CN107418708A - A kind of method that oil of sea cucumber is extracted in the internal organ from sea cucumber - Google Patents
A kind of method that oil of sea cucumber is extracted in the internal organ from sea cucumber Download PDFInfo
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- CN107418708A CN107418708A CN201710749544.1A CN201710749544A CN107418708A CN 107418708 A CN107418708 A CN 107418708A CN 201710749544 A CN201710749544 A CN 201710749544A CN 107418708 A CN107418708 A CN 107418708A
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- sea cucumber
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/025—Pretreatment by enzymes or microorganisms, living or dead
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/104—Production of fats or fatty oils from raw materials by extracting using super critical gases or vapours
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
- Peptides Or Proteins (AREA)
Abstract
The invention discloses a kind of method that oil of sea cucumber is extracted in internal organ from sea cucumber, it passes through the following steps：（I）Take new fresh sea cucumber internal organ to clean, drain, stripping and slicing；（II）The fragment heating stirring that step I is obtained is added water into mixing；（III）Ethanol, food grade kieselguhr are added in the mixture that step II is obtained, sodium carbonate is added after adding Papain enzyme fermentation；（IV）The mixture obtained in step III is vacuumized under agitation；（V）The mixture obtained in step III is evaporated under reduced pressure, freeze-drying；（VI）The sea cucumber lyophilized products that step IV is obtained carry out carbon dioxide supercritical extraction, obtain sea cucumber oily product.The method rational technology of the present invention, operation is feasible, and the low oil of sea cucumber of histamine content can efficiently be made, and takes full advantage of the rejectable waste of processing sea cucumber, adds value-added content of product, avoids waste.
Description
Technical field
It is especially a kind of to extract oil of sea cucumber from sea cucumber internal organ the present invention relates to the method that fatty material is extracted from waste material
Method.
Background technology
Sea cucumber, belong to Holothuroidea（Holothuroidea）, it is the ocean echinoderm to 8000 meters by the sea that lives, it is
Using seabed algae and planktonic organism as food.Sea cucumber whole body covers with corn, is not only the food of preciousness, and rare medicinal material.According to
《A Supplement to the Compendium of Materia Medica》Described in：Sea cucumber, sweet-salty, kidney tonifying, benefiting quintessence take the photograph urine, and impotence, its warm-natured benefit, sufficient enemy are treated in establishing-Yang
Ginseng, therefore named sea cucumber.Sea cucumber have improve memory, delay sexual gland aging, prevent artery sclerosis and it is antitumor wait act on.With
Sea cucumber is worth the popularization of knowledge, and sea cucumber progresses into common people's dining table.
In recent years, developing sea cucumber extract health products turns into people field interested.Contain abundant phosphorus in oil of sea cucumber
The nutritional ingredients such as fat, unrighted acid, there is good meal supplement to act on for the elderly and women.However, traditional sea
Ginseng oil is often due to bring serious seafood allergy containing histamine so that a large amount of crowds can not take.And traditional sea
Ginseng oil often extracts from sea cucumber, and the sea cucumber after extraction oil of sea cucumber is difficult to secondary operation use.At the same time, sea cucumber internal organ exist
Typically it is dropped in process or as feed, fertilizers for potted flowers, brings serious waste.Therefore, it is further to sea cucumber internal organ
It is a urgent problem to be solved to be processed into the high product of added value.
The content of the invention
For overcome the deficiencies in the prior art, it is an object of the invention to provide a kind of rational technology, operation are feasible, additional
Value is high, the method that oil of sea cucumber is extracted from sea cucumber internal organ at histamine content bottom.
The technical solution adopted for the present invention to solve the technical problems is：The side of oil of sea cucumber is extracted in a kind of internal organ from sea cucumber
Method, it is characterised in that：It passes through the following steps：
（I）New fresh sea cucumber internal organ are chosen, cleans, drains, and be cut into 5-10 mm fragment；
（II）By the fragment that step I is obtained in 90-100 degrees Celsius of lower heating stirring 10-20 minute, and with 1-1.5 times of weight
Water mixing；
（III）Ethanol 80-120 parts by weight, food grade kieselguhr are added in the mixture that the step II of 10000 parts by weight is obtained
400-700 parts by weight, add papain and reach 4000-6000 U/mL, and fermentation 4-12 is small under 40-45 degrees Celsius
When, and add sodium carbonate 200-400 parts by weight；
（IV）The mixture obtained in step III is evacuated to 0.1-0.3 atmospheric pressure under agitation, is kept for 10-15 minutes；
（V）The mixture obtained in step III is evaporated under reduced pressure, and is further freeze-dried, under 0.1-0.05 atmospheric pressure
Vacuumize and kept for 30-60 minutes；
（VI）The sea cucumber lyophilized products that step IV is obtained carry out carbon dioxide supercritical extraction, obtain sea cucumber oily product.
In currently preferred aspect, in described step I, described sea cucumber internal organ are spent for sea cucumber.
In currently preferred aspect, in described step II, described fragment is in 95 degrees Celsius of lower heating stirrings 14
Minute, and mixed with the water of 1.2 times of weight.
In currently preferred aspect, in described step III, in the mixing that the step II of 10000 parts by weight is obtained
The parts by weight of ethanol 105 are added in thing, the parts by weight of food grade kieselguhr 600, papain is added and reaches 5500 U/mL, and
Fermented 10 hours under 42 degrees Celsius, and add the parts by weight of sodium carbonate 300.
In currently preferred aspect, in described step III, after sodium carbonate is added, 40-120 weights are additionally added
Measure the ammonium carbonate of part.
In currently preferred aspect, in described step IV, the mixture obtained in step III is taken out under agitation
Vacuum is kept for 12 minutes to 0.12 atmospheric pressure.
In currently preferred aspect, in described step IV, ultrasound also is carried out to mixture while vacuumizing
Processing.
In currently preferred aspect, in described step VI, extracting pressure is 25-35 Mpa, and temperature is taken the photograph for 37-45
Family name's degree, extraction time are 1.5-3 hours.
The present invention is to choose new fresh sea cucumber internal organ cleaning, chopping；Water mixing is added after fragment heating stirring, adds second
Alcohol, food grade kieselguhr, sodium carbonate is added after adding Papain enzyme fermentation；Mixture vacuumizes under agitation, is evaporated under reduced pressure,
Freeze-drying, lyophilized products carry out carbon dioxide supercritical extraction, obtain sea cucumber oily product.The method rational technology of the present invention, behaviour
Make feasible, can efficiently prepare oil of sea cucumber, resulting oil of sea cucumber has relatively low histamine content, therefore is adapted to seafood allergy
Crowd take.The method of the present invention is raw material using sea cucumber internal organ, takes full advantage of the rejectable waste of processing sea cucumber, adds
Value-added content of product, avoid waste.
Embodiment
With reference to embodiment, the present invention will be further described.
Unless additionally illustrating, the sea cucumber internal organ that this implementation uses are sea cucumber flower, and sea cucumber flower is collected from the application
The cucumber product workshop of people, i.e. freezing collection is standby after collection for it.
Unless additionally illustrating, the papain in the present embodiment is purchased from Dong Henghua roads bio tech ltd, should
Kind of enzyme is 800,000 U/ grams of dry powder.When adding, add water that 100,000 U/mL enzyme solutions are made in the dry powder first, then incite somebody to action certain
The enzyme solutions of volume are added in enzymolysis mixture, reach the amount of expectation.
Embodiment 1
In the present embodiment, a kind of method that oil of sea cucumber is extracted in internal organ from sea cucumber, it passes through the following steps：
（I）New fresh sea cucumber internal organ are chosen, is cleaned, is drained and be cut into 5-10 mm fragment；
（II）By the fragment that step I is obtained in 95 degrees Celsius of lower heating stirrings 14 minutes, and mixed with the water of 1.2 times of weight；
（III）The parts by weight of ethanol 105, food grade kieselguhr 600 are added in the mixture that the step II of 10000 parts by weight is obtained
Parts by weight, add papain and reach 5500 U/mL, and fermented 10 hours under 42 degrees Celsius, and add sodium carbonate
300 parts by weight；
（IV）The mixture obtained in step III is evacuated to 0.12 atmospheric pressure under agitation, kept for 12 minutes；
（V）The mixture obtained in step III is evaporated under reduced pressure, and is further freeze-dried, is taken out under 0.05 atmospheric pressure true
Sky is kept for 45 minutes；
（VI）The sea cucumber lyophilized products that step IV is obtained carry out carbon dioxide supercritical extraction, and extracting pressure is 28 Mpa, temperature
For 38 degrees Celsius, extraction time is 2 hours, obtains sea cucumber oily product.
Sea cucumber oil extract experiment is carried out using 10 kilograms of sea cucumbers in the present embodiment, the weight for finally giving oil product is
216 grams.
Embodiment 2
In the present embodiment, a kind of method that oil of sea cucumber is extracted in internal organ from sea cucumber, it passes through the following steps：
（I）New fresh sea cucumber internal organ are chosen, is cleaned, is drained and be cut into 5-10 mm fragment；
（II）By the fragment that step I is obtained in 90 degrees Celsius of lower heating stirrings 20 minutes, and mixed with the water of 1.5 times of weight；
（III）The parts by weight of ethanol 120, food grade kieselguhr 700 are added in the mixture that the step II of 10000 parts by weight is obtained
Parts by weight, add papain and reach 4000 U/mL, and fermented 4 hours under 45 degrees Celsius, and add sodium carbonate
400 parts by weight；
（IV）The mixture obtained in step III is evacuated to 0.3 atmospheric pressure under agitation, kept for 15 minutes；
（V）The mixture obtained in step III is evaporated under reduced pressure, and is further freeze-dried, is vacuumized under 0.1 atmospheric pressure
Kept for 60 minutes；
（VI）The sea cucumber lyophilized products that step IV is obtained carry out carbon dioxide supercritical extraction, and extracting pressure is 25 Mpa, temperature
For 45 degrees Celsius, extraction time is 1.5 hours, obtains sea cucumber oily product.
Sea cucumber oil extract experiment is carried out using 10 kilograms of sea cucumbers in the present embodiment, the weight for finally giving oil product is
187 grams.
Embodiment 3
In the present embodiment, a kind of method that oil of sea cucumber is extracted in internal organ from sea cucumber, it passes through the following steps：
（I）New fresh sea cucumber internal organ are chosen, is cleaned, is drained and be cut into 5-10 mm fragment；
（II）By the fragment that step I is obtained in 100 degrees Celsius of lower heating stirrings 10 minutes, and mixed with the water of 1 times of weight；
（III）The parts by weight of ethanol 80, food grade kieselguhr 400 are added in the mixture that the step II of 10000 parts by weight is obtained
Parts by weight, add papain and reach 6000 U/mL, and fermented 12 hours under 40 degrees Celsius, and add sodium carbonate
200 parts by weight；
（IV）The mixture obtained in step III is evacuated to 0.1 atmospheric pressure under agitation, kept for 10 minutes；
（V）The mixture obtained in step III is evaporated under reduced pressure, and is further freeze-dried, is taken out under 0.05 atmospheric pressure true
Sky is kept for 30 minutes；
（VI）The sea cucumber lyophilized products that step IV is obtained carry out carbon dioxide supercritical extraction, and extracting pressure is 35 Mpa, temperature
For 37 degrees Celsius, extraction time is 3 hours, obtains sea cucumber oily product.
Sea cucumber oil extract experiment is carried out using 10 kilograms of sea cucumbers in the present embodiment, the weight for finally giving oil product is
194 grams.
Embodiment 4
The step of the present embodiment, is substantially the same manner as Example 1, and difference is also to carry out ultrasound to mixture while vacuumizing
Processing.Sea cucumber oil extract experiment is carried out using 10 kilograms of sea cucumbers in the present embodiment, the weight for finally giving oil product is 205
Gram.
Embodiment 5
The step of the present embodiment, is substantially the same manner as Example 1, distinguishes in described step III, add sodium carbonate it
Afterwards, it is additionally added the ammonium carbonate of 120 parts by weight.Sea cucumber oil extract experiment is carried out using 10 kilograms of sea cucumbers in the present embodiment, it is final to obtain
Weight to oil product is 219 grams.
Embodiment 6
The step of the present embodiment, is substantially the same manner as Example 1, distinguishes in described step III, add sodium carbonate it
Afterwards, it is additionally added the ammonium carbonate of 40 parts by weight.Sea cucumber oil extract experiment is carried out using 10 kilograms of sea cucumbers in the present embodiment, is finally given
The weight of oil product is 212 grams.
Embodiment 7
The step of the present embodiment, is substantially the same manner as Example 1, distinguishes in described step III, add sodium carbonate it
Afterwards, it is additionally added the ammonium carbonate of 70 parts by weight.Sea cucumber oil extract experiment is carried out using 10 kilograms of sea cucumbers in the present embodiment, is finally given
The weight of oil product is 203 grams.
Comparative example 1
The step of the present embodiment, is substantially the same manner as Example 1, and difference is not perform step III.10,000 are used in the present embodiment
Gram sea cucumber carries out sea cucumber oil extract experiment, and the weight for finally giving oil product is 186 grams.
Comparative example 2
The step of the present embodiment, is substantially the same manner as Example 1, and difference is not perform step IV-V, is depressurized after step III
Evaporation, is freeze-dried and carries out step VI.Sea cucumber oil extract experiment is carried out using 10 kilograms of sea cucumbers in the present embodiment, it is final to obtain
Weight to oil product is 192 grams.
Comparative example 3
The step of the present embodiment, is substantially the same manner as Example 1, difference be not perform step II-V, by fragment at 95 degrees Celsius
Lower heating stirring is evaporated under reduced pressure after 14 minutes, is freeze-dried and carries out step VI.Entered in the present embodiment using 10 kilograms of sea cucumbers
Row sea cucumber oil extract is tested, and the weight for finally giving oil product is 201 grams.
First, histamine content is tested
This experiment is before and after fermentation test, measures the histamine content in baste using HPLC and internal standard method, as a result shows
Show in table 1.Wherein, histamine content is expressed as the milligram number of histamine in every kilogram of oil of sea cucumber.
Table 1：The content of histamine in embodiment 1-7 and comparative example 1-3 oil of sea cucumber, and the reduction relative to comparative example 3
Percentage.
| Group number | Histamine content（mg/kg） | Reduce percentage（%） |
| Embodiment 1 | 33.7 | 94.54 |
| Embodiment 2 | 39.4 | 93.62 |
| Embodiment 3 | 41.2 | 93.33 |
| Embodiment 4 | 27.0 | 95.63 |
| Embodiment 5 | 8.1 | 98.69 |
| Embodiment 6 | 11.5 | 98.14 |
| Embodiment 7 | 7.5 | 98.79 |
| Comparative example 1 | 417.5 | 32.39 |
| Comparative example 2 | 628.1 | -1.72 |
| Comparative example 3 | 617.5 | ---- |
It can see from the data of table 1, after it have passed through the processing of method of the present invention, the histamine content in oil of sea cucumber is significantly
Reduce, well below European Food standard（400 mg/kg）.Wherein, the histamine content of embodiment 1 is significantly lower than embodiment 2-3.
After ultrasound treatment step is added, histamine content reduce further（Embodiment 4）.It is real after ammonium carbonate is added
Apply a 5-7 and show that highest histamine goes division result.Find simultaneously, its reducing effect when adding the ammonium carbonate of 70 parts by weight
It has been substantially saturated.
2nd, hypersensitive test
20 subjects for there are allergies to seafood have been recruited, oral examination has been carried out to the oil of sea cucumber of embodiments herein 1,7
Test.Every group of 10 subjects, every group of subject take oil of sea cucumber 100mg in the morning, at night respectively, taken 3 days respectively.Embodiment
1 subject only has 1 patient's report to have slight allergy and fash phenomenon.Whole subjects of embodiment 7 do not have reported allergenic
Phenomenon.
Claims (8)
1. the method for oil of sea cucumber is extracted in a kind of internal organ from sea cucumber, it is characterised in that：It passes through the following steps：
（I）New fresh sea cucumber internal organ are chosen, cleans, drains, and be cut into 5-10 mm fragment；
（II）By the fragment that step I is obtained in 90-100 degrees Celsius of lower heating stirring 10-20 minute, and with 1-1.5 times of weight
Water mixing；
（III）Ethanol 80-120 parts by weight, food grade kieselguhr are added in the mixture that the step II of 10000 parts by weight is obtained
400-700 parts by weight, add papain and reach 4000-6000 U/mL, and fermentation 4-12 is small under 40-45 degrees Celsius
When, and add sodium carbonate 200-400 parts by weight；
（IV）The mixture obtained in step III is evacuated to 0.1-0.3 atmospheric pressure under agitation, is kept for 10-15 minutes；
（V）The mixture obtained in step III is evaporated under reduced pressure, and is further freeze-dried, under 0.1-0.05 atmospheric pressure
Vacuumize and kept for 30-60 minutes；
（VI）The sea cucumber lyophilized products that step IV is obtained carry out carbon dioxide supercritical extraction, obtain sea cucumber oily product.
2. the method for oil of sea cucumber is extracted in a kind of internal organ from sea cucumber according to claim 1, it is characterised in that：Described
In step I, described sea cucumber internal organ are spent for sea cucumber.
3. the method for oil of sea cucumber is extracted in a kind of internal organ from sea cucumber according to claim 1, it is characterised in that：Described
In step II, described fragment mixes in 95 degrees Celsius of lower heating stirrings 14 minutes with the water of 1.2 times of weight.
4. the method for oil of sea cucumber is extracted in a kind of internal organ from sea cucumber according to claim 1, it is characterised in that：Described
In step III, the parts by weight of ethanol 105, food grade kieselguhr are added in the mixture that the step II of 10000 parts by weight is obtained
600 parts by weight, add papain and reach 5500 U/mL, and fermented 10 hours under 42 degrees Celsius, and add carbonic acid
The parts by weight of sodium 300.
5. the method for oil of sea cucumber is extracted in a kind of internal organ from sea cucumber according to claim 1, it is characterised in that：Described
In step III, after sodium carbonate is added, the ammonium carbonate of 40-120 parts by weight is additionally added.
6. the method for oil of sea cucumber is extracted in a kind of internal organ from sea cucumber according to claim 1, it is characterised in that：Described
In step IV, the mixture obtained in step III is evacuated to 0.12 atmospheric pressure under agitation, kept for 12 minutes.
7. the method for oil of sea cucumber is extracted in a kind of internal organ from sea cucumber according to claim 1, it is characterised in that：Described
In step IV, also mixture is ultrasonically treated while vacuumizing.
8. the method for oil of sea cucumber is extracted in a kind of internal organ from sea cucumber according to claim 1, it is characterised in that：Described
In step VI, extracting pressure is 25-35 Mpa, and temperature is 37-45 degrees Celsius, and extraction time is 1.5-3 hours.
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| CN201710749544.1A CN107418708B (en) | 2017-08-28 | 2017-08-28 | Method for extracting sea cucumber oil from internal organs of sea cucumber |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107981357A (en) * | 2017-12-14 | 2018-05-04 | 荣成市飞创科技有限公司 | A kind of method that sea cucumber oil capsule is prepared using sea cucumber internal organ |
| CN111096457A (en) * | 2019-12-21 | 2020-05-05 | 池州市月亮湾生物科技有限公司 | Sea cucumber oil microcapsule powder and preparation method thereof |
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