CN107418388A - A kind of preparation method containing active mineral matter powder environmental protection lampshade - Google Patents

A kind of preparation method containing active mineral matter powder environmental protection lampshade Download PDF

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CN107418388A
CN107418388A CN201710134993.5A CN201710134993A CN107418388A CN 107418388 A CN107418388 A CN 107418388A CN 201710134993 A CN201710134993 A CN 201710134993A CN 107418388 A CN107418388 A CN 107418388A
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essential oil
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史玉桂
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    • C09D7/40—Additives
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    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
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    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
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Abstract

A kind of preparation method containing active mineral matter powder environmental protection lampshade, including lampshade shell, the lampshade shell includes basic unit and functional coating, the basic unit and functional coating from-inner-to-outer are arranged in order, the functional coating coats the outer surface of basic unit completely, the functional coating includes active mineral matter powder and essential oil of traditional Chinese medicine composition, the present invention not only has the effect of expelling mosquito, anion can also be discharged, with certain function of removing the pollutants such as formaldehyde, toluene and TVOC, fragrant odour simultaneously, property is gentle, enriches the use function of conventional lamp.

Description

A kind of preparation method containing active mineral matter powder environmental protection lampshade
Technical field
The present invention relates to field of illuminating lamps, more particularly to a kind of preparation side containing active mineral matter powder environmental protection lampshade Method.
Background technology
With the development and progress of society, the illumination that the green idea of people is more and more stronger thus green fills Put more to be favored by people, and increasingly ripe LED technology is because it is with efficient, energy-saving and environmental protection, service life length, work( The low advantage of rate, LED illumination lamp have gradually started to substitute traditional illuminator.
On the one hand, as the continuous rise of Global Temperature, the population of mosquito and quantity will all greatly improve, just increasingly threaten The health of the mankind.Mosquito except directly sting thorn suck blood, harass sleep in addition to, more seriously propagate a variety of diseases.The mosquito in China passes disease There are malaria, Filariasis, Japanese Type-B encephalitis and dengue fever（Or dengue hemorrhagic fever）Four classes, mosquito pass more important virosis Also yellow fever and various equine encephalitis etc..
On the other hand, by negative aeroion Technology application in electricity-saving lamp product, the electricity-saving lamp after use is long-term indoors Discharge negative aeroion, especially negative oxygen ion.Due to its in structure it is similar to ultra-oxygen anion free radical, therefore there is phase As bioactivity, biological cell living can be made negatively charged, so that virus loses attacking ability to cell；Meanwhile Negative oxygen ion can react with finishing pollution things such as formaldehyde, toluene, TVOC, product be nonpoisonous and tasteless carbon dioxide and Water, the generation of non-secondary pollution, with certain the effect of purifying the air of a room, for example, in artificial air's anion environment, Mould, bacterial population can reduce by more than 90% in air after measured.After negative oxygen ion is inhaled into human body, it can adjust neural emerging Put forth energy state, improve the ventilatory of lung, improve blood circulation, enhance metabolism, strengthen immune system ability, making one spirit and shake Put forth energy, improve operating efficiency etc., it also has certain treatment to make to many diseases such as hypertension, asthma, influenza, insomnia, arthritis With so people's anion is referred to as " vitamin in air " " long-lived element ".
So far, make conventional lamp product while there is mosquito dispersing and the Technology design of negative ion-releasing function not to have also See.
The content of the invention
In view of the deficienciess of the prior art, the technical problems to be solved by the invention, which are to provide one kind, contains active mineral The preparation method of matter powder environmental protection lampshade, not only long-term negative ion release, also with certain expelling mosquito effect, while also has Certain antibacterial action, there is the effect achieved many things at one stroke.
The purpose of the present invention is achieved by the following technical solution：
A kind of preparation method containing active mineral matter powder environmental protection lampshade, described LED lamp cover include lampshade shell, the lampshade Housing includes basic unit and functional coating, and the basic unit and functional coating from-inner-to-outer are arranged in order, and the functional coating wraps completely Cover the outer surface of lampshade basic unit, the functional coating by following component by weight：Environment-friendly resin 15-25 weight Part；Fire retardant 3-6 parts by weight；Curing agent 2-3.5 parts by weight；Nano-phosphor 0.1-0.2 parts by weight；Vapour Ba Yan Good solid 754 light trigger 1.5-3 parts by weight；Polyethers amine catalyst 0.5-0.7 parts by weight；Hydroxyethyl cellulose 2-3 parts by weight；Two Cerium oxide 0.1-0.15 parts by weight；Active mineral matter powder 0.75-1.3 parts by weight；Essential oil of traditional Chinese medicine 0.6-1.1 parts by weight；Wherein, institute Environment-friendly resin is stated as epoxy soybean oil acrylate and the mixture of bisphenol A-type E51 epoxy resin, the epoxidized soybean oil propylene The mass ratio of acid esters and bisphenol A-type E51 epoxy resin is 1.5:1, the fire retardant is ammonium polyphosphate, melamine and swollen The mixture of swollen type graphite, the mass ratio 1.5 of the ammonium polyphosphate, melamine and expanded graphites:1.2:1, it is described Nano-phosphor be Ce and YAG mixture, particle diameter≤13 μm of the nano-phosphor, described active mineral matter powder is Germanite, fluorite, tourmaline, six ring stones are by weight 2.5：3：3.7：2 mixture, wherein tourmaline are dravite and lithium electricity Gas stone is by weight 5：3 mixture, particle diameter≤13 μm of the active mineral matter powder, the functional coating is as follows It is prepared：
S1, by the environment-friendly resin of required parts by weight, fire retardant, nano-phosphor, hydroxyethyl cellulose, vapour Ba Yan good solid 754 Light trigger and polyethers amine catalyst are placed in mixer, are mixed well in 65-85 DEG C of next part high speed stirring, mixing time is 15-30 minutes, it is to be mixed uniformly after taken out from mixer, that is, mixture A is made, it is standby；
S2, by material anemone vitifolia 65-85 parts by weight, folium isatidis 15-20 parts by weight, rhizome of cyrtomium 4-6 parts by weight, Pu'er tea 4-6 Parts by weight, clore basil 1.5-2.5 parts by weight, radix bupleuri 1-3 parts by weight, aloe 1-3 parts by weight, golden cypress 1-3 parts by weight, capsule of weeping forsythia 1- 3 parts by weight and RADIX PAEONIAE ALBA 1-3 parts by weight decontaminations, -20 DEG C of vacuum kettle 2-3 hours are placed in together, are then placed in microwave again Drying machine is pre-processed, and wherein drying time is 30-40 minutes, microwave power 17kw；
S3, the material after step S2 processing put into micronizer and be crushed to 60 mesh together, bulk drug powder is made, it is standby With；
S4, obtained bulk drug powder in step S3 put into the extraction kettle of supercritical carbon dioxide extraction apparatus, regulation extraction Pressure power 28MPa, 45 DEG C, carbon dioxide flow 1100L/h of extraction temperature, dynamic extraction 2 hours, directly exported in separating still Crude oil is collected with triangular flask, it is standby；
S5, obtained crude oil in step S4 is placed in 5 DEG C of environment freezed 70 minutes, then the crude oil after freezing is placed in rotating speed and is Centrifuged 25 minutes in 17000r/min high speed freezing centrifuge, remove after the removal of impurity to be placed in 85 DEG C of vacuum tanks and vacuumize 3 hours, i.e., Obtained volatile oil B, it is standby；
S6, by Moschus 0.6-1 parts by weight, purslane 3-4 parts by weight, red sage root 3-4 parts by weight, flaccid knotweed herb 3-4 parts by weight, tuber of stemona 7- 9 parts by weight, wrinkled giant hyssop 3-4 parts by weight, root of langdu 3-4 parts by weight, cape jasmine 3-4 parts by weight, Radix Isatidis 15-18 parts by weight and spina date seed 3-4 parts by weight clean drying, put into micronizer be crushed to 30 mesh together, and then plus deionized water is soaked 5 hours, adds water Measure by 7 times of immersion bulk drug quality, be dispersed with stirring and mix well, Traditional Chinese drug mixture is made, it is standby；
S7, by Traditional Chinese drug mixture made from step S6 in 80 DEG C decoct 2 hours, collect distillate, and add ether extraction, distillation The volume ratio of liquid and ether is 2.5:1, upper oil phase is taken, then plus place is dried in anhydrous sodium sulfate 0.1-0.25 parts by weight Reason, i.e., obtained volatile oil C are standby；
S8, step S5 and S7 made volatile oil B and volatile oil C are mixed and mix well obtained miscella, then sequentially added while stirring Peppermint essential oil, Rosa Damascana, sarranine flower essential oil and needle juniper essential oil, it is sufficiently stirred 45 minutes, stands 30 minutes, filtering and impurity removing, i.e., Essential oil of traditional Chinese medicine is obtained, wherein, the mass ratio of the miscella and Peppermint essential oil, Rosa Damascana, sarranine flower essential oil and needle juniper essential oil is 2：0.5：0.4：0.6：0.5；
S9, by mixture A made from essential oil of traditional Chinese medicine made from step S8 and step S1, at 70-80 DEG C, concentrated in mixer It is stirred 15 minutes, obtains premix, ceria, active mineral matter powder and modified aromatic is then added in premix Amine hardener, at 65-85 DEG C, then concentrated compactness casts in the outer surface of basic unit, the solidification demoulding, produces work(after 35 minutes Can coating.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following parts by weight：Surface-active 1.7 parts of agent, 0.2 part of Metadelphene, 1 part of butyl butyrate, 1.2 parts of eucalyptus oil, 0.5 part of acetic acid chlorhexidine, AEO 0.2 part of 1 part of sodium sulphate and sodium benzoate.
A kind of LED lamp, the LED lamp include LED illumination component, base and the lampshade prepared by the above method A。
It should be noted that the experiment proved that, appropriate ceria is added in active mineral matter powder（CeO2）, utilize The emittance of the rare earth element is high, and the characteristics of half degradation period limit for length, the anion production of active mineral matter powder can be significantly increased Rate, its principle are as follows：Ce in ceria4+Ce is changed under photoenvironment3+, in conversion process, electron-hole Recombination probability reduces, then in active mineral matter powder in the presence of the material electric field such as tourmaline, part electronics is passively with electric field side To displacement, electron-hole recombination probability reduces, so as in tourmaline/CeO2Substantial amounts of electricity is gathered in composite powder surface The energy of air molecule is solved, and then generates the negative aeroion of high concentration, while Ce3+Ce is oxidized into again4+, then repeat Foregoing conversion process；Meanwhile detected through practice, add titanium dioxide in the active mineral matter powder by the compound proportioning of the present invention Cerium component, the concentration than the active mineral matter powder anion of not added ceria is high more than 10 times, r rays and natural environment It is identical.
The present invention be based on traditional Chinese medicine, with reference to modern Chinese medicine pharmacological research, from the drug screening of existing Chinese medicine and instead Card is reviewed, gives full play to each component synergy, the effect of wherein primary raw material is described as follows.
Anemone vitifolia：①《Shaanxi Chinese herbal medicine》：" it is bitter, it is cool, it is slightly poisonous.”②《Often use Chinese herbal medicine in Sichuan》：" toil, temperature, It is slightly poisonous." removing toxic substances, apocenosis myogenic, scattered stasis detumescence, have and kill maggot, wriggler, change product, detumescence, dissipate the stasis of blood, control stubborn dermatitis, the favus of the scalp, malaria Disease, infantile malnutrition, dysentery, carbuncle furuncle sore swell, scrofula, traumatic injury.
Folium isatidis：To staphylococcus aureus, alpha streptococcus, diplococcus meningitidis, streptococcus pneumonia, micrococcus catarrhalis, Typhoid bacillus, Escherichia coli, Bacillus influenzae, corynebacterium diphtheriae and shigella dysenteriae have certain inhibitory action；Folium isatidis is to encephalitis B Virus, mumps virus, influenza virus etc. also play the role of inhibitory action, and folium isatidis has killing Leptospira in addition.
Rhizome of cyrtomium：Hardship is slightly cold, Return liver the spleen channel, slightly poisonous.Desinsection, clearing heat and detoxicating, hemostasis.
Pu'er tea：The tea that the exclusive large leaf tea tree in Yunnan is produced, there is inhibiting bacteria and diminishing inflammation, antitoxin, sterilizing, Constipation etc..
Clore basil:It is pungent, temperature, there is mosquito repellent, inducing sweat and dispelling exogenous evils, expelling wind and removing dampness, the effect of blood stasis removing analgesic.
Radix bupleuri:Harmonizing Sharyang, relax liver and stomach, yang invigorating.Fevers and chills alternate is controlled, fullness in the chest and hypochondriac pain, bitter taste is deaf, mesh of having a headache It is dizzy, malaria, lower sharp prolapse of the anus, irregular menstruation, metroptosis, the invasion of blood chamber by heat.
Aloe：《Bencao Jingshu》：Aloe, tremble with fear can except heat, hardship can expel the heat-evil eliminating dampness, it is bitter can desinsection, to bitter to cold, therefore be except heat The key medicine of desinsection.Its main hot blast is unhappy, hot gas between chest side of body, improving eyesight, relieving palpitation, children epilepsy cool breeze, treats five infantile malnutrition due to digestive disturbances or intestinalparasites, kills three worm persons, heat Wind is then given birth to, heat energy makes one unhappy, and heat is except then hot gas self solves between wind-heat unhappiness and chest diaphragm.
Golden cypress：To staphylococcus aureus, pneumococcus, corynebacterium diphtheriae, Streptococcus viridans, shigella dysenteriae（Sonnei Except）, hemolytic streptococcus, meningococcus, comma bacillus, bacillus anthracis effectively or have a stronger inhibitory action；To withered Careless bacillus, Bordetella pertussis, clostridium tetani also have inhibitory action.
The capsule of weeping forsythia：It is clearing heat and detoxicating, dispersing swelling and dissipating binds, dispelling wind and heat from the body, there is the title of " persons particularly liable to develop skin infection's panacea ", typhoid bacillus, secondary wound can be suppressed Cold bacillus, Escherichia coli, shigella dysenteriae, corynebacterium diphtheriae and comma bacillus, staphylococcus, streptococcus etc..
RADIX PAEONIAE ALBA：Wherein Paeoniflorin have antibacterial, antipyretic, anti-inflammatory, increase coronary flow, improve myocardial nutritional flow, Expand blood vessel, confrontation acute myocardial ischemia, suppress platelet aggregation, calmness, analgesia, spasmolysis, antiulcer, the work for adjusting blood glucose With.Root of herbaceous peony decoction can suppress shigella dysenteriae, streptococcus pneumonia, Escherichia coli, typhoid bacillus, hemolytic streptococcus, Pseudomonas aeruginosa Deng.
Moschus:With having one's ideas straightened out, ward off dirty, dredging collateral, dissipate the stasis of blood the effect of；Control apoplexy, coma due to blocking of the respiratory system, frightened epilepsy, middle evil unhappiness, Xin Fubao The pain, Disorder lump in the abdomen hypochondriac lumps, traumatic injury, swollen ulcer drug.《This warp》：Master wards off bad odor, a kind of malaria, epilepsy convulsion, goes three worms.
Purslane：Portulacaceae annual herb plant.Plump succulence, hairless, high 10-30cm, be born in field roadside and The area without shade such as flower garden ruins.Domestic various regions are distributed.This kind is medical and edible dual purpose plant.Herb hyoscine, there are clearing heat and promoting diuresis, solution Malicious detumescence, anti-inflammatory, quench the thirst, diuresis.
The red sage root：It is bitter in taste, it is slightly cold.The thoughts of returning home, Liver Channel.《The southern regions of the Yunnan Province book on Chinese herbal medicine》Record：Bushing sedate, calming heart and tranquilizing mind.Control forgetful seized with terror Punching, palpitation with fear is insomnia, and has a stasis-dispelling and pain-killing, invigorate blood circulation, the effect of relieving restlessness that clears away heart-fire, for irregular menstruation, closed dysmenorrhea, abdominal mass product It is poly-, chest and abdomen shouting pain, hot numbness pain, sore.
Flaccid knotweed herb：To various shigella dysenteriaes in there is inhibitory action in test tube, current clinical medicine research shows, polygonum flaccidum tool There are antibacterial, antiviral, anti-inflammatory, anti-oxidant and other effects.
The tuber of stemona：Can mosquito expelling, resisting pathogenic microbes effect, to beta hemolytic streptococcus, meningococcus, golden yellow A variety of pathomycetes such as staphylococcus, staphylococcus albus, typhoid bacillus, pneumobacillus, yersinia pestis, bacillus anthracis have necessarily Inhibitory action, its infusion has killing action to mosquitos and flies larva, head louse, clothing lice and bedbug etc..
Wrinkled giant hyssop：Acrid flavour, slightly warm in nature.Effect：Dampness elimination inducing diaphoresis, solves the effect of administration, cures mainly dampness taste with, and chest gastral cavity is vexed swollen, Appetite is not fragrant, Nausea and vomiting；Summer summer-heat and damp is sleepy, uncomfortable in chest not relax, and the illnesss such as aversion to cold of catching cold is uncomfortable in chest, have compared with Strong suppression fungi effect and antibacterial action.
The root of langdu：The alias river root of langdu, continuous poison, RADIX STELLERAE, chervil, vexed fresh idea, Re Jiaba, eliminate completely, Chinese atropanthe root, one perfume, Medicine sieve foretells, it is raw pull, flourishing bavin headdress flower, monkey root, gelsemium elegan, with its root eliminating the phlegm, analgesic, disperse accumulations, desinsection in traditional Chinese medicine.
Cape jasmine：Its fruit is traditional Chinese medicine, the l batch medicine-food two-purpose resources that the category Ministry of Public Health promulgates, have protect liver, cholagogic, The effect such as decompression, calm, hemostasis, detumescence, has inhibitory action, to a variety of to corynebacterium diphtheriae, staphylococcus aureus, typhoid bacillus Dermatophyte also has different degrees of inhibitory action.
Radix Isatidis：Have inhibitory action to various bacteria, infusion to hay bacillus, staphylococcus aureus, sarcine, Escherichia coli, typhoid bacillus, paratyphosum Bacterium, dysentery（Will is congratulated, Freund）Bacillus, bacillus enteritidis etc. have different degrees of suppression Effect；Acetone leachate also has similar effect, and effective to hemolytic streptococcus.
Spina date seed:There are significant calm and syngignoscism and anticonvulsant action, according to《Book on Chinese herbal medicine is new again》Record：Soothing the liver is managed Gas, moisten the lung and nourish yin, middle benefit gas dampness removing, hold back gas hidroschesis, beneficial will, hearing-improing and eyesight improving.
It should be noted that it is proven, after the red sage root, flaccid knotweed herb and the tuber of stemona of certain part by weight are compounded, no The ability of degerming antibacterial is only remarkably improved, can also produce a kind of delicate fragrance taste having no toxic side effect, it is refreshing, have certain Effect of refreshing oneself；Meanwhile be proven, by the folium isatidis of certain part by weight, Pu'er tea, aloe, Moschus and anemone vitifolia After being compounded, the mosquito dispersing ability of said composition is set to be significantly improved；In addition, the component such as radix bupleuri, golden cypress and capsule of weeping forsythia is carried out After compatibility, the antibacterial degerming ability of composition is substantially increased, is detected through practice, the composition after compounding is to Staphylococcus aureus Bacterium, bacillus anthracis, Bacillus influenzae, micrococcus catarrhalis, pneumococcus, Escherichia coli, beta streptococcus, corynebacterium diphtheriae, typhoid bacillus, Green pus liver bacterium, shigella dysenteriae etc. more than 30, which plants germ, has certain suppression and killing action, the present invention is provided with certain resist Bacterium degerming ability.
The effect of the present invention：
The present invention is compounded using Chinese medicine and active mineral matter, the present invention not only can also be discharged anion with expelling mosquito, Fresh air, while fragrant odour, property is gentle, has the effect of body-building, mosquito repellent, antimycotic antiseptic.
Brief description of the drawings
Fig. 1 is overall schematic of the present invention.
Fig. 2 is lampshade shell schematic cross-section of the present invention.
Embodiment
Embodiment 1：
Refer to shown in Fig. 1, Fig. 2, a kind of preparation method containing active mineral matter powder environmental protection lampshade, described LED lamp cover bag Include lampshade shell A, the lampshade shell A includes basic unit 1 and functional coating 2, the basic unit 1 and the from-inner-to-outer of functional coating 2 according to Secondary arrangement, the functional coating 2 coat the outer surface of lampshade basic unit 1 completely, and the functional coating 2 is by following component according to weight Number forms：
The parts by weight of environment-friendly resin 15；The parts by weight of fire retardant 6；The parts by weight of curing agent 2；The weight of nano-phosphor 0.2 Part；The good solid parts by weight of 754 light trigger 1.5 of vapour Ba Yan；The parts by weight of polyethers amine catalyst 0.7；The parts by weight of hydroxyethyl cellulose 2； The parts by weight of ceria 0.15；The parts by weight of active mineral matter powder 0.75；The parts by weight of essential oil of traditional Chinese medicine 1.1；Wherein, the environment-friendly resin For epoxy soybean oil acrylate and the mixture of bisphenol A-type E51 epoxy resin, the epoxy soybean oil acrylate and bis-phenol The mass ratio of A type E51 epoxy resin is 1.5:1, the fire retardant is ammonium polyphosphate, melamine and expanded graphites Mixture, the mass ratio 1.5 of the ammonium polyphosphate, melamine and expanded graphites:1.2:1, described nano fluorescent Powder be Ce and YAG mixture, particle diameter≤13 μm of the nano-phosphor, described active mineral matter powder be germanite, fluorite, Tourmaline, six ring stones are by weight 2.5：3：3.7：2 mixture, wherein tourmaline be dravite and elbaite by weight Than 5：3 mixture, particle diameter≤13 μm of the active mineral matter powder, the functional coating, which is made by the steps, to be formed：
S1, by the environment-friendly resin of required parts by weight, fire retardant, nano-phosphor, hydroxyethyl cellulose, vapour Ba Yan good solid 754 Light trigger and polyethers amine catalyst are placed in mixer, are mixed well in 65 DEG C of next part high speed stirrings, mixing time is 30 points Clock, it is to be mixed uniformly after taken out from mixer, that is, mixture A is made, it is standby；
S2, by the parts by weight of material anemone vitifolia 85, the parts by weight of folium isatidis 15, the parts by weight of rhizome of cyrtomium 6, the parts by weight of Pu'er tea 4, cloves The parts by weight of sweet basil 2.5, the parts by weight of radix bupleuri 1, the parts by weight of aloe 3, the parts by weight of golden cypress 1, the parts by weight of the capsule of weeping forsythia 3, the parts by weight of RADIX PAEONIAE ALBA 1 are gone Impurity, is placed in -20 DEG C of vacuum kettle 2 hours together, and being then placed in microwave dryer again is pre-processed, and wherein drying time is 40 minutes, microwave power 17kw；
S3, the material after step S2 processing put into micronizer and be crushed to 60 mesh together, bulk drug powder is made, it is standby With；
S4, obtained bulk drug powder in step S3 put into the extraction kettle of supercritical carbon dioxide extraction apparatus, regulation extraction Pressure power 28MPa, 45 DEG C, carbon dioxide flow 1100L/h of extraction temperature, dynamic extraction 2 hours, directly exported in separating still Crude oil is collected with triangular flask, it is standby；
S5, obtained crude oil in step S4 is placed in 5 DEG C of environment freezed 70 minutes, then the crude oil after freezing is placed in rotating speed and is Centrifuged 25 minutes in 17000r/min high speed freezing centrifuge, remove after the removal of impurity to be placed in 85 DEG C of vacuum tanks and vacuumize 3 hours, i.e., Obtained volatile oil B, it is standby；
S6, by the parts by weight of Moschus 1, the parts by weight of purslane 3, the parts by weight of the red sage root 4, the parts by weight of flaccid knotweed herb 3, the parts by weight of the tuber of stemona 9, wrinkled giant hyssop 3 parts by weight, the parts by weight of the root of langdu 4, the parts by weight of cape jasmine 3, the parts by weight of Radix Isatidis 18, the parts by weight of spina date seed 3 are cleaned drying, put into together 30 mesh are crushed in micronizer, then plus deionized water is soaked 5 hours, amount of water by 7 times of immersion bulk drug quality, It is dispersed with stirring and mixes well, Traditional Chinese drug mixture is made, it is standby；
S7, by Traditional Chinese drug mixture made from step S6 in 80 DEG C decoct 2 hours, collect distillate, and add ether extraction, distillation The volume ratio of liquid and ether is 2.5:1, upper oil phase is taken, then plus processing is dried in the parts by weight of anhydrous sodium sulfate 0.1, that is, makes Volatile oil C, it is standby；
S8, step S5 and S7 made volatile oil B and volatile oil C are mixed and mix well obtained miscella, then sequentially added while stirring Peppermint essential oil, Rosa Damascana, sarranine flower essential oil and needle juniper essential oil, it is sufficiently stirred 45 minutes, stands 30 minutes, filtering and impurity removing, i.e., Essential oil of traditional Chinese medicine is obtained, wherein, the mass ratio of the miscella and Peppermint essential oil, Rosa Damascana, sarranine flower essential oil and needle juniper essential oil is 2：0.5：0.4：0.6：0.5；
S9, by mixture A made from essential oil of traditional Chinese medicine made from step S8 and step S1, at 70 DEG C, concentrate and stir in mixer Mixing 15 minutes is mixed, obtains premix, ceria, active mineral matter powder and modified aromatic amine are then added in premix Curing agent, at 65 DEG C, then concentrated compactness casts in the outer surface of basic unit, the solidification demoulding, produces function painting after 35 minutes Layer.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following parts by weight：Surface-active 1.7 parts of agent, 0.2 part of Metadelphene, 1 part of butyl butyrate, 1.2 parts of eucalyptus oil, 0.5 part of acetic acid chlorhexidine, AEO 0.2 part of 1 part of sodium sulphate and sodium benzoate.
A kind of LED lamp, the LED lamp include LED illumination component, base and the lampshade prepared by the above method A。
Embodiment 2：
A kind of preparation method containing active mineral matter powder environmental protection lampshade, described LED lamp cover include lampshade shell A, the lamp Over body case A includes basic unit 1 and functional coating 2, and the basic unit 1 and the from-inner-to-outer of functional coating 2 are arranged in order, the functional coating The outer surfaces of 2 cladding lampshade basic units 1 completely, the functional coating 2 by following component by weight：
The parts by weight of environment-friendly resin 19；The parts by weight of fire retardant 5；The parts by weight of curing agent 3；The weight of nano-phosphor 0.15 Part；The good solid parts by weight of 754 light trigger 2 of vapour Ba Yan；The parts by weight of polyethers amine catalyst 0.6；The parts by weight of hydroxyethyl cellulose 2.5； The parts by weight of ceria 0.15；The parts by weight of active mineral matter powder 1；The parts by weight of essential oil of traditional Chinese medicine 1；Wherein, the environment-friendly resin is ring The mixture of oxygen soybean oil acrylate and bisphenol A-type E51 epoxy resin, the epoxy soybean oil acrylate and bisphenol A-type The mass ratio of E51 epoxy resin is 1.5:1, the fire retardant is the mixed of ammonium polyphosphate, melamine and expanded graphites Compound, the mass ratio 1.5 of the ammonium polyphosphate, melamine and expanded graphites:1.2:1, described nano-phosphor For Ce and YAG mixture, particle diameter≤13 μm of the nano-phosphor, described active mineral matter powder is germanite, fluorite, electricity Gas stone, six ring stones are by weight 2.5：3：3.7：2 mixture, wherein tourmaline be dravite and elbaite by weight 5：3 mixture, particle diameter≤13 μm of the active mineral matter powder, the functional coating, which is made by the steps, to be formed：
S1, by the environment-friendly resin of required parts by weight, fire retardant, nano-phosphor, hydroxyethyl cellulose, vapour Ba Yan good solid 754 Light trigger and polyethers amine catalyst are placed in mixer, are mixed well in 75 DEG C of next part high speed stirrings, mixing time is 25 points Clock, it is to be mixed uniformly after taken out from mixer, that is, mixture A is made, it is standby；
S2, by material anemone vitifolia 65- parts by weight, the parts by weight of folium isatidis 20, the parts by weight of rhizome of cyrtomium 4, the parts by weight of Pu'er tea 6, fourth The fragrant parts by weight of sweet basil 1.5, the parts by weight of radix bupleuri 13, the parts by weight of aloe 1, the parts by weight of golden cypress 3, the parts by weight of the capsule of weeping forsythia 1, the weight of RADIX PAEONIAE ALBA 3 Part decontamination, is placed in -20 DEG C of vacuum kettle 2.5 hours together, and being then placed in microwave dryer again is pre-processed, wherein drying Time is 35 minutes, microwave power 17kw；
S3, the material after step S2 processing put into micronizer and be crushed to 60 mesh together, bulk drug powder is made, it is standby With；
S4, obtained bulk drug powder in step S3 put into the extraction kettle of supercritical carbon dioxide extraction apparatus, regulation extraction Pressure power 28MPa, 45 DEG C, carbon dioxide flow 1100L/h of extraction temperature, dynamic extraction 2 hours, directly exported in separating still Crude oil is collected with triangular flask, it is standby；
S5, obtained crude oil in step S4 is placed in 5 DEG C of environment freezed 70 minutes, then the crude oil after freezing is placed in rotating speed and is Centrifuged 25 minutes in 17000r/min high speed freezing centrifuge, remove after the removal of impurity to be placed in 85 DEG C of vacuum tanks and vacuumize 3 hours, i.e., Obtained volatile oil B, it is standby；
S6, by the parts by weight of Moschus 0.6, the parts by weight of purslane 4, the parts by weight of the red sage root 3, the parts by weight of flaccid knotweed herb 4, the parts by weight of the tuber of stemona 7, the leaves of pulse plants Fragrant 4 parts by weight, the parts by weight of the root of langdu 3, the parts by weight of cape jasmine 4, the parts by weight of Radix Isatidis 15, the parts by weight of spina date seed 4 are cleaned drying, thrown together Enter and 30 mesh be crushed in micronizer, then plus deionized water soak 5 hours, amount of water by immersion bulk drug quality 7 Times, it is dispersed with stirring and mixes well, Traditional Chinese drug mixture is made, it is standby；
S7, by Traditional Chinese drug mixture made from step S6 in 80 DEG C decoct 2 hours, collect distillate, and add ether extraction, distillation The volume ratio of liquid and ether is 2.5:1, upper oil phase is taken, then plus processing is dried in the parts by weight of anhydrous sodium sulfate 0.2, that is, makes Volatile oil C, it is standby；
S8, step S5 and S7 made volatile oil B and volatile oil C are mixed and mix well obtained miscella, then sequentially added while stirring Peppermint essential oil, Rosa Damascana, sarranine flower essential oil and needle juniper essential oil, it is sufficiently stirred 45 minutes, stands 30 minutes, filtering and impurity removing, i.e., Essential oil of traditional Chinese medicine is obtained, wherein, the mass ratio of the miscella and Peppermint essential oil, Rosa Damascana, sarranine flower essential oil and needle juniper essential oil is 2：0.5：0.4：0.6：0.5；
S9, by mixture A made from essential oil of traditional Chinese medicine made from step S8 and step S1, at 75 DEG C, concentrate and stir in mixer Mixing 15 minutes is mixed, obtains premix, ceria, active mineral matter powder and modified aromatic amine are then added in premix Curing agent, at 75 DEG C, then concentrated compactness casts in the outer surface of basic unit, the solidification demoulding, produces function painting after 35 minutes Layer.
Remaining is the same as embodiment 1.
The test index of Example 1 and Example 2 of the present invention is as follows：
（1）Smell inspection：Sense organ, nonirritant peculiar smell.
（2）Anionic textiles.
Using negative ion testing equipment, it is made primarily directed to timber, ore, ceramic material, negative ion powder to related Commodity（Such as negative ion clothing, necklace, woollen blanket）Measurement is made Deng the anion quantity discharged, test result see the table below.
Sequence number Detection project Unit Measured result
Ordinary lamp and lantern Anion quantity Individual/cm3 0
The embodiment of the present invention 1,2 Anion quantity Individual/cm3 >1000
Conclusion：The embodiment of the present invention 1, embodiment 2 can be with sustained release negative aeroions, with ordinary lamps of the prior art Tool compares, and the present invention has obviously advantage.

Claims (2)

  1. A kind of 1. preparation method containing active mineral matter powder environmental protection lampshade, it is characterised in that：Described LED lamp cover includes lampshade Housing（A）, the lampshade shell（A）Including basic unit（1）And functional coating（2）, the basic unit（1）And functional coating（2）From interior And it is arranged in order outside, the functional coating（2）Cladding lampshade basic unit completely（1）Outer surface, the functional coating（2）By following Component is by weight：
    Environment-friendly resin 15-25 parts by weight；Fire retardant 3-6 parts by weight；Curing agent 2-3.5 parts by weight；Nano fluorescent Powder 0.1-0.2 parts by weight；The good solid 754 light trigger 1.5-3 parts by weight of vapour Ba Yan；Polyethers amine catalyst 0.5-0.7 parts by weight；Hydroxyl Ethyl cellulose 2-3 parts by weight；Ceria 0.1-0.15 parts by weight；Active mineral matter powder 0.75-1.3 parts by weight；Chinese medicine essence Oily 0.6-1.1 parts by weight；Wherein, the environment-friendly resin is the mixed of epoxy soybean oil acrylate and bisphenol A-type E51 epoxy resin The mass ratio of compound, the epoxy soybean oil acrylate and bisphenol A-type E51 epoxy resin is 1.5:1, the fire retardant is more The mixture of APP, melamine and expanded graphites, the ammonium polyphosphate, melamine and expanded graphites Mass ratio 1.5:1.2:1, described nano-phosphor is Ce and YAG mixture, the μ of the particle diameter of the nano-phosphor≤13 M, described active mineral matter powder are germanite, fluorite, tourmaline, six ring stones by weight 2.5：3：3.7：2 mixture, wherein Tourmaline is dravite and elbaite by weight 5：3 mixture, particle diameter≤13 μm of the active mineral matter powder, institute State functional coating and be made by the steps and form：
    S1, by the environment-friendly resin of required parts by weight, fire retardant, nano-phosphor, hydroxyethyl cellulose, vapour Ba Yan good solid 754 Light trigger and polyethers amine catalyst are placed in mixer, are mixed well in 65-85 DEG C of next part high speed stirring, mixing time is 15-30 minutes, it is to be mixed uniformly after taken out from mixer, that is, mixture A is made, it is standby；
    S2, by material anemone vitifolia 65-85 parts by weight, folium isatidis 15-20 parts by weight, rhizome of cyrtomium 4-6 parts by weight, Pu'er tea 4-6 Parts by weight, clore basil 1.5-2.5 parts by weight, radix bupleuri 1-3 parts by weight, aloe 1-3 parts by weight, golden cypress 1-3 parts by weight, capsule of weeping forsythia 1- 3 parts by weight and RADIX PAEONIAE ALBA 1-3 parts by weight decontaminations, -20 DEG C of vacuum kettle 2-3 hours are placed in together, are then placed in microwave again Drying machine is pre-processed, and wherein drying time is 30-40 minutes, microwave power 17kw；
    S3, the material after step S2 processing put into micronizer and be crushed to 60 mesh together, bulk drug powder is made, it is standby With；
    S4, obtained bulk drug powder in step S3 put into the extraction kettle of supercritical carbon dioxide extraction apparatus, regulation extraction Pressure power 28MPa, 45 DEG C, carbon dioxide flow 1100L/h of extraction temperature, dynamic extraction 2 hours, directly exported in separating still Crude oil is collected with triangular flask, it is standby；
    S5, obtained crude oil in step S4 is placed in 5 DEG C of environment freezed 70 minutes, then the crude oil after freezing is placed in rotating speed and is Centrifuged 25 minutes in 17000r/min high speed freezing centrifuge, remove after the removal of impurity to be placed in 85 DEG C of vacuum tanks and vacuumize 3 hours, i.e., Obtained volatile oil B, it is standby；
    S6, by Moschus 0.6-1 parts by weight, purslane 3-4 parts by weight, red sage root 3-4 parts by weight, flaccid knotweed herb 3-4 parts by weight, tuber of stemona 7- 9 parts by weight, wrinkled giant hyssop 3-4 parts by weight, root of langdu 3-4 parts by weight, cape jasmine 3-4 parts by weight, Radix Isatidis 15-18 parts by weight and spina date seed 3-4 parts by weight clean drying, put into micronizer be crushed to 30 mesh together, and then plus deionized water is soaked 5 hours, adds water Measure by 7 times of immersion bulk drug quality, be dispersed with stirring and mix well, Traditional Chinese drug mixture is made, it is standby；
    S7, by Traditional Chinese drug mixture made from step S6 in 80 DEG C decoct 2 hours, collect distillate, and add ether extraction, distillation The volume ratio of liquid and ether is 2.5:1, upper oil phase is taken, then plus place is dried in anhydrous sodium sulfate 0.1-0.25 parts by weight Reason, i.e., obtained volatile oil C are standby；
    S8, step S5 and S7 made volatile oil B and volatile oil C are mixed and mix well obtained miscella, then sequentially added while stirring Peppermint essential oil, Rosa Damascana, sarranine flower essential oil and needle juniper essential oil, it is sufficiently stirred 45 minutes, stands 30 minutes, filtering and impurity removing, i.e., Essential oil of traditional Chinese medicine is obtained, wherein, the mass ratio of the miscella and Peppermint essential oil, Rosa Damascana, sarranine flower essential oil and needle juniper essential oil is 2：0.5：0.4：0.6：0.5；
    S9, by mixture A made from essential oil of traditional Chinese medicine made from step S8 and step S1, at 70-80 DEG C, concentrated in mixer It is stirred 15 minutes, obtains premix, ceria, active mineral matter powder and modified aromatic is then added in premix Amine hardener, at 65-85 DEG C, then concentrated compactness casts in the outer surface of described basic unit after 35 minutes, solidification is stripped, Produce functional coating.
  2. A kind of 2. preparation method containing active mineral matter powder environmental protection lampshade according to claim 1, it is characterised in that： Essential oil of traditional Chinese medicine in step S8 also includes the component of following parts by weight：1.7 parts of surfactant, 0.2 part of Metadelphene, butyl butyrate 0.2 part of 1 part, 1.2 parts of eucalyptus oil, 0.5 part of acetic acid chlorhexidine, 1 part of sodium sulfate of polyethenoxy ether of fatty alcohol and sodium benzoate.
CN201710134993.5A 2016-05-23 2017-03-08 A kind of preparation method containing active mineral matter powder environmental protection lampshade Pending CN107418388A (en)

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