CN105166939A - Tea seed polypeptide lozenge and preparation method therefor - Google Patents

Tea seed polypeptide lozenge and preparation method therefor Download PDF

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Publication number
CN105166939A
CN105166939A CN201510501527.7A CN201510501527A CN105166939A CN 105166939 A CN105166939 A CN 105166939A CN 201510501527 A CN201510501527 A CN 201510501527A CN 105166939 A CN105166939 A CN 105166939A
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CN
China
Prior art keywords
tea seeds
polypeptide
tea seed
parts
tea
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Pending
Application number
CN201510501527.7A
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Chinese (zh)
Inventor
魏星
陈伟
魏柱银
陈同铸
郝中存
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ANHUI HUAYIN CAMELLIA OIL Co Ltd
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ANHUI HUAYIN CAMELLIA OIL Co Ltd
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Priority to CN201510501527.7A priority Critical patent/CN105166939A/en
Publication of CN105166939A publication Critical patent/CN105166939A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J1/00Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
    • A23J1/001Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from waste materials, e.g. kitchen waste
    • A23J1/005Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from waste materials, e.g. kitchen waste from vegetable waste materials
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J3/00Working-up of proteins for foodstuffs
    • A23J3/14Vegetable proteins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J3/00Working-up of proteins for foodstuffs
    • A23J3/30Working-up of proteins for foodstuffs by hydrolysis
    • A23J3/32Working-up of proteins for foodstuffs by hydrolysis using chemical agents
    • A23J3/34Working-up of proteins for foodstuffs by hydrolysis using chemical agents using enzymes
    • A23J3/346Working-up of proteins for foodstuffs by hydrolysis using chemical agents using enzymes of vegetable proteins

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Medicinal Preparation (AREA)

Abstract

The invention discloses a tea seed polypeptide lozenge. The tea seed polypeptide lozenge is characterized in that the tea seed polypeptide lozenge is composed of the following raw materials, by weight, 1300-1500 parts of tea seed meal, 15-25 parts of xylitol, 20-30 parts of citric acid, 10-20 parts of mannitol, 300-350 parts of soluble sweet potato starch, 10-15 parts of carboxymethylcellulose sodium, 5-7 parts of magnesium stearate and a proper amount of neutral proteases. In the method, firstly, tea seed proteins are extracted from the tea seed meal, then the tea seed proteins are hydrolyzed to generate substances such as polypeptides, amino acids and the like, the utilization rate of tea seeds is raised, the economic benefit is raised, and the prepared polypeptide products have good functions of antioxidation, cholesterol reduction and the like are convenient to take and have good palatability.

Description

A kind of tea seeds polypeptide lozenge and preparation method thereof
Technical field
The invention belongs to food processing field, specifically a kind of tea seeds polypeptide lozenge and preparation method thereof.
Background technology
China is the native place of tealeaves, 2,500 ten thousand mu, existing tea place, and generally every mu can be produced tea seeds about 200Kg, and tea seeds is the fruit of tea tree, is the accessory substance of Tea Production.For a long time, people are not enough for the exploitation of tea seeds.Extract together except grease except minority tea seeds is mixed in camellia seed, major part is by incineration of waste or naturally come off, and rots in the ground, causes the waste of resource.How rounded tea seeds is or oval, and appearance is coarse, dry, matt, and color is comparatively dark, in ink black; Tea seeds benevolence is white or faint yellow.Without oily taste, bitter and puckery.Result of study is had to show: ripe tea seeds is made up of 23%-27% shell, 23%-27% kind shell and 43%-47% kind benevolence.Wherein plant benevolence and contain fat about 35%, starch about 20%, protein about 11%, saponin about 12%, lignin about 11%, ash content about 2%.
The leading products of current tea seeds are tea seed oils, are now confirmed as country-level edible oil by national departments concerned quality inspection, not only can for cooking and having good health care.Equally, tea seeds Hectometer nutritive value after tea seeds oil expression is also very high, tea seeds grouts are containing crude protein 11% ~ 16%, tea seeds albumen is rich in amino acid needed by human body, be of high nutritive value, at present domestic mainly carried out detoxification treatment (removal Tea Saponin) as gramineous crop feed protein, base acid and energy supplement, also as manufacture mixed feed basis, making fertilizer with it can be absorbed by plants effectively.The extraction of tea seeds albumen and functional Quality Research thereof are reported all less both at home and abroad, tea seeds cake protein has very high economic worth, can it can be used as and produce protein beverage, reconstituted food, the protein fortifier of bakery product and the protein raw materials as fermented products such as soy sauce.
Tea seeds albumen is under biological enzyme condition, hydrolysis generates the material such as polypeptide and amino acid, there is very high nutritive value and functional characteristic, the polypeptide produced after protein digestion except there is easily digested characteristic, also have very strong anti-oxidant, reduce the functional characteristics such as cholesterol.Therefore, carry out the research of tea seeds polypeptide health care functional activity is had important practical significance.
Summary of the invention
For solving the problems of the technologies described above, the object of this invention is to provide a kind of tea seeds polypeptide lozenge and preparation method thereof.
For achieving the above object, the technical solution used in the present invention is as follows:
A kind of tea seeds polypeptide lozenge, it is characterized in that, be made up of the raw material of following weight portion: tea seeds Hectometer 1300-1500, xylitol 15-25, citric acid 20-30, sweet mellow wine 10-20, solubility starch from sweet potato 300-350, sodium carboxymethylcellulose 10-15, dolomol 5-7, neutral proteinase are appropriate.
A preparation method for tea seeds polypeptide lozenge, is characterized in that, comprise the following steps:
(1) particle that granularity is 55-60 order size is ground into after tea seeds Hectometer being carried out ungrease treatment, then being sent to its weight 13-15 PH is doubly in the sodium hydroxide solution of 9-10, ultrasonic wave process 80-90min is carried out under the condition of temperature 45-50 DEG C, supersonic frequency is 35-40kHz, then centrifugal 30-35min under 3800-4000r/min, get supernatant, obtain protein extraction liquid;
(2) being 3.5 to obtaining adding in protein extraction liquid hydrochloric acid to the pH value of solution, leaving standstill after 20-30min centrifugal 20-30min under 3000-3500r/min, obtaining proteins precipitate, then carry out spraying dry, obtain tea seeds albumen powder;
(3) tea seeds albumen powder is broken into the particle of 75-85 order size, add water and make the suspension that concentration is 3%-3.5%, then 85-90 DEG C is heated to, 50-55 DEG C is cooled to after insulation 20-25min, regulate PH to be the neutral proteinase adding 4300-4500u/g after 7 by the weight portion of protein, go out after enzymolysis 4-4.5h enzyme, then centrifugal 15-20min under 3800-4200r/min, get supernatant and carry out desalting processing postlyophilization, obtain tea seeds polypeptide;
(4) tea seeds polypeptide, xylitol, citric acid, sweet mellow wine, solubility starch from sweet potato were pulverized 100 mesh sieves respectively, the water of 10% weight portion is added after mixing, stir be placed on 55-65 DEG C vacuum drying chamber in dry 120-140min, obtain polypeptide and mix soft material;
(5) polypeptide is mixed after soft material is pulverized and cross 12-16 mesh sieve, then add sodium carboxymethylcellulose, dolomol, after mixing, carry out compressing tablet, obtain described tea seeds polypeptide lozenge.
Beneficial effect of the present invention:
The present invention is by first extracting tea seeds albumen by tea seeds Hectometer, then under the effect of biology enzyme, hydrolysis generates the material such as polypeptide and amino acid, not only increase the utilization rate of tea seeds, add economic benefit, and obtained polypeptide products also have very strong anti-oxidant, reduce the functions such as cholesterol, there is the advantage such as taking convenience, good palatability.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further illustrated.
Embodiment:
A kind of tea seeds polypeptide lozenge of the present invention, it is characterized in that, be made up of the raw material of following weight portion (kg): tea seeds Hectometer 1400, xylitol 20, citric acid 25, sweet mellow wine 15, solubility starch from sweet potato 325, sodium carboxymethylcellulose 12.5, dolomol 6, neutral proteinase are appropriate.
A preparation method for tea seeds polypeptide lozenge, is characterized in that, comprise the following steps:
(1) particle that granularity is 55-60 order size is ground into after tea seeds Hectometer being carried out ungrease treatment, then being sent to its weight 13-15 PH is doubly in the sodium hydroxide solution of 9-10, ultrasonic wave process 80-90min is carried out under the condition of temperature 45-50 DEG C, supersonic frequency is 35-40kHz, then centrifugal 30-35min under 3800-4000r/min, get supernatant, obtain protein extraction liquid;
(2) being 3.5 to obtaining adding in protein extraction liquid hydrochloric acid to the pH value of solution, leaving standstill after 20-30min centrifugal 20-30min under 3000-3500r/min, obtaining proteins precipitate, then carry out spraying dry, obtain tea seeds albumen powder;
(3) tea seeds albumen powder is broken into the particle of 75-85 order size, add water and make the suspension that concentration is 3%-3.5%, then 85-90 DEG C is heated to, 50-55 DEG C is cooled to after insulation 20-25min, regulate PH to be the neutral proteinase adding 4300-4500u/g after 7 by the weight portion of protein, go out after enzymolysis 4-4.5h enzyme, then centrifugal 15-20min under 3800-4200r/min, get supernatant and carry out desalting processing postlyophilization, obtain tea seeds polypeptide;
(4) tea seeds polypeptide, xylitol, citric acid, sweet mellow wine, solubility starch from sweet potato were pulverized 100 mesh sieves respectively, the water of 10% weight portion is added after mixing, stir be placed on 55-65 DEG C vacuum drying chamber in dry 120-140min, obtain polypeptide and mix soft material;
(5) polypeptide is mixed after soft material is pulverized and cross 12-16 mesh sieve, then add sodium carboxymethylcellulose, dolomol, after mixing, carry out compressing tablet, obtain described tea seeds polypeptide lozenge.

Claims (2)

1. a tea seeds polypeptide lozenge, it is characterized in that, be made up of the raw material of following weight portion: tea seeds Hectometer 1300-1500, xylitol 15-25, citric acid 20-30, sweet mellow wine 10-20, solubility starch from sweet potato 300-350, sodium carboxymethylcellulose 10-15, dolomol 5-7, neutral proteinase are appropriate.
2. the preparation method of a kind of tea seeds polypeptide lozenge according to claim 1, is characterized in that, comprise the following steps:
(1) particle that granularity is 55-60 order size is ground into after tea seeds Hectometer being carried out ungrease treatment, then being sent to its weight 13-15 PH is doubly in the sodium hydroxide solution of 9-10, ultrasonic wave process 80-90min is carried out under the condition of temperature 45-50 DEG C, supersonic frequency is 35-40kHz, then centrifugal 30-35min under 3800-4000r/min, get supernatant, obtain protein extraction liquid;
(2) being 3.5 to obtaining adding in protein extraction liquid hydrochloric acid to the pH value of solution, leaving standstill after 20-30min centrifugal 20-30min under 3000-3500r/min, obtaining proteins precipitate, then carry out spraying dry, obtain tea seeds albumen powder;
(3) tea seeds albumen powder is broken into the particle of 75-85 order size, add water and make the suspension that concentration is 3%-3.5%, then 85-90 DEG C is heated to, 50-55 DEG C is cooled to after insulation 20-25min, regulate PH to be the neutral proteinase adding 4300-4500u/g after 7 by the weight portion of protein, go out after enzymolysis 4-4.5h enzyme, then centrifugal 15-20min under 3800-4200r/min, get supernatant and carry out desalting processing postlyophilization, obtain tea seeds polypeptide;
(4) tea seeds polypeptide, xylitol, citric acid, sweet mellow wine, solubility starch from sweet potato were pulverized 100 mesh sieves respectively, the water of 10% weight portion is added after mixing, stir be placed on 55-65 DEG C vacuum drying chamber in dry 120-140min, obtain polypeptide and mix soft material;
(5) polypeptide is mixed after soft material is pulverized and cross 12-16 mesh sieve, then add sodium carboxymethylcellulose, dolomol, after mixing, carry out compressing tablet, obtain described tea seeds polypeptide lozenge.
CN201510501527.7A 2015-08-17 2015-08-17 Tea seed polypeptide lozenge and preparation method therefor Pending CN105166939A (en)

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105476033A (en) * 2016-01-07 2016-04-13 安徽省华银茶油有限公司 High-dietary-fiber tea seed polypeptide lozenge and preparation method thereof
CN105476029A (en) * 2016-01-07 2016-04-13 安徽省华银茶油有限公司 Green tea flavor tea seed polypeptide buccal tablets with effects of replenishing qi and nourishing blood and preparing method of green tea flavor tea seed polypeptide buccal tablets
CN105982328A (en) * 2016-01-07 2016-10-05 安徽省华银茶油有限公司 Trepang nourishing tea leaf seed polypeptide lozenge and preparation method thereof
CN105982327A (en) * 2016-01-07 2016-10-05 安徽省华银茶油有限公司 Momordica grosvenori tea-seed polypeptide lozenges capable of clearing heat and moistening lung and production method thereof
CN105982326A (en) * 2016-01-07 2016-10-05 安徽省华银茶油有限公司 Cheese-flavored roselle anti-fatigue tea-seed polypeptide lozenges and production method thereof
CN105982325A (en) * 2016-01-07 2016-10-05 安徽省华银茶油有限公司 Chocolate-flavored tea seed polypeptide buccal tablet and preparation method thereof
CN105982324A (en) * 2016-01-07 2016-10-05 安徽省华银茶油有限公司 Tea seed polypeptide buccal tablet suitable for people suffering from high blood pressure, high blood fat and high blood glucose
CN105982330A (en) * 2016-01-07 2016-10-05 安徽省华银茶油有限公司 Mint-flavored tea-seed polypeptide lozenges rich in tea polyphenols and production method of mint-flavored tea-seed polypeptide lozenges
CN106281942A (en) * 2016-08-18 2017-01-04 安徽天乾健食品科技有限公司 A kind of tea-seed polypeptide health care pomegranate fruit vinegar beverage and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101228918A (en) * 2007-01-24 2008-07-30 西北农林科技大学 Method of preparing walnut polypeptide powder
CN103627765A (en) * 2013-11-29 2014-03-12 衢州刘家香食品有限公司 Preparation method for camellia seed polypeptide
CN103876146A (en) * 2014-04-01 2014-06-25 吉林大学 Rana japonica oil polypeptide lozenges and preparation method thereof
CN104177508A (en) * 2014-08-06 2014-12-03 南昌大学 Method for comprehensively extracting tea seed saponin, tea seed polypeptide and tea seed polysaccharide from tea seed cake

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101228918A (en) * 2007-01-24 2008-07-30 西北农林科技大学 Method of preparing walnut polypeptide powder
CN103627765A (en) * 2013-11-29 2014-03-12 衢州刘家香食品有限公司 Preparation method for camellia seed polypeptide
CN103876146A (en) * 2014-04-01 2014-06-25 吉林大学 Rana japonica oil polypeptide lozenges and preparation method thereof
CN104177508A (en) * 2014-08-06 2014-12-03 南昌大学 Method for comprehensively extracting tea seed saponin, tea seed polypeptide and tea seed polysaccharide from tea seed cake

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105476033A (en) * 2016-01-07 2016-04-13 安徽省华银茶油有限公司 High-dietary-fiber tea seed polypeptide lozenge and preparation method thereof
CN105476029A (en) * 2016-01-07 2016-04-13 安徽省华银茶油有限公司 Green tea flavor tea seed polypeptide buccal tablets with effects of replenishing qi and nourishing blood and preparing method of green tea flavor tea seed polypeptide buccal tablets
CN105982328A (en) * 2016-01-07 2016-10-05 安徽省华银茶油有限公司 Trepang nourishing tea leaf seed polypeptide lozenge and preparation method thereof
CN105982327A (en) * 2016-01-07 2016-10-05 安徽省华银茶油有限公司 Momordica grosvenori tea-seed polypeptide lozenges capable of clearing heat and moistening lung and production method thereof
CN105982326A (en) * 2016-01-07 2016-10-05 安徽省华银茶油有限公司 Cheese-flavored roselle anti-fatigue tea-seed polypeptide lozenges and production method thereof
CN105982325A (en) * 2016-01-07 2016-10-05 安徽省华银茶油有限公司 Chocolate-flavored tea seed polypeptide buccal tablet and preparation method thereof
CN105982324A (en) * 2016-01-07 2016-10-05 安徽省华银茶油有限公司 Tea seed polypeptide buccal tablet suitable for people suffering from high blood pressure, high blood fat and high blood glucose
CN105982330A (en) * 2016-01-07 2016-10-05 安徽省华银茶油有限公司 Mint-flavored tea-seed polypeptide lozenges rich in tea polyphenols and production method of mint-flavored tea-seed polypeptide lozenges
CN106281942A (en) * 2016-08-18 2017-01-04 安徽天乾健食品科技有限公司 A kind of tea-seed polypeptide health care pomegranate fruit vinegar beverage and preparation method thereof

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