CN107440920A - A kind of deep layer chelating beauty face cleaning facial mask and preparation method - Google Patents

A kind of deep layer chelating beauty face cleaning facial mask and preparation method Download PDF

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CN107440920A
CN107440920A CN201710691812.9A CN201710691812A CN107440920A CN 107440920 A CN107440920 A CN 107440920A CN 201710691812 A CN201710691812 A CN 201710691812A CN 107440920 A CN107440920 A CN 107440920A
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parts
facial mask
deep layer
oil
acid
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CN107440920B (en
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陈庆
曾军堂
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Yuhuan Yimin Cosmetics Co.,Ltd.
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Chengdu New Keli Chemical Science Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8105Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • A61K8/8111Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/737Galactomannans, e.g. guar; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/817Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
    • A61K8/8176Homopolymers of N-vinyl-pyrrolidones. Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/925Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/965Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

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Abstract

The present invention relates to cosmetic technical field, chelates beauty face cleaning facial mask and preparation method more particularly to a kind of deep layer, the deep layer chelates beauty face cleaning facial mask, including following material:VAE emulsions, acrylate copolymer, polyvinylpyrrolidone, guar gum, surfactant, chelating agent, diatomite.The present invention is with VAE emulsions, acrylate copolymer, polyvinylpyrrolidone, guar gum is base-material, with surfactant, chelating agent, diatomite is expected for cleaning, micro-elasticity paste is formed by kneading, that is deep layer face cleaning facial mask, the facial mask is easy to uniformly smear facial, cementability can be formed in face, the film of elasticity, absorption affinity between the film and skin is very big, it is dirty that bacterium and the blackhead of skin surface etc. can be adsorbed, and there is good compatibility to skin, injury very little to skin, film is directly thrown off after use, the dirty of absorption is bonded by its viscoplasticity completely, prevent from being retained in face.Easy to use, cleaning effect is notable.

Description

A kind of deep layer chelating beauty face cleaning facial mask and preparation method
Technical field
The present invention relates to cosmetic technical field, and beauty face cleaning facial mask and preparation side are chelated more particularly to a kind of deep layer Method.
Background technology
Everyone wants to possess the delicate skin of health in actual life.Skin is one of important organ of our human bodies, It protects our health, therefore people just have using cosmetics to be nursed to our skin from ancient times.With people Pursuit of the raising and people of quality of the life to U.S., cosmetics species are more and more various.Facial mask is important in skin nursing Content, for the regular application facial mask of all kinds of skin characteristics, Oily degreasing can be made, thick pore is restrained, and is dried up The skin of gauffer recovers gloss, and the inflammation of dark sore skin is inhibited.Facial mask makes skin seem salubrious, smooth and pure white after Delicacy, because when facial mask is coated on skin, facial mask produces affinity with skin, with the gradual drying of facial mask, skin temperature Rise, blood circulation are accelerated, and skin-tightening and tension force are strengthened, and the sebum and moisture reverse osmosis of skin secretion make epidermis in cuticula Softness is unfolded, and pore instinct is opened, and is promoted sweat gland secretion and metabolism, the oxygen content of skin is increased, and is advantageous to skin row Except the product of epidermal cell metabolism and the oil substances of accumulation, the active ingredient in facial mask is penetrated into skin and is absorbed, Facial mask is tightly connected with skin simultaneously, and when removing facial mask, deep layer dirt is also by band simultaneously in the aging cutin, pore on skin Under, make skin pure and fresh clean.Moisture in facial mask penetrates into the cuticula of skin epidermis, and skin becomes soft, and skin is naturally bright It is flexible.Facial mask is generally divided into mud cream type facial mask, tears stripping type facial mask, gel-type facial mask, creams type facial mask, cloth facial mask etc.;Cloth Formula facial mask does not have cleaning effect, is not suitable for needing the people of deep layer clean skin, and other several facial masks have certain cleaning effect;But Application method is coated on skin, after 20~40 minutes dry, takes off or washes off, so as to reach the mesh of cleaning and caring skin 's.
Work growing day by day, life stress, environmental pollution, make the skin of many people face the threat of inferior health.It is various Disease of skin occurs again and again, and this is relevant with the various nutriments of skin shortage.Modern does not move all day, and is not careful in one's diet, The sagging symptom of facial muscle occurs in some people very early, and this has two kinds of protein in skin corium just because of skin:Glue Former albumen and elastic fibers albumen, they, which have supported skin, makes its full compact.After 25 years old, both albumen are declined due to human body Old process and reduce naturally, the support force of skin also declines therewith, elastic force reduce, then occur relaxation and wrinkle.
The radiation sources such as keyboard, computer screen, mobile phone directly influence whether the steady unrest of the internal system of our bodies, so that Skin metabolism is irregular etc., is magnetic plus computer, can build up some dusts and unclean air etc., these can all have influence on me Skin, aggravate the degree of aging of skin.
In addition, with the aggravation of atmosphere pollution, the destruction of ozone layer, injury of the ultraviolet to human body, which turns into, has to pay attention to The problem of daylight in ultraviolet be divided into three types:Ultraviolet (UV)-C (200-290nm);Ultraviolet (UV)-B (290~ 320nm);Ultraviolet (UV)-A (320-400nm).UV-C can be fully absorbed by earth atmosphere, and UV-B only has part by air Ozone layer absorbs, and UV-A is by Atmospheric Absorption, the ultraviolet of earth surface by more than 90% UV-A and less than 10% UVB structures Into.Damage to human body skin is extremely serious.Often show as skin burn, cause erythema, aging, or even induce leucoderma Wind or canceration.Therefore, antiultraviolet skin care item turn into daily necessary article.
Existing sunlight screening skin-protecting product mostly using TiO2, ZnO or benzophenone, hexichol first phthalein methane, benzo three oh, meat Cinnamic acid vinegar, using the characteristic absorption ultraviolet of its energy-absorbing, is reduced and endangered caused by ultraviolet radiation as additive.But hexichol Ketone, hexichol first phthalein methane, benzo three oh, cinnamic acid aceto chemical sun-screening agent be small molecule chemicals, because photostability is poor, easily Oxidation deterioration, performance degradation is serious when sun-proof, and easily penetrate into skin cause it is allergic, to be applicable crowd have particular/special requirement, So as to limit its application.TiO2, ZnO easily block pore and are equally not easy to connect throughout the year with skin because bioaffinity is poor Touch.Therefore, antiultraviolet skincare product develops to biological, stability.
With the growth of global Cosmetic Market and the continuous growth of consumer demand, in global cosmetics in the market There are some new trend:1. environmental protection, with growing to even greater heights for global environmentally friendly cry, consumer is to consumer safety requirement More and more higher;2. safety, the security of cosmetics is not only related to the physical and mental health of consumer, is also related to enterprise and industry Final and decisive juncture;3. natural plants especially medicinal herb componentses;4. anti-aging and sun-proof;5. effect cosmetic.Wash one's face be day usually Cleaning mode.But due to it is simple wash one's face be difficult to thoroughly to remove it is dirty in the entrance pore such as debris, particularly skin care item Easily cause pore to block, cause skin oil and fat water oil dyssecretosis, so as to cause acne, acne and blackhead etc. to make us puzzlement Skin problem.Therefore, washing one's face except routine, a deep layer cleaning face is needed within usual one week.Existing deep layer cleaning is mainly adopted With face cleaning cream or interface face mask cream, but it is required to after the completion of face cleaning to elute face cleaning face mask cream, thus is difficult to clean, or even causes The dirty residual of face, use are extremely inconvenient.
The content of the invention
Face cleaning cream or interface face mask cream mainly are used for the cleaning of current deep layer, but is required to after the completion of face cleaning to elute clean Face face mask cream, thus be difficult to clean, or even cause the dirty residual of face, the shortcomings that use is extremely inconvenient, the purpose of the present invention is A kind of easy to use, the significant deep layer chelating beauty face cleaning facial mask of cleaning effect is provided.
To solve the above problems, the present invention uses following technical scheme:
A kind of deep layer chelates beauty face cleaning facial mask, including following material:VAE emulsions, acrylate copolymer, polyvinylpyrrolidine Ketone, guar gum, surfactant, chelating agent, diatomite.
VAE emulsions, it is the abbreviation of vinyl acetate-ethylene copolymerization emulsions.The present inventor is in the clean surface that studies for a long period of time Found during film, VAE emulsions, acrylate copolymer, polyvinylpyrrolidone, guar gum mix according to a certain percentage Afterwards, film can be formed in face, the absorption affinity between the film and skin is very big, can adsorb bacterium and the blackhead of skin surface Etc. dirty, and there is good compatibility to skin, the injury very little to skin.
In the present invention, the proportioning of each material is very big to the performance impact of facial mask, it is preferred that the deep layer chelates beauty face cleaning Facial mask, include the material of following parts by weight:10 ~ 35 parts of VAE emulsions, 15 ~ 28 parts of acrylate copolymer, polyvinylpyrrolidone 5 ~ 32 parts, 5 ~ 30 parts of guar gum, 2 ~ 6 parts of surfactant, 3 ~ 8 parts of chelating agent, 2 ~ 18 parts of diatomite.
It is furthermore preferred that the deep layer chelates beauty face cleaning facial mask, include the material of following parts by weight:VAE emulsions 15 ~ 25 Part, 18 ~ 26 parts of acrylate copolymer, 10 ~ 28 parts of polyvinylpyrrolidone, 8 ~ 16 parts of guar gum, 2 ~ 6 parts of surfactant, 3 ~ 8 parts of chelating agent, 5 ~ 12 parts of diatomite.
Surfactant can improve compatibility of each material in mixed system, improve the degrees of fusion between each material, so as to Enable each material dispersed, the surfactant be in ammonium salt class, pyridine salt, PEG, POE and stearic acid at least It is a kind of.
Preferably, the chelating agent be ethylenediamine tetra-acetic acid, aminotriacetic acid, diethylene-triamine pentaacetic acid, citric acid, Tartaric acid and grape credit I acid, 1,2,3 ,-tetracarboxylic acid cyclopentane, 2- fluoroacetic acid propylmalonic acid and 2- fluoroacetic acid base fourths are led in acid It is at least one.
In order to increase the function of facial mask, it is preferred that also include epidermal growth factor in the deep layer chelating beauty face cleaning facial mask Son, fibroblast growth factor, bleeding agent, consolidant, preservative, plants essential oil, NMF, emulsifying agent, film forming agent, thickening At least one of agent and lecithin.
Grease crop base starting material occupies larger specific gravity in cosmetic formulations, and it, which is acted on, can make skin emolliency, lubrication and Surface cleaning, friction effect is played on skin inner feelings face, while form hydrophobic film, play protection skin, and can prevented outer The harmful substance invasion and attack come, can also suppress the evaporation of skin table and moisture when cold;As excessively fatty agent protection skin, can also make The solvent of special composition.In addition, plants essential oil contains aromatic odor, can pleasant mental and body, the plants essential oil is olive oil, coconut palm Seed oil, camellia oil, jojoba oil, Rosa Damascana, Lavender, jasmine essential oil, Rosemary Oil, Bergamot, sieve Strangle essential oil, clove oil, oil of Cymbopogon winterianus, sweet orange oil, tea tree ethereal oil, Salvia japonica essential oil, eucalyptus quintessence oil, grapefruit essential oil, At least one of Geranium Essential, Peppermint essential oil, lemon, chamomile essential oil, marjoram essential oil.
Deep layer chelating beauty face cleaning facial mask provided by the invention also includes bleeding agent, and in the present invention, the lecithin is Soybean lecithin, egg yolk lecithin, DSPC, palmitoylphosphatidyl choline, phosphatidylserine, phosphatide At least one of acid, hydrolecithin.
Deep layer chelating beauty face cleaning facial mask provided by the invention also includes bleeding agent, in the present invention, the bleeding agent choosing One or more from potassium chloride, sodium sulphate, sodium chloride, preferably potassium chloride.
Deep layer provided by the invention chelating beauty face cleaning facial mask also includes NMF, and the NMF is glycerine, propane diols, Butanediol, pentanediol, hexylene glycol, ethohexadiol, decanediol, ethoxy urea, glycine betaine, pyrrolidone sodium carboxylate, hyaluronic acid and At least one of salt, plant polyose class, stearyl alcohol, stearic acid, isopropyl palmitate, dimethyl silicone polymer, sweet almond oil.
Deep layer chelating beauty face cleaning facial mask provided by the invention also includes emulsifying agent, and the emulsifying agent is selected from glycerol stearate At least one of ester, polysorbate -20, sorbitan sesquioleate, olein, the polyricinoleate of polyglycereol -3.
Deep layer chelating beauty face cleaning facial mask provided by the invention also includes consolidant, and in the present invention, the consolidant is excellent Elect allantoin as.
Deep layer chelating beauty face cleaning facial mask provided by the invention also includes preservative, and in the present invention, the preservative is excellent Elect DP-300 as.
Deep layer chelating beauty face cleaning facial mask provided by the invention also includes thickener, in the present invention, the thickener choosing From hydroxyethyl cellulose, polyvinyl alcohol, xanthan gum, Magnesiumaluminumsilicate, the crosslinking of the alkylol acrylamide acid esters of acrylic acid (ester) class/C10- 30 One or more of mixing of polymer, pectin, carbomer;
A kind of preparation method of deep layer chelating beauty face cleaning facial mask, comprises the following steps:
(1)By VAE emulsions, acrylate copolymer, polyvinylpyrrolidone, guar gum, ultrasonic disperse mixes in organic solvent Uniformly, 15 ~ 120min is then incubated at 60 ~ 80 DEG C;Obtain mixed system;
(2)Surfactant, chelating agent, diatomite and water are added in mixed system, it is incubated 30 at 50 ~ 80 DEG C ~ After 240min, high speed homogenization 20 minutes, start to cool, discharged when being then down to 38 DEG C.
In order that the compatible degree of facial mask and skin increases, it is preferred that the pH value range control of the discharging product 5.0~ 6.5。
In step(1)In, the organic solvent is ethanol, ethylene glycol, propane diols, glycerine, White Mineral Oil, palmitic acid isopropyl One or more in ester, ethyl acetate, acetone ester, white oil, Seabuckthorn Oil and avocado oil, preferably glycerine, White Mineral Oil, palmitic acid Isopropyl ester and lanolin, wherein, 3 kinds of White Mineral Oil, isopropyl palmitate and lanolin compositions are used in mixed way with good moisturizing Effect.
A kind of deep layer of present invention chelating beauty face cleaning facial mask and preparation method, compared with prior art, the characteristics of it is protruded It is with excellent effect:
The present invention using VAE emulsions, acrylate copolymer, polyvinylpyrrolidone, guar gum as base-material, with surfactant, Chelating agent, diatomite are expected for cleaning, form micro-elasticity paste by kneading, i.e. deep layer face cleaning facial mask, facial mask is easy to It is facial uniformly to smear, can be in face formation cementability, the film of elasticity, the absorption affinity between the film and skin is very big, can It is dirty to adsorb bacterium and the blackhead of skin surface etc., and there is good compatibility to skin, the injury very little to skin, makes Film is directly thrown off after, the dirty of absorption is bonded by its viscoplasticity completely, prevents from being retained in face.It is easy to use, cleaning effect Fruit is notable.
Embodiment
Below by way of embodiment, the present invention is described in further detail, but this should not be interpreted as to the present invention Scope be only limitted to following example.In the case where not departing from above method thought of the present invention, according to ordinary skill The various replacements or change that knowledge and customary means are made, should be included in the scope of the present invention.
Embodiment 1
A kind of deep layer chelates beauty face cleaning facial mask, is made up of the material of following parts by weight:20 parts of VAE emulsions, acrylate copolymer 22 parts, 18 parts of polyvinylpyrrolidone, 15 parts of guar gum, POE3 parts, 5 parts of ethylenediamine tetra-acetic acid, 8 parts of diatomite, epidermis life Long 0.5 part of the factor, 0.3 part of fibroblast growth factor, 1 part of sodium chloride, 0.6 part of allantoin, 2 parts of DP-300, jojoba oil 1.2 parts of 5 parts, 3 parts of Rosa Damascana, 1 part of propane diols, 6 parts of stearine, 1 part of film forming agent, 3 parts of pectin and soybean lecithin.
The preparation method of the deep layer chelating beauty face cleaning facial mask, comprises the following steps:
(1)By VAE emulsions, acrylate copolymer, polyvinylpyrrolidone, guar gum, ultrasonic disperse mixes in ethylene glycol It is even, then it is incubated 90min at 60 DEG C;Obtain mixed system;
(2)POE, ethylenediamine tetra-acetic acid, diatomite, fibroblast growth factor, sodium chloride, urine are added in mixed system Bursin, DP-300, jojoba oil, Rosa Damascana, propane diols, stearine, film forming agent, pectin, soybean lecithin, water, Regulation system pH value is 6.2, after being incubated 120min at 80 DEG C, high speed homogenization 20 minutes, starts to cool, when being then down to 38 DEG C Discharging.
Embodiment 2
A kind of deep layer chelates beauty face cleaning facial mask, is made up of the material of following parts by weight:15 parts of VAE emulsions, acrylate copolymer 26 parts, 28 parts of polyvinylpyrrolidone, 8 parts of guar gum, 6 parts of PEG, 3 parts of aminotriacetic acid, 12 parts of diatomite, epidermal growth 0.6 part of the factor, 0.4 part of fibroblast growth factor, 1.5 parts of sodium sulphate, 0.3 part of allantoin, 1.2 parts of DP-300, sweet basil essence 2 parts of oil, 5 parts of clove oil, 3 parts of stearyl alcohol, 10 parts of olein, 0.5 part of film forming agent, 6 parts of carbomer and hydrolecithin 2 Part.
The preparation method of the deep layer chelating beauty face cleaning facial mask, comprises the following steps:
(1)By VAE emulsions, acrylate copolymer, polyvinylpyrrolidone, guar gum in isopropyl palmitate ultrasonic disperse It is well mixed, then it is incubated 30min at 65 DEG C;Obtain mixed system;
(2)PEG, aminotriacetic acid, diatomite, fibroblast growth factor, sodium sulphate, allantois are added in mixed system Element, DP-30, Basil Essential, clove oil, stearyl alcohol, olein, film forming agent, carbomer and hydrolecithin and water, adjust It is 5.0 to save system pH, after being incubated 150min at 50 DEG C, high speed homogenization 20 minutes, starts to cool, goes out when being then down to 38 DEG C Material.
Embodiment 3
A kind of deep layer chelates beauty face cleaning facial mask, is made up of the material of following parts by weight:25 parts of VAE emulsions, acrylate copolymer 18 parts, 10 parts of polyvinylpyrrolidone, 16 parts of guar gum, 2 parts of PEG, 8 parts of diethylene-triamine pentaacetic acid, 5 parts of diatomite, 0.1 part of EGF, 0.5 part of fibroblast growth factor, 2 parts of sodium chloride, 0.1 part of allantoin, DP-300 1.5 Part, 2 parts of jasmine essential oil, 5 parts of propane diols, 8 parts of the polyricinoleate of polyglycereol -3,1 part of polyvinyl alcohol, 6 parts of carbomer and phosphorus 5 parts of acyl serine.
The preparation method of the deep layer chelating beauty face cleaning facial mask, comprises the following steps:
(1)By VAE emulsions, acrylate copolymer, polyvinylpyrrolidone, guar gum, ultrasonic disperse mixes in ethyl acetate Uniformly, then it is incubated 60min at 70 DEG C;Obtain mixed system;
(2)Added in mixed system PEG, diethylene-triamine pentaacetic acid, diatomite, EGF, into fiber finer The intracellular growth factor, sodium chloride, allantoin, DP-300, jasmine essential oil, propane diols, the polyricinoleate of polyglycereol -3, poly- second Enol, carbomer and phosphatidylserine and water regulation system pH value are 6.5, after being incubated 120min at 75 DEG C, high speed homogenization 20 minutes, start to cool, discharged when being then down to 38 DEG C.
Embodiment 4
A kind of deep layer chelates beauty face cleaning facial mask, is made up of the material of following parts by weight:35 parts of VAE emulsions, acrylate copolymer 28 parts, 5 parts of polyvinylpyrrolidone, 30 parts of guar gum, 6 parts of pyridine salt, 3 parts of 2- fluoroacetic acid propylmalonic acid, diatomite 18 Part, 0.8 part of EGF, 0.2 part of fibroblast growth factor, 1.6 parts of sodium chloride, 0.5 part of allantoin, DP-300 1.2 parts, 5 parts of olive oil, 3 parts of Lavender, 6 parts of ethoxy urea, 5 parts of sorbitan sesquioleate, 0.3 part of Magnesiumaluminumsilicate, 3 parts of DSPC.
The preparation method of the deep layer chelating beauty face cleaning facial mask, comprises the following steps:
(1)By VAE emulsions, acrylate copolymer, polyvinylpyrrolidone, guar gum, ultrasonic disperse mixes in avocado oil It is even, then it is incubated 120min at 75 DEG C;Obtain mixed system;
(2)Added in mixed system pyridine salt, 2- fluoroacetic acid propylmalonic acid, diatomite, epidermal growth factor, into fiber finer The intracellular growth factor, sodium chloride, allantoin, DP-30, olive oil, Lavender, ethoxy urea, sorbitan sesquioleate, silicon Sour magnalium, DSPC and water regulation system pH value are 5.5, after being incubated 30min at 60 DEG C, high speed homogenization 20 Minute, start to cool, discharged when being then down to 38 DEG C.
Embodiment 5
A kind of deep layer chelates beauty face cleaning facial mask, is made up of the material of following parts by weight:10 parts of VAE emulsions, acrylate copolymer 15 parts, 32 parts of polyvinylpyrrolidone, 5 parts of guar gum, 2 parts of pyridine salt, 1,2,3,8 parts of-tetracarboxylic acid cyclopentane, diatomite 2 parts, 0.5 part of EGF, 0.1 part of fibroblast growth factor, 2.3 parts of sodium sulphate, 0.8 part of allantoin, DP-300 1 part, 5 parts of grapefruit essential oil, 0.5 part of decanediol, -203 parts of polysorbate, 1 part of alkylol acrylamide acid esters cross-linked polymer and yolk 2.5 parts of lecithin.
The preparation method of the deep layer chelating beauty face cleaning facial mask, comprises the following steps:
(1)By VAE emulsions, acrylate copolymer, polyvinylpyrrolidone, guar gum, ultrasonic disperse mixes in acetone ester It is even, then it is incubated 120min at 80 DEG C;Obtain mixed system;
(2)Add pyridine salt, 1,2,3 in mixed system ,-tetracarboxylic acid cyclopentane, diatomite, EGF, into Fibroblast growth factor, sodium sulphate, allantoin, DP-300, grapefruit essential oil, decanediol, polysorbate -20, alkylol acrylamide Acid esters cross-linked polymer and egg yolk lecithin and water regulation system pH value are 5.8, after being incubated 240min at 65 DEG C, high speed homogenization 20 minutes, start to cool, discharged when being then down to 38 DEG C.
Comparative example 1:
A kind of deep layer chelates beauty face cleaning facial mask, is made up of the material of following parts by weight:22 parts of acrylate copolymer, polyethylene pyrrole 18 parts of pyrrolidone, 15 parts of guar gum, POE3 parts, 5 parts of ethylenediamine tetra-acetic acid, 8 parts of diatomite, 0.5 part of EGF, into 0.3 part of fibroblast growth factor, 1 part of sodium chloride, 0.6 part of allantoin, 2 parts of DP-300,5 parts of jojoba oil, Rosa Damascana 3 Part, 1 part of propane diols, 6 parts of stearine, 1 part of film forming agent, 3 parts of pectin and 1.2 parts of soybean lecithin.
The preparation method of the deep layer chelating beauty face cleaning facial mask, comprises the following steps:
(1)By acrylate copolymer, polyvinylpyrrolidone, guar gum, ultrasonic disperse is well mixed in ethylene glycol, then 90min is incubated at 60 DEG C;Obtain mixed system;
(2)In mixed system add POE, ethylenediamine tetra-acetic acid, diatomite, fibroblast growth factor, sodium chloride, Allantoin, DP-300, jojoba oil, Rosa Damascana, propane diols, stearine, film forming agent, pectin, soybean lecithin, Water, regulation system pH value are 6.2, after being incubated 120min at 80 DEG C, high speed homogenization 20 minutes, start to cool, are then down to 38 DEG C when discharge.
Comparative example 2:
A kind of deep layer chelates beauty face cleaning facial mask, is made up of the material of following parts by weight:20 parts of VAE emulsions, acrylate copolymer 22 parts, 18 parts of polyvinylpyrrolidone, 15 parts of guar gum, POE3 parts, 5 parts of ethylenediamine tetra-acetic acid, EGF 0.5 Part, 0.3 part of fibroblast growth factor, 1 part of sodium chloride, 0.6 part of allantoin, 2 parts of DP-300,5 parts of jojoba oil, rose 1.2 parts of 3 parts of essential oil, 1 part of propane diols, 6 parts of stearine, 1 part of film forming agent, 3 parts of pectin and soybean lecithin.
The preparation method of the deep layer chelating beauty face cleaning facial mask, comprises the following steps:
(1)By VAE emulsions, acrylate copolymer, polyvinylpyrrolidone, guar gum, ultrasonic disperse mixes in ethylene glycol It is even, then it is incubated 90min at 60 DEG C;Obtain mixed system;
(2)POE, ethylenediamine tetra-acetic acid, fibroblast growth factor, sodium chloride, allantoin, DP- are added in mixed system 300th, jojoba oil, Rosa Damascana, propane diols, stearine, film forming agent, pectin, soybean lecithin, water, regulation system PH value is 6.2, after being incubated 120min at 80 DEG C, high speed homogenization 20 minutes, starts to cool, is discharged when being then down to 38 DEG C.
Experimental method:
Volunteer's number is 210, and the deep layer in testing example 1 ~ 5 and comparative example 1 ~ 2 chelates beauty face cleaning facial mask respectively Clean-up performance, every group of 30 people.Using left face as test zone, smear the deep layer chelating beauty of embodiment 1 ~ 5 and comparative example 1 ~ 2 Face cleaning facial mask;The right corresponding symmetrical region of face is blank control.Washed away after 15min.
Volunteer's subjective assessment cleaning efficacy and excitant.
Number/30 of cleaning efficacy=have cleaning effect
Excitant=number/30 stimulated are produced to skin
Experimental result is as shown in table 1:
Table 1:
Test event Cleaning efficacy(%) Allergy(%)
Embodiment 1 100 0
Embodiment 2 100 0
Embodiment 3 97 0
Embodiment 4 97 0.03
Embodiment 5 93.3 0.03
Comparative example 1 53.3 0.03
Comparative example 2 50 0.06

Claims (10)

1. a kind of deep layer chelates beauty face cleaning facial mask, it is characterised in that including following material:VAE emulsions, acrylate copolymer, Polyvinylpyrrolidone, guar gum, surfactant, chelating agent, diatomite.
2. deep layer according to claim 1 chelates beauty face cleaning facial mask, it is characterised in that includes the thing of following parts by weight Matter:10 ~ 35 parts of VAE emulsions, 15 ~ 28 parts of acrylate copolymer, 5 ~ 32 parts of polyvinylpyrrolidone, 5 ~ 30 parts of guar gum, table 2 ~ 6 parts of face activating agent, 3 ~ 8 parts of chelating agent, 2 ~ 18 parts of diatomite.
3. deep layer according to claim 2 chelates beauty face cleaning facial mask, it is characterised in that includes the thing of following parts by weight Matter:15 ~ 25 parts of VAE emulsions, 18 ~ 26 parts of acrylate copolymer, 10 ~ 28 parts of polyvinylpyrrolidone, 8 ~ 16 parts of guar gum, table 2 ~ 6 parts of face activating agent, 3 ~ 8 parts of chelating agent, 5 ~ 12 parts of diatomite.
4. the deep layer chelating beauty face cleaning facial mask according to claim 1 ~ 3 any one, it is characterised in that live on the surface Property agent be at least one of ammonium salt class, pyridine salt, PEG, POE and stearic acid.
5. the deep layer chelating beauty face cleaning facial mask according to claim 1 ~ 3 any one, it is characterised in that the chelating agent For ethylenediamine tetra-acetic acid, aminotriacetic acid, diethylene-triamine pentaacetic acid, citric acid, tartaric acid and grape shine I acid, 1,2,3 ,- Tetracarboxylic acid cyclopentane, 2- fluoroacetic acid propylmalonic acid and 2- fluoroacetic acid base fourths lead at least one of acid.
6. deep layer according to claim 5 chelates beauty face cleaning facial mask, it is characterised in that also including EGF, Fibroblast growth factor, bleeding agent, consolidant, preservative, plants essential oil, NMF, film forming agent, emulsifying agent, thickener At least one of with lecithin.
7. deep layer according to claim 6 chelates beauty face cleaning facial mask, it is characterised in that the plants essential oil is olive Oil, coconut oil, camellia oil, jojoba oil, Rosa Damascana, Lavender, jasmine essential oil, Rosemary Oil, bergamot essence Oil, Basil Essential, clove oil, oil of Cymbopogon winterianus, sweet orange oil, tea tree ethereal oil, Salvia japonica essential oil, eucalyptus quintessence oil, grape fruit At least one of essential oil, Geranium Essential, Peppermint essential oil, lemon, chamomile essential oil, marjoram essential oil.
8. deep layer according to claim 6 chelates beauty face cleaning facial mask, it is characterised in that the lecithin is soybean lecithin Fat, egg yolk lecithin, DSPC, palmitoylphosphatidyl choline, phosphatidylserine, phosphatidic acid, hydrogenation ovum At least one of phosphatide.
9. a kind of preparation method of deep layer chelating beauty face cleaning facial mask according to claim 1 ~ 8 any one, its feature It is, comprises the following steps:
(1)By VAE emulsions, acrylate copolymer, polyvinylpyrrolidone, guar gum, ultrasonic disperse mixes in organic solvent Uniformly, 15 ~ 120min is then incubated at 60 ~ 80 DEG C;Obtain mixed system;
(2)Surfactant, chelating agent, diatomite are added in mixed system, after being incubated 30 ~ 240min at 50 ~ 80 DEG C, High speed homogenization 20 minutes, starts to cool, and is discharged when being then down to 38 DEG C.
10. the preparation method of deep layer chelating beauty face cleaning facial mask according to claim 9, it is characterised in that discharging product PH value range control 5.0~6.5.
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CN108815005A (en) * 2018-07-27 2018-11-16 华南理工大学 Adulterate the cream pack and preparation method thereof of Cellulose nanocrystal palpus deep layer cleaning
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CN117653563B (en) * 2023-12-13 2024-06-04 奥俐莱雅(广东)家化科技有限公司 Recombinant collagen peptide with high transdermal property and preparation process and application thereof

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