CN106046693A - Preparation process of illuminating lampshade with air purification function - Google Patents

Preparation process of illuminating lampshade with air purification function Download PDF

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CN106046693A
CN106046693A CN201610574155.5A CN201610574155A CN106046693A CN 106046693 A CN106046693 A CN 106046693A CN 201610574155 A CN201610574155 A CN 201610574155A CN 106046693 A CN106046693 A CN 106046693A
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史玉桂
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
    • C08L63/10—Epoxy resins modified by unsaturated compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L91/00—Compositions of oils, fats or waxes; Compositions of derivatives thereof
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F21—LIGHTING
    • F21V—FUNCTIONAL FEATURES OR DETAILS OF LIGHTING DEVICES OR SYSTEMS THEREOF; STRUCTURAL COMBINATIONS OF LIGHTING DEVICES WITH OTHER ARTICLES, NOT OTHERWISE PROVIDED FOR
    • F21V3/00—Globes; Bowls; Cover glasses
    • F21V3/04—Globes; Bowls; Cover glasses characterised by materials, surface treatments or coatings
    • F21V3/06—Globes; Bowls; Cover glasses characterised by materials, surface treatments or coatings characterised by the material
    • F21V3/062—Globes; Bowls; Cover glasses characterised by materials, surface treatments or coatings characterised by the material the material being plastics
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/002—Physical properties
    • C08K2201/003—Additives being defined by their diameter
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Abstract

The invention discloses a preparation process of an illuminating lampshade with an air purification function, which consists of environment-friendly resin, a flame retardant, a modified aromatic amine curing agent, nano fluorescent powder, a Qibayan Jiaguo 754 photoinitiator, a polyether amine catalyst, hydroxyethyl cellulose, cerium dioxide, active mineral substance powder and the like.

Description

A kind of preparation technology of the illuminating lamp shade with air-cleaning function
Technical field
The present invention relates to field of illuminating lamps, particularly relate to the preparation work of a kind of illuminating lamp shade with air-cleaning function Skill.
Background technology
Along with the development and progress of society, the environmental protection idea of people is increasingly stronger, thus the illumination dress of environmental protection Put and can more be favored by people, day by day ripe LED technology due to its have efficiently, energy-saving and environmental protection, length in service life, merit The advantages such as rate is low, LED illumination lamp the most gradually starts to replace traditional lighting.
On the one hand, along with the continuous rising of Global Temperature, the population of mosquito and quantity all will be greatly improved, the most day by day threaten The health of the mankind.Mosquito, in addition to directly stining thorn and sucking blood, harass sleep, more seriously propagates multiple disease.The mosquito of China passes disease Having malaria, Filariasis, epidemic encephalitis type B and dengue fever (or dengue hemorrhagic fever) four class, mosquito passes more important virosis Also have yellow fever and various equine encephalitis etc..
On the other hand, by negative aeroion Technology application in electricity-saving lamp product, the electricity-saving lamp after using is long-term in indoor Release negative aeroion, especially negative oxygen ion.Owing to it is structurally similar to ultra-oxygen anion free radical, therefore there is phase As biological activity, it is possible to make live biological cell electronegative, so that virus loses the attacking ability to cell；Meanwhile, Negative oxygen ion can react with the finishing pollution thing such as formaldehyde, toluene, TVOC, product be nonpoisonous and tasteless carbon dioxide and Water, the generation of non-secondary pollution, there is certain effect purified the air of a room, such as, in artificial air's anion environment, In air, mycete, bacterial population can reduce by more than 90% after measured.After negative oxygen ion is inhaled into human body, can regulate neural emerging Put forth energy state, improve the ventilatory of lung, improve blood circulation, enhance metabolism, strengthen immune system ability, make people's spirit shake Putting forth energy, improve work efficiency etc., the numerous diseases such as hypertension, asthma, influenza, insomnia, arthritis are also had certain treatment to make by it With, so people's anion is called " vitamin in air " " long-lived element ".
So far, the Technology design making conventional lamp product simultaneously have mosquito dispersing and negative ion-releasing function does not also have See.
Summary of the invention
The deficiency existed for prior art, the technical problem to be solved is to provide one and has air cleaning The preparation technology of the illuminating lamp shade of function, prepared coating not only long-term negative ion release, also there is certain expelling mosquito Effect, also has certain antibacterial action simultaneously, has the effect achieved many things at one stroke.
It is an object of the invention to be achieved through the following technical solutions:
A kind of preparation technology of the illuminating lamp shade with air-cleaning function, it is characterised in that: described lampshade is by following steps It is prepared from:
S1, by good to environment-friendly resin 15-25 weight portion, fire retardant 3-6 weight portion, nano-phosphor 0.1-0.2 weight portion, vapour Ba Yan Gu 754 light trigger 1.5-3 weight portions, hydroxyethyl cellulose 2-3 weight portion and polyetheramine catalyst 0.5-0.7 weight portion one With being placed in blender, mixing well 65-85 DEG C of next part high speed stirring, mixing time is 15-30 minute, to be mixed uniformly after from Blender takes out, i.e. prepares mixture A, standby；Wherein, described environment-friendly resin is epoxy soybean oil acrylate and bisphenol-A The mixture of type E51 epoxy resin, the mass ratio of described epoxy soybean oil acrylate and bisphenol A-type E51 epoxy resin is 1.5:1, described fire retardant is the mixture of ammonium polyphosphate, tripolycyanamide and expanded graphites, described ammonium polyphosphate, three The mass ratio 1.5:1.2:1 of poly cyanamid and expanded graphites, described nano-phosphor is the mixture of Ce and YAG, described Particle diameter≤13 μm of nano-phosphor；
S2, by material Omphalia 65-85 weight portion, Semen Torreyae 20-25 weight portion, Herba Portulacae 3-4 weight portion, lavandula angustifolia 15-20 weight Part, Herba anemones vitifoliae 3-5 weight portion, Herba Anemones Hupehensis 3-5 weight portion, Caulis Polygoni Multiflori 3-5 weight portion, Herba Menthae 1-3 weight portion, Rhizoma Cimicifugae 1-3 Weight portion, Origanum majorana 1.5-2.5 weight portion and vanilla 1.5-2 weight portion decontamination, be placed in the vacuum still of-20 DEG C together 2-3 hour, being placed in microwave dryer the most again and carry out pretreatment, wherein drying time is 30-40 minute, and microwave power is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still Crude oil is collected with triangular flask, standby；
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e. Prepare volatile oil B, standby；
S6, by Olibanum 4-6 weight portion, Radix Salviae Miltiorrhizae 3-4 weight portion, Herba polygoni hydropiperis 3-4 weight portion, Radix Stemonae 7-9 weight portion, Herba Pogostemonis 3-4 weight Amount part, Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 3-4 weight portion, Fructus Gardeniae 3-4 weight portion, Radix Isatidis 15-18 weight portion and Semen Ziziphi Spinosae 3-4 weight portion are cleaned and are dried Dry, put in super micron mill together and be crushed to 30 mesh, then add deionized water and soak 5 hours, amount of water is by being soaked raw material 7 times of medicine quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.1-0.25 weight portion and be dried place Reason, i.e. prepares volatile oil C, standby；
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil, be sufficiently stirred for 45 minutes, stands 30 minutes, filtering and impurity removing, i.e. Obtaining essential oil of traditional Chinese medicine, wherein, described miscella with the mass ratio of Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil is 2:0.5:0.4:0.6:0.5；
The mixture A that S9, essential oil of traditional Chinese medicine 0.6-1.1 weight portion step S8 prepared prepare with step S1, at 70-80 DEG C, In blender, concentrated compactness mixes 15 minutes, obtains premix material, then adds ceria 0.1-0.15 weight in premix material Amount part, active mineral matter powder 0.75-1.3 weight portion and curing agent 2-3.5 weight portion, at 65-85 DEG C, then Concentrated compactness 35 minutes, then casts in the outer surface of glass lamp shade, solidifies the demoulding, to obtain final product；Wherein, described active mineral matter Powder be germanite, fluorite, tourmaline, hexacyclic ring stone by weight the mixture of 2.5:3:3.7:2, wherein tourmaline be dravite and Elbaite is by weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following weight portion: surface activity Agent 1.7 parts, diethyltoluamide 0.2 part, butyl butyrate 1 part, Eucalyptus oil 1.2 parts, chlorhexidine acetate 0.5 part, fatty alcohol-polyoxyethylene ether 1 part of sodium sulfate and sodium benzoate 0.2 part.
It should be noted that the experiment proved that, active mineral matter powder adds appropriate ceria (CeO2), utilize The emittance of this rare earth element is high, the feature of half degradation period limit for length, and the anion that active mineral matter powder can be significantly increased produces Rate, its principle is as follows: the Ce in ceria4+Ce is changed under photoenvironment3+, in conversion process, electron-hole Recombination probability reduces, then in active mineral matter powder under the effect of the material electric field such as tourmaline, part electronics is passively with electric field side To displacement, electron-hole recombination probability reduces, thus at tourmaline/CeO2Substantial amounts of electricity has been gathered on composite powder surface The energy of solution air molecule, and then create the negative aeroion of high concentration, Ce simultaneously3+It is oxidized into again Ce4+, then repeat Aforesaid conversion process；Meanwhile, through practice detection, interpolation titanium dioxide it is being combined in the active mineral matter powder of proportioning through the present invention Cerium component, higher more than 10 times than the concentration without the active mineral matter powder anion adding ceria, r ray and natural environment Identical.
The present invention is based on motherland's traditional medicine, with reference to modern Chinese medicine pharmacological research, from the drug screening of existing Chinese medicine with anti- Reviewing card, give full play to each component synergism, wherein the effect brief introduction of primary raw material is as follows.
Omphalia: bitter cold, returns stomach large intestine channel, slightly poisonous.Parasite killing.
Semen Torreyae " herbal classic ": pathogen in main abdomen, goes three worms, and Serpentis stings.
Olibanum: ooze out for olive subject plant Boswellia carterii Boswellia carterii Birdw and congener skin zone thereof Resin, has effect of blood-activating and qi-promoting pain relieving, detumescence and promoting granulation.
Lavandula angustifolia can remove ant, except roach, acaricide, the when of being placed under wardrobe, medicated pillow, not only can replace camphor ball, moreover it is possible to stay The fragrance of one people that oozes lower, research finds, lavandula angustifolia has obvious antibacterial action, and the linalool contained in lavandula angustifolia is lavandula angustifolia Antibacterial main component, it can suppress 17 kinds of antibacterials (including gram-negative bacteria and gram-positive bacteria), the life of 10 kinds of funguses Long.
Herba anemones vitifoliae: have another name called Herba anemones vitifoliae, blow Paeonia suffruticosa, soil Paeonia suffruticosa, Qiu Mingju, your ship chrysanthemum, parasite killing；Heat-clearing and toxic substances removing, parasite killing；Clearly Pyrolysis poison.
Herba Anemones Hupehensis: 1. " Shaanxi Chinese herbal medicine ": " bitter, cool, slightly poisonous." 2. " Chinese herbal medicine is commonly used in Sichuan ": " and toil, temperature, Slightly poisonous." removing toxic substances, evacuation of pus granulation promoting, dissipating blood stasis of subsiding a swelling, have and kill maggot, wriggler, change long-pending, detumescence, dissipating blood stasis, control stubborn dermatitis, tinea alba, malaria Disease, infantile malnutrition, dysentery, carbuncle furuncle swells, scrofula, traumatic injury.
Caulis Polygoni Multiflori: Caulis Polygoni Multiflori is put down nontoxic, sweet and slightly bitter taste, enter the heart, Liver Channel, have effect of tranquilizing and blood nourishing, dispelling wind and removing obstruction in the collateral, Cure mainly the diseases such as deficiency of YIN insufficiency of blood, restlessness of asrhenia type and insomnia, rheumatic arthralgia, itchy skin eruption.
Herba Menthae: for the dry aerial parts of labiate Herba Menthae, dispelling wind and heat pathogens, the clear profit head, sore-throat relieving rash, soothing the liver row Gas.
Rhizoma Cimicifugae: have antibacterial action, to being permitted blue achorion, Du big belly microspore tinea bacterium, rust microspore tinea bacterium, redness difficult to understand Epidermophyton, staphylococcus aureus, anthrax bacillus have stronger inhibitory action；To group B streptococcus, diphtheria corynebacterium, typhoid fever bar Bacterium, bacillus pyocyaneus, escherichia coli, dysentery bacterium also have inhibitory action in various degree, also have calmness, convulsion work simultaneously With.
Origanum majorana: can improve that mood is depressed and addictive disease, especially effective to liberal-mindedness and vigorous endurance stress symptom, can expand blood vessel, Blood pressure lowering, alleviate and burden, help to eliminate cardiopalmus, have the nerve of excellence to pacify and calm function.
Vanilla: have special fragrance, has resisting fatigue and mood is gloomy, help hormone secretion, anxiety of releiving and improvement The effects such as insomnia.There is heart tonifying, supplementing the brain, stomach invigorating, removing toxic substances, wind dispelling, effect of enhancing muscle strength, make aroma type nervous system emerging Put forth energy agent and kidney-reinforcing drug, be used for treating hysteria, melancholia, sexual impotence, deficiency-heat and rheumatism.
Herba Portulacae: Portulacaceae annual herb plant.Plump succulence, without hair, high 10-30cm, be born in roadside, field and The area without shade such as ruins, flower garden.All there is distribution domestic various places.This kind is medicine food dual purpose plant.Herb hyoscine, has clearing away heat-damp and promoting diuresis, solution Poison detumescence, antiinflammatory, quench the thirst, diuresis.
Radix Salviae Miltiorrhizae: nature and flavor are bitter, are slightly cold.GUIXIN, Liver Channel." the southern regions of the Yunnan Province book on Chinese herbal medicine " is recorded: reinforcing the heart sedate, calming heart and tranquilizing mind.Control forgetful seized with terror Punching, palpitation with fear is insomnia, and has stasis-dispelling and pain-killing, promoting blood circulation to restore menstrual flow, the effect of the relieving restlessness that clears away heart-fire, and for menoxenia, amenorrhea dysmenorrhea, lump in the abdomen amasss Poly-, chest and abdomen twinge, pyretic arthralgia pain, skin infection.
Herba polygoni hydropiperis: all have inhibitory action, current clinical medicine research to show in test tube to various dysentery bacteriums, Herba polygoni hydropiperis has There are the effects such as antibacterial, antiviral, antiinflammatory, antioxidation.
The Radix Stemonae: can driving away mosquito, resisting pathogenic microbes effect, to beta hemolytic streptococcus, meningococcus, golden yellow The multiple pathomycetes such as staphylococcus, Staphylococcus albus, Bacillus typhi, pneumobacillus, bacillus pestis, anthrax bacillus have necessarily Inhibitory action, its infusion all has killing action to mosquitos and flies larva, head louse, clothing louse and Cimex bedbug etc..
Herba Pogostemonis: acrid in the mouth, slightly warm in nature.Effect: removing dampness for regulating stomach, the effect of administration of inducing sweat, solve, cure mainly dampness taste, breast gastral cavity is vexed swollen, Appetite is the most fragrant, Nausea and vomiting；Summer, heat-damp in summer was sleepy, uncomfortable in chest did not relaxed, and affection of exogenous wind-cold. the diseases such as aversion to cold is uncomfortable in chest, and have and have relatively Strong Fungistasis and antibacterial action.
The Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae): the another name river Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae), continuous poison, Radix Stellerae, chervil, vexed fresh idea, Re Jiaba, Herba Senecionis Dianthui, Radix scopoliae sinensis, perfume, Medicine sieve foretells, raw pull, flourishing bavin headdress flower, monkey root, Gelsemium elegans Benth., in Chinese medicine with its root eliminate the phlegm, pain relieving, removing food stagnancy, parasite killing.
Fructus Gardeniae: its fruit is Chinese medicine, belong to Ministry of Public Health promulgate l criticize medicine-food two-purpose resource, have hepatoprotective, function of gallbladder promoting, Blood pressure lowering, calmness, stop blooding, the effect such as detumescence, diphtheria corynebacterium, staphylococcus aureus, Bacillus typhi are had inhibitory action, to multiple Dermatophytes also has inhibitory action in various degree.
Radix Isatidis: various bacteria is had inhibitory action, infusion to bacillus subtilis, staphylococcus aureus, sarcine, Escherichia coli, Bacillus typhi, Salmonella paratyphi, dysentery (will he, Freund) bacillus, bacillus enteritidis etc. have suppression in various degree Effect；Acetone leachate also has similar effect, and effective to Hemolytic streptococcus.
Semen Ziziphi Spinosae: have the calmest and syngignoscism and anticonvulsant action, record according to " book on Chinese herbal medicine is the newest ": suppressing the hyperactive liver is managed Gas, nourishing lung-YIN, warming middle-JIAO dampness removing, astringing QI hidroschesis, benefit will, hearing-improing and eyesight improving.
It should be noted that be proven, after carrying out the Radix Salviae Miltiorrhizae of certain part by weight, Herba polygoni hydropiperis and the Radix Stemonae compounding, no Only it is remarkably improved degerming antibacterial ability, also can produce a kind of delicate fragrance taste having no side effect, refreshing, have certain Effect of refreshing oneself；, it is proven meanwhile, the Omphalia of certain part by weight, Olibanum, Semen Torreyae and Herba Anemones Hupehensis are compounded After, make the mosquito dispersing ability of said composition be significantly improved；It addition, the components such as Herba anemones vitifoliae, Rhizoma Cimicifugae, Fructus Gardeniae and Radix Isatidis are carried out After compatibility, substantially increasing the antibacterial degerming ability of compositions, through practice detection, the compositions after compounding is to Staphylococcus aureus Bacterium, anthrax bacillus, hemophilus influenza, micrococcus catarrhalis, streptococcus pneumoniae, escherichia coli, group B streptococcus, diphtheria corynebacterium, Bacillus typhi, Green pus liver bacterium, dysentery bacteriums etc. more than 30 are planted pathogenic bacteria and have certain suppression and killing action, make the present invention be provided with certain resisting Bacterium degerming ability.
The effect of the present invention:
The present invention uses Chinese medicine to compound with active mineral matter, makes the present invention be possible not only to expelling mosquito, it is also possible to anion releasing, Fresh air, simultaneously fragrant odour, character is gentle, has effect of body-building, anophelifuge, antimycotic antiseptic.
Detailed description of the invention
Embodiment 1:
A kind of preparation technology of the illuminating lamp shade with air-cleaning function, it is characterised in that: described lampshade is by following steps It is prepared from:
S1, environment-friendly resin 15 weight portion, fire retardant 6 weight portion, good solid 754 light of nano-phosphor 0.1 weight portion, vapour Ba Yan are drawn Send out agent 3 weight portion, hydroxyethyl cellulose 2 weight portion and polyetheramine catalyst 0.7 weight portion to be together placed in blender, 65 The stirring of DEG C next part high speed is mixed well, and mixing time is 30 minutes, to be mixed uniformly after take out from blender, i.e. prepare mixture A, standby；Wherein, described environment-friendly resin is epoxy soybean oil acrylate and the mixture of bisphenol A-type E51 epoxy resin, described The mass ratio of epoxy soybean oil acrylate and bisphenol A-type E51 epoxy resin is 1.5:1, described fire retardant be ammonium polyphosphate, Tripolycyanamide and the mixture of expanded graphites, the mass ratio of described ammonium polyphosphate, tripolycyanamide and expanded graphites 1.5:1.2:1, described nano-phosphor is the mixture of Ce and YAG, particle diameter≤13 μm of described nano-phosphor；
S2, by material Omphalia 65 weight portion, Semen Torreyae 25 weight portion, Herba Portulacae 4 weight portion, lavandula angustifolia 20 weight portion, Herba anemones vitifoliae 3 weight Amount part, Herba Anemones Hupehensis 5 weight portion, Caulis Polygoni Multiflori 3 weight portion, Herba Menthae 3 weight portion, Rhizoma Cimicifugae 1 weight portion, Origanum majorana 2.5 weight Part, vanilla 1.5 weight portion decontamination, it is placed in the vacuum still 2 hours of-20 DEG C together, is placed in microwave dryer the most again and carries out Pretreatment, wherein drying time is 40 minutes, and microwave power is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still Crude oil is collected with triangular flask, standby；
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e. Prepare volatile oil B, standby；
S6, by Olibanum 4 weight portion, Radix Salviae Miltiorrhizae 3 weight portion, Herba polygoni hydropiperis 4 weight portion, the Radix Stemonae 7 weight portion, Herba Pogostemonis 4 weight portion, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 3 Weight portion, Fructus Gardeniae 4 weight portion, Radix Isatidis 15 weight portion, Semen Ziziphi Spinosae 4 weight portion is cleaned and is dried, and puts in super micron mill together Be crushed to 30 mesh, then add deionized water and soak 5 hours, amount of water by 7 times of immersions crude drug quality, dispersed with stirring tune Even, prepare Traditional Chinese drug mixture, standby；
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.1 weight portion and be dried process, i.e. make Obtain volatile oil C, standby；
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil, be sufficiently stirred for 45 minutes, stands 30 minutes, filtering and impurity removing, i.e. Obtaining essential oil of traditional Chinese medicine, wherein, described miscella with the mass ratio of Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil is 2:0.5:0.4:0.6:0.5；
The mixture A that S9, essential oil of traditional Chinese medicine 1.1 weight portion step S8 prepared prepare with step S1, at 70 DEG C, at blender Middle concentrated compactness mixes 15 minutes, obtains premix material, then adds ceria 0.15 weight portion, active mineral in premix material Matter powder 0.75 weight portion and curing agent 3.5 weight portion, at 65 DEG C, then concentrated compactness 35 minutes, then water Cast the outer surface at glass lamp shade, solidify the demoulding, to obtain final product；Wherein, described active mineral matter powder be germanite, fluorite, tourmaline, Hexacyclic ring stone is by weight the mixture of 2.5:3:3.7:2, and wherein tourmaline is dravite and elbaite 5:3 by weight Mixture, particle diameter≤13 μm of described active mineral matter powder.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following weight portion: surface activity Agent 1.7 parts, diethyltoluamide 0.2 part, butyl butyrate 1 part, Eucalyptus oil 1.2 parts, chlorhexidine acetate 0.5 part, fatty alcohol-polyoxyethylene ether 1 part of sodium sulfate and sodium benzoate 0.2 part.
Embodiment 2:
A kind of preparation technology of the illuminating lamp shade with air-cleaning function, it is characterised in that: described lampshade is by following steps It is prepared from:
S1, environment-friendly resin 25 weight portion, fire retardant 3 weight portion, good solid 754 light of nano-phosphor 0.2 weight portion, vapour Ba Yan are drawn Send out agent 1.5 weight portion, hydroxyethyl cellulose 3 weight portion and polyetheramine catalyst 0.5 weight portion to be together placed in blender, The stirring of 85 DEG C of next part high speeds is mixed well, and mixing time is 15 minutes, to be mixed uniformly after take out from blender, i.e. prepare mixing Thing A, standby；Wherein, described environment-friendly resin is epoxy soybean oil acrylate and the mixture of bisphenol A-type E51 epoxy resin, institute The mass ratio stating epoxy soybean oil acrylate and bisphenol A-type E51 epoxy resin is 1.5:1, and described fire retardant is polyphosphoric acids The mixture of ammonium, tripolycyanamide and expanded graphites, the quality of described ammonium polyphosphate, tripolycyanamide and expanded graphites Ratio 1.5:1.2:1, described nano-phosphor is the mixture of Ce and YAG, particle diameter≤13 μm of described nano-phosphor；
S2, by material Omphalia 85 weight portion, Semen Torreyae 20 weight portion, Herba Portulacae 3 weight portion, lavandula angustifolia 15 weight portion, Herba anemones vitifoliae 5 weight Amount part, Herba Anemones Hupehensis 3 weight portion, Caulis Polygoni Multiflori 5 weight portion, Herba Menthae 1 weight portion, Rhizoma Cimicifugae 3 weight portion, Origanum majorana 1.5 weight Part, vanilla 2 weight portion decontamination, it is placed in the vacuum still 3 hours of-20 DEG C together, is placed in microwave dryer the most again and carries out pre- Processing, wherein drying time is 30 minutes, and microwave power is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still Crude oil is collected with triangular flask, standby；
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e. Prepare volatile oil B, standby；
S6, by Olibanum 6 weight portion, Radix Salviae Miltiorrhizae 4 weight portion, Herba polygoni hydropiperis 3 weight portion, the Radix Stemonae 9 weight portion, Herba Pogostemonis 3 weight portion, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 4 Weight portion, Fructus Gardeniae 3 weight portion, Radix Isatidis 18 weight portion, Semen Ziziphi Spinosae 3 weight portion is cleaned and is dried, and puts in super micron mill together Be crushed to 30 mesh, then add deionized water and soak 5 hours, amount of water by 7 times of immersions crude drug quality, dispersed with stirring tune Even, prepare Traditional Chinese drug mixture, standby；
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.25 weight portion and be dried process, i.e. Prepare volatile oil C, standby；
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil, be sufficiently stirred for 45 minutes, stands 30 minutes, filtering and impurity removing, i.e. Obtaining essential oil of traditional Chinese medicine, wherein, described miscella with the mass ratio of Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil is 2:0.5:0.4:0.6:0.5；
The mixture A that S9, essential oil of traditional Chinese medicine 0.6 weight portion step S8 prepared prepare with step S1, at 80 DEG C, at blender Middle concentrated compactness mixes 15 minutes, obtains premix material, then adds ceria 0.1 weight portion, active mineral in premix material Matter powder 1.3 weight portion and curing agent 2 weight portion, at 85 DEG C, then concentrated compactness 35 minutes, then cast in The outer surface of glass lamp shade, solidifies the demoulding, to obtain final product；Wherein, described active mineral matter powder is germanite, fluorite, tourmaline, six rings Stone is by weight the mixture of 2.5:3:3.7:2, and wherein tourmaline is dravite and the mixing of elbaite 5:3 by weight Thing, particle diameter≤13 μm of described active mineral matter powder.
Remaining is with embodiment 1.
The test index of the lampshade prepared by Example 1 and Example 2 of the present invention is as follows:
(1) abnormal smells from the patient inspection: sense organ, nonirritant abnormal flavour.
(2) repelling effect test.
Contrast test is carried out according to the repelling effect of ordinary lamp and lantern of the prior art with above-described embodiment 1 and embodiment 2, Test data ask for an interview table 1.
Conclusion: Example 1 and Example 2 of the present invention all can play preferable mosquito-repelling function, with ordinary lamp and lantern on market
Comparing, the present invention has obviously repelling effect.
(3) anionic textiles.
Use anion test instrument, be primarily directed to timber, Ore, ceramic material, negative ion powder are made to relevant The anion quantity that commodity (such as anion medicated clothing, necklace, woollen blanket) etc. are discharged makes measurement.
Test result is shown in Table 2.
Conclusion: the embodiment of the present invention 1, embodiment 2 can be with sustained release negative aeroions, with ordinary lamps of the prior art Tool compares, and the present invention has obviously advantage.

Claims (2)

1. the preparation technology of an illuminating lamp shade with air-cleaning function, it is characterised in that: described lampshade is by walking as follows Suddenly it is prepared from:
S1, by good to environment-friendly resin 15-25 weight portion, fire retardant 3-6 weight portion, nano-phosphor 0.1-0.2 weight portion, vapour Ba Yan Gu 754 light trigger 1.5-3 weight portions, hydroxyethyl cellulose 2-3 weight portion and polyetheramine catalyst 0.5-0.7 weight portion one With being placed in blender, mixing well 65-85 DEG C of next part high speed stirring, mixing time is 15-30 minute, to be mixed uniformly after from Blender takes out, i.e. prepares mixture A, standby；Wherein, described environment-friendly resin is epoxy soybean oil acrylate and bisphenol-A The mixture of type E51 epoxy resin, the mass ratio of described epoxy soybean oil acrylate and bisphenol A-type E51 epoxy resin is 1.5:1, described fire retardant is the mixture of ammonium polyphosphate, tripolycyanamide and expanded graphites, described ammonium polyphosphate, three The mass ratio 1.5:1.2:1 of poly cyanamid and expanded graphites, described nano-phosphor is the mixture of Ce and YAG, described Particle diameter≤13 μm of nano-phosphor；
S2, by material Omphalia 65-85 weight portion, Semen Torreyae 20-25 weight portion, Herba Portulacae 3-4 weight portion, lavandula angustifolia 15-20 weight Part, Herba anemones vitifoliae 3-5 weight portion, Herba Anemones Hupehensis 3-5 weight portion, Caulis Polygoni Multiflori 3-5 weight portion, Herba Menthae 1-3 weight portion, Rhizoma Cimicifugae 1-3 Weight portion, Origanum majorana 1.5-2.5 weight portion and vanilla 1.5-2 weight portion decontamination, be placed in the vacuum still of-20 DEG C together 2-3 hour, being placed in microwave dryer the most again and carry out pretreatment, wherein drying time is 30-40 minute, and microwave power is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still Crude oil is collected with triangular flask, standby；
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e. Prepare volatile oil B, standby；
S6, by Olibanum 4-6 weight portion, Radix Salviae Miltiorrhizae 3-4 weight portion, Herba polygoni hydropiperis 3-4 weight portion, Radix Stemonae 7-9 weight portion, Herba Pogostemonis 3-4 weight Amount part, Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 3-4 weight portion, Fructus Gardeniae 3-4 weight portion, Radix Isatidis 15-18 weight portion and Semen Ziziphi Spinosae 3-4 weight portion are cleaned and are dried Dry, put in super micron mill together and be crushed to 30 mesh, then add deionized water and soak 5 hours, amount of water is by being soaked raw material 7 times of medicine quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.1-0.25 weight portion and be dried place Reason, i.e. prepares volatile oil C, standby；
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil, be sufficiently stirred for 45 minutes, stands 30 minutes, filtering and impurity removing, i.e. Obtaining essential oil of traditional Chinese medicine, wherein, described miscella with the mass ratio of Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil is 2:0.5:0.4:0.6:0.5；
The mixture A that S9, essential oil of traditional Chinese medicine 0.6-1.1 weight portion step S8 prepared prepare with step S1, at 70-80 DEG C, In blender, concentrated compactness mixes 15 minutes, obtains premix material, then adds ceria 0.1-0.15 weight in premix material Amount part, active mineral matter powder 0.75-1.3 weight portion and curing agent 2-3.5 weight portion, at 65-85 DEG C, then Concentrated compactness 35 minutes, then casts in the outer surface of glass lamp shade, solidifies the demoulding, to obtain final product；Wherein, described active mineral matter Powder be germanite, fluorite, tourmaline, hexacyclic ring stone by weight the mixture of 2.5:3:3.7:2, wherein tourmaline be dravite and Elbaite is by weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder.
The preparation technology of a kind of illuminating lamp shade with air-cleaning function the most according to claim 1, it is characterised in that: Essential oil of traditional Chinese medicine in step s 8 also includes the component of following weight portion: 1.7 parts of surfactant, diethyltoluamide 0.2 part, butanoic acid fourth Ester 1 part, Eucalyptus oil 1.2 parts, chlorhexidine acetate 0.5 part, polyoxyethylenated alcohol sodium sulfate 1 part and sodium benzoate 0.2 part.
CN201610574155.5A 2016-05-23 2016-07-20 Preparation process of illuminating lampshade with air purification function Pending CN106046693A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109749357A (en) * 2017-11-01 2019-05-14 丹阳百斯特智能系统有限公司 A kind of high intensity table lamp lampshade

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109749357A (en) * 2017-11-01 2019-05-14 丹阳百斯特智能系统有限公司 A kind of high intensity table lamp lampshade

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