CN107496282A - A kind of tea facial mask containing EGCG and preparation method thereof - Google Patents

A kind of tea facial mask containing EGCG and preparation method thereof Download PDF

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Publication number
CN107496282A
CN107496282A CN201710662787.1A CN201710662787A CN107496282A CN 107496282 A CN107496282 A CN 107496282A CN 201710662787 A CN201710662787 A CN 201710662787A CN 107496282 A CN107496282 A CN 107496282A
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egcg
extract
facial mask
deionized water
preparation
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CN201710662787.1A
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Inventor
郑琳
龚自明
高士伟
刘盼盼
王雪萍
郑鹏程
叶飞
滕靖
王胜鹏
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Institute of Fruit and Tea of Hubei Academy of Agricultural Sciences
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Institute of Fruit and Tea of Hubei Academy of Agricultural Sciences
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Priority to CN201710662787.1A priority Critical patent/CN107496282A/en
Publication of CN107496282A publication Critical patent/CN107496282A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4953Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom containing pyrimidine ring derivatives, e.g. minoxidil
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Dermatology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Cosmetics (AREA)

Abstract

A kind of tea facial mask containing EGCG and preparation method thereof, tea facial mask rich in EGCG monomers, dipotassium glycyrrhizinate, mulberry root extract, dried tremella extract, Bacillus acidi lactici/fermented soybean product extract, folic acid, EGF, step because Roripa montana root extract, passion fruit extract, aloe barbadensis Miller leaf juice and hydrolysis fibroin elite;Preparation method includes:Deionized water, propane diols, glycerine, Sodium Hyaluronate, methyl hydroxybenzoate, hydroxyethyl cellulose have been weighed according to recipe ingredient and have been sequentially added in homogeneous agitator tank, add triethanolamine and adjust pH value to 6.5 7.0, EGCG monomer powders are dissolved in standby deionized water, obtain elite material body, filling elite material body step.Integrate antibacterial, maintenance, moisturizing, senile-resistant efficacy, realization settles maintenance skin at one go;And film cloth selects silk, it is clear it is docile effectively facilitate percutaneous absorption nutrition, there are wide market prospects.

Description

A kind of tea facial mask containing EGCG and preparation method thereof
Technical field
The present invention relates to a kind of facial mask, more specifically to a kind of tea facial mask containing EGCG and preparation method thereof.
Background technology
EGCG (Epigallo-catechin gallate (EGCG)) is isolated catechin monomer from tealeaves, and it can Stop ultraviolet and remove the free radical of ultraviolet induction, so as to protect the normal function of melanocyte, suppress melanin Formed, mitigate pigmentation;The greasy of face can be also removed simultaneously, restrain pore, antibacterial, resisting age of skin.
Modern faces computer and mobile phone for a long time, and overtime work is stayed up late as normality, along with the getting worse of environmental pollution, is caused Skin problem is taken place frequently, and various aging phenomenons, which advance to, to be come;For health and beauty, many women select easy-to-use facial masks Nursing skin.At present, facial mask category is numerous on the market;But numerous more effects of mask product are single, lack it is a with the addition of it is pure Green extraction EGCG monomers, integrate the facial mask of antibacterial, maintenance, moisturizing, anti-aging.
The content of the invention
The present invention for the mask product effect that presently, there are it is single, lack the face of pure green extraction EGCG monomers of with the addition of A kind of the problem of film, there is provided tea facial mask containing EGCG and preparation method thereof.
To achieve the above object, technical solution of the invention is:A kind of tea facial mask containing EGCG, it is by following heavy The component of amount part is made:Deionized water 70-80, Sodium Hyaluronate 0.05-0.1, dipotassium glycyrrhizinate 0.5-1.0, mulberry root extract 0.1-0.5, dried tremella extract 0.1-0.5, Bacillus acidi lactici/fermented soybean product extract 0.01-0.05, folic acid 0.005- 0.01st, EGF0.003-0.01, step because of Roripa montana root extract 0.1-0.5, passion fruit extract 0.01-0.03, Aloe Barbadensis Miller Juice 0.1-0.5, hydrolysis fibroin 0.1-0.5, EGCG monomer 0.2-0.4, glycerine 0.5-1.0, propane diols 10-15, carbomer 0.03-0.08, triethanolamine 0.03-0.08, HEC0.3-0.5, Cremophor RH40 0.1-0.3, methyl hydroxybenzoate 0.1- 0.3。
Described EGCG monomer purity >=90%.
A kind of preparation method of the tea facial mask containing EGCG, comprises the following steps:Step 1: weighed according to recipe ingredient Deionized water, propane diols, glycerine, Sodium Hyaluronate, methyl hydroxybenzoate, hydroxyethyl cellulose, mass unit is g, and leaves and takes portion Divide deionized water standby, the deionized water left and taken herein is 100 with EGCG monomer weight ratios:1, then by deionized water, the third two Alcohol, glycerine, Sodium Hyaluronate, methyl hydroxybenzoate, hydroxyethyl cellulose are sequentially added in homogeneous agitator tank, liter while homogeneous stirs Temperature adds carbomer, then homogeneous stirring 5min, is then incubated 30 minutes to 80-85 DEG C;Step 2: treat the temperature of homogeneous agitator tank When degree is down to 60 DEG C, triethanolamine is added, and adjust pH value to 6.5-7.0;Step 3: will be load weighted according to recipe ingredient EGCG monomer powders, which are dissolved in, to be left and taken in step 1 in standby deionized water;Step 4: treat that the temperature of homogeneous agitator tank is down to 45 DEG C, sequentially add EGCG monomers lysate, the glycyrrhizic acid two that deionized water is dissolved in Cremophor RH40, step 3 Potassium, mulberry root extract, dried tremella extract, Bacillus acidi lactici/fermented soybean product extract, folic acid, EGF, step because Roripa montana root extract Thing, passion fruit extract, aloe barbadensis Miller leaf juice and hydrolysis fibroin, it is stirring while adding, elite material body is produced after 30min; Step 5: silk film cloth is fixed with pearl film, then fold and be put into aluminium foil bag, facial mask is put into after ozone sterilization and is automatically filled Install, the elite material body 20mL/ bags obtained in filling step 4 simultaneously seal.
Ozone sterilization method in the step 4 is:In closing space, under unmanned state, and relative humidity is 70% More than, using 20mg/m3The ozone of concentration, act on 60min.
Described step one is operated to step 5 in 300,000 grades of dust proof workshops.
Compared with prior art, the beneficial effects of the invention are as follows:
Tea facial mask in the present invention is rich in EGCG monomers, dipotassium glycyrrhizinate, mulberry root extract, dried tremella extract, lactic acid bar Bacterium/fermented soybean product extract, folic acid, EGF, step because Roripa montana root extract, passion fruit extract, aloe barbadensis Miller leaf juice and Fibroin elite is hydrolyzed, integrates antibacterial, maintenance, moisturizing, senile-resistant efficacy, realization settles maintenance skin at one go;And film Cloth selects silk, it is clear it is docile effectively facilitate percutaneous absorption nutrition, there are wide market prospects.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail.
A kind of tea facial mask containing EGCG, it is made up of the component of following parts by weight:Deionized water 70-80, hyaluronic acid Sodium 0.05-0.1, dipotassium glycyrrhizinate 0.5-1.0, mulberry root extract 0.1-0.5, dried tremella extract 0.1-0.5, Bacillus acidi lactici/big Beans tunning extract 0.01-0.05, folic acid 0.005-0.01, EGF (oligopeptides -1) 0.003-0.01, step because Roripa montana root extracts Thing 0.1-0.5, passion fruit extract 0.01-0.03, aloe barbadensis Miller leaf juice 0.1-0.5, hydrolysis fibroin 0.1-0.5, EGCG monomers 0.2-0.4, glycerine 0.5-1.0, propane diols 10-15, carbomer 0.03-0.08, triethanolamine 0.03-0.08, HEC (hydroxyethyl cellulose) 0.3-0.5, Cremophor RH40 0.1-0.3, methyl hydroxybenzoate 0.1-0.3.
Specifically, described EGCG monomer purity >=90%.
EGCG in the tea facial mask can stop ultraviolet and remove the free radical of ultraviolet induction, so as to protect melanin The normal function of cell, suppress the formation of melanin, mitigate pigmentation;The greasy of face can be also removed simultaneously, restrain pore, Antibacterial, resisting age of skin.Sodium Hyaluronate (also known as sodium hyaluronate) is referred to as NMF, its lasting replenishing water and preserving moisture, increase Skin gloss, increase elasticity, it is anti-wrinkle, anti-ageing.Dipotassium glycyrrhizinate good penetrability, antibacterial, anti-inflammatory, antiallergic.Mulberry root extract is controllable Oily pore cleanser, it is effectively antibacterial.Dried tremella extract has the effect of beautifying face and moistering lotion, delay skin aging, nourishes skin, desalination is thin Line, enhancing cell viability, adjust cutaneous immunisation power, Bergamot Mint Extract.Bacillus acidi lactici/fermented soybean extract contains small molecule Amino acid, peptide, nucleotides, the active skull cap components such as vitamin, moisturizing, assign and live.Folic acid is water-soluble B vitamin, and it promotees Enter skin metabolism, there is whitening, anti-oxidation function.EGF (oligopeptides -1, being called EGF) can anti-acne and repair by Skin is damaged, its careful pore, increases skin elasticity.Step because Roripa montana extract can be obviously improved skin gloss, nourish skin simultaneously Do not increase burden, compact healthy skin, and it is generally from Peru highlands, the activating cell energy, promoting cell metabolism, being to repair The conductive membranes of multiple U.S. flesh.Passion fruit extract is rich in 17 kinds of amino acid, VC, carrotene and SOD enzymes, can effectively remove free radical, Face nourishing antidebilitation.Aloe vera extract is anti-oxidant, moisturizing, anti-inflammatory, have anti-acne repairing effect.Hydrolyze fibroin increase Skin gloss and elasticity, it is protected skin from desiccation, assigns the soft and smooth sense of skin.
A kind of preparation method of the tea facial mask containing EGCG, comprises the following steps:
Step 1: deionized water, propane diols, glycerine, Sodium Hyaluronate, methyl hydroxybenzoate, hydroxyl are weighed according to recipe ingredient Ethyl cellulose, mass unit are g, and leave and take that portions of de-ionized water is standby, the deionized water left and taken herein and EGCG monomers Mass ratio is 100:1;Then by the non-deionized water for leaving and taking part, propane diols, glycerine, Sodium Hyaluronate, methyl hydroxybenzoate, hydroxyl second Base cellulose is sequentially added in homogeneous agitator tank, and homogeneous is warming up to 80-85 DEG C while stirring, adds carbomer, then homogeneous stirs 5min is mixed, is then incubated 30 minutes.
Step 2: when the temperature of homogeneous agitator tank is down to 60 DEG C, triethanolamine is added, and adjust pH value to 6.5-7.0.
Step 3: will be dissolved according to the load weighted EGCG monomer powders of recipe ingredient left and taken in step 1 it is standby go from In sub- water.
Step 4: treating that the temperature of homogeneous agitator tank is down to 45 DEG C, sequentially add molten in Cremophor RH40, step 3 Solution is in the EGCG monomers lysate of deionized water, dipotassium glycyrrhizinate, mulberry root extract, dried tremella extract, Bacillus acidi lactici/soybean hair Ferment product extract, folic acid, EGF (oligopeptides -1), step because Roripa montana root extract, passion fruit extract, aloe barbadensis Miller leaf juice and Fibroin is hydrolyzed, it is stirring while adding, elite material body is produced after 30min.
Step 5: silk film cloth is fixed with pearl film, then fold and be put into aluminium foil bag, facial mask is put into after ozone sterilization Automatic filling machine, the elite material body 20mL/ bags obtained in filling step 4 simultaneously seal.Silk contains 18 kinds of amino acid in itself, Effectively supplement skin tissue's elastin laminin and collagenic protein, facial lines, the rapid elasticity for improving skin can be eliminated, brought back to life Cell, prevent melanin from being formed, brightening skin;, can be uniform and the moisturizing degree of silk mask cloth is 5-10 times of common facial mask cloth Essence is discharged, gos deep into skin nexine moisturizing, maintains the moist sense of skin for a long time.
Specifically, the ozone sterilization method in the step 4 is:In closing space, under unmanned state, and it is relatively wet Degree is more than 70%, using 20mg/m3The ozone of (about 10ppm) concentration, act on 60min.
Further, specifically, described step one to step 5 must be operated in 300,000 grades of dust proof workshops.30 Ten thousand grades of clean area standards:Grit maximum allowable number/m3;>=0.5 micron of population must not exceed 10500000, >=5 microns Population must not exceed 60000;Microorganism maximum allowable number:Bacterium number of swimming must not exceed 1000/m3, sedimentation bacterium number must not More than 15/ware.
Tea facial mask in the present invention is rich in EGCG monomers, dipotassium glycyrrhizinate, mulberry root extract, dried tremella extract, lactic acid bar Bacterium/fermented soybean product extract, folic acid, EGF, step because Roripa montana root extract, passion fruit extract, aloe barbadensis Miller leaf juice and Fibroin elite is hydrolyzed, integrates antibacterial, maintenance, moisturizing, senile-resistant efficacy, realization settles maintenance skin at one go.And film Cloth selects silk, it is clear it is docile effectively facilitate percutaneous absorption nutrition, there are wide market prospects.
Above content is to combine specific preferred embodiment further description made for the present invention, it is impossible to is assert The specific implementation of the present invention is confined to these explanations.For general technical staff of the technical field of the invention, On the premise of not departing from present inventive concept, some simple deduction or replace can also be made, said structure should be all considered as belonging to Protection scope of the present invention.

Claims (5)

1. a kind of tea facial mask containing EGCG, it is characterised in that it is made up of the component of following parts by weight:Deionized water 70-80, Sodium Hyaluronate 0.05-0.1, dipotassium glycyrrhizinate 0.5-1.0, mulberry root extract 0.1-0.5, dried tremella extract 0.1-0.5, lactic acid Bacillus/fermented soybean product extract 0.01-0.05, folic acid 0.005-0.01, EGF0.003-0.01, step because Roripa montana root extracts Thing 0.1-0.5, passion fruit extract 0.01-0.03, aloe barbadensis Miller leaf juice 0.1-0.5, hydrolysis fibroin 0.1-0.5, EGCG monomers 0.2-0.4, glycerine 0.5-1.0, propane diols 10-15, carbomer 0.03-0.08, triethanolamine 0.03-0.08, HEC0.3-0.5, Cremophor RH40 0.1-0.3, methyl hydroxybenzoate 0.1-0.3.
A kind of 2. tea facial mask containing EGCG according to claim 1, it is characterised in that:Described EGCG monomer purities >= 90%.
3. the preparation method of a kind of tea facial mask containing EGCG according to claim 1, it is characterised in that including following step Suddenly:
Step 1: deionized water, propane diols, glycerine, Sodium Hyaluronate, methyl hydroxybenzoate, ethoxy are weighed according to recipe ingredient Cellulose, mass unit are g, and leave and take that portions of de-ionized water is standby, the deionized water left and taken herein and EGCG monomer masses Than for 100:1, then deionized water, propane diols, glycerine, Sodium Hyaluronate, methyl hydroxybenzoate, hydroxyethyl cellulose are sequentially added In homogeneous agitator tank, homogeneous is warming up to 80-85 DEG C while stirring, adds carbomer, then homogeneous stirring 5min, is then incubated 30 Minute;
Step 2: when the temperature of homogeneous agitator tank is down to 60 DEG C, triethanolamine is added, and adjust pH value to 6.5-7.0;
Step 3: standby deionized water is left and taken in step 1 by being dissolved according to the load weighted EGCG monomer powders of recipe ingredient In;
Step 4: treating that the temperature of homogeneous agitator tank is down to 45 DEG C, sequentially add and be dissolved in Cremophor RH40, step 3 EGCG monomers lysate, dipotassium glycyrrhizinate, mulberry root extract, dried tremella extract, the Bacillus acidi lactici/fermented soybean production of deionized water Thing extract, folic acid, EGF, step because Roripa montana root extract, passion fruit extract, aloe barbadensis Miller leaf juice and hydrolysis fibroin, It is stirring while adding, elite material body is produced after 30min;
Step 5: silk film cloth is fixed with pearl film, then fold and be put into aluminium foil bag, facial mask is put into after ozone sterilization entirely certainly Bottle placer is moved, the elite material body 20mL/ bags obtained in filling step 4 simultaneously seal.
A kind of 4. preparation method of tea facial mask containing EGCG according to claim 3, it is characterised in that the step 4 In ozone sterilization method be:In closing space, under unmanned state, and relative humidity is more than 70%, using 20mg/m3It is dense The ozone of degree, act on 60min.
A kind of 5. preparation method of tea facial mask containing EGCG according to claim 3, it is characterised in that:Described step One is operated to step 5 in 300,000 grades of dust proof workshops.
CN201710662787.1A 2017-08-04 2017-08-04 A kind of tea facial mask containing EGCG and preparation method thereof Pending CN107496282A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111529434A (en) * 2020-05-11 2020-08-14 山东农业大学 Lip prevention and health care product containing EGCG and application thereof
CN112057359A (en) * 2020-10-22 2020-12-11 北京唯爱生物科技有限公司 Deep-sea pinus hirsuta moisturizing composition and preparation method and application thereof
CN113151067A (en) * 2021-03-31 2021-07-23 绽妍生物科技有限公司 Extraction and separation process of lactobacillus fermentation extract

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111529434A (en) * 2020-05-11 2020-08-14 山东农业大学 Lip prevention and health care product containing EGCG and application thereof
CN111529434B (en) * 2020-05-11 2021-09-03 山东农业大学 Lip prevention and health care product containing EGCG and application thereof
CN112057359A (en) * 2020-10-22 2020-12-11 北京唯爱生物科技有限公司 Deep-sea pinus hirsuta moisturizing composition and preparation method and application thereof
CN112057359B (en) * 2020-10-22 2021-07-27 北京唯爱生物科技有限公司 Deep-sea pinus hirsuta moisturizing composition and preparation method and application thereof
CN113151067A (en) * 2021-03-31 2021-07-23 绽妍生物科技有限公司 Extraction and separation process of lactobacillus fermentation extract
CN113151067B (en) * 2021-03-31 2023-03-24 绽妍生物科技有限公司 Extraction and separation process of lactobacillus fermentation extract

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