CN107496271A - Anti-dandruff nourishing camellia oleifera fruit leaves shampoo and preparation method thereof - Google Patents
Anti-dandruff nourishing camellia oleifera fruit leaves shampoo and preparation method thereof Download PDFInfo
- Publication number
- CN107496271A CN107496271A CN201710972997.0A CN201710972997A CN107496271A CN 107496271 A CN107496271 A CN 107496271A CN 201710972997 A CN201710972997 A CN 201710972997A CN 107496271 A CN107496271 A CN 107496271A
- Authority
- CN
- China
- Prior art keywords
- fresh
- parts
- camellia oleifera
- dandruff
- oleifera fruit
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Biophysics (AREA)
- Molecular Biology (AREA)
- Emergency Medicine (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
A kind of anti-dandruff nourishing camellia oleifera fruit leaves shampoo, is made up according to mass fraction of following component:105 170 parts of water, water-soluble 0.5 1 parts of jojoba oil；12 parts of glycerine；2 parts of phosphatidase 0 .5；0.1 0.3 parts of chitosan；0.02 0.05 parts of Tea Polyphenols；12 parts of salt；Wherein water is made up in terms of weight fraction of following component：50 80 parts of fresh fried flour fruit；Fresh 5 10 parts of golden larch root skin；Fresh 10 20 parts of ginkgo leaf；Fresh 10 20 parts of felwort；5 10 parts of Chinese twinleaf rhizome rhizome；Fresh 20 30 parts of Chinese honey locust fruit；Fresh 5 10 parts of cloves.The anti-dandruff nourishing camellia oleifera fruit leaves shampoo uses raw material based on fresh tea fruit pulp, rich in the materials such as camellia oil, Tea Saponin, tea polysaccharide, tea albumen, flavones, compound botanical bacterial remediation composition, has extraordinary anti-dandruff and nourishing repair.
Description
Technical field
The present invention relates to a kind of shampoo, particularly a kind of anti-dandruff nourishing camellia oleifera fruit leaves shampoo and preparation method thereof.
Background technology
Squeezed the juice using fresh tea fruit and extract tea oil and tea fruit juice in tea fruit, retain Tea Saponin, tea polysaccharide, tea egg in tea fruit
In vain, the material such as flavones, this stability is high, the high emulsion of nutritional ingredient, in the exploitation applied to all kinds of cosmetics, have non-
Often good skin and hair nursing effect.
The content of the invention
The purpose of the present invention, fresh squeezing tea fruit latex composite compounding had into anti-dandruff nourishing camellia oleifera fruit leaves shampoo into one kind；This is anti-dandruff
Nourish camellia oleifera fruit leaves shampoo and use raw material based on fresh tea fruit pulp, rich in camellia oil, Tea Saponin, tea polysaccharide, tea albumen, Huang
The materials such as ketone, compound botanical bacterial remediation composition, there is extraordinary anti-dandruff and nourishing repair.
The technical scheme is that：A kind of anti-dandruff nourishing camellia oleifera fruit leaves shampoo, according to mass fraction by following component system
Into:
Water 105-170 parts, water-soluble jojoba oil 0.5-1 parts；Glycerine 1-2 parts；Phosphatidase 0 .5-2 parts；Chitosan 0.1-
0.3 part；Tea Polyphenols 0.02-0.05 parts；Salt 1-2 parts.
Wherein water is made up in terms of weight fraction of following component：
Fresh fried flour fruit 50-80 parts；Fresh golden larch root skin 5-10 parts；Fresh ginkgo leaf 10-20 parts；Fresh felwort 10-20 parts；Chinese twinleaf rhizome
Rhizome 5-10 parts；Fresh Chinese honey locust fruit 20-30 parts；Fresh cloves 5-10 parts.
Preferably, described water preparation technology is：
（1）Selection：Selection just harvesting, fresh full camellia oleifera fruit and just plucks fresh golden larch root skin, fresh ginkgo leaf, fresh rough gentian
Grass, Chinese twinleaf rhizome rhizome, fresh Chinese honey locust fruit, fresh cloves；
（2）Cleaning：By step（1）Gained camellia oleifera fruit machinery peels off, and removes shell, and cleaning obtains fresh tea seed；By fresh golden larch
Root skin, fresh ginkgo leaf, fresh felwort, Chinese twinleaf rhizome rhizome, fresh Chinese honey locust fruit, fresh cloves are washed respectively, draining, after removing spot, obtain
Obtain plant material；
（3）Crush：By step（2）Gained tea seed and plant material put into pulverizer in proportion, obtain plant material particle, water
Divide content 40%-60%；
（4）Split-phase：By step（3）Gained plant material particle puts into juice extractor, and extruding obtains solid fiber powder and serum；
（5）Purification：By step（4）Gained serum is transported in retort, and regulation PH is in 2-4, paving chromatography media, by chromatographing
Filter obtains filtrate；
（6）It is refined：By step（5）The filtrate regulation PH of acquisition adds filter aid, is filtered, stablized by filter in 5-6
Water.
Preferably, described camellia oleifera fruit is plucked for August-September, oil-containing 5%-10%, now camellia oleifera fruit prematurity, camellia
Oil content is moderate（Too high emulsification is difficult, and easily oil separates out, become sour, too low without enhancing moisturizing effect）, Tea Saponin, tea it is more
Sugar, starch, OPC, tea albumen, flavones equal size are maximum, can preferably embody the anti-dandruff effect of anti-inflammatory and joint is nourished.
Preferably, step（3）Described crusher sifting aperture 2-10 millimeters, pulverized particles are less than 1 millimeter, and surface is without obvious
White or yellowish coloured particles；Particle is big, and crushing juice rate is low；Particle is small, not juice.
Preferably, step（4）Described juice extractor squeezes 0.1 millimeter ~ 1 millimeter of gap, carries out separation of solid and liquid well.
Preferably, step（5）Described in plant granule in moisture 40-60%, if moisture is too low, juice
Rate is especially low, does not go out even；Moisture is high, and compounding water content is big, reduces active quantities, it is difficult to form emulsion.
Preferably, it is characterised in that step（5）Described in chromatography media be using 30-100 mesh silica gel sand, activated carbon,
One or more in atlapulgite；Adsorption specific surface area 1000m2/g-1500m2/ g or adsorption capacity reach 80%-100%, layer
The 2%-5% chromatography medias of paving filtrate weight in tank are analysed, is filtered by chromatographing tank, carries out purification desensitization；In specific decolorization adsorption
It is to be operated under environment temperature because whole technical process does not heat under aperture, it is white by silica gel sand and/or activated carbon and activity
Soil, it can effectively remove sensitizer and pigment, and retentive activity thing very well.
Preferably, wherein step（5）Described in regulation PH in 2-4, the acidity can be good at separate out sensitizer and with
Muddy thing caused by time change, is analysed after precipitation by silica gel sand bed, adsorbs the material of this particle diameter very well；So that subsequent liquid is not
Allergy be present and deposit muddy problem for a long time, influence subsequently to use.
Preferably, wherein step（6）Described regulation PH is in 5-6, it is therefore an objective to neutralization procedure（5）Acidity, the acidity can
The compounding of fusion unclassified stores well, makes subsequent applications more extensive.
Wherein step（6）Described in filtering use sedimentation centrifuge or leaf-type filter.
Wherein step（6）Using filter aid diatomite, addition is the 1%-6% of liquid weight.
The anti-dandruff nourishing camellia oleifera fruit leaves shampoo preparation method of the present invention, comprises the following steps：
In water, water-soluble jojoba oil, glycerine, phosphatide, chitosan, Tea Polyphenols, salt are proportionally added into, is opened equal
Matter machine, homogeneous 10-30 minutes, speed are 3000-4000 revs/min, obtain anti-dandruff nourishing camellia oleifera fruit leaves shampoo.
The beneficial effects of the present invention are：
（1）This method processing step is simple, effectively desensitization, the characteristics of warm camellia oleifera fruit and other components, forms stabilising system
Technology；
（2）The anti-dandruff camellia oleifera fruit leaves shampoo that nourishes of gained is to use raw material based on fresh tea fruit pulp, rich in camellia oil, tea soap
The materials such as element, tea polysaccharide, tea albumen, flavones, being re-dubbed leaves shampoo, there is extraordinary nourish to repair anti-dandruff effect.
Primary raw material used in the present invention is described as follows：
Camellia oleifera fruit：It is the fruit of tea oil tree；Tea oil tree is the main woody oleiferous plants tree in China, is described as " east tree ", belongs to camellia
Section's Camellia evergreen dungarunga, it is the distinctive woody vegetable oil resource in China；3-6 meters of the height of tree, the diameter of a cross-section of a tree trunk 1.3 meters above the ground is up to 24-30 lis
Rice, smooth bark is taupe.Tea oil tree list leaf alternate, flower are both sexes white, and October, Post flowering was until fruit between October next year
Can be ripe, therefore, tea oil tree has rare flowers and fruits homophyletic phenomenon；Fruit is capsule, is mostly ellipse, has fine, soft fur；Seed
Mostly yellowish-brown, glossy, triangular shape；Tea oil tree is grown in remote mountains, inhales natural nutrient to the greatest extent, evergreen longevity, the age of tree up to 200 years with
On；It is untouched to retain fresh tea fruit nutritional ingredient using fresh tea fruit cold pressing, rich in unsaturated oils, protein, starch, tea
Saponin, flavones, polyphenol, VE etc., there is moisturizing, moist, antibacterial, anti-inflammatory and other effects, for taking care of hair, favus of the scalp, dandruff can be prevented, taken off
Hair and black hair and other effects.
Golden larch root skin：Containing organic acid, the 10 kind pathomycetes common to China have certain antibacterial action；Its dosage
0.1-1mg/ml, trichophyton schoenleini, acrothesium floccosum, the small gemma tinea bacterium of rust, Microsporum gypseum and white are read
Pearl bacterium has bactericidal action.
Ginkgo leaf：Level of lipid is reduced, improves skin microcirculation.
Felwort:Heat-clearing and damp-drying drug.
Cloves：There are inhibitory action and expelling parasite to make to staphylococcus, streptococcus, Escherichia coli, typhoid bacillus, Pseudomonas aeruginosa etc.
With.
Coptis rhizome：Containing a variety of alkaloids, mainly jamaicin, also known as berberine.It has significant bacteriostasis.
Chinese honey locust fruit：Containing triterpenoid saponin, there is a very strong cleaning action, the medicine of the constituents containing gleditsia sinensis, can clearing away heat and eliminating dampeness, dispel
Except superabundant fats, unobstructed obstruction hair follicle, scalp will not be stimulated；To Escherichia coli, bacterium sonnei, proteus, typhoid fever bar
The Grain-negative enteral pathogenic bacteria such as bacterium, paratyphosum Bacterium, Pseudomonas aeruginosa, comma bacillus have inhibitory action.
Chitosan：Chitin is called, is the polysaccharose substance by chitins such as crab shrimp, insects after deacetylated, to large intestine bar
Bacterium, proteus vulgaris, hay bacillus, staphylococcus aureus have stronger inhibitory action.
Tea Polyphenols：Acted on good anti-corrosive fresh-keeping, to hay bacillus, staphylococcus aureus, Escherichia coli, tomato
Routed sore, S.mutans, and mucor, Penicillium notatum, gibberella, anthrax bacteria, saccharomyces cerevisiae etc. have inhibitory action.
Phosphatide：With stronger emulsification, wetting, peptizaiton, promote body fat metabolism, muscle growth, nervous system
Development and internal anti-oxidative damage etc. play critically important effect.
Water-soluble jojoba oil：Water-soluble assignment agent, shampoo flushing, wet comb, the smoothness of dry comb are can effectively improve, is prevented
Only hair winding, knotting.
Salt：Main component is NaCl, and the viscosity of liquid is matched somebody with somebody in increase.
Glycerine：A kind of polyalcohol NMF, hair washing process surfactant is avoided to remain, while it is steady to improve shampoo low temperature
It is qualitative.
Embodiment
Camellia oleifera fruit in embodiment is harvesting mid-August, oil content 7.2%, and the phosphatide in embodiment is soybean lecithin.
Embodiment 1
The anti-dandruff nourishing camellia oleifera fruit leaves shampoo of embodiment 1, is made up of following processing step：
（One）It is prepared by water
（1）Selection：Selection just harvesting, fresh full camellia oleifera fruit and just plucks fresh golden larch root skin, fresh ginkgo leaf, fresh rough gentian
Grass, Chinese twinleaf rhizome rhizome, fresh Chinese honey locust fruit, fresh cloves；
（2）Cleaning：By step（1）Gained camellia oleifera fruit machinery peels off, and removes shell, and cleaning obtains fresh tea seed；By fresh golden larch
Root skin, fresh ginkgo leaf, fresh felwort, Chinese twinleaf rhizome rhizome, fresh Chinese honey locust fruit, fresh cloves are washed respectively, draining, after removing spot, obtain
Obtain plant material；
（3）Crush：By step（2）Gained tea seed and plant material put into pulverizer in proportion（3 millimeters of crusher sifting aperture）,
Obtain plant material particle（Particle is less than 1 millimeter）, moisture 52%；
（4）Split-phase：By step（3）Gained plant material particle puts into juice extractor（Squeeze 0.2 millimeter of gap）, extruding acquisition solid
Fiber powder and serum；
（5）Purification：By step（4）Gained serum is transported in retort, and PH is 2 for regulation, spreads the mesh silica gel sand 6.6 of chromatography media 50
Kg, filtrate is obtained by chromatographing to filter；
（6）It is refined：By step（5）The filtrate regulation PH of acquisition adds filter aid diatomite 5, and addition is liquid weight
3%, filtered by filter, obtain stable water.
（Two）Anti-dandruff nourishing camellia oleifera fruit leaves shampoo configuration
In water, water-soluble jojoba oil, glycerine, phosphatide, chitosan, Tea Polyphenols, salt are proportionally added into, is opened equal
Matter machine, homogeneous 20 minutes, speed are 3000 revs/min, obtain anti-dandruff nourishing camellia oleifera fruit leaves shampoo.
Embodiment 2-7
Embodiment 2-7 anti-dandruff nourishing camellia oleifera fruit leaves shampoo, its preparation process condition is substantially with embodiment 1, simply reaction raw materials
And the condition such as proportion scale, temperature, time is slightly different, specifically as listed in table 1.
The embodiment 1-6 of table 1 anti-dandruff nourishing camellia oleifera fruit leaves shampoo preparation process condition
。
Comparative example 1
Comparative example 1 is identical with the formula of embodiment 1, and difference is that the camellia fruit emulsion of comparative example 6 uses well-done fresh fried flour fruit, contains
Oil mass 29%.
Embodiment 1-6, the gained of comparative example 1 anti-dandruff nourishing camellia oleifera fruit leaves shampoo are tested into its cold-resistant heat-resistant stability, head
Skin anaphylaxis, moisten moisturizing, be cleaning, anti-dandruff.
The anti-dandruff its functional attributes test result for nourishing camellia oleifera fruit leaves shampoo of the embodiment 1-6 of table 2, comparative example 1
。
Its functional attributes of anti-dandruff nourishing camellia oleifera fruit leaves shampoo obtained by embodiment 1-6, comparative example 1 and physical and chemical index test
Used method of testing has：
（1）Cold-resistant heat-resistant stability
Carried out according to 6.2.1 in GB/T 29680 and 6.2.2.
（2）Degree of allergic reaction is tested
Experimental procedure：
Step 1：The gauze of four thickness is cut into a diameter of 1cm circle with scissors, totally 8, with 1 gram of anti-dandruff nourishing oil of steel bale-out
Tea fruit leaves shampoo, is coated on circular gauze, and blank is done with deionized water.
Step 2：The gripping of gauze tweezers is placed at the anteflexion arm of subject, fixed with adhesive tape, starts timing.
Step 3：Torn after 48h adhesive tape, and observe the reaction of skin at gauze covering immediately；Observe result.
（3）Cleanliness testing, specific method are as follows：
Anti-dandruff nourishing camellia oleifera fruit leaves shampoo obtained by embodiment 1-6 is uniformly applied to three days and not done on the hair cleaned, finger
Grab and rub 10 minutes, when all hairs are all in uniform white, wiped clean white bits with dry towel after two minutes.With white oil suction
Paper again send out by rubbing head, checks oil-Absorbing Sheets.Contrast does not carry out the hair of any cleaning.
（4）The method of testing for moistening maintenance performance of keeping humidity is tested for head, and specific method is as follows：
Anti-dandruff nourishing camellia oleifera fruit leaves shampoo obtained by embodiment 1-6 is uniformly applied to coarse, dry damaged hair, impression is moistened
Moistening effect and reparation situation, and record（- expression almost do not have ,+represents, ++ represent very well, +++ expression is very good）, note
Moisture preserving time is recorded, untill no moisture feeling.Contrast coarse, dry damaged hair.
（5）The method of testing of anti-dandruff performance is tested for head, and specific method is as follows：
Anti-dandruff nourishing camellia oleifera fruit leaves shampoo obtained by embodiment 1-6 is uniformly applied on the hair of dandruff crowd, finger
Grab and rub hair and massaging scalp, be used continuously one week, record（- expression almost do not have ,+represents, ++ represent it is fine, +++ table
It is very good to show）Contrast uses front heat condition.
From table 2, the anti-dandruff nourishing camellia oleifera fruit leaves shampoo of the present invention uses raw material based on fresh tea fruit pulp, rich in camellia
The materials such as oil, Tea Saponin, tea polysaccharide, tea albumen, flavones, decontamination is compounded, maintenance composition, the deep enough hair of energy, moisturizing of taking care of hair, is repaiied
The tip, cleaning, anti-dandruff and other effects are recurred, and without anaphylaxis.
In addition, by the anti-dandruff nourishing camellia oleifera fruit leaves shampoo obtained by embodiment 1-6, by examining microbiological indicator, health to refer to
Mark《Cosmetics safety technical specification》（Version in 2015）, obtain the testing result shown in table 3 below.
The embodiment 1-6 camellia oleifera fruit leaves shampoos microorganism of table 3, sanitary index
。
The anti-dandruff nourishing camellia oleifera fruit leaves shampoo toxicology test of the present invention：Skin irritation test（Multiple skin irritation examination
Test）.
Test objective：Observe rabbit intact skin long-time multiple-contact tested material（The leaves shampoo of embodiments of the invention）
Caused skin irritation reaction afterwards, for embodiments of the invention anti-dandruff nourishing camellia oleifera fruit leaves shampoo provide security according to
According to.
Test basis：《Cosmetics safety technical specification》Version in 2015；Test method：From white New Zealand rabbits 8, with
Machine is divided into 2 groups, every group 4；A groups:Experimental group, B groups:Deionized water control group；24h is by family's rabbit back backbone both sides before experiment
Hair is cut, and skin surface is not damaged in cropping, and unhairing scope is 3cm × 3cm, and application area is 2.5cm × 2.5cm, tested
Anti-dandruff nourishing camellia oleifera fruit leaves shampoo of the thing group to various embodiments of the present invention, takes tested material 0.5ml to be coated directly on back backbone
Side, opposite side apply 0.5ml control group deionized waters, smear 1 time daily, continuously smear 14d；Since second day, apply every time
Cropping when smearing, residual tested material is removed with deionized water；Result is observed after one hour, according to《Cosmetics safety technical specification》
（Version in 2015）Skin irritation test table scoring, check plot and trial zone are equally handled.
Evaluation of result：Every rabbit average integral daily is calculated according to the following formula, is pierced by specification list deciding rabbit skin
Swash intensity, and observe other toxic actions in addition to excitant.
。
Result of the test：Tested material was carried out in the multiple skin irritation test observation period, gave various embodiments of the present invention
Anti-dandruff nourishing camellia oleifera fruit leaves shampoo after, rabbit has no erythema, oedema；Have no systemic toxicity profiles performance and death condition, animal body
Increase again, on breathing, circulating, central nervous system, four limbs activity etc. is without influence.
Conclusion (of pressure testing)：The anti-dandruff nourishing camellia oleifera fruit leaves shampoo of various embodiments of the present invention is to white New Zealand rabbits intact skin
It is nonirritant.
Claims (9)
1. a kind of anti-dandruff nourishing camellia oleifera fruit leaves shampoo, is made up according to mass fraction of following component:Water 105-170 parts,
Water-soluble jojoba oil 0.5-1 parts, glycerine 1-2 parts, phosphatidase 0 .5-2 parts, chitosan 0.1-0.3 parts, Tea Polyphenols 0.02-0.05
Part, salt 1-2 parts.
2. according to the anti-dandruff nourishing camellia oleifera fruit leaves shampoo described in claim 1, it is characterised in that the water is with weight
Fraction meter, is made up of following component：Fresh fried flour fruit 50-80 parts；Fresh golden larch root skin 5-10 parts；Fresh ginkgo leaf 10-20 parts；Fresh dragon
Courage grass 10-20 parts；Chinese twinleaf rhizome rhizome 5-10 parts；Fresh Chinese honey locust fruit 20-30 parts；Fresh cloves 5-10 parts.
3. according to the anti-dandruff nourishing camellia oleifera fruit leaves shampoo described in claim 2, it is characterised in that prepared by described water
Method is as follows：
（1）Selection：Selection just harvesting, fresh full camellia oleifera fruit and just plucks fresh golden larch root skin, fresh ginkgo leaf, fresh rough gentian
Grass, Chinese twinleaf rhizome rhizome, fresh Chinese honey locust fruit, fresh cloves；
（2）Cleaning：By step（1）Gained camellia oleifera fruit machinery peels off, and removes shell, and cleaning obtains fresh tea seed；By fresh golden larch
Root skin, fresh ginkgo leaf, fresh felwort, Chinese twinleaf rhizome rhizome, fresh Chinese honey locust fruit, fresh cloves are washed respectively, draining, after removing spot, obtain
Obtain plant material；
（3）Crush：By step（2）Gained tea seed and plant material put into pulverizer in proportion, obtain plant material particle, water
Divide content 40-60%；
（4）Split-phase：By step（3）Gained plant material particle puts into juice extractor, and extruding obtains solid fiber powder and serum；
（5）Purification：By step（4）Gained serum is transported in retort, and regulation pH value spreads chromatography media, passes through chromatography in 2-4
Filtering obtains filtrate；
（6）It is refined：By step（5）The filtrate regulation pH value of acquisition adds filter aid, is filtered, planted by filter in 5-6
Thing juice.
4. according to the anti-dandruff nourishing camellia oleifera fruit leaves shampoo described in claim 3, it is characterised in that step（1）Described oil tea
Fruit is plucked for 8-September, oil-containing 5-10%.
5. according to the anti-dandruff nourishing camellia oleifera fruit leaves shampoo described in claim 3, it is characterised in that step（5）Described in layer
Analysis medium is the one or more in 30-100 mesh silica gel sand, activated carbon, atlapulgite.
6. according to the anti-dandruff nourishing camellia oleifera fruit leaves shampoo described in claim 3, it is characterised in that step（5）Described in crushing
Machine discharging sieve aperture is 2-10 millimeters.
7. according to the anti-dandruff nourishing camellia oleifera fruit leaves shampoo described in claim 3, it is characterised in that step（6）Described in squeeze the juice
Machine uses single-screw oil press, 0.1 millimeter ~ 1 millimeter of fence gap.
8. anti-dandruff nourishing camellia oleifera fruit leaves shampoo according to claim 3, it is characterised in that step（6）Using filter aid diatom
Soil, addition are the 1-6% of filtrate weight.
9. the anti-dandruff preparation method for nourishing camellia oleifera fruit leaves shampoo according to claim 1, comprises the following steps：
In water, water-soluble jojoba oil, glycerine, phosphatide, chitosan, Tea Polyphenols, salt are proportionally added into, is opened equal
Matter machine, homogeneous 10-30 minutes, speed are 3000-4000 revs/min, obtain anti-dandruff nourishing camellia oleifera fruit leaves shampoo.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710972997.0A CN107496271A (en) | 2017-10-18 | 2017-10-18 | Anti-dandruff nourishing camellia oleifera fruit leaves shampoo and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710972997.0A CN107496271A (en) | 2017-10-18 | 2017-10-18 | Anti-dandruff nourishing camellia oleifera fruit leaves shampoo and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107496271A true CN107496271A (en) | 2017-12-22 |
Family
ID=60701994
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710972997.0A Pending CN107496271A (en) | 2017-10-18 | 2017-10-18 | Anti-dandruff nourishing camellia oleifera fruit leaves shampoo and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107496271A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103860428A (en) * | 2014-03-11 | 2014-06-18 | 安徽亿宏生物科技有限公司 | Tea oil shampoo and preparation method thereof |
| CN104000772A (en) * | 2014-06-18 | 2014-08-27 | 福建春辉生物工程有限公司 | Camellia oleirea aberl oil cake shampoo |
| CN106309175A (en) * | 2015-06-19 | 2017-01-11 | 焦爱军 | Traditional Chinese medicine shampoo for stopping alopecia and regenerating hair as well as preparation method thereof |
| CN106937926A (en) * | 2017-03-24 | 2017-07-11 | 福建师范大学泉港石化研究院 | A kind of preparation method of the natural shampoo of anti-dandruff and itching-relieving maintenance unification |
| CN107213067A (en) * | 2017-06-28 | 2017-09-29 | 赣州市惠丽生物科技有限公司 | A kind of shampoo formula for considering antipruritic and maintenance hair to be worth doing with Eradicates and preparation method thereof |
-
2017
- 2017-10-18 CN CN201710972997.0A patent/CN107496271A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103860428A (en) * | 2014-03-11 | 2014-06-18 | 安徽亿宏生物科技有限公司 | Tea oil shampoo and preparation method thereof |
| CN104000772A (en) * | 2014-06-18 | 2014-08-27 | 福建春辉生物工程有限公司 | Camellia oleirea aberl oil cake shampoo |
| CN106309175A (en) * | 2015-06-19 | 2017-01-11 | 焦爱军 | Traditional Chinese medicine shampoo for stopping alopecia and regenerating hair as well as preparation method thereof |
| CN106937926A (en) * | 2017-03-24 | 2017-07-11 | 福建师范大学泉港石化研究院 | A kind of preparation method of the natural shampoo of anti-dandruff and itching-relieving maintenance unification |
| CN107213067A (en) * | 2017-06-28 | 2017-09-29 | 赣州市惠丽生物科技有限公司 | A kind of shampoo formula for considering antipruritic and maintenance hair to be worth doing with Eradicates and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108158869B (en) | Antibacterial wet tissue liquid, wet tissue and preparation method of wet tissue | |
| Rahman et al. | Taxonomy and traditional medicine practices on Malvaceae (Mallow Family) of Rajshahi, Bangladesh | |
| CN105596253B (en) | Edible toothpaste which is prepared from olive extracts and does not contain fluorine and preparation method thereof | |
| CN105076246A (en) | Antibacterial traditional Chinese medicine composition, preparing method of antibacterial traditional Chinese medicine composition and application of antibacterial traditional Chinese medicine composition | |
| KR102276213B1 (en) | Cosmetic composition for hair loss care applied to the natural plant composite material extract | |
| CN112841233A (en) | Traditional Chinese medicine pesticide | |
| CN111066828A (en) | Plant extraction sterilization and disinfection composition special for farm and preparation method thereof | |
| Jikah et al. | Moringa oleifera: a valuable insight into recent advances in medicinal uses and pharmacological activities | |
| Tiwari et al. | Evaluation of aqueous extract of Roots of Carica papaya on wound healing activity in albino Rats | |
| CN107693419A (en) | Nourish moisturizing camellia oleifera fruit shower cream and preparation method thereof | |
| KR100712249B1 (en) | Oily to acne skin cosmetics composite containing oriental herb extract and manufacturing method thereof | |
| Ugbabe et al. | Preliminary phytochemical, antimicrobial and acute toxicity studies of the stem, bark and the leaves of a cultivated Syzygium cumini Linn.(Family: Myrtaceae) in Nigeria | |
| CN107320758B (en) | Air purifying agent for efficiently removing bacteria in livestock and poultry breeding environment | |
| Shermin et al. | Antioxidant and Cytotoxic Activitiy of Limonia acidissima L. | |
| US11607437B2 (en) | Cosmetic and pharmaceutical compositions each containing aloe extract and upland rice extract | |
| CN107496274A (en) | Nourish moistening bath and preparation method | |
| CN107550794A (en) | Camellia oleifera fruit hair care and nourishing cream and preparation method thereof | |
| CN107496271A (en) | Anti-dandruff nourishing camellia oleifera fruit leaves shampoo and preparation method thereof | |
| CN104586682A (en) | Antibacterial deodorant cosmetic composition and preparation method thereof | |
| KR102151045B1 (en) | Cosmetic Composition Having Anti-Inflammation and Skin-Irritation Mitigating Effect Containing Catalpa ovata and Vitex trifolia L. Mixed Extract | |
| CN107625689A (en) | Camellia oleifera fruit disposable clean hair agent, preparation method and application method | |
| CN107693445A (en) | Gentle camellia oleifera fruit skin cream and preparation method thereof | |
| CN107496273A (en) | Camellia oleifera fruit mildy wash and preparation method thereof | |
| Nasution et al. | An experiment for extracted Citrus hystrix leaf effectiveness on Pityrosporum ovale fungi growth | |
| CN110179733A (en) | A kind of kiss-me with anti-acne effect skims the cream off milk liquid and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171222 |