 times of sucrose, and heat is low, also
Containing fructose, glucose, vitamin C and various trace elements needed by human, protein, there is good healthcare function, mainly
Originate in the ground such as Guangxi, Guangdong, Hunan, Jiangxi.The dry fruit of Momordica grosvenori is oval or circular, shell sepia or smoking color,
It is more bigger than goose egg with a large amount of tiny black pubescences.Dry fruit is lighter, and seed, pericarp and pulp can be used as medicine.The nutrition of Momordica grosvenori
It is worth high, contains substantial amounts of carbohydrate, protein, vitamin, aliphatic acid, a variety of amino acid and trace element needed by human.
In recent years, it is increasing in southern cultivated area.Momordica grosvenori plant growth is vigorous, tendril length, up to 3-10 rice.
Publication No. CN102719485A Introduction To Cn Patent is a kind of to utilize Starch Conversion ethanol in Momordica grosvenori root tuber
Method, step includes：(1) Momordica grosvenori root tuber is eluted with water, cut into slices, rubbed with pulverizer；(2) by Momordica grosvenori
Root tuber and petroleum ether are mixed by a certain percentage, static to place more than 3 hours；(3) upper strata oil ether moiety is removed, adds rice
Aspergillus and root arrhizus fermentation liquid, while add complex cellulase and carry out starch degradation, obtain starch and cellulosic hydrolysate；(4) to
Certain active dry yeast is added in its hydrolyzate, 0.04% dipotassium hydrogen phosphate is added and 0.05% ammonium chloride is sent out
Ferment；(5) after fermentation ends, zymotic fluid is distilled according to conventional method, obtains ethanol finished product.
A kind of method for preparing fertilizer of Publication No. CN101948340A Introduction To Cn Patent, is concretely comprised the following steps：(1)
Raw material presses following percentage by weight dispensing：Grosvener siraitia waste residue 70%~75%, Brewery Wastewater Treatment sludge 5%~12%, ferment
Plain bacterium 0.1%, micro- fertile 10%~14%, phosphate fertilizer 2%~4% and urea 3%~5%；Grosvener siraitia waste residue is crushed to 2.0 centimetres
Below；(2) grosvener siraitia waste residue and ferment bacterium, Brewery Wastewater Treatment sludge, micro- fertilizer, phosphate fertilizer, urea after step (1) is crushed
8~15min is mixed, its moisture content is maintained at 55%~65%, is stacked after mixing by wide 2~3m, high 1.5m or so bar shaped, first
Anaerobic fermentation 2 days, once, continuous turning 5~6 days, temperature control is 5~6 days between 55~75 DEG C for daily turning after the 3rd day；
(3) material that step (2) ferments is dispersed in ground cooling 1~2 day, rear concentrate stacks in heaps, turning again in 10~13 days
Once, and stacking is continued 10~13 days；(4) heap, natural air drying 1 day are dissipated；Or the granulation drying below 60 DEG C；Described arhat
Fruit waste residue squeezes the juice or extracted the waste residue after glucoside for Momordica grosvenori；Described Brewery Wastewater Treatment sludge is beer brewery water processing
The dewatered sludge stood；Described micro- fertilizer is the one or more in boron fertilizer, ca and mg fertilizer, siliceous fertilizer and ferroso-ferric oxide.
A kind of octagonal slag biological fertilizer of Publication No. CN101219912 Introduction To Cn Patent, it is characterised in that：By
Anistree slag, filter mud of sugarcane, paulownia bran, organic materials leavening, microorganism fungus kind composition, it is anistree slag 15~45%, sweet according to weight ratio
Sugarcane filter mud 30~65%, paulownia bran 10~40%, 10~50ml of microorganism fungus kind bacterium solutions/100g, organic materials leavening 1~
10%, wherein leavening living bacteria count >=0.50 hundred million/g.
A kind of special fertilizer for increasing anistree ecosystem fragrance of Publication No. CN104671992A Introduction To Cn Patent, its
It is characterised by the dedicated fertilizer being made up of the following raw material parts by weight for including flavouring derivant：Decomposed peanut press pulp 20~40%,
Ammonium nitrate 20~30%, potassium dihydrogen phosphate 5~10%, potassium sulfate 10~20%, EDTA chelated zincs 1~5%, EDTA chelated coppers 1
~5%, borax 1~5%, flavouring derivant 2~10%；Wherein, described flavouring derivant is by aliphatic hydroxyl acid, rare earth member
Element and surfactant are 1 in mass ratio:0.2~0.5:0.05~0.1 composition.
A kind of anistree plantation dedicated fertilizer of selenium-rich of Publication No. CN106083253A Introduction To Cn Patent, including root
Portion's fertilising, florescence fertilising and young fruit fertilising, root fertilising raw material used is by tealeaves, zymophyte, potassium dihydrogen phosphate, selenium ore deposit
Stone flour is to match as 100-130:3‐5:1‐2:10-30 is prepared, and operating method is as follows：(1) lunar calendar 9-10 months are to tea tree
On leaf be acquired, then cover stacking 15-30 days on the spot, then biofermentation bacterium turned with tealeaves and mixed, continue to cover
Lid fermentation 10-15 days；(2) it is more than 80 mesh selenium mineral dust and fermented tea mixing with fineness, and turns uniformly；(3) will
Potassium dihydrogen phosphate is watered the potassium dihydrogen phosphate to form that concentration is 0.5-1.5%, is then sprinkled into tealeaves heap, spreads biphosphate
It while potassium solution, need to constantly turn, be further continued for covering fermentation 30-50 days, you can obtain root selenium-rich fertilizer；The florescence fertilising
Applied fertilizer with young fruit by following parts by weight of raw materials：1-2 parts manganese sulfate, 10-30 parts urea, 2-5 parts potassium dihydrogen phosphate, 1-5 part selenic acids
Salt and 1000 portions of water mixed preparing solutions.
A kind of fertilizer additive with dual-sustained-release effect of Publication No. CN106083253A Introduction To Cn Patent
Preparation method, including following steps：(1) by 40~60min of plant source raw mill into uniform slurry, ultrasonication
Slurries are made, by material-water ratio 1:2~3 add distilled water diluting, and the water of extract solution must be rich in using 2~3h of vapor refluxing extraction
Solution；(2) by medical stone be put into pyrolysis oven carry out high-temperature closed heat treatment, 900~110 DEG C, after the completion of rapid hardening, treat stone
Surface crushed 120~160 mesh sieves after being overflowed there is no bubble, mix flyash and activated carbon composition mixing powder is standby；(3)
Mixing triazolone, urease inhibitor and other following residual components being not directed to, add into the aqueous solution described in (1), stir
Dissolving, the mixing powder described in (2) is then added while stirring and is adsorbed, 30~40min of process；(4) finally starch is added
Enter into the mixed liquor described in (3), 75~85 DEG C of stirrings that heated up under water bath condition are cooled to after room temperature and added successively to starch gelatinization
Enter acrylic acid and N, N'- methylene-bisacrylamides, 5~10min of stirring reacts 1.5~2h in 60~70 DEG C of water-baths, completed
Dried afterwards at 70~80 DEG C, be finally ground into pulvis.
In summary, the utilization rate of Momordica grosvenori root tuber is low at present, does not make full use of much starch in Momordica grosvenori root tuber
And cellulose substances, a large amount of waste water can be produced during starch is prepared, made starch contains a small amount of cucurbitacin in addition, slightly
Bitter, also cellulose is not also utilized in Momordica grosvenori root tuber.
The content of the invention
It is an object of the invention to overcome the deficiency of prior art and a kind of rational technology is provided, simple to operate, technique is all
The high production technique for fertilizer of the content of phase short, effective N P and K.
Therefore, the present invention provides the method that organic fertilizer is prepared using Momordica grosvenori root tuber, and specific steps include as follows：
(1) take dried fructus momordicae root tuber to crush, rinsed with the water of twice to four times of weight, collect water lotion and Momordica grosvenori is residual
Slag, a period of time is stood, obtains upper strata aqueous and Crude starch；
(2) take half upper strata aqueous to be added in Momordica grosvenori residue, add 35 DEG C~50 DEG C stirring immersions 8 in anistree waste residue
~10h, filter to obtain filter residue and filtrate；
(3) after filter residue air-dries, 300 DEG C~500 DEG C are carried out after directly carbonizing, and obtain activated carbon granule；
(4) after filtrate adds final concentration of 5~15% potassium dihydrogen phosphate, 5~15% potassium nitrate, it is withered that 5~15% are added
Careless 24~48h of fermentation of bacillus, obtains zymotic fluid, and wherein % is quality kg and filtrate volume L ratios；
(5) after Crude starch adds remaining upper strata aqueous, 80 DEG C~100 DEG C 20~40min of gelatinization, add 10~25% the third
Olefin(e) acid, 2.5~5% catalyst and 1~3% crosslinking agent, 3~6h of reaction obtain starch gel, then 40 DEG C~50 DEG C low temperature dryings, powder
5~10 mesh are broken to, obtain dry gel particle；
(6) activated carbon granule obtained by step (3) is added into zymotic fluid, stands a period of time, is added obtained by step (5)
Dry gel particle, wind to water content are organic fertilizer below 25%.
The preparation of the anistree waste residue：Take anistree fruit to bakee to dry to water content 2.4%, the mistake after pulverizer crushes
60 mesh sieves, electronic scale weigh anistree powder 100kg, add 1000~1200L of water, both are mixed, be positioned over steam distillation
Start to distill in steam receiving bottle in device, vapo(u)rizing temperature is 75~85 DEG C, and distillation time is 3~6h, removes the miscellaneous of distillation
Matter, collection slip out liquid, add analytically pure sodium chloride to occur white solid sodium chloride into aqueous phase, be layered profit, draw upper strata
Oil reservoir, obtain star anise oil and anistree waste residue.
The mixed proportion of the Momordica grosvenori residue and anistree waste residue is 5kg：3~6kg.
The bacillus subtilis can be bought with direct market, liquid bacterial medium culture can also be used to obtain.
In a specific embodiment, time of repose is 3~6h in the step (1).
In a specific embodiment, time of repose is 1~3h in the step (6).
In a specific embodiment, catalyst refers to ammonium persulfate in the step (5).
In a specific embodiment, crosslinking agent refers to tetramethylethylenediamine, methylene bisacrylamide in the step (5)
Acid amides etc..
Technique effect
1st, using microbial fermentation, the content of organic nitrogen in organic fertilizer, phosphorus, potassium is effectively increased, and can avoids completely
The discharge of waste water and waste residue.
2nd, cellulose and lignin in Momordica grosvenori and anistree waste residue are made full use of, is converted into activated carbon, is easy to adsorb
Substantial amounts of organic matter, slowly release organic nitrogen, phosphorus, potassium are reached under the influence of gel, turn avoid nutrient in fertilizer
It is lost in.
3rd, it is water absorbent gel particle directly to utilize Starch Conversion in Momordica grosvenori root tuber, reduces the production cost of fertilizer, again
The purpose of fertilizer water conservation itself is reached.
4th, due to ensure that the vigor of bacillus subtilis in whole production process, in the nutriment and guarantor for having abundance
Under conditions of hydrogel, it can continue to keep the propagation of microorganism, to improve the beneficial bacterium such as bacillus subtilis in soil
Ratio.
Embodiment
Below, the present invention will be further detailed with embodiment, but it is not limited to any of these embodiments
Individual or similar example.
Embodiment 1
Take 100kg dried fructus momordicaes root tuber to crush, rinsed with 300kg water, collect water lotion and Momordica grosvenori residue, stand one
The section time, obtain 240L upper stratas aqueous and 35kg precipitations；Take 120L upper stratas aqueous to be added in Momordica grosvenori residue, add 75kg anises
35 DEG C~50 DEG C stirring 8~10h of immersion, filter to obtain 160kg filter residues and 100L filtrates in waste residue；After filter residue air-dries, 300 DEG C~
500 DEG C are carried out after directly carbonizing, and obtain 64kg activated carbon granules；After filtrate adds 12kg potassium dihydrogen phosphates, 15kg potassium nitrate, then add
Enter 8kg bacillus subtilis powders fermentation 36h, obtain zymotic fluid；After 35kg Crude starch adds 120L upper stratas aqueous, 90 DEG C of gelatinizations
30min, 20kg acrylic acid, 4kg catalyst and 2kg crosslinking agents being added, reaction 4h must obtain starch gel, then 45 DEG C of low temperature dryings,
5~10 mesh are crushed to, obtain 45kg dry gel particles；64kg activated carbon granules are added into zymotic fluid, stand a period of time, then add
Enter 45kg dry gel particles, wind to water content is organic fertilizer below 25%.
Claims (7)
1. preparing the method for organic fertilizer using Momordica grosvenori root tuber, specific steps include as follows：
(1) take dried fructus momordicae root tuber to crush, rinsed with the water of twice to four times of weight, collect water lotion and Momordica grosvenori residue, it is quiet
A period of time is put, obtains upper strata aqueous and Crude starch；
(2) take half upper strata aqueous to be added in Momordica grosvenori residue, add in anistree waste residue 35 DEG C~50 DEG C stirring immersions 8~
10h, filter to obtain filter residue and filtrate；
(3) after filter residue air-dries, 300 DEG C~500 DEG C are carried out after directly carbonizing, and obtain activated carbon granule；
(4) after filtrate adds final concentration of 5~15% potassium dihydrogen phosphate, 5~15% potassium nitrate, 5~15% withered grass buds are added
Spore 24~48h of bacillus fermentation, obtains zymotic fluid；
(5) after Crude starch adds remaining upper strata aqueous, 80 DEG C~100 DEG C 20~40min of gelatinization, 10~25% propylene are added
Acid, 2.5~5% catalyst and 1~3% crosslinking agent, 3~6h of reaction obtain starch gel, then 40 DEG C~50 DEG C low temperature dryings, crushed
To 5~10 mesh, dry gel particle is obtained；
(6) activated carbon granule obtained by step (3) is added into zymotic fluid, stands a period of time, is added dry solidifying obtained by step (5)
Glue particle, wind to water content are organic fertilizer below 25%.
2. method according to claim 1, the preparation method of the anistree waste residue：Take anistree fruit baking to dry to water content to exist
2.4%, 60 mesh sieves are crossed after pulverizer crushes, electronic scale weighs anistree powder 100kg, adds 1000~1200L of water, incite somebody to action both
Mix, start to distill in the steam receiving bottle being positioned in steam distillation device, vapo(u)rizing temperature is 75~85 DEG C, distillation time
For 3~6h, the impurity of distillation is removed, collects and slips out liquid, add analytically pure sodium chloride to occur white solid sodium chloride into aqueous phase,
Profit is layered, upper strata oil reservoir is drawn, obtains star anise oil and anistree waste residue.
3. method according to claim 1, the mixed proportion of the Momordica grosvenori residue and anistree waste residue is 5kg：3~6kg.
4. method according to claim 1, time of repose is 3~6h in the step (1).
5. method according to claim 1, time of repose is 1~3h in the step (6).
6. method according to claim 1, catalyst refers to ammonium persulfate in the step (5).
7. method according to claim 1, crosslinking agent refers to tetramethylethylenediamine, methylene bisacrylamide acyl in the step (5)
Amine etc..
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108147926A (en) * | 2018-02-10 | 2018-06-12 | 广西金茂生物化工有限公司 | A kind of Slow release organic fertilizer prepared using manioc waste and preparation method thereof |
| CN108314513A (en) * | 2018-02-10 | 2018-07-24 | 广西金茂生物化工有限公司 | A kind of water keeping fertilizer and preparation method thereof prepared using manioc waste |
| CN108641135A (en) * | 2018-04-28 | 2018-10-12 | 深圳方塔科技有限公司 | Curdling glue composite material and preparation method |
| CN109400409A (en) * | 2018-07-19 | 2019-03-01 | 中国科学院城市环境研究所 | A kind of method and device thereof of the useless fruit harmless treatment of honey shaddock |
| CN109503039A (en) * | 2018-10-29 | 2019-03-22 | 吴伟华 | A kind of preparation method of high fertilizer efficiency slow-release eco-cement material |
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| CN101948340A (en) * | 2010-09-09 | 2011-01-19 | 桂林理工大学 | Method for preparing biological organic fertilizer by using grosvener siraitia waste residue |
| CN105036830A (en) * | 2015-08-07 | 2015-11-11 | 灵川县億旺养殖专业合作社 | Pig manure fermentation organic fertilizer and preparation method thereof |
| CN106242758A (en) * | 2016-08-03 | 2016-12-21 | 桂林实力科技有限公司 | The Application way of Fructus Momordicae marc |
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2017
- 2017-10-10 CN CN201710934179.1A patent/CN107500930A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101948340A (en) * | 2010-09-09 | 2011-01-19 | 桂林理工大学 | Method for preparing biological organic fertilizer by using grosvener siraitia waste residue |
| CN105036830A (en) * | 2015-08-07 | 2015-11-11 | 灵川县億旺养殖专业合作社 | Pig manure fermentation organic fertilizer and preparation method thereof |
| CN106242758A (en) * | 2016-08-03 | 2016-12-21 | 桂林实力科技有限公司 | The Application way of Fructus Momordicae marc |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108147926A (en) * | 2018-02-10 | 2018-06-12 | 广西金茂生物化工有限公司 | A kind of Slow release organic fertilizer prepared using manioc waste and preparation method thereof |
| CN108314513A (en) * | 2018-02-10 | 2018-07-24 | 广西金茂生物化工有限公司 | A kind of water keeping fertilizer and preparation method thereof prepared using manioc waste |
| CN108641135A (en) * | 2018-04-28 | 2018-10-12 | 深圳方塔科技有限公司 | Curdling glue composite material and preparation method |
| CN109400409A (en) * | 2018-07-19 | 2019-03-01 | 中国科学院城市环境研究所 | A kind of method and device thereof of the useless fruit harmless treatment of honey shaddock |
| CN109503039A (en) * | 2018-10-29 | 2019-03-22 | 吴伟华 | A kind of preparation method of high fertilizer efficiency slow-release eco-cement material |
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