CN107418360A - A kind of environment-friendly type is except aldehyde is except benzene LED decorations heat radiation coating - Google Patents

A kind of environment-friendly type is except aldehyde is except benzene LED decorations heat radiation coating Download PDF

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CN107418360A
CN107418360A CN201710125767.0A CN201710125767A CN107418360A CN 107418360 A CN107418360 A CN 107418360A CN 201710125767 A CN201710125767 A CN 201710125767A CN 107418360 A CN107418360 A CN 107418360A
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庄可香
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Abstract

A kind of environment-friendly type is prepared except aldehyde is except benzene LED decorations heat radiation coating by following component according to parts by weight：60 75 parts of hybrid resin, 3 4.5 parts of sodium-based montmorillonite, 4 6.5 parts of carboxylic styrene butadiene latex, 1.5 2 parts of silicones metlyl branching silicone oil, 0.7 1.2 parts of polyethylene glycol, 0.7 1.8 parts of pentane, 1 2.5 parts of nano silicon, 79 parts of polyacrylonitrile-based carbon fibre, 5 6.5 parts of graphene, 12 parts of aerosil, 5.5 7 parts of fire retardant etc., the present invention not only has great heat radiation effect, there is certain removal formaldehyde simultaneously, toluene, the effect of finishing pollution thing such as TVOC, realize the function that conventional lamp heat radiation coating does not have, with very extensive market prospects.

Description

A kind of environment-friendly type is except aldehyde is except benzene LED decorations heat radiation coating
Technical field
The present invention relates to LED lamp heat radiation coating technical field, and in particular to a kind of environment-friendly type is except aldehyde except benzene LED decorations dissipate Hot coating.
Background technology
With the development and progress of society, the illumination that the green idea of people is more and more stronger thus green fills Put more to be favored by people, and increasingly ripe LED technology is because it is with efficient, energy-saving and environmental protection, service life length, work( The low advantage of rate, LED illumination lamp have gradually started to substitute traditional illuminator.
LED electricity-saving lamps are actually a kind of compact, carry the LED of ballast, and lamp tube ends voltage is directly over Plasma state turns on and sends 253.7nm ultraviolet, and ultraviolet evokes light-emitting phosphor, filament during due to fluorescent lamp operation Temperature in 1160K or so, the temperature 2200-2700K than incandescent lamp work is much lower, so its life-span also prolongs significantly It is long, reach more than 5000 hours, due to the higher electric ballast of its operation efficiency, while electric current as incandescent lamp is not present Fuel factor, the energy conversion efficiency of fluorescent material is also very high, reaches more than every watt of 50 lumens, saves electric energy.
On the one hand, as the continuous rise of Global Temperature, the population of mosquito and quantity will all greatly improve, just increasingly threaten The health of the mankind.Mosquito except directly sting thorn suck blood, harass sleep in addition to, more seriously propagate a variety of diseases.The mosquito in China passes disease There are malaria, Filariasis, Japanese Type-B encephalitis and dengue fever（Or dengue hemorrhagic fever）Four classes, mosquito pass more important virosis Also yellow fever and various equine encephalitis etc..
On the other hand, by negative aeroion Technology application in electricity-saving lamp product, the electricity-saving lamp after use is long-term indoors Discharge negative aeroion, especially negative oxygen ion.Due to its in structure it is similar to ultra-oxygen anion free radical, therefore there is phase As bioactivity, biological cell living can be made negatively charged, so that virus loses attacking ability to cell；Meanwhile Negative oxygen ion can react with finishing pollution things such as formaldehyde, toluene, TVOC, product be nonpoisonous and tasteless carbon dioxide and Water, the generation of non-secondary pollution, with certain the effect of purifying the air of a room, for example, in artificial air's anion environment, Mould, bacterial population can reduce by more than 90% in air after measured.After negative oxygen ion is inhaled into human body, it can adjust neural emerging Put forth energy state, improve the ventilatory of lung, improve blood circulation, enhance metabolism, strengthen immune system ability, making one spirit and shake Put forth energy, improve operating efficiency etc., it also has certain treatment to make to many diseases such as hypertension, asthma, influenza, insomnia, arthritis With so people's anion is referred to as " vitamin in air " " long-lived element ".
So far, make conventional lamp heat radiation coating product while there is expelling mosquito and discharge the technology of negative ion health function Design, which does not have also, to be seen.
The content of the invention
In view of the deficienciess of the prior art, the technical problems to be solved by the invention are to provide a kind of dissipating for LED lamp Heat structure and light fixture, not only with preferable radiating effect, anion can be discharged, while have certain with expelling mosquito The effect of removing the finishing pollution things such as formaldehyde, toluene, TVOC, there is the health-care efficacy of certain mosquito repellent and antibacterial.
The purpose of the present invention is achieved by the following technical solution：
A kind of environment-friendly type is except aldehyde is except benzene LED decorations heat radiation coating, and described heat radiation coating is by following component according to parts by weight numeral system It is standby to form：Hybrid resin 60-75 parts by weight, sodium-based montmorillonite 3-4.5 parts by weight, carboxylic styrene butadiene latex 4-6.5 parts by weight, silicon tree Fat metlyl branching silicone oil 1.5-2 parts by weight, polyethylene glycol 0.7-1.2 parts by weight, pentane 0.7-1.8 parts by weight, nano-silica SiClx 1-2.5 parts by weight, polyacrylonitrile-based carbon fibre 7-9 parts by weight, graphene 5-6.5 parts by weight, aerosil 1-2 weights Measure part, fire retardant 5.5-7 parts by weight, curing agent 4-6 parts by weight, solvent 15-20 parts by weight, ceria 0.1- 0.15 parts by weight, active mineral matter powder 1.5-2 parts by weight, essential oil of traditional Chinese medicine 1.5-2.5 parts by weight；Wherein, the hybrid resin is The mass ratio of the mixture of phenolic resin and epoxy resin, phenolic resin and epoxy resin is 2：1-3：1；The polyacrylonitrile-radical Carbon fiber length is 0.01mm；The fire retardant is the mixture of APP, melamine and expanded graphites, described poly- The mass ratio 2 of ammonium phosphate, melamine and expanded graphites:1.5:1.3；Described solvent is the mixed of DAA and butyl ester Compound, the mass ratio of the DAA and butyl ester is 3:1-3:2；Described active mineral matter powder be germanite, fluorite, electrically Stone, gahnite are by weight 2.5：3：3.5：1.7 mixture, wherein tourmaline be dravite and elbaite by weight Than 4：3 mixture, particle diameter≤15 μm of the active mineral matter powder, the heat radiation coating, which is made by the steps, to be formed：
S1, hybrid resin, sodium-based montmorillonite, carboxylic styrene butadiene latex, silicones metlyl branching silicone oil, poly- second two are weighed by weight Alcohol, pentane, nano silicon, polyacrylonitrile-based carbon fibre, graphene, aerosil, fire retardant and solvent are put In mixer, mixed well in the stirring of 80 DEG C of next part high speeds, mixing time is 40 minutes, it is to be mixed uniformly after taken from mixer Go out, i.e., obtained mixture A is standby；
S2, by material fly expelling plum 65-85 parts by weight, perilla leaf 15-20 parts by weight, lavender 15-20 parts by weight, origanum oil 4-6 Parts by weight, purslane 3-4 parts by weight, anemone vitifolia 3-5 parts by weight, root of langdu 3-4 parts by weight, red sage root 3-4 parts by weight, flaccid knotweed herb 3-4 parts by weight, tuber of stemona 5-8 parts by weight decontaminations, -20 DEG C of vacuum kettle 2-3 hours are placed in together, are then placed in microwave drying again Machine is pre-processed, and wherein drying time is 30-40 minutes, microwave power 17kw；
S3, the material after step S2 processing put into micronizer and be crushed to 60 mesh together, bulk drug powder is made, it is standby With；
S4, obtained bulk drug powder in step S3 put into the extraction kettle of supercritical carbon dioxide extraction apparatus, regulation extraction Pressure power 28MPa, 45 DEG C, carbon dioxide flow 1100L/h of extraction temperature, dynamic extraction 2 hours, directly exported in separating still Crude oil is collected with triangular flask, it is standby；
S5, obtained crude oil in step S4 is placed in 5 DEG C of environment freezed 70 minutes, then the crude oil after freezing is placed in rotating speed and is Centrifuged 25 minutes in 17000r/min high speed freezing centrifuge, remove after the removal of impurity to be placed in 85 DEG C of vacuum tanks and vacuumize 3 hours, i.e., Obtained volatile oil B, it is standby；
S6, by wrinkled giant hyssop 3-4 parts by weight, fruit of negundo 4-6 parts by weight, frutus cnidii 15-20 parts by weight, spina date seed 3-4 parts by weight, elm Skin 15-25 parts by weight, cordate houttuynia 4-6 parts by weight, corydlis bungeana 3-5 parts by weight, Polygonum multiflower knotweed 3-5 parts by weight, peppermint 1-3 parts by weight, Moschus 1-3 parts by weight, marjoram 1.5-2.5 parts by weight, vanilla 1.5-2 parts by weight, ambergris 0.5-1 parts by weight, which are cleaned, dries It is dry, put into micronizer be crushed to 30 mesh together, then plus deionized water is soaked 5 hours, and amount of water is is soaked raw material 7 times of medicine quality, are dispersed with stirring and mix well, and Traditional Chinese drug mixture is made, standby；
S7, by Traditional Chinese drug mixture made from step S6 in 80 DEG C decoct 2 hours, collect distillate, and add ether extraction, distillation The volume ratio of liquid and ether is 2.5:1, upper oil phase is taken, then plus place is dried in anhydrous sodium sulfate 0.13-0.2 parts by weight Reason, i.e., obtained volatile oil C are standby；
S8, step S5 and S7 made volatile oil B and volatile oil C are mixed and mix well obtained miscella, then sequentially added while stirring Wheat malt essential oil, Geranium Essential, snow lotus herb soap essential oil, lemon and grapefruit essential oil, it is sufficiently stirred 45 minutes, stands 30 points Clock, filtering and impurity removing, essential oil of traditional Chinese medicine is produced, wherein, the miscella and wheat malt essential oil, Geranium Essential, snow lotus herb soap essential oil, lemon Lemon essential oil and the mass ratio of grapefruit essential oil are 2：0.5：0.5：0.6：0.4：0.5；
S9, by mixture A made from essential oil of traditional Chinese medicine made from step S8 and step S1, at 70-80 DEG C, concentrated in mixer It is stirred 15 minutes, obtains premix, it is standby；
S10, by made from step S9 premix put into ball mill, then add ceria, active mineral matter powder and change Property aromatic amine curing agent, at 70-80 DEG C, concentrate grinding 4.5 hours, filter decontamination, that is, obtain heat radiation coating.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following parts by weight：Surface-active Agent 3-5 parts by weight, Metadelphene 0.1-0.2, butyl butyrate 9-15 parts by weight, eucalyptus oil 10-13 parts by weight, isopropyl myristate 1-2 parts by weight, sodium sulfate of polyethenoxy ether of fatty alcohol 10-15 parts by weight and sodium benzoate 0.1-0.3 parts by weight.
It should be noted that the experiment proved that, appropriate ceria is added in active mineral matter powder（CeO2）, utilize The emittance of the rare earth element is high, and the characteristics of half degradation period limit for length, the anion production of active mineral matter powder can be significantly increased Rate, its principle are as follows：Ce in ceria4+Ce is changed under photoenvironment3+, in conversion process, electron-hole Recombination probability reduces, then in active mineral matter powder in the presence of the material electric field such as tourmaline, part electronics is passively with electric field side To displacement, electron-hole recombination probability reduces, so as in tourmaline/CeO2Substantial amounts of electricity is gathered in composite powder surface The energy of air molecule is solved, and then generates the negative aeroion of high concentration, while Ce3+Ce is oxidized into again4+, then repeat Foregoing conversion process；Meanwhile detected through putting into practice, added in right amount in the active mineral matter powder by the compound proportioning of the present invention Ceria component, the concentration than the active mineral matter powder anion of not added ceria is high more than 10 times, r rays with from Right environment is identical.
The present invention be based on traditional Chinese medicine, with reference to modern Chinese medicine pharmacological research, from the drug screening of existing Chinese medicine and instead Card is reviewed, each group parts by weight synergy is given full play to, wherein the effect of each raw material is described as follows.
Fly expelling plum：Verenaceae Lantana, belongs to perennial plant, evergreen half tendril shrub, the prismatic of sprig four, it is long and under Hanging down has reverse sharp thorn, and the sensitive smell of mosquitos and flies is volatilized in its branches and leaves and flower, has very strong expulsion mosquitos and flies effect, And there is " mosquito repellent seven becomes flower " good reputation without any injury to human body.
Perilla leaf：For the dried leaf of labiate purple perilla（Or with spray）, there is relieving exterior syndrome and dispelling cold, the work(of relieving QI stagnancy in the stomach Effect, for anemofrigid cold, evil of vomitting of coughing, there is inhibitory action to staphylococcus.
Lavender can remove ant, except roach, except mite, when being placed under wardrobe, pillow, can not only replace camphor ball, moreover it is possible to stay The fragrance of one lower people that oozes, research find that lavender has obvious antibacterial action, and the linalool contained in lavender is lavender The main component of antibacterial, it can suppress 17 kinds of bacteriums（Including gram-negative bacteria and gram-positive bacteria）, 10 kinds of fungies life It is long.
Origanum oil：Labiatae origanum wild marjoram ORIGZNUM VUL-GAREL. herb, also known as stop dysentery is careless, wild chaste tree The ground such as mustard accord with name, have the extremely strong sterilization of heat-clearing, dampness elimination, driving away summer heat, inducing diaphoresis, qi-regulating, bacteriostasis, the volatilization extracted from wild marjoram Oil, cause enteritis bacterium common to 31 kinds and shigella flexneri, it is the pure Chinese medicine additive of most broad-spectrum antiseptic.
Purslane：Portulacaceae annual herb plant.Plump succulence, hairless, high 10-30cm, be born in field roadside and The area without shade such as flower garden ruins.Domestic various regions are distributed.This kind is medical and edible dual purpose plant.Herb hyoscine, there are clearing heat and promoting diuresis, solution Malicious detumescence, anti-inflammatory, quench the thirst, diuresis.
Anemone vitifolia：①《Shaanxi Chinese herbal medicine》：" it is bitter, it is cool, it is slightly poisonous.”②《Often use Chinese herbal medicine in Sichuan》：" toil, temperature, It is slightly poisonous." removing toxic substances, apocenosis myogenic, scattered stasis detumescence, have and kill maggot, wriggler, change product, detumescence, dissipate the stasis of blood, control stubborn dermatitis, the favus of the scalp, malaria Disease, infantile malnutrition, dysentery, carbuncle furuncle sore swell, scrofula, traumatic injury.
The root of langdu：The alias river root of langdu, continuous poison, RADIX STELLERAE, chervil, vexed fresh idea, Re Jiaba, eliminate completely, Chinese atropanthe root, one perfume, Medicine sieve foretells, it is raw pull, flourishing bavin headdress flower, monkey root, gelsemium elegan, with its root eliminating the phlegm, analgesic, disperse accumulations, desinsection in traditional Chinese medicine.
The red sage root：It is bitter in taste, it is slightly cold.The thoughts of returning home, Liver Channel.《The southern regions of the Yunnan Province book on Chinese herbal medicine》Record：Bushing sedate, calming heart and tranquilizing mind.Control forgetful seized with terror Punching, palpitation with fear is insomnia, and has a stasis-dispelling and pain-killing, invigorate blood circulation, the effect of relieving restlessness that clears away heart-fire, for irregular menstruation, closed dysmenorrhea, abdominal mass product It is poly-, chest and abdomen shouting pain, hot numbness pain, sore.
Flaccid knotweed herb：To various shigella dysenteriaes in there is inhibitory action in test tube, current clinical medicine research shows, polygonum flaccidum tool There are antibacterial, antiviral, anti-inflammatory, anti-oxidant and other effects.
The tuber of stemona：Can mosquito expelling, resisting pathogenic microbes effect, to beta hemolytic streptococcus, meningococcus, golden yellow A variety of pathomycetes such as staphylococcus, staphylococcus albus, typhoid bacillus, pneumobacillus, yersinia pestis, bacillus anthracis have necessarily Inhibitory action, its infusion has killing action to mosquitos and flies larva, head louse, clothing lice and bedbug etc..
Wrinkled giant hyssop：Acrid flavour, slightly warm in nature.Effect：Dampness elimination inducing diaphoresis, solves the effect of administration, cures mainly dampness taste with, and chest gastral cavity is vexed swollen, Appetite is not fragrant, Nausea and vomiting；Summer summer-heat and damp is sleepy, uncomfortable in chest not relax, and the illnesss such as aversion to cold of catching cold is uncomfortable in chest, have compared with Strong suppression fungi effect and antibacterial action.
Fruit of negundo：Acrid flavour is bitter, warm-natured, return lung, stomach, Liver Channel；Gas perfume (or spice) row dissipates；With expelling pathogenic wind from the body surface, preventing phlegm from forming and stopping coughing, qi-regulating stops The effect of pain, there is inhibitory action to staphylococcus aureus, micrococcus catarrhalis.
Frutus cnidii：Nature and flavor：It is warm-natured, acrid flavour, hardship.Major function：Warming kidney and enhancing body, eliminating dampness, wind-dispelling, desinsection.For impotence, Gong Leng, morbid leucorrhoea duye, arthritis with fixed pain caused by dampness pain in the back；Control eczema of vulva, married woman's pruritus vulvae, trichomonas vaginitis outside.
Spina date seed:There are significant calm and syngignoscism and anticonvulsant action, according to《Book on Chinese herbal medicine is new again》Record：Soothing the liver is managed Gas, moisten the lung and nourish yin, middle benefit gas dampness removing, hold back gas hidroschesis, beneficial will, hearing-improing and eyesight improving.
Peppermint：For the dry aerial parts of labiate peppermint, dispelling wind and heat from the body, head clearing, relieving sore-throat promoting eruption, soothing the liver row Gas.
Moschus:With having one's ideas straightened out, ward off dirty, dredging collateral, dissipate the stasis of blood the effect of；Control apoplexy, coma due to blocking of the respiratory system, frightened epilepsy, middle evil unhappiness, Xin Fubao The pain, Disorder lump in the abdomen hypochondriac lumps, traumatic injury, swollen ulcer drug.《This warp》：Master wards off bad odor, a kind of malaria, epilepsy convulsion, goes three worms.
Marjoram：Can improve that mood is depressed and addictive disease, it is especially effective to liberal-mindedness and vigorous endurance stress symptom, can expand blood vessel, Hypotensive, mitigation and burden, help eliminate palpitaition, have excellent nerve to pacify and calm function.
Vanilla:There is special fragrance, have that antifatigue and mood is gloomy, help hormone secretion, anxiety of releiving and improvement Insomnia and other effects.The effect of with cardiac stimulant, cerebrum tonifying, stomach invigorating, removing toxic substances, wind dispelling, enhancing muscle strength, it is emerging to make aroma type nervous system Put forth energy agent and kidney-reinforcing drug, for treating hysteria, melancholia, impotence, abnormal heat and rheumatism.
Ambergris：It is the most lasting spices of lasting, any spices can not all compare favourably therewith in the world, be known as " dragon The perfume of saliva coexists with life " saying.《Compendium of Materia Medica》Carry：It can invigorate blood circulation, benefiting quintessence, supporing yang road, promoting blood circulation, resolving sputum are put down Asthma；A lump in the abdomen causing distension and pain；Trusted subordinate's pain；Coma；Liao Yongyan：Promoting diuresis for stranguria, San Disorder are tied, knot of cooling down, by labor worm.
It should be noted that it is proven, after the red sage root, flaccid knotweed herb and the tuber of stemona of certain part by weight are compounded, no The ability of degerming antibacterial is only remarkably improved, can also produce a kind of delicate fragrance taste having no toxic side effect, it is refreshing, have certain Effect of refreshing oneself；Meanwhile be proven, after the fly expelling plum, Moschus and anemone vitifolia of certain part by weight are compounded, make The mosquito dispersing ability of said composition is significantly improved；In addition, the group such as origanum oil, fruit of negundo, frutus cnidii, corydlis bungeana and cordate houttuynia Divide after carrying out compatibility, substantially increase the antibacterial degerming ability of composition, detected through practice, the composition after compounding is to golden yellow Staphylococcus, bacillus anthracis, Bacillus influenzae, micrococcus catarrhalis, pneumococcus, Escherichia coli, beta streptococcus, corynebacterium diphtheriae, wound The kind germ of cold bacillus, green pus liver bacterium, shigella dysenteriae etc. more than 40 has certain suppression and killing action.
The effect of the present invention：
The present invention is compounded using Chinese medicine and active mineral matter, the present invention is not only had preferable radiating effect, can also be driven Mosquito, anion, fresh air, while fragrant odour are discharged, property is gentle, has the effect of mosquito repellent, antibacterial and health care.
Embodiment
Embodiment 1：
A kind of environment-friendly type is except aldehyde except benzene LED decorations heat radiation coating, the heat radiation coating are prepared by following component according to parts by weight Form：The parts by weight of hybrid resin 60, the parts by weight of sodium-based montmorillonite 4.5, the parts by weight of carboxylic styrene butadiene latex 4, silicones methyl branch The parts by weight of silicone oil 2, the parts by weight of polyethylene glycol 0.7, the parts by weight of pentane 1.8, the parts by weight of nano silicon 1, polyacrylonitrile-radical The parts by weight of carbon fiber 9, the parts by weight of graphene 5, the parts by weight of aerosil 2, the parts by weight of fire retardant 5.5, modified aromatic amine are consolidated The parts by weight of agent 6, the parts by weight of solvent 15, the parts by weight of ceria 0.1, the parts by weight of active mineral matter powder 2, the weight of essential oil of traditional Chinese medicine 1.5 Measure part；Wherein, the hybrid resin is the mass ratio of the mixture of phenolic resin and epoxy resin, phenolic resin and epoxy resin For 3：1；The polyacrylonitrile-based carbon fibre length is 0.01mm；The fire retardant is APP, melamine and expansion The mixture of type graphite, the mass ratio 2 of the APP, melamine and expanded graphites:1.5:1.3；Described is molten Agent is the mixture of DAA and butyl ester, and the mass ratio of the DAA and butyl ester is 3:1；Described active mineral matter powder It is germanite, fluorite, tourmaline, gahnite by weight 2.5：3：3.5：1.7 mixture, wherein tourmaline are dravite With elbaite by weight 4：3 mixture, particle diameter≤15 μm of the active mineral matter powder, the heat radiation coating pass through such as Lower step is prepared：
S1, hybrid resin, sodium-based montmorillonite, carboxylic styrene butadiene latex, silicones metlyl branching silicone oil, poly- second two are weighed by weight Alcohol, pentane, nano silicon, polyacrylonitrile-based carbon fibre, graphene, aerosil, fire retardant and solvent are put In mixer, mixed well in the stirring of 80 DEG C of next part high speeds, mixing time is 40 minutes, it is to be mixed uniformly after taken from mixer Go out, i.e., obtained mixture A is standby；
S2, by the parts by weight of material fly expelling plum 65, the parts by weight of perilla leaf 20, the parts by weight of lavender 15, the parts by weight of origanum oil 6, dent The parts by weight of amaranth 3, the parts by weight of anemone vitifolia 5, the parts by weight of the root of langdu 3, the parts by weight of the red sage root 4, the parts by weight of flaccid knotweed herb 3, the parts by weight of the tuber of stemona 8 Decontamination, is placed in -20 DEG C of vacuum kettle 2 hours together, and being then placed in microwave dryer again is pre-processed, wherein drying time For 30 minutes, microwave power 17kw；
S3, the material after step S2 processing put into micronizer and be crushed to 60 mesh together, bulk drug powder is made, it is standby With；
S4, obtained bulk drug powder in step S3 put into the extraction kettle of supercritical carbon dioxide extraction apparatus, regulation extraction Pressure power 28MPa, 45 DEG C, carbon dioxide flow 1100L/h of extraction temperature, dynamic extraction 2 hours, directly exported in separating still Crude oil is collected with triangular flask, it is standby；
S5, obtained crude oil in step S4 is placed in 5 DEG C of environment freezed 70 minutes, then the crude oil after freezing is placed in rotating speed and is Centrifuged 25 minutes in 17000r/min high speed freezing centrifuge, remove after the removal of impurity to be placed in 85 DEG C of vacuum tanks and vacuumize 3 hours, i.e., Obtained volatile oil B, it is standby；
S6, by the parts by weight of wrinkled giant hyssop 3, the parts by weight of fruit of negundo 6, the parts by weight of frutus cnidii 15, the parts by weight of spina date seed 4, the weight of elm bark 15 Part, the parts by weight of cordate houttuynia 6, the parts by weight of corydlis bungeana 3, the parts by weight of Polygonum multiflower knotweed 5, the parts by weight of peppermint 1, the parts by weight of Moschus 3, marjoram 1.5 parts by weight, the parts by weight of vanilla 2, the parts by weight of ambergris 0.5 clean drying, put into micronizer be crushed to 30 together Mesh, then plus deionized water is soaked 5 hours, amount of water for 7 times of immersion bulk drug quality, be dispersed with stirring and mix well, in obtained Medicine mixture, it is standby；
S7, by Traditional Chinese drug mixture made from step S6 in 80 DEG C decoct 2 hours, collect distillate, and add ether extraction, distillation The volume ratio of liquid and ether is 2.5:1, upper oil phase is taken, then plus processing is dried in the parts by weight of anhydrous sodium sulfate 0.13, i.e., Obtained volatile oil C, it is standby；
S8, step S5 and S7 made volatile oil B and volatile oil C are mixed and mix well obtained miscella, then sequentially added while stirring Wheat malt essential oil, Geranium Essential, snow lotus herb soap essential oil, lemon and grapefruit essential oil, it is sufficiently stirred 45 minutes, stands 30 points Clock, filtering and impurity removing, essential oil of traditional Chinese medicine is produced, wherein, the miscella and wheat malt essential oil, Geranium Essential, snow lotus herb soap essential oil, lemon Lemon essential oil and the mass ratio of grapefruit essential oil are 2：0.5：0.5：0.6：0.4：0.5；
S9, by mixture A made from essential oil of traditional Chinese medicine made from step S8 and step S1, at 70 DEG C, concentrate and stir in mixer Mixing 15 minutes is mixed, obtains premix, it is standby；
S10, by made from step S9 premix put into ball mill, then add ceria, active mineral matter powder and change Property aromatic amine curing agent, at 73 DEG C, concentrate grinding 4.5 hours, filter decontamination, that is, obtain heat radiation coating.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following parts by weight：Surface-active The parts by weight of agent 3, the parts by weight of Metadelphene 0. 2, the parts by weight of butyl butyrate 9, the parts by weight of eucalyptus oil 4, the weight of isopropyl myristate 1 Part, the parts by weight of sodium sulfate of polyethenoxy ether of fatty alcohol 15 and the parts by weight of sodium benzoate 0.1.
Embodiment 2：
A kind of environment-friendly type is except aldehyde except benzene LED decorations heat radiation coating, the heat radiation coating are prepared by following component according to parts by weight Form：The parts by weight of hybrid resin 75, the parts by weight of sodium-based montmorillonite 3, the parts by weight of carboxylic styrene butadiene latex 6.5, silicones methyl branch The parts by weight of silicone oil 1.5, the parts by weight of polyethylene glycol 1.2, the parts by weight of pentane 0.7, the parts by weight of nano silicon 2.5, polypropylene The parts by weight of itrile group carbon fiber 8, the parts by weight of graphene 6, the parts by weight of aerosil 1.5, the parts by weight of fire retardant 6, modified aromatic The parts by weight of amine hardener 5, the parts by weight of solvent 17, the parts by weight of ceria 0.15, the parts by weight of active mineral matter powder 1.7, Chinese medicine essence Oily 2 parts by weight；Wherein, the hybrid resin is the mixture of phenolic resin and epoxy resin, phenolic resin and epoxy resin Mass ratio is 3：1；The polyacrylonitrile-based carbon fibre length is 0.01mm；The fire retardant be APP, melamine with And the mixture of expanded graphites, the mass ratio 2 of the APP, melamine and expanded graphites:1.5:1.3；Institute The solvent stated is the mixture of DAA and butyl ester, and the mass ratio of the DAA and butyl ester is 3:2；Described active ore deposit Material powder is germanite, fluorite, tourmaline, gahnite by weight 2.5：3：3.5：1.7 mixture, wherein tourmaline are magnesium Tourmaline and elbaite are by weight 4：3 mixture, particle diameter≤15 μm of the active mineral matter powder, the heat radiation coating It is made by the steps and forms：
S1, hybrid resin, sodium-based montmorillonite, carboxylic styrene butadiene latex, silicones metlyl branching silicone oil, poly- second two are weighed by weight Alcohol, pentane, nano silicon, polyacrylonitrile-based carbon fibre, graphene, aerosil, fire retardant and solvent are put In mixer, mixed well in the stirring of 80 DEG C of next part high speeds, mixing time is 40 minutes, it is to be mixed uniformly after taken from mixer Go out, i.e., obtained mixture A is standby；
S2, by the parts by weight of material fly expelling plum 85, the parts by weight of perilla leaf 15, the parts by weight of lavender 20, the parts by weight of origanum oil 4, dent The parts by weight of amaranth 4, the parts by weight of anemone vitifolia 3, the parts by weight of the root of langdu 4, the parts by weight of the red sage root 3, the parts by weight of flaccid knotweed herb 4, the parts by weight of the tuber of stemona 5 Decontamination, is placed in -20 DEG C of vacuum kettle 3 hours together, and being then placed in microwave dryer again is pre-processed, wherein drying time For 40 minutes, microwave power 17kw；
S3, the material after step S2 processing put into micronizer and be crushed to 60 mesh together, bulk drug powder is made, it is standby With；
S4, obtained bulk drug powder in step S3 put into the extraction kettle of supercritical carbon dioxide extraction apparatus, regulation extraction Pressure power 28MPa, 45 DEG C, carbon dioxide flow 1100L/h of extraction temperature, dynamic extraction 2 hours, directly exported in separating still Crude oil is collected with triangular flask, it is standby；
S5, obtained crude oil in step S4 is placed in 5 DEG C of environment freezed 70 minutes, then the crude oil after freezing is placed in rotating speed and is Centrifuged 25 minutes in 17000r/min high speed freezing centrifuge, remove after the removal of impurity to be placed in 85 DEG C of vacuum tanks and vacuumize 3 hours, i.e., Obtained volatile oil B, it is standby；
S6, by the parts by weight of wrinkled giant hyssop 4, the parts by weight of fruit of negundo 4, the parts by weight of frutus cnidii 20, the parts by weight of spina date seed 3, the weight of elm bark 25 Part, the parts by weight of cordate houttuynia 4, the parts by weight of corydlis bungeana 5, the parts by weight of Polygonum multiflower knotweed 3, the parts by weight of peppermint 3, the parts by weight of Moschus 1, marjoram 2.5 parts by weight, the parts by weight of vanilla 1.5, the parts by weight of ambergris 1 clean drying, put into micronizer be crushed to 30 together Mesh, then plus deionized water is soaked 5 hours, amount of water for 7 times of immersion bulk drug quality, be dispersed with stirring and mix well, in obtained Medicine mixture, it is standby；
S7, by Traditional Chinese drug mixture made from step S6 in 80 DEG C decoct 2 hours, collect distillate, and add ether extraction, distillation The volume ratio of liquid and ether is 2.5:1, upper oil phase is taken, then plus processing is dried in the parts by weight of anhydrous sodium sulfate 0.18, i.e., Obtained volatile oil C, it is standby；
S8, step S5 and S7 made volatile oil B and volatile oil C are mixed and mix well obtained miscella, then sequentially added while stirring Wheat malt essential oil, Geranium Essential, snow lotus herb soap essential oil, lemon and grapefruit essential oil, it is sufficiently stirred 45 minutes, stands 30 points Clock, filtering and impurity removing, essential oil of traditional Chinese medicine is produced, wherein, the miscella and wheat malt essential oil, Geranium Essential, snow lotus herb soap essential oil, lemon Lemon essential oil and the mass ratio of grapefruit essential oil are 2：0.5：0.5：0.6：0.4：0.5；
S9, by mixture A made from essential oil of traditional Chinese medicine made from step S8 and step S1, at 75 DEG C, concentrate and stir in mixer Mixing 15 minutes is mixed, obtains premix, it is standby；
S10, by made from step S9 premix put into ball mill, then add ceria, active mineral matter powder and change Property aromatic amine curing agent, at 80 DEG C, concentrate grinding 4.5 hours, filter decontamination, that is, obtain heat radiation coating.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following parts by weight：Surface-active The parts by weight of agent 5, the parts by weight of Metadelphene 0.1, the parts by weight of butyl butyrate 15, the parts by weight of eucalyptus oil 7, the weight of isopropyl myristate 2 Part, the parts by weight of sodium sulfate of polyethenoxy ether of fatty alcohol 10 and the parts by weight of sodium benzoate 0.3.
Remaining is the same as embodiment 1.
The test index of Example 1 and Example 2 of the present invention is as follows：
（1）Smell inspection：Sense organ, nonirritant peculiar smell.
（2）Technical performance index, testing result such as table 1：
（3）Anionic textiles.
Using negative ion testing equipment, it is made primarily directed to timber, ore, ceramic material, negative ion powder to related Commodity（Such as negative ion clothing, necklace, woollen blanket）Measurement is made Deng the anion quantity discharged.
Test result is shown in Table 2.
Conclusion：The embodiment of the present invention 1, embodiment 2 can be with sustained release negative aeroions, with ordinary lamps of the prior art The heat radiation coating of tool compares, and the present invention has obviously advantage.

Claims (2)

1. a kind of environment-friendly type is except aldehyde is except benzene LED decorations heat radiation coating, it is characterised in that：Described heat radiation coating is by following component It is prepared according to parts by weight：Hybrid resin 60-75 parts by weight, sodium-based montmorillonite 3-4.5 parts by weight, carboxylic styrene butadiene latex 4- 6.5 parts by weight, silicones metlyl branching silicone oil 1.5-2 parts by weight, polyethylene glycol 0.7-1.2 parts by weight, pentane 0.7-1.8 weights Measure part, nano silicon 1-2.5 parts by weight, polyacrylonitrile-based carbon fibre 7-9 parts by weight, graphene 5-6.5 parts by weight, gas phase The parts by weight of silica 1-2, fire retardant 5.5-7 parts by weight, curing agent 4-6 parts by weight, solvent 15-20 weight Part, ceria 0.1-0.15 parts by weight, active mineral matter powder 1.5-2 parts by weight, essential oil of traditional Chinese medicine 1.5-2.5 parts by weight；Wherein, The hybrid resin is the mixture of phenolic resin and epoxy resin, and the mass ratio of phenolic resin and epoxy resin is 2：1-3：1； The polyacrylonitrile-based carbon fibre length is 0.01mm；The fire retardant is APP, melamine and expanded graphites Mixture, the mass ratio 2 of the APP, melamine and expanded graphites:1.5:1.3；Described solvent is two The mixture of pyruvic alcohol and butyl ester, the mass ratio of the DAA and butyl ester is 3:1-3:2；Described active mineral matter powder is Germanite, fluorite, tourmaline, gahnite are by weight 2.5：3：3.5：1.7 mixture, wherein tourmaline be dravite and Elbaite is by weight 4：3 mixture, particle diameter≤15 μm of the active mineral matter powder, the heat radiation coating passes through as follows Step is prepared：
S1, hybrid resin, sodium-based montmorillonite, carboxylic styrene butadiene latex, silicones metlyl branching silicone oil, poly- second two are weighed by weight Alcohol, pentane, nano silicon, polyacrylonitrile-based carbon fibre, graphene, aerosil, fire retardant and solvent are put In mixer, mixed well in the stirring of 80 DEG C of next part high speeds, mixing time is 40 minutes, it is to be mixed uniformly after taken from mixer Go out, i.e., obtained mixture A is standby；
S2, by material fly expelling plum 65-85 parts by weight, perilla leaf 15-20 parts by weight, lavender 15-20 parts by weight, origanum oil 4-6 Parts by weight, purslane 3-4 parts by weight, anemone vitifolia 3-5 parts by weight, root of langdu 3-4 parts by weight, red sage root 3-4 parts by weight, flaccid knotweed herb 3-4 parts by weight, tuber of stemona 5-8 parts by weight decontaminations, -20 DEG C of vacuum kettle 2-3 hours are placed in together, are then placed in microwave drying again Machine is pre-processed, and wherein drying time is 30-40 minutes, microwave power 17kw；
S3, the material after step S2 processing put into micronizer and be crushed to 60 mesh together, bulk drug powder is made, it is standby With；
S4, obtained bulk drug powder in step S3 put into the extraction kettle of supercritical carbon dioxide extraction apparatus, regulation extraction Pressure power 28MPa, 45 DEG C, carbon dioxide flow 1100L/h of extraction temperature, dynamic extraction 2 hours, directly exported in separating still Crude oil is collected with triangular flask, it is standby；
S5, obtained crude oil in step S4 is placed in 5 DEG C of environment freezed 70 minutes, then the crude oil after freezing is placed in rotating speed and is Centrifuged 25 minutes in 17000r/min high speed freezing centrifuge, remove after the removal of impurity to be placed in 85 DEG C of vacuum tanks and vacuumize 3 hours, i.e., Obtained volatile oil B, it is standby；
S6, by wrinkled giant hyssop 3-4 parts by weight, fruit of negundo 4-6 parts by weight, frutus cnidii 15-20 parts by weight, spina date seed 3-4 parts by weight, elm Skin 15-25 parts by weight, cordate houttuynia 4-6 parts by weight, corydlis bungeana 3-5 parts by weight, Polygonum multiflower knotweed 3-5 parts by weight, peppermint 1-3 parts by weight, Moschus 1-3 parts by weight, marjoram 1.5-2.5 parts by weight, vanilla 1.5-2 parts by weight, ambergris 0.5-1 parts by weight, which are cleaned, dries It is dry, put into micronizer be crushed to 30 mesh together, then plus deionized water is soaked 5 hours, and amount of water is is soaked raw material 7 times of medicine quality, are dispersed with stirring and mix well, and Traditional Chinese drug mixture is made, standby；
S7, by Traditional Chinese drug mixture made from step S6 in 80 DEG C decoct 2 hours, collect distillate, and add ether extraction, distillation The volume ratio of liquid and ether is 2.5:1, upper oil phase is taken, then plus place is dried in anhydrous sodium sulfate 0.13-0.2 parts by weight Reason, i.e., obtained volatile oil C are standby；
S8, step S5 and S7 made volatile oil B and volatile oil C are mixed and mix well obtained miscella, then sequentially added while stirring Wheat malt essential oil, Geranium Essential, snow lotus herb soap essential oil, lemon and grapefruit essential oil, it is sufficiently stirred 45 minutes, stands 30 points Clock, filtering and impurity removing, essential oil of traditional Chinese medicine is produced, wherein, the miscella and wheat malt essential oil, Geranium Essential, snow lotus herb soap essential oil, lemon Lemon essential oil and the mass ratio of grapefruit essential oil are 2：0.5：0.5：0.6：0.4：0.5；
S9, by mixture A made from essential oil of traditional Chinese medicine made from step S8 and step S1, at 70-80 DEG C, concentrated in mixer It is stirred 15 minutes, obtains premix, it is standby；
S10, by made from step S9 premix put into ball mill, then add ceria, active mineral matter powder and change Property aromatic amine curing agent, at 70-80 DEG C, concentrate grinding 4.5 hours, filter decontamination, that is, obtain heat radiation coating.
2. a kind of environment-friendly type according to claim 1 is except aldehyde is except benzene LED decorations heat radiation coating, it is characterised in that：In step Essential oil of traditional Chinese medicine in S8 also includes the component of following parts by weight：Surfactant 3-5 parts by weight, Metadelphene 0.1-0.2 parts by weight, Butyl butyrate 9-15 parts by weight, eucalyptus oil 4-7 parts by weight, isopropyl myristate 1-2 parts by weight, AEO sulphur Sour sodium 10-15 parts by weight and sodium benzoate 0.1-0.3 parts by weight.
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