CN105919909A - Eggshell membrane active peptide silk mask and preparation method thereof - Google Patents
Eggshell membrane active peptide silk mask and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/88—Polyamides
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention discloses an eggshell membrane active peptide silk mask and a preparation method of the eggshell membrane active peptide silk mask. The eggshell membrane active peptide silk mask is prepared by dipping facial mask paper in liquid prepared from the following raw materials in parts by weight: 0.5-30 parts of eggshell membrane extract, 5-30 parts of glycerol, 5-50 parts of butanediol, 4-20 parts of diglycerol, 5-8 parts of poly(sodium L-glutamate), 6-10 parts of sodium hyaluronate, 4-8 parts of sodium pyrrolidonecarboxylate, 5-10 parts of betaine, 6-15 parts of 1,2-pentanediol, 2-9 parts of hydrolyzed sclerotium gum, 0.5-5 parts of dipotassium glycyrrhizinate, 0.7-5 parts of PPG-26-buteth-26, 0.7-8 parts of PEG-40 hydrogenated castor oil, 0.1-1 part of methylparaben, 0.1-1 part of bis(hydroxymethyl) imidazolidinyl urea, 0.1-0.2 part of iodopropynyl butylcarbamate, 0.5-2 parts of essence, and the balance water, and the number of the total weight parts of the raw materials is 1000. The eggshell membrane active peptide silk mask can replenish water and lock water, repair the damaged cells, promote the cytothesis, and clean up the garbage in the cells and the blood, so that the face is bright and ruddy, and no stimulation, allergy or injury is caused to the skin.
Description
Technical field
The present invention relates to cosmetic field, specifically eggshell membrane bioactive peptide silk mask and preparation method thereof.
Background technology
The living environment of modern is more and more severe, operating pressure is the most increasing, these the most disadvantageous factors can accelerate the aging and dead of cell, reduce the self-repairing capability of body, face is then that the first of human spirit's looks intuitively reflect, under the pressure of all environment, the skin of human body can show dry, yellowing, black dull, lax, mottle etc. symptom, at this time need exist for one fast and effectively method to go to improve this state, good facial film exactly can play such effect, the most therefore becomes the indispensable selection of a lot of people seeking beauty.
Current market, facial film is of a great variety, very different, and that can really do is good and few, and the present invention adheres to following several principles to believe surely can bring brand-new experience to by consumption: the first, must green pure sky however harmless；The second, must be able to play effect that long term maintenance whitening skin and preserving moisture is repaired；3rd, skin will not be caused allergy or injury.
Eggshell membrane is described as one of moisturizing material the most powerful in nature, and in daily life, goes to eat almost without people, can not be absorbed by human body even if being eaten.The eggshell membrane that every day is abandoned by the mankind is the most innumerable, and this is a kind of wasting of resources greatly.Progress along with science and technology, we are by advanced biological high-tech technology, the micromolecule polypeptide (patent of invention number: ZL2010101377581, production licence number: QS320806010166) eggshell membrane is hydrolyzed into high activity, being easily absorbed by organisms, this micromolecule polypeptide is dissolved in facial film and spreads on face, can directly be absorbed by skin cell, thus really playing whitening and skin-protecting, the effect of moisturizing reparation, this most necessarily brings huge economic benefit, social benefit and ecological benefits.
Summary of the invention
It is an object of the invention to provide eggshell membrane bioactive peptide silk mask and preparation method thereof, it is dropped partly in order to solve eggshell membrane as life and trade waste, cause the technical problem of the wasting of resources, on the other hand it is to meet market, meet consumer demand, be truly realized effect that the whitening skin and preserving moisture to human skin is repaired.
For achieving the above object, the present invention provides following technical scheme:
nullEggshell membrane bioactive peptide silk mask，The liquid infiltration being made up of following raw material prepares in face paper: egg shell membrane extract: 0.5-30 part，Glycerol: 5-30 part，Butanediol: 5-50 part，Diglycerol: 4-20 part，Polyglutamic acid sodium: 5-8 part，Hyaluronate sodium: 6-10 part，Pyrrolidone sodium carboxylate: 4-8 part，Glycine betaine: 5-10 part，1,2-pentanediol: 6-15 part，Hydrolysis Scleroglucan: 2-9 part，Glycyrrhizic acid dipotassium: 0.5-5 part，PPG-26-butylol polyether-26:0.7-5 part，Cremophor RH40: 0.7-8 part，Methyl hydroxybenzoate: 0.1-1 part，Bis(hydroxymethyl)imidazolidinyl urea: 0.1-1 part，Iodine propilolic alcohol butyl mephenesin Carbamate: 0.1-0.2 part，Essence: 0.5-2 part，Surplus is water，And the total weight parts of all raw materials is 1000 parts.
As the further scheme of the present invention: described egg shell membrane extract be highly soluble in water, molecular weight control 300-2000Da, aqueous solution surface tension at the powder of 34-36mN/m.
As the further scheme of the present invention: described wet concentration is from deionized water, distilled water or purified water.
As the further scheme of the present invention: the material of described face paper is silkworm silk or fruit fiber.
As the further scheme of the present invention: described egg shell membrane extract is the micromolecule polypeptide using biofermentation, biodegradation, bio-separation, high-new membrane technology to be refined into by eggshell membrane.
As the further scheme of the present invention: described egg shell membrane extract itself contains whitening skin and preserving moisture lock water and the reparative factor of many pure naturals, and its composition includes: collagen protein, keratin, albumin, sialoglycoprotein, chondroitin sulfate, hyaluronic acid, lysozyme, somatomedin, trace element.
The preparation method of described eggshell membrane bioactive peptide silk mask, comprises the steps:
1) glycerol, butanediol, diglycerol, egg shell membrane extract, methyl hydroxybenzoate, hydrolysis Scleroglucan, glycine betaine are obtained A liquid with water mixed dissolution；
2) polyglutamic acid sodium, hyaluronate sodium, pyrrolidone sodium carboxylate, 1,2-pentanediol, glycyrrhizic acid dipotassium, PPG-26-butylol polyether-26, essence, Cremophor RH40, Bis(hydroxymethyl)imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate are mixed to get B liquid；
3) A liquid is put in main cooker, be warming up to 75 DEG C and stir；
4) it is cooled to the A liquid stirred when 45 DEG C add B liquid, after stirring, filters discharging；
5) by face paper 4) feed liquid of gained is soaked, take out, packaging.
As the further scheme of the present invention: the equipment used during the stirring of described step step 3) and step 4) is blender or homogenizer.
As the further scheme of the present invention: when using blender, speed is 1000-2000rpm, and the time is 10-20 minute.
As the further scheme of the present invention: when using homogenizer, speed is 10000-20000rpm, and batch (-type) is carried out 4-5 time, and each time is the 5-8 second.
Glycerol (glycerol) in the present invention, is the clear and bright thick liquid sweet without color and taste, can dissolve in any proportion with water, low concentration glycerin solution can do lubricating oil and moisten skin.Glycerol is used as hygroscopic agent, wetting agent and solvent, is also used for doing diffusant, penetrating agent, antifreezing agent and sweeting agent, it is also possible to be used for decomposing the tannin in natural extract composition, remove abnormal flavour bitter, puckery.
Butanediol, the English name often occurred is: Butylene Glycol, and another name is named again: 1,3-dihydroxy butane, is the one of polyhydric alcohol, and its action and efficacy is mainly used in adsorbed water molecule, moisturizing and is used as solvent；In terms of moisturizing, owing to butanediol is little molecule moisturizing ingredient, so it is the least to grab water ratio, also there is certain bacteriostasis simultaneously.Clearly, without sticky sense, moisturizing is fabulous, is not yet found to have any irritating inflammation.
Diglycerol, is the clear and bright thick liquid that yellow taste is sweet, can dissolve in any proportion with water, low concentration diglycerol can do lubricating oil and moisten skin.Diglycerol is used as in hygroscopic agent, wetting agent and solvent, with cosmetics, and its effect is as glycerol.
Polyglutamic acid sodium, the resistance to hard water of polyglutamic acid sodium, can use under alkalescence, neutrality and mild acid conditions.This surfactant has obvious advantages for development; its new serviceability includes having good cleaning strength and foaming power; harmless to human non-toxic, free from extraneous odour, character is soft non-stimulated; the activity of enzyme can be stablized; it is high-grade shampoo and the primary raw material of body lotion, can be firmly adsorbed on hair and skin, increase and keep the softness of hair, fluffy, gloss; make skin comfort bright and clean, the protected and reparation to the damage of hair cutin.
Hyaluronate sodium, moisture-keeping function is hyaluronate sodium most important effect in cosmetics, and compared with other wetting agents, the relative humidity of surrounding is less on the impact of its moisture retention.Experiment shows, hyaluronate sodium hygroscopic capacity under low relative humidity (33%) is the highest, and the hygroscopic capacity under high relative humidity (75%) is minimum.Hyaluronate sodium is used alone as wetting agent is less, often and other wetting agents with the use of.Hyaluronate sodium belongs to high molecular polymer, has the strongest lubrication sense and film property.When skin care item containing hyaluronate sodium are smeared, substantially, feel is good in lubrication sense.After being applied to skin, thin film can be formed at skin surface, make skin produce good smooth feeling and moist feeling, skin is played a protective role.Hyaluronate sodium has the highest viscosity in aqueous, and its aqueous solution of 1% is gel, is added in cosmetics and can play thickening and Stabilization.
Pyrrolidone sodium carboxylate [Pyrrolidonecarboxylicacid-Na], chemical name is: 2-Pyrrolidone-5-carboxylic acid sodium, being a kind of natural moisture preserving agent with excellent moisture pick-up properties, the main composition as nature moisturizing factor [Natural Moisturizing Factor] is present in keratodermatitis in a large number.PCA-Na is increasingly subject to people as cosmetic humectant and pays close attention to, and applies more prevalent.The material playing moisture-keeping function in human body skin claims nature moisturizing factor (NMF), according to document introduction, NMF forms as follows substantially: other Organic substance 29.5% of aminoacid 40% 2-pyrrolidone-5-carboxylic acid 12% inorganic salts (Na, K, Ca, Mg) 18.5% is in the composition of NMF, PCA-Na occupies very important status, experiment proves, from epidermis, take out NMF will promote hardness physically, giving PCA-Na, then can to strengthen it flexible and elastic, therefore, PCA-Na plays the maincenter function effect of NMF.PCA-Na development at home and use start from the nineties, and it is a kind of novel wetting agent, its performance of keeping humidity highly significant, good more than glycerol, sorbitol, propylene glycol.
Glycine betaine, it it is a kind of alkaline matter, there is strong moisture pick-up properties, being widely used in middle-and-high-ranking shampoo, bath foam, handwashing liquid, foam cleanser etc. and the preparation of household detergent is a kind of excellent softening amendment in hair care and skin care formula, also act as detergent, wetting agent, thickening agent, antistatic additive and antibacterial etc., it is the amphoteric surfactant of and gentleness, non-stimulated, without anaphylactic reaction to skin, eye mucosa.
1,2-pentanediol, is a kind of water white oily liquids, all has good moistening effect to skin.The growth of microorganism can be suppressed, improve antibacterial ability, reduce the consumption of preservative, make product safer, gentle, be widely used in cosmetic material.In addition, it also has the effect of solubilising, can strengthen the water-resistance of sunscreen formulas, have good skinfeel.
Hydrolysis pyrenomycetes (SCLEROTIUM ROLFSSII) glue, is a kind of stabilizer and thickening agent, is typically rendered as gel, it is a kind of polysaccharide, can be used for reducing the ratio of oil in formula, have and releive and the innate efficacy of glabrous skin, it is also possible in hair care product, be used as conditioner.Scleroglucan can help emulsion-stabilizing and control viscosity.It is also prevented from pigment separated in cosmetics.It is typically considered a kind of composition that is natural and that releive, not studies have found that the adverse side effect relevant with this composition.
Glycyrrhizic acid dipotassium, glycyrrhizic acid dipotassium is white or off-white color fine powder, and purity reaches 98%, has a special sweet taste, water-soluble good, mouthfeel is pure.Glycyrrhizic acid dipotassium has the multiple efficacies such as antibacterial, antiinflammatory, removing toxic substances, antiallergic, deodorization.It is widely used in the industry such as medicine, cosmetics daily use chemicals, food.It can neutralize or lower the noxious substance of cosmetics, it is also possible to the anaphylaxis of the cosmetics prevented, and is particularly suited for senior hair or in cosmetics.
PPG-26-butylol polyether-26, Main Function is exactly to promote two kinds of immiscible liquid to form stabilized emulsion, when it is dispersed in the surface of dispersate, form thin film or electric double layer, dispersion phase can be made with electric charge, the droplet of dispersion phase thus can be stoped to condense mutually, the emulsion making formation is more stable, thus extends the shelf-life of cosmetics.
Cremophor RH40, is a kind of conventional efficient solubilizing agents, can be evenly dispersed in water by the oily matter such as essence, quintessence oil, forms stable, transparent solution.
Methyl hydroxybenzoate, also known as methyl parahydroxybenzoate.Methylparaben.Present white crystalline powder or colourless crystallization, be soluble in alcohol, ether and acetone, atomic be dissolved in water, be mainly used as organic synthesis, food, cosmetics, the sterilization antiseptic of medicine.Maximum limit consumption is 0.4%, and usage amount in the present invention is less than 0.1%.
Bis(hydroxymethyl)imidazolidinyl urea, is generally used as cosmetics preservative, almost can with cosmetics all component interworkings, to skin avirulence, without allergy, nonirritant.Maximum limit consumption is 0.5%, and usage amount in the present invention is less than 0.1%.
Iodine propilolic alcohol butyl mephenesin Carbamate, is a kind of novel cosmetic preservative, has good fungistatic effect, and have preferable dissolubility in surfactant, emulsifying agent, polar solvent, be therefore widely used in resident class and drip washing class cosmetic formulations.Maximum limit consumption is 0.05%, and the usage amount in basis is less than 0.01%.
Essence, is the imitation fruit by synthetic and the concentration aromatic oil of natural perfume material abnormal smells from the patient, is a kind of artificial perfume, be used for manufacturing food, cosmetics.Play the effect of aromatic.
Egg shell membrane extract, is with eggshell membrane as raw material, utilizes biological high-tech technology that eggshell membrane carries out biofermentation, biodegradation, bio-separation, concentration, finally carries out being spray-dried the powdered substance prepared, and this powdered substance is referred to as bioactive peptide；The pure physical method membrance separation extractive technique used because of it, thus ensure that its biological activity, and the molecular weight of this small active peptides all controls, between 300-2000 dalton, have rigorous scientific basis, epidermis entrance skin cell can be directed through and repair；And absorption efficiency is exceedingly fast, excellent.Eggshell membrane medical book in ancient times is referred to as " Membrana Follicularis ovi "
, it is used for treating the diseases such as decubital ulcer, brothers' body addiction, scald, celostomia, and can directly spread on face and carry out whitening reparation.Today, scientific research finds that eggshell membrane is a kind of fiber plasma membrane being wrapped in outside ovalbumin, is the organic fiber net being made up of tough and tensile keratin (keratin) etc..Eggshell membrane contains the protein of more than 90%, liposome about 3%, polysaccharide about 2%.Its protein mainly has keratin, collagen protein, albumin；Polysaccharide is based on chondroitin sulfate, hyaluronic acid.There is natural whitening, moisturizing, the skin-care effect of reparation.
Compared with prior art, the invention has the beneficial effects as follows:
Present component is chosen proper, and collocation rationally, so that the effective ingredient of various interpolation is coordinated mutually, promotes the absorption of various effective ingredient, plays the effect of various effective ingredient fully, produces the good result of anticipation.The egg shell membrane extract that the present invention selects, has production technology and scientific basis scrupulously, combines non-stimulated and be composited the raw material that human body is useful.
1, downright bad skin can be repaired, regenerate by the present invention effectively.
2, the present invention can clear up cell and the rubbish in blood, dispelling stain effectively, removes dark yellow, recovers skin ruddy.
3, the present invention can effectively slow down the cutis laxa and facial wrinkles caused due to human senility.
4, the present invention can effectively supplement the moisture that skin is lacked, and can be good at pinning moisture and make skin beauty water tender smooth, distributes the expression of skin natural health.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, broadly fall into the scope of protection of the invention.
Embodiment 1
Weigh raw material by weight: egg shell membrane extract: 1 part, glycerol: 5 parts, butanediol: 5 parts, diglycerol: 4 parts, polyglutamic acid sodium: 5 parts, hyaluronate sodium: 6 parts, pyrrolidone sodium carboxylate: 4 parts, glycine betaine: 5 parts, 1, 2-pentanediol: 6 parts, hydrolysis pyrenomycetes (SCLEROTIUM ROLFSSII) glue: 2 parts, glycyrrhizic acid dipotassium: 0.5 part, PPG-26-butylol polyether-26:0.7 part, Cremophor RH40: 0.7 part, methyl hydroxybenzoate: 0.1 part, Bis(hydroxymethyl)imidazolidinyl urea: 0.1 part, iodine propilolic alcohol butyl mephenesin Carbamate: 0.1 part, essence: 0.5 part；Water adds to 1000 parts, is the total amount of above-mentioned all the components and the difference of 1000 parts.
Described egg shell membrane extract is powder.
Described wet concentration is from deionized water.
1) glycerol, butanediol, diglycerol, egg shell membrane extract, methyl hydroxybenzoate, hydrolysis pyrenomycetes (SCLEROTIUM ROLFSSII) glue, glycine betaine with water, are mixed together dissolving and obtain A liquid；
2) polyglutamic acid sodium, hyaluronate sodium, pyrrolidone sodium carboxylate, 1,2-pentanediol, glycyrrhizic acid dipotassium, PPG-26-butylol polyether-26, essence, Cremophor RH40, Bis(hydroxymethyl)imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate are mixed together and obtain B liquid；
3) A liquid is put in main cooker, be warming up to 75 DEG C and stir；Employing blender stirs, and mixing speed is 1000rpm, and the time is 20 minutes.
4) it is cooled to the A liquid stirred when 45 DEG C add B liquid, after stirring, filters discharging；Employing blender stirs, and mixing speed is 1000rpm, and the time is 10 minutes.
5) by face paper 4) feed liquid of gained is soaked, take out, packaging.
Embodiment 2
Weigh raw material by weight: egg shell membrane extract: 2 parts, glycerol: 15 parts, butanediol: 35 parts, diglycerol: 15 parts, polyglutamic acid sodium: 7 parts, hyaluronate sodium: 8 parts, pyrrolidone sodium carboxylate: 7 parts, glycine betaine: 8 parts, 1, 2-pentanediol: 12 parts, hydrolysis pyrenomycetes (SCLEROTIUM ROLFSSII) glue: 7 parts, glycyrrhizic acid dipotassium: 3 parts, PPG-26-butylol polyether-26:3 part, Cremophor RH40: 6 parts, methyl hydroxybenzoate: 0.7 part, Bis(hydroxymethyl)imidazolidinyl urea: 0.6 part, iodine propilolic alcohol butyl mephenesin Carbamate: 0.15 part, essence: 1.5 parts；Water adds to 1000 parts, is the total amount of above-mentioned all the components and the difference of 1000 parts.
Described egg shell membrane extract is powder.
Described wet concentration is from purified water.
1) glycerol, butanediol, diglycerol, egg shell membrane extract, methyl hydroxybenzoate, hydrolysis pyrenomycetes (SCLEROTIUM ROLFSSII) glue, glycine betaine with water, are mixed together dissolving and obtain A liquid；
2) polyglutamic acid sodium, hyaluronate sodium, pyrrolidone sodium carboxylate, 1,2-pentanediol, glycyrrhizic acid dipotassium, PPG-26-butylol polyether-26, essence, Cremophor RH40, Bis(hydroxymethyl)imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate are mixed together and obtain B liquid；
3) A liquid is put in main cooker, be warming up to 75 DEG C and stir；Employing blender stirs, and mixing speed is 1500rpm, and the time is 15 minutes.
4) it is cooled to the A liquid stirred when 45 DEG C add B liquid, after stirring, filters discharging；Employing blender stirs, and mixing speed is 1500rpm, and the time is 15 minutes.
5) by face paper 4) feed liquid of gained is soaked, take out, packaging.
Embodiment 3
Weigh raw material by weight: egg shell membrane extract: 3 parts, glycerol: 30 parts, butanediol: 50 parts, diglycerol: 20 parts, polyglutamic acid sodium: 8 parts, hyaluronate sodium: 10 parts, pyrrolidone sodium carboxylate: 8 parts, glycine betaine: 10 parts, 1, 2-pentanediol: 15 parts, hydrolysis pyrenomycetes (SCLEROTIUM ROLFSSII) glue: 9 parts, glycyrrhizic acid dipotassium: 5 parts, PPG-26-butylol polyether-26:5 part, Cremophor RH40: 8 parts, methyl hydroxybenzoate: 1 part, Bis(hydroxymethyl)imidazolidinyl urea: 1 part, iodine propilolic alcohol butyl mephenesin Carbamate: 0.2 part, essence: 2 parts；Water adds to 1000 parts, is the total amount of above-mentioned all the components and the difference of 1000 parts.
Described egg shell membrane extract is powder.
Described wet concentration is from distilled water.
1) glycerol, butanediol, diglycerol, egg shell membrane extract, methyl hydroxybenzoate, hydrolysis pyrenomycetes (SCLEROTIUM ROLFSSII) glue, glycine betaine with water, are mixed together dissolving and obtain A liquid；
2) polyglutamic acid sodium, hyaluronate sodium, pyrrolidone sodium carboxylate, 1,2-pentanediol, glycyrrhizic acid dipotassium, PPG-26-butylol polyether-26, essence, Cremophor RH40, Bis(hydroxymethyl)imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate are mixed together and obtain B liquid；
3) A liquid is put in main cooker, be warming up to 75 DEG C and stir；Using homogenizer, mixing speed is 10000rpm, and batch (-type) is carried out 4 times, and each time is 8 seconds.
4) it is cooled to the A liquid stirred when 45 DEG C add B liquid, after stirring, filters discharging；Using homogenizer, mixing speed is 10000rpm, and batch (-type) is carried out 4 times, and each time is 5 seconds.
5) by face paper 4) feed liquid of gained is soaked, take out, packaging.
Embodiment 4
Weigh raw material by weight: egg shell membrane extract: 5 parts, glycerol: 5 parts, butanediol: 35 parts, diglycerol: 20 parts, polyglutamic acid sodium: 7 parts, hyaluronate sodium: 6 parts, pyrrolidone sodium carboxylate: 7 parts, glycine betaine: 10 parts, 1, 2-pentanediol: 12 parts, hydrolysis pyrenomycetes (SCLEROTIUM ROLFSSII) glue: 2 parts, glycyrrhizic acid dipotassium: 5 parts, PPG-26-butylol polyether-26:3 part, Cremophor RH40: 0.7 part, methyl hydroxybenzoate: 0.7 part, Bis(hydroxymethyl)imidazolidinyl urea: 1 part, iodine propilolic alcohol butyl mephenesin Carbamate: 0.15 part, essence: 0.5 part；Water adds to 1000 parts, is the total amount of above-mentioned all the components and the difference of 1000 parts.
Described egg shell membrane extract is powder.
Described wet concentration is from purified water.
1) glycerol, butanediol, diglycerol, egg shell membrane extract, methyl hydroxybenzoate, hydrolysis pyrenomycetes (SCLEROTIUM ROLFSSII) glue, glycine betaine with water, are mixed together dissolving and obtain A liquid；
2) polyglutamic acid sodium, hyaluronate sodium, pyrrolidone sodium carboxylate, 1,2-pentanediol, glycyrrhizic acid dipotassium, PPG-26-butylol polyether-26, essence, Cremophor RH40, Bis(hydroxymethyl)imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate are mixed together and obtain B liquid；
3) A liquid is put in main cooker, be warming up to 75 DEG C and stir；Using homogenizer, mixing speed is 15000rpm, and batch (-type) is carried out 5 times, and each time is 7 seconds.
4) it is cooled to the A liquid stirred when 45 DEG C add B liquid, after stirring, filters discharging；Using homogenizer, mixing speed is 15000rpm, and batch (-type) is carried out 5 times, and each time is 7 seconds.
5) by face paper 4) feed liquid of gained is soaked, take out, packaging.
The present invention can remove face rubbish, improves the colour of skin, keeps face moistening, moisturizing lock water；In the present invention, distinctive eggshell membrane bioactive peptide can be directed through epidermis and enter corium, repairs impaired cell, promotes cell regeneration, and can clear up cell and the rubbish in blood, keeps face beautiful ruddy, not stimulates skin, allergy and injury.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and without departing from the spirit or essential characteristics of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter from the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is limited by claims rather than described above, it is intended that all changes fallen in the implication of equivalency and scope of claim included in the present invention.
In addition, it is to be understood that, although this specification is been described by according to embodiment, but the most each embodiment only comprises an independent technical scheme, this narrating mode of description is only for clarity sake, description should can also be formed, through appropriately combined, other embodiments that it will be appreciated by those skilled in the art that as an entirety, the technical scheme in each embodiment by those skilled in the art.
Claims (10)
- null1. eggshell membrane bioactive peptide silk mask，It is characterized in that，The liquid infiltration being made up of following raw material prepares in face paper: egg shell membrane extract: 0.5-30 part，Glycerol: 5-30 part，Butanediol: 5-50 part，Diglycerol: 4-20 part，Polyglutamic acid sodium: 5-8 part，Hyaluronate sodium: 6-10 part，Pyrrolidone sodium carboxylate: 4-8 part，Glycine betaine: 5-10 part，1,2-pentanediol: 6-15 part，Hydrolysis Scleroglucan: 2-9 part，Glycyrrhizic acid dipotassium: 0.5-5 part，PPG-26-butylol polyether-26:0.7-5 part，Cremophor RH40: 0.7-8 part，Methyl hydroxybenzoate: 0.1-1 part，Bis(hydroxymethyl)imidazolidinyl urea: 0.1-1 part，Iodine propilolic alcohol butyl mephenesin Carbamate: 0.1-0.2 part，Essence: 0.5-2 part，Surplus is water，And the total weight parts of all raw materials is 1000 parts.
- Eggshell membrane bioactive peptide silk mask the most according to claim 1, it is characterised in that described egg shell membrane extract be molecular weight control 300-2000Da, aqueous solution surface tension at the powder of 34-36mN/m.
- Eggshell membrane bioactive peptide silk mask the most according to claim 1, it is characterised in that described wet concentration is from deionized water, distilled water or purified water.
- Eggshell membrane bioactive peptide silk mask the most according to claim 1, it is characterised in that the material of described face paper is silkworm silk or fruit fiber.
- Eggshell membrane bioactive peptide silk mask the most according to claim 1, it is characterised in that described egg shell membrane extract is the micromolecule polypeptide using biofermentation, biodegradation, bio-separation, high-new membrane technology to be refined into by eggshell membrane.
- Eggshell membrane bioactive peptide silk mask the most according to claim 1, it is characterized in that, the composition of described egg shell membrane extract includes: collagen protein, keratin, albumin, sialoglycoprotein, chondroitin sulfate, hyaluronic acid, lysozyme, somatomedin, trace element.
- 7. the preparation method of the eggshell membrane bioactive peptide silk mask as described in claim 1-6 is arbitrary, it is characterised in that comprise the steps:1) glycerol, butanediol, diglycerol, egg shell membrane extract, methyl hydroxybenzoate, hydrolysis Scleroglucan, glycine betaine are obtained A liquid with water mixed dissolution；2) polyglutamic acid sodium, hyaluronate sodium, pyrrolidone sodium carboxylate, 1,2-pentanediol, glycyrrhizic acid dipotassium, PPG-26-butylol polyether-26, essence, Cremophor RH40, Bis(hydroxymethyl)imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate are mixed to get B liquid；3) A liquid is put in main cooker, be warming up to 75 DEG C and stir；4) it is cooled to the A liquid stirred when 45 DEG C add B liquid, after stirring, filters discharging；5) by face paper 4) feed liquid of gained is soaked, take out, packaging.
- The preparation method of eggshell membrane bioactive peptide silk mask the most according to claim 7, it is characterised in that the equipment used during the stirring of described step step 3) and step 4) is blender or homogenizer.
- The preparation method of eggshell membrane bioactive peptide silk mask the most according to claim 8, it is characterised in that when using blender, speed is 1000-2000rpm, and the time is 10-20 minute.
- The preparation method of eggshell membrane bioactive peptide silk mask the most according to claim 8, it is characterised in that when using homogenizer, speed is 10000-20000rpm, and batch (-type) is carried out 4-5 time, and each time is the 5-8 second.
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| CN106860231A (en) * | 2017-01-18 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment antiallergic mask |
| CN108619059A (en) * | 2018-07-06 | 2018-10-09 | 广州英桐生物科技有限公司 | A kind of bright face Face-protecting mask liquid and preparation method thereof |
| CN108852992A (en) * | 2018-08-10 | 2018-11-23 | 武汉乐神三宝蜂业有限公司 | Crease-resistant face cleaning honey of compound royal jelly and preparation method thereof |
| CN112336680A (en) * | 2020-11-27 | 2021-02-09 | 奥克斯路株式会社 | Egg shell membrane fermentation liquor with functions of resisting aging and free radical damage and preparation method thereof |
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| CN101805773A (en) * | 2010-03-25 | 2010-08-18 | 淮安鸿玛生物科技有限公司 | Method for producing egg membrane protein |
| CN104940090A (en) * | 2015-07-17 | 2015-09-30 | 东莞市发达服饰有限公司 | Chlorella silk mask for eliminating the turbid, beautifying skin and repairing radiation damage |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR20090110996A (en) * | 2008-04-21 | 2009-10-26 | 주식회사 케이피엠테크 | Mask pack |
| CN101805773A (en) * | 2010-03-25 | 2010-08-18 | 淮安鸿玛生物科技有限公司 | Method for producing egg membrane protein |
| CN104940090A (en) * | 2015-07-17 | 2015-09-30 | 东莞市发达服饰有限公司 | Chlorella silk mask for eliminating the turbid, beautifying skin and repairing radiation damage |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106860231A (en) * | 2017-01-18 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment antiallergic mask |
| CN108619059A (en) * | 2018-07-06 | 2018-10-09 | 广州英桐生物科技有限公司 | A kind of bright face Face-protecting mask liquid and preparation method thereof |
| CN108619059B (en) * | 2018-07-06 | 2021-03-30 | 广州英桐生物科技有限公司 | Brightening and repairing mask liquid and preparation method thereof |
| CN108852992A (en) * | 2018-08-10 | 2018-11-23 | 武汉乐神三宝蜂业有限公司 | Crease-resistant face cleaning honey of compound royal jelly and preparation method thereof |
| CN112336680A (en) * | 2020-11-27 | 2021-02-09 | 奥克斯路株式会社 | Egg shell membrane fermentation liquor with functions of resisting aging and free radical damage and preparation method thereof |
| CN112336680B (en) * | 2020-11-27 | 2022-12-13 | 奥克斯路株式会社 | Egg shell membrane fermentation liquor with functions of resisting aging and free radical damage and preparation method thereof |
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| CN105919909B (en) | 2020-06-05 |
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