CN106281007A - A kind of preparation method of multi-functional environment-protection LED lamp cover - Google Patents

A kind of preparation method of multi-functional environment-protection LED lamp cover Download PDF

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CN106281007A
CN106281007A CN201610652253.6A CN201610652253A CN106281007A CN 106281007 A CN106281007 A CN 106281007A CN 201610652253 A CN201610652253 A CN 201610652253A CN 106281007 A CN106281007 A CN 106281007A
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史玉桂
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    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
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Abstract

A kind of preparation method of multi-functional environment-protection LED lamp cover, it is made up of environment-friendly resin, fire retardant, curing agent, nano-phosphor, good solid 754 light triggers of vapour Ba Yan, polyetheramine catalyst, hydroxyethyl cellulose, ceria and active mineral matter powder etc., the present invention not only has effect of expelling mosquito, can be with anion releasing, there is certain function removing the pollutant such as formaldehyde, toluene and TVOC, fragrant odour simultaneously, character is gentle, enriches the use function of conventional lamp.

Description

A kind of preparation method of multi-functional environment-protection LED lamp cover
The application is the Application No. 2016105742083 submitted to July 20 2016 applying date, invention entitled " one The preparation method of kind of multi-functional environment-protection LED lamp cover " the divisional application of Chinese invention patent application.
Technical field
The present invention relates to field of illuminating lamps, particularly relate to the preparation method of a kind of multi-functional environment-protection LED lamp cover.
Background technology
Along with the development and progress of society, the environmental protection idea of people is increasingly stronger, thus the illumination dress of environmental protection Put and can more be favored by people, day by day ripe LED technology due to its have efficiently, energy-saving and environmental protection, length in service life, merit The advantages such as rate is low, LED illumination lamp the most gradually starts to replace traditional lighting.
On the one hand, along with the continuous rising of Global Temperature, the population of mosquito and quantity all will be greatly improved, the most day by day threaten The health of the mankind.Mosquito, in addition to directly stining thorn and sucking blood, harass sleep, more seriously propagates multiple disease.The mosquito of China passes disease Having malaria, Filariasis, epidemic encephalitis type B and dengue fever (or dengue hemorrhagic fever) four class, mosquito passes more important virosis Also have yellow fever and various equine encephalitis etc..
On the other hand, by negative aeroion Technology application in electricity-saving lamp product, the electricity-saving lamp after using is long-term in indoor Release negative aeroion, especially negative oxygen ion.Owing to it is structurally similar to ultra-oxygen anion free radical, therefore there is phase As biological activity, it is possible to make live biological cell electronegative, so that virus loses the attacking ability to cell；Meanwhile, Negative oxygen ion can react with the finishing pollution thing such as formaldehyde, toluene, TVOC, product be nonpoisonous and tasteless carbon dioxide and Water, the generation of non-secondary pollution, there is certain effect purified the air of a room, such as, in artificial air's anion environment, In air, mycete, bacterial population can reduce by more than 90% after measured.After negative oxygen ion is inhaled into human body, can regulate neural emerging Put forth energy state, improve the ventilatory of lung, improve blood circulation, enhance metabolism, strengthen immune system ability, make people's spirit shake Putting forth energy, improve work efficiency etc., the numerous diseases such as hypertension, asthma, influenza, insomnia, arthritis are also had certain treatment to make by it With, so people's anion is called " vitamin in air " " long-lived element ".
So far, the Technology design making conventional lamp product simultaneously have mosquito dispersing and negative ion-releasing function does not also have See.
Summary of the invention
The deficiency existed for prior art, the technical problem to be solved is to provide a kind of multi-functional environment-protection The preparation method of LED lamp cover, prepared coating not only long-term negative ion release, also there is certain expelling mosquito effect, with Time also there is certain antibacterial action, there is the effect achieved many things at one stroke.
It is an object of the invention to be achieved through the following technical solutions:
A kind of preparation method of multi-functional environment-protection LED lamp cover, it is characterised in that: described lampshade is prepared from by following steps:
S1, by good to environment-friendly resin 15-25 weight portion, fire retardant 3-6 weight portion, nano-phosphor 0.1-0.2 weight portion, vapour Ba Yan Gu 754 light trigger 1.5-3 weight portions, hydroxyethyl cellulose 2-3 weight portion and polyetheramine catalyst 0.5-0.7 weight portion one With being placed in blender, mixing well 65-85 DEG C of next part high speed stirring, mixing time is 15-30 minute, to be mixed uniformly after from Blender takes out, i.e. prepares mixture A, standby；Wherein, described environment-friendly resin is epoxy soybean oil acrylate and bisphenol-A The mixture of type E51 epoxy resin, the mass ratio of described epoxy soybean oil acrylate and bisphenol A-type E51 epoxy resin is 1.5:1, described fire retardant is the mixture of ammonium polyphosphate, tripolycyanamide and expanded graphites, described ammonium polyphosphate, three The mass ratio 1.5:1.2:1 of poly cyanamid and expanded graphites, described nano-phosphor is the mixture of Ce and YAG, described Particle diameter≤13 μm of nano-phosphor；
S2, by material Fructus Carpesii 65-85 weight portion, Herba Artemisiae Scopariae 20-25 weight portion, Mallotus repandus (Willd.) Muell. Arg. 4-6 weight portion, lavandula angustifolia 15-20 weight Part, Herba Anemones Hupehensis 3-5 weight portion, Caulis Polygoni Multiflori 3-5 weight portion, rhododendron molle (bl.) g.don 1-3 weight portion, Rhizoma Atractylodis Macrocephalae 1-3 weight portion and sweet horse Yu Lan 1.5-2.5 weight portion decontamination, is placed in vacuum still 2-3 hour of-20 DEG C together, is placed in microwave dryer the most again and carries out Pretreatment, wherein drying time is 30-40 minute, and microwave power is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still Crude oil is collected with triangular flask, standby；
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e. Prepare volatile oil B, standby；
S6, by vanilla 1.5-2 weight portion, Herba Portulacae 3-4 weight portion, Radix Salviae Miltiorrhizae 3-4 weight portion, Herba polygoni hydropiperis 3-4 weight portion, the Radix Stemonae 7-9 weight portion, Herba Pogostemonis 3-4 weight portion, Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 3-4 weight portion, Fructus Gardeniae 3-4 weight portion, Radix Isatidis 15-18 weight portion and Ziziphi Spinosae Core 3-4 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 30 mesh, then adds deionized water and soaks 5 hours, adds The water yield by 7 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.1-0.25 weight portion and be dried place Reason, i.e. prepares volatile oil C, standby；
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil, be sufficiently stirred for 45 minutes, stands 30 minutes, filtering and impurity removing, i.e. Obtaining essential oil of traditional Chinese medicine, wherein, described miscella with the mass ratio of Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil is 2:0.5:0.4:0.6:0.5；
The mixture A that S9, essential oil of traditional Chinese medicine 0.6-1.1 weight portion step S8 prepared prepare with step S1, at 70-80 DEG C, In blender, concentrated compactness mixes 15 minutes, obtains premix material, then adds ceria 0.1-0.15 weight in premix material Amount part, active mineral matter powder 0.75-1.3 weight portion and curing agent 2-3.5 weight portion, at 65-85 DEG C, then Concentrated compactness 35 minutes, then casts in the outer surface of glass lamp shade, solidifies the demoulding, to obtain final product；Wherein, described active mineral matter Powder be germanite, fluorite, tourmaline, hexacyclic ring stone by weight the mixture of 2.5:3:3.7:2, wherein tourmaline be dravite and Elbaite is by weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following weight portion: surface activity Agent 1.7 parts, diethyltoluamide 0.2 part, butyl butyrate 1 part, Eucalyptus oil 1.2 parts, chlorhexidine acetate 0.5 part, fatty alcohol-polyoxyethylene ether 1 part of sodium sulfate and sodium benzoate 0.2 part.
It should be noted that the experiment proved that, active mineral matter powder adds appropriate ceria (CeO2), utilize The emittance of this rare earth element is high, the feature of half degradation period limit for length, and the anion that active mineral matter powder can be significantly increased produces Rate, its principle is as follows: the Ce in ceria4+Ce is changed under photoenvironment3+, in conversion process, electron-hole Recombination probability reduces, then in active mineral matter powder under the effect of the material electric field such as tourmaline, part electronics is passively with electric field side To displacement, electron-hole recombination probability reduces, thus at tourmaline/CeO2Substantial amounts of electricity has been gathered on composite powder surface The energy of solution air molecule, and then create the negative aeroion of high concentration, Ce simultaneously3+It is oxidized into again Ce4+, then repeat Aforesaid conversion process；Meanwhile, through practice detection, interpolation titanium dioxide it is being combined in the active mineral matter powder of proportioning through the present invention Cerium component, higher more than 10 times than the concentration without the active mineral matter powder anion adding ceria, r ray and natural environment Identical.
The present invention is based on motherland's traditional medicine, with reference to modern Chinese medicine pharmacological research, from the drug screening of existing Chinese medicine with anti- Reviewing card, give full play to each component synergism, wherein the effect brief introduction of primary raw material is as follows.
Fructus Carpesii: [mongolian medicine] capsule gives a chapter ancient: fruit is used for ascariasis, enterobiasis, skin infection, and joint wound, " illiteracy plants medicine to scrofula Will " fruit: bitter, pungent, flat.Eliminating stagnated food and killing intestinal worms
Herba Artemisiae Scopariae: have significant hepatic cholagogic effect, improves microcirculation, and has blood pressure lowering, blood fat reducing, anticoagulation, and diuresis is antipyretic flat Breathe heavily, drive away ascarid and suppress the effect of multiple pathogenic dermatophytes and antibacterial.
Mallotus repandus (Willd.) Muell. Arg.: be distributed in Guangxi, Guangdong, Hainan and Taiwan in China, also there is distribution in the country such as southeast, Asia more.Enter Medicine has the effect dispeled the wind.
Lavandula angustifolia can remove ant, except roach, acaricide, the when of being placed under wardrobe, medicated pillow, not only can replace camphor ball, moreover it is possible to stay The fragrance of one people that oozes lower, research finds, lavandula angustifolia has obvious antibacterial action, and the linalool contained in lavandula angustifolia is lavandula angustifolia Antibacterial main component, it can suppress 17 kinds of antibacterials (including gram-negative bacteria and gram-positive bacteria), the life of 10 kinds of funguses Long.
Herba Anemones Hupehensis: 1. " Shaanxi Chinese herbal medicine ": " bitter, cool, slightly poisonous." 2. " Chinese herbal medicine is commonly used in Sichuan ": " and toil, temperature, Slightly poisonous." removing toxic substances, evacuation of pus granulation promoting, dissipating blood stasis of subsiding a swelling, have and kill maggot, wriggler, change long-pending, detumescence, dissipating blood stasis, control stubborn dermatitis, tinea alba, malaria Disease, infantile malnutrition, dysentery, carbuncle furuncle swells, scrofula, traumatic injury.
Caulis Polygoni Multiflori: Caulis Polygoni Multiflori is put down nontoxic, sweet and slightly bitter taste, enter the heart, Liver Channel, have effect of tranquilizing and blood nourishing, dispelling wind and removing obstruction in the collateral, Cure mainly the diseases such as deficiency of YIN insufficiency of blood, restlessness of asrhenia type and insomnia, rheumatic arthralgia, itchy skin eruption.
Rhododendron molle (bl.) g.don: have another name called Flos Rhododendri Mollis, Azalea pontica, yellow Rhododendron simsii Planch., there is expelling wind and removing dampness；Analgesic therapy；Effect of parasite killing.
The Rhizoma Atractylodis Macrocephalae: belong to Compositae, acrothesium floccosum, star nocardia are had suppression to make by [WTBX herbaceos perennial With.Decoct also has inhibitory action to meningococcus.Nearly report Rhizoma Atractylodis Macrocephalae decoct and decoction of four noble drugs are to Bacillus typhi, paratyphoid A Bacillus, shigella flexneri, escherichia coli, bacillus pyocyaneus etc. all have bacteriostasis in various degree.
Origanum majorana: can improve that mood is depressed and addictive disease, especially effective to liberal-mindedness and vigorous endurance stress symptom, can expand blood vessel, Blood pressure lowering, alleviate and burden, help to eliminate cardiopalmus, have the nerve of excellence to pacify and calm function.
Vanilla: have special fragrance, has resisting fatigue and mood is gloomy, help hormone secretion, anxiety of releiving and improvement The effects such as insomnia.There is heart tonifying, supplementing the brain, stomach invigorating, removing toxic substances, wind dispelling, effect of enhancing muscle strength, make aroma type nervous system emerging Put forth energy agent and kidney-reinforcing drug, be used for treating hysteria, melancholia, sexual impotence, deficiency-heat and rheumatism.
Herba Portulacae: Portulacaceae annual herb plant.Plump succulence, without hair, high 10-30cm, be born in roadside, field and The area without shade such as ruins, flower garden.All there is distribution domestic various places.This kind is medicine food dual purpose plant.Herb hyoscine, has clearing away heat-damp and promoting diuresis, solution Poison detumescence, antiinflammatory, quench the thirst, diuresis.
Radix Salviae Miltiorrhizae: nature and flavor are bitter, are slightly cold.GUIXIN, Liver Channel." the southern regions of the Yunnan Province book on Chinese herbal medicine " is recorded: reinforcing the heart sedate, calming heart and tranquilizing mind.Control forgetful seized with terror Punching, palpitation with fear is insomnia, and has stasis-dispelling and pain-killing, promoting blood circulation to restore menstrual flow, the effect of the relieving restlessness that clears away heart-fire, and for menoxenia, amenorrhea dysmenorrhea, lump in the abdomen amasss Poly-, chest and abdomen twinge, pyretic arthralgia pain, skin infection.
Herba polygoni hydropiperis: all have inhibitory action, current clinical medicine research to show in test tube to various dysentery bacteriums, Herba polygoni hydropiperis has There are the effects such as antibacterial, antiviral, antiinflammatory, antioxidation.
The Radix Stemonae: can driving away mosquito, resisting pathogenic microbes effect, to beta hemolytic streptococcus, meningococcus, golden yellow The multiple pathomycetes such as staphylococcus, Staphylococcus albus, Bacillus typhi, pneumobacillus, bacillus pestis, anthrax bacillus have necessarily Inhibitory action, its infusion all has killing action to mosquitos and flies larva, head louse, clothing louse and Cimex bedbug etc..
Herba Pogostemonis: acrid in the mouth, slightly warm in nature.Effect: removing dampness for regulating stomach, the effect of administration of inducing sweat, solve, cure mainly dampness taste, breast gastral cavity is vexed swollen, Appetite is the most fragrant, Nausea and vomiting；Summer, heat-damp in summer was sleepy, uncomfortable in chest did not relaxed, and affection of exogenous wind-cold. the diseases such as aversion to cold is uncomfortable in chest, and have and have relatively Strong Fungistasis and antibacterial action.
The Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae): the another name river Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae), continuous poison, Radix Stellerae, chervil, vexed fresh idea, Re Jiaba, Herba Senecionis Dianthui, Radix scopoliae sinensis, perfume, Medicine sieve foretells, raw pull, flourishing bavin headdress flower, monkey root, Gelsemium elegans Benth., in Chinese medicine with its root eliminate the phlegm, pain relieving, removing food stagnancy, parasite killing.
Fructus Gardeniae: its fruit is Chinese medicine, belong to Ministry of Public Health promulgate l criticize medicine-food two-purpose resource, have hepatoprotective, function of gallbladder promoting, Blood pressure lowering, calmness, stop blooding, the effect such as detumescence, diphtheria corynebacterium, staphylococcus aureus, Bacillus typhi are had inhibitory action, to multiple Dermatophytes also has inhibitory action in various degree.
Radix Isatidis: various bacteria is had inhibitory action, infusion to bacillus subtilis, staphylococcus aureus, sarcine, Escherichia coli, Bacillus typhi, Salmonella paratyphi, dysentery (will he, Freund) bacillus, bacillus enteritidis etc. have suppression in various degree Effect；Acetone leachate also has similar effect, and effective to Hemolytic streptococcus.
Semen Ziziphi Spinosae: have the calmest and syngignoscism and anticonvulsant action, record according to " book on Chinese herbal medicine is the newest ": suppressing the hyperactive liver is managed Gas, nourishing lung-YIN, warming middle-JIAO dampness removing, astringing QI hidroschesis, benefit will, hearing-improing and eyesight improving.
It should be noted that be proven, after carrying out the Radix Salviae Miltiorrhizae of certain part by weight, Herba polygoni hydropiperis and the Radix Stemonae compounding, no Only it is remarkably improved degerming antibacterial ability, also can produce a kind of delicate fragrance taste having no side effect, refreshing, have certain Effect of refreshing oneself；, it is proven meanwhile, the Fructus Carpesii of certain part by weight, Herba Artemisiae Scopariae, rhododendron molle (bl.) g.don and Herba Anemones Hupehensis are compounded After, make the mosquito dispersing ability of said composition be significantly improved；It addition, Mallotus repandus (Willd.) Muell. Arg., lavandula angustifolia, the Rhizoma Atractylodis Macrocephalae, Radix Isatidis and Fructus Gardeniae etc. After component carries out compatibility, substantially increasing the antibacterial degerming ability of compositions, through practice detection, the compositions after compounding is to golden yellow Color staphylococcus, anthrax bacillus, hemophilus influenza, micrococcus catarrhalis, streptococcus pneumoniae, escherichia coli, group B streptococcus, diphtheria corynebacterium, Bacillus typhi, green pus liver bacterium, dysentery bacteriums etc. more than 40 are planted pathogenic bacteria and have certain suppression and killing action, make the present invention be provided with Certain antibacterial degerming ability.
The effect of the present invention:
The present invention uses Chinese medicine to compound with active mineral matter, makes the present invention be possible not only to expelling mosquito, it is also possible to anion releasing, Fresh air, simultaneously fragrant odour, character is gentle, has effect of body-building, anophelifuge, antimycotic antiseptic.
Detailed description of the invention
Embodiment 1:
A kind of preparation method of multi-functional environment-protection LED lamp cover, it is characterised in that: described lampshade is prepared from by following steps:
S1, environment-friendly resin 15 weight portion, fire retardant 6 weight portion, good solid 754 light of nano-phosphor 0.1 weight portion, vapour Ba Yan are drawn Send out agent 3 weight portion, hydroxyethyl cellulose 2 weight portion and polyetheramine catalyst 0.7 weight portion to be together placed in blender, 65 The stirring of DEG C next part high speed is mixed well, and mixing time is 30 minutes, to be mixed uniformly after take out from blender, i.e. prepare mixture A, standby；Wherein, described environment-friendly resin is epoxy soybean oil acrylate and the mixture of bisphenol A-type E51 epoxy resin, described The mass ratio of epoxy soybean oil acrylate and bisphenol A-type E51 epoxy resin is 1.5:1, described fire retardant be ammonium polyphosphate, Tripolycyanamide and the mixture of expanded graphites, the mass ratio of described ammonium polyphosphate, tripolycyanamide and expanded graphites 1.5:1.2:1, described nano-phosphor is the mixture of Ce and YAG, particle diameter≤13 μm of described nano-phosphor；
S2, by material Fructus Carpesii 65 weight portion, Herba Artemisiae Scopariae 25 weight portion, Mallotus repandus (Willd.) Muell. Arg. 4 weight portion, lavandula angustifolia 20 weight portion, Hubei anemone Spend 3 weight portions, Caulis Polygoni Multiflori 5 weight portion, rhododendron molle (bl.) g.don 1 weight portion, the Rhizoma Atractylodis Macrocephalae 3 weight portion, Origanum majorana 1.5 weight portion decontamination, one Acting the vacuum still 2 hours being placed in-20 DEG C, be placed in microwave dryer the most again and carry out pretreatment, wherein drying time is 40 minutes, Microwave power is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still Crude oil is collected with triangular flask, standby；
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e. Prepare volatile oil B, standby；
S6, by vanilla 2 weight portion, Herba Portulacae 3 weight portion, Radix Salviae Miltiorrhizae 4 weight portion, Herba polygoni hydropiperis 3 weight portion, the Radix Stemonae 9 weight portion, the leaves of pulse plants Fragrant 3 weight portions, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 4 weight portion, Fructus Gardeniae 3 weight portion, Radix Isatidis 18 weight portion, Semen Ziziphi Spinosae 3 weight portion is cleaned and is dried, throws together Enter and super micron mill be crushed to 30 mesh, then add deionized water soak 5 hours, amount of water by immersion crude drug quality 7 Times, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.1 weight portion and be dried process, i.e. make Obtain volatile oil C, standby；
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil, be sufficiently stirred for 45 minutes, stands 30 minutes, filtering and impurity removing, i.e. Obtaining essential oil of traditional Chinese medicine, wherein, described miscella with the mass ratio of Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil is 2:0.5:0.4:0.6:0.5；
The mixture A that S9, essential oil of traditional Chinese medicine 1.1 weight portion step S8 prepared prepare with step S1, at 70 DEG C, at blender Middle concentrated compactness mixes 15 minutes, obtains premix material, then adds ceria 0.15 weight portion, active mineral in premix material Matter powder 0.75 weight portion and curing agent 3.5 weight portion, at 65 DEG C, then concentrated compactness 35 minutes, then water Cast the outer surface at glass lamp shade, solidify the demoulding, to obtain final product；Wherein, described active mineral matter powder be germanite, fluorite, tourmaline, Hexacyclic ring stone is by weight the mixture of 2.5:3:3.7:2, and wherein tourmaline is dravite and elbaite 5:3 by weight Mixture, particle diameter≤13 μm of described active mineral matter powder.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following weight portion: surface activity Agent 1.7 parts, diethyltoluamide 0.2 part, butyl butyrate 1 part, Eucalyptus oil 1.2 parts, chlorhexidine acetate 0.5 part, fatty alcohol-polyoxyethylene ether 1 part of sodium sulfate and sodium benzoate 0.2 part.
Embodiment 2:
A kind of preparation method of multi-functional environment-protection LED lamp cover, it is characterised in that: described lampshade is prepared from by following steps:
S1, environment-friendly resin 25 weight portion, fire retardant 3 weight portion, good solid 754 light of nano-phosphor 0.2 weight portion, vapour Ba Yan are drawn Send out agent 1.5 weight portion, hydroxyethyl cellulose 3 weight portion and polyetheramine catalyst 0.5 weight portion to be together placed in blender, The stirring of 85 DEG C of next part high speeds is mixed well, and mixing time is 15 minutes, to be mixed uniformly after take out from blender, i.e. prepare mixing Thing A, standby；Wherein, described environment-friendly resin is epoxy soybean oil acrylate and the mixture of bisphenol A-type E51 epoxy resin, institute The mass ratio stating epoxy soybean oil acrylate and bisphenol A-type E51 epoxy resin is 1.5:1, and described fire retardant is polyphosphoric acids The mixture of ammonium, tripolycyanamide and expanded graphites, the quality of described ammonium polyphosphate, tripolycyanamide and expanded graphites Ratio 1.5:1.2:1, described nano-phosphor is the mixture of Ce and YAG, particle diameter≤13 μm of described nano-phosphor；
S2, by material Fructus Carpesii 85 weight portion, Herba Artemisiae Scopariae 20 weight portion, Mallotus repandus (Willd.) Muell. Arg. 6 weight portion, lavandula angustifolia 15 weight portion, Hubei anemone Spend 5 weight portions, Caulis Polygoni Multiflori 3 weight portion, rhododendron molle (bl.) g.don 3 weight portion, the Rhizoma Atractylodis Macrocephalae 1 weight portion, Origanum majorana 2.5 weight portion decontamination, one Acting the vacuum still 3 hours being placed in-20 DEG C, be placed in microwave dryer the most again and carry out pretreatment, wherein drying time is 30 minutes, Microwave power is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still Crude oil is collected with triangular flask, standby；
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e. Prepare volatile oil B, standby；
S6, by vanilla 1.5 weight portion, Herba Portulacae 4 weight portion, Radix Salviae Miltiorrhizae 3 weight portion, Herba polygoni hydropiperis 4 weight portion, the Radix Stemonae 7 weight portion, Herba Pogostemonis 4 weight portion, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 3 weight portion, Fructus Gardeniae 4 weight portion, Radix Isatidis 15 weight portion, Semen Ziziphi Spinosae 4 weight portion is cleaned and is dried, together Put in super micron mill and be crushed to 30 mesh, then add deionized water and soak 5 hours, amount of water by immersion crude drug quality 7 times, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.25 weight portion and be dried process, i.e. Prepare volatile oil C, standby；
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil, be sufficiently stirred for 45 minutes, stands 30 minutes, filtering and impurity removing, i.e. Obtaining essential oil of traditional Chinese medicine, wherein, described miscella with the mass ratio of Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil is 2:0.5:0.4:0.6:0.5；
The mixture A that S9, essential oil of traditional Chinese medicine 0.6 weight portion step S8 prepared prepare with step S1, at 80 DEG C, at blender Middle concentrated compactness mixes 15 minutes, obtains premix material, then adds ceria 0.1 weight portion, active mineral in premix material Matter powder 1.3 weight portion and curing agent 2 weight portion, at 85 DEG C, then concentrated compactness 35 minutes, then cast in The outer surface of glass lamp shade, solidifies the demoulding, to obtain final product；Wherein, described active mineral matter powder is germanite, fluorite, tourmaline, six rings Stone is by weight the mixture of 2.5:3:3.7:2, and wherein tourmaline is dravite and the mixing of elbaite 5:3 by weight Thing, particle diameter≤13 μm of described active mineral matter powder.
Remaining is with embodiment 1.
The test index of the lampshade prepared by Example 1 and Example 2 of the present invention is as follows:
(1) abnormal smells from the patient inspection: sense organ, nonirritant abnormal flavour.
(2) repelling effect test.
Contrast test is carried out according to the repelling effect of ordinary lamp and lantern of the prior art with above-described embodiment 1 and embodiment 2, Test data ask for an interview table 1.
Conclusion: Example 1 and Example 2 of the present invention all can play preferable mosquito-repelling function, with ordinary lamp and lantern on market
Comparing, the present invention has obviously repelling effect.
(3) anionic textiles.
Use anion test instrument, be primarily directed to timber, Ore, ceramic material, negative ion powder are made to relevant The anion quantity that commodity (such as anion medicated clothing, necklace, woollen blanket) etc. are discharged makes measurement.
Test result is shown in Table 2.
Conclusion: the embodiment of the present invention 1, embodiment 2 can be with sustained release negative aeroions, with ordinary lamps of the prior art Tool compares, and the present invention has obviously advantage.

Claims (1)

1. the preparation method of a multi-functional environment-protection LED lamp cover, it is characterised in that: described lampshade prepared by following steps and Become:
S1, by good to environment-friendly resin 15-25 weight portion, fire retardant 3-6 weight portion, nano-phosphor 0.1-0.2 weight portion, vapour Ba Yan Gu 754 light trigger 1.5-3 weight portions, hydroxyethyl cellulose 2-3 weight portion and polyetheramine catalyst 0.5-0.7 weight portion one With being placed in blender, mixing well 65-85 DEG C of next part high speed stirring, mixing time is 15-30 minute, to be mixed uniformly after from Blender takes out, i.e. prepares mixture A, standby；Wherein, described environment-friendly resin is epoxy soybean oil acrylate and bisphenol-A The mixture of type E51 epoxy resin, the mass ratio of described epoxy soybean oil acrylate and bisphenol A-type E51 epoxy resin is 1.5:1, described fire retardant is the mixture of ammonium polyphosphate, tripolycyanamide and expanded graphites, described ammonium polyphosphate, three The mass ratio 1.5:1.2:1 of poly cyanamid and expanded graphites, described nano-phosphor is the mixture of Ce and YAG, described Particle diameter≤13 μm of nano-phosphor；
S2, by material Fructus Carpesii 65-85 weight portion, Herba Artemisiae Scopariae 20-25 weight portion, Mallotus repandus (Willd.) Muell. Arg. 4-6 weight portion, lavandula angustifolia 15-20 weight Part, Herba Anemones Hupehensis 3-5 weight portion, Caulis Polygoni Multiflori 3-5 weight portion, rhododendron molle (bl.) g.don 1-3 weight portion, Rhizoma Atractylodis Macrocephalae 1-3 weight portion and sweet horse Yu Lan 1.5-2.5 weight portion decontamination, is placed in vacuum still 2-3 hour of-20 DEG C together, is placed in microwave dryer the most again and carries out Pretreatment, wherein drying time is 30-40 minute, and microwave power is 17kw；
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby With；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still Crude oil is collected with triangular flask, standby；
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e. Prepare volatile oil B, standby；
S6, by vanilla 1.5-2 weight portion, Herba Portulacae 3-4 weight portion, Radix Salviae Miltiorrhizae 3-4 weight portion, Herba polygoni hydropiperis 3-4 weight portion, the Radix Stemonae 7-9 weight portion, Herba Pogostemonis 3-4 weight portion, Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 3-4 weight portion, Fructus Gardeniae 3-4 weight portion, Radix Isatidis 15-18 weight portion and Ziziphi Spinosae Core 3-4 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 30 mesh, then adds deionized water and soaks 5 hours, adds The water yield by 7 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.1-0.25 weight portion and be dried place Reason, i.e. prepares volatile oil C, standby；
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil, be sufficiently stirred for 45 minutes, stands 30 minutes, filtering and impurity removing, i.e. Obtaining essential oil of traditional Chinese medicine, wherein, described miscella with the mass ratio of Peppermint essential oil, Flos Rosae Rugosae quintessence oil, Stigma Croci quintessence oil and Juniperus rigida Sieb.et Zucc. quintessence oil is 2:0.5:0.4:0.6:0.5；Wherein, described essential oil of traditional Chinese medicine also includes the component of following weight portion: 1.7 parts of surfactant, keep away Mosquito amine 0.2 part, butyl butyrate 1 part, Eucalyptus oil 1.2 parts, chlorhexidine acetate 0.5 part, polyoxyethylenated alcohol sodium sulfate 1 part and Sodium benzoate 0.2 part；
The mixture A that S9, essential oil of traditional Chinese medicine 0.6-1.1 weight portion step S8 prepared prepare with step S1, at 70-80 DEG C, In blender, concentrated compactness mixes 15 minutes, obtains premix material, then adds ceria 0.1-0.15 weight in premix material Amount part, active mineral matter powder 0.75-1.3 weight portion and curing agent 2-3.5 weight portion, at 65-85 DEG C, then Concentrated compactness 35 minutes, then casts in the outer surface of glass lamp shade, solidifies the demoulding, to obtain final product；Wherein, described active mineral matter Powder be germanite, fluorite, tourmaline, hexacyclic ring stone by weight the mixture of 2.5:3:3.7:2, wherein tourmaline be dravite and Elbaite is by weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder.
CN201610652253.6A 2016-05-23 2016-07-20 A kind of preparation method of multi-functional environment-protection LED lamp cover Withdrawn CN106281007A (en)

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