CN107375007B - Skin care product composition, amino acid soap and preparation method thereof - Google Patents
Skin care product composition, amino acid soap and preparation method thereof Download PDFInfo
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- CN107375007B CN107375007B CN201710626705.8A CN201710626705A CN107375007B CN 107375007 B CN107375007 B CN 107375007B CN 201710626705 A CN201710626705 A CN 201710626705A CN 107375007 B CN107375007 B CN 107375007B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/004—Aftersun preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/225—Polymers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
Abstract
The invention provides a skin care composition, which comprises: 0.01-0.3 parts by weight of creatine; 0.02-6.5 parts of B vitamins. According to the invention, the skin care product composition finally prepared is mild and clean through the creatine and the B vitamins in a specific ratio, the degreasing force is moderate, the skin feeling is fresh and cool without slipping during washing, the skin feeling after washing is moist and not tight, and the skin care product composition also has the functions of removing dark skin color, and fading acne marks and chloasma; black heads and acnes are reduced; enhancing moisture retention and skin elasticity; meanwhile, the after-sun repairing effect is good.
Description
Technical Field
The invention relates to the technical field of daily necessities, in particular to a skin care product composition, an amino acid soap and a preparation method thereof.
Background
Due to increasingly serious atmospheric water and soil pollution, living pressure, over-clean skin and abuse of skin care products containing hormone or heavy metal exceeding standards, skin problems of human skin stratum corneum metabolic disturbance, dark skin color, acne marks, chloasma, skin inflammation after sunburn and the like are caused, and the population base of sensitive skin is huge, so that a safe and mild facial product suitable for sensitive skin is required to improve the skin condition. The conventional skin quality improvement is mainly performed by the steps of cleansing (face soap or facial cleanser), basic care (mask, toner, lotion, eye cream or face cream), isolation, sun protection, color makeup, and the like. Generally, people have high requirements on selection of basic care products and hope that the basic care products have multiple functions of moisturizing, whitening, anti-wrinkle and the like, but for cleaning products, people may pay more attention to the cleaning effect, and the fact that the facial cleaning products are short in facial retention time and whether other functions have little influence on skin protection and skin quality improvement is considered.
However, with the deep research of science and technology on dermatology, the whole skin care consciousness of people is improved, the improvement of understanding that nutritional ingredients need to be supplemented in the face cleaning process is improved, the demand of people on multi-effect skin cleaning products is more and more urgent, and the corresponding product development technology is developed. For example, the Chinese patent application (CN104586655A) discloses a whitening facial cleanser which comprises the following components in parts by weight: 1-3 parts of caryophyllin extract, 1-3 parts of perilla frutescens extract, 1-2 parts of interleukin, 0.5-2 parts of vitamin C, 5-10 parts of sodium hyaluronate, 2-5 parts of coconut diethanolamide, 5-10 parts of isopropyl palmitate, 0.5-2 parts of cocamidopropyl betaine, 1-5 parts of lanolin, 5-10 parts of butanediol and 150 parts of water, and the obtained facial cleanser can play a good cleaning role on skin, but only has the functions of whitening and moisturizing, and has no remarkable effect of reducing blackheads, acnes and the like. For another example, the Chinese patent application (CN104288025A) discloses a whitening facial cleanser, which is composed of the following substances in parts by weight: 1-3 parts of vitamin E, 4-8 parts of eucalyptus oil, 6-10 parts of violet magnolia flower bud, 3-6 parts of cocamidopropyl betaine, 1-4 parts of cyclosiloxane, 7-11 parts of white ginseng, 3-7 parts of pollen typhae, 4-10 parts of lanolin, 2-7 parts of mint, 2-6 parts of angelica dahurica, 1-5 parts of dipotassium glycyrrhizinate, 2-4 parts of lecithin, 1-6 parts of liquorice and 2-6 parts of tribulus terrestris. The obtained facial cleanser has good skin cleaning effect, remarkable whitening effect, and no significant effect on reducing blackheads, acnes, etc.
The amino acid soap is a novel face-washing soap which is started in recent years, has the greatest characteristic that an amino acid surfactant is used for replacing fatty acid salt to prepare a soap base, has various advantages of high safety to environment and organisms, good skin affinity and the like, has a pH value close to that of human skin, and is soft and not tight after being washed and dried. Therefore, the prior art avoids the defects of the traditional alkaline toilet soap, and ensures that the soap body is crystal and transparent, has rich foam, is soft and moisture-keeping and low in irritation, and is suitable for people with various skin types. But also has the functions of removing dark complexion, lightening acne marks and chloasma; black heads and acnes are reduced; enhancing moisture retention and skin elasticity; amino acid soaps for comprehensively improving skin quality such as after-sun repair and the like are still to be developed.
Disclosure of Invention
In view of the above, the technical problem to be solved by the present invention is to provide a skin care composition, which can remove dark complexion, and reduce acne marks and chloasma; black heads and acnes are reduced; has effects in keeping moisture, improving skin elasticity, and repairing after sunburn.
The invention provides a skin care composition, which comprises:
0.01-0.3 parts by weight of creatine;
0.02-6.5 parts of B vitamins.
Preferably, the B vitamins include:
preferably, the skin care composition comprises
0.02-0.25 parts of creatine;
0.05-5 parts of B vitamins.
The invention provides application of the composition in any one of the technical schemes in preparation of cosmetics.
The invention provides a cosmetic comprising the composition according to any one of the above technical schemes.
Preferably, the formulation of the cosmetic is one or more of soap, cream and milk.
The invention provides an amino acid soap, which comprises a solvent and the following components:
preferably, the amino acid is selected from one or more of lauroyl glutamic acid, cocoyl glutamic acid, myristoyl glutamic acid, stearoyl glutamic acid, palmitoyl glutamic acid and cocamido propionic acid; the amino acid salt is selected from one or more of potassium lauroyl glutamate, sodium cocoyl glutamate, disodium cocoyl glutamate, sodium cocoyl methyl taurate, potassium cocoyl glutamate, sodium myristoyl glutamate, potassium myristoyl glutamate, sodium stearoyl glutamate, potassium stearoyl glutamate, sodium palmitoyl glutamate, potassium palmitoyl glutamate and sodium cocoyl amido propionate; the humectant is selected from one or more of glycerol, sorbitol, propylene glycol and polyethylene glycol; the skin feeling regulator is one or more selected from polyglycerol-10, betaine, urea, allantoin, seaweed extract, hyaluronic acid, sodium hyaluronate, trehalose, maltitol, erythritol, mannitol and sucrose.
Preferably, the amino acid soap further comprises the following raw materials:
0-5 parts by weight of an aromatic agent;
0-0.5 parts by weight of an appearance modifier;
the flavoring agent is selected from one or more of essence and essential oil;
the appearance modifier is selected from one or more of pigment, dried flower, titanium dioxide and bamboo charcoal powder.
The invention provides a preparation method of amino acid soap, which comprises the following steps:
A) mixing amino acid, amino acid salt, a humectant and a solvent, and heating and stirring to obtain a first mixed solution;
mixing and heating triethanolamine and a solvent to obtain a second mixed solution;
B) mixing the first mixed solution and the second mixed solution, mixing with a skin feel regulator, cooling after mixing, and mixing with B vitamins and creatine to obtain a third mixed solution;
C) and filling the third mixed solution into a mold to obtain the amino acid soap.
Compared with the prior art, the invention provides a skin care product composition, which comprises the following components: 0.01-0.3 parts by weight of creatine; 0.02-6.5 parts of B vitamins. According to the invention, the skin care product composition finally prepared is mild and clean through the creatine and the B vitamins in a specific ratio, the degreasing force is moderate, the skin feeling is fresh and cool without slipping during washing, the skin feeling after washing is moist and not tight, and the skin care product composition also has the functions of removing dark skin color, and fading acne marks and chloasma; black heads and acnes are reduced; enhancing moisture retention and skin elasticity; meanwhile, the after-sun repairing effect is good.
Detailed Description
The invention provides a skin care composition, which comprises:
0.01-0.3 parts by weight of creatine;
0.02-6.5 parts of B vitamins.
The skin care composition provided by the invention comprises 0.01-0.3 part by weight of creatine; preferably 0.02-0.25 weight part of creatine; more preferably 0.05 to 0.20 parts by weight of creatine; most preferably, the creatine is contained in an amount of 0.05 to 0.15 parts by weight.
The creatine is not limited in the present invention, and creatine known to those skilled in the art may be used.
Creatine (creatine), a nitrogenous organic acid naturally found in vertebrates, assists in providing energy to muscle and nerve cells. Michel euroren scherrel (Michel eugenechevrel) found Creatine in skeletal muscle for the first time in 1832, and then, according to the greek language "Kreas" (meat), named "Creatine".
Creatine is a substance synthesized by three amino acids, arginine (arginine), glycine (glycine) and methionine (methionine), and can rapidly provide energy (various activities of a human body are provided by ATP, namely adenosine triphosphate, and the storage amount of ATP in the human body is very small, so that ATP is rapidly consumed during exercise, and creatine can rapidly resynthesize ATP to supply energy). The storage amount of the adenosine triphosphate in the human body is small, and the adenosine triphosphate needs to be synthesized continuously, but the synthesis speed of the human body is slow, so that the human body is fatigued. Therefore, the muscle strength, speed and endurance can be effectively improved by timely supplementing creatine. Improving physical ability and training level, and preventing fatigue.
The skin care product composition provided by the invention comprises 0.02-6.5 parts by weight of B vitamins; preferably, the vitamin B complex comprises 0.05-5 parts by weight of B vitamins; more preferably 0.1 to 4 parts by weight of B vitamins; most preferably 0.2 to 3 parts by weight of B vitamins.
The B vitamins of the present invention are not limited and are well known to those skilled in the art. The vitamin B includes vitamin B1, vitamin B2, vitamin B6, vitamin B12, nicotinic acid, pantothenic acid, folic acid, etc. The B vitamins are substances essential for promoting metabolism in the body and converting sugar, fat, protein, etc. into heat. If vitamin B is absent, cell function is immediately reduced, and metabolic disorder is caused, at which the human body suffers from malaise and inappetence.
According to the present invention, the B vitamins preferably include:
according to the present invention, the B vitamins preferably include 0.01 to 1.5 parts by weight of folic acid; more preferably 0.05 to 1.3 parts by weight of folic acid; most preferably 0.05 to 1.0 parts by weight of folic acid.
The B vitamins preferably comprise 0.01-3.5 parts by weight of nicotinamide; more preferably 0.1 to 3.0 parts by weight of nicotinamide; most preferably from 0.2 to 2.0 parts by weight of niacinamide.
The B vitamins preferably comprise 0-2 parts by weight of vitamin B6, and more preferably comprise 0.02-1.5 parts by weight of vitamin B6; most preferably 0.02-1.3 parts by weight of vitamin B6.
The B vitamins preferably comprise 0-2 parts by weight of vitamin B12, and more preferably comprise 0.02-1.5 parts by weight of vitamin B12; most preferably 0.02-1.3 parts by weight of vitamin B12.
In one embodiment of the present invention, the skin care composition comprises
0.02-0.25 parts of creatine;
0.05-5 parts of B vitamins.
The skin care composition provided by the invention can also comprise other components and auxiliaries which can be used for skin care and are well known to those skilled in the art.
The inventor creatively discovers that the creatine and the B vitamins with the specific mass ratio can act synergistically, and can remove dark complexion, and fade acne marks and chloasma; black heads and acnes are reduced; has effects in keeping moisture, improving skin elasticity, and repairing after sunburn.
According to the invention, the skin care product composition finally prepared is mild and clean through the creatine and the B vitamins in a specific ratio, the degreasing force is moderate, the skin feeling is fresh and cool without slipping during washing, the skin feeling after washing is moist and not tight, and the skin care product composition also has the functions of removing dark skin color, and fading acne marks and chloasma; black heads and acnes are reduced; enhancing moisture retention and skin elasticity; meanwhile, the after-sun repairing effect is good.
The invention provides application of the composition in any one of the technical schemes in preparation of cosmetics.
The invention provides a cosmetic comprising the composition according to any one of the above technical schemes.
Preferably, the formulation of the cosmetic is one or more of soap, cream and milk.
Wherein the soap is preferably an amino acid soap; the cream is preferably a face cream; the milk is preferably body milk.
While specific bases for creams and body milks may be well known to those skilled in the art, the inventors are not limited thereto.
The invention provides an amino acid soap, which comprises a solvent and the following components:
the amino acid soap raw material provided by the invention comprises a solvent; the solvent is preferably one or more selected from deionized water, calendula water, lavender water, rose water, chamomile water, primrose water and witch hazel flower water.
The amino acid soap raw material provided by the invention comprises 0.01-0.3 weight part of creatine; preferably 0.02-0.25 weight part of creatine; more preferably 0.05 to 0.20 parts by weight of creatine; most preferably, the creatine is contained in an amount of 0.05 to 0.15 parts by weight.
The amino acid soap raw material provided by the invention comprises 0.02-6.5 parts by weight of B vitamins; preferably, the vitamin B complex comprises 0.05-5 parts by weight of B vitamins; more preferably 0.1 to 4 parts by weight of B vitamins; most preferably 0.2 to 3 parts by weight of B vitamins.
According to the present invention, the B vitamins preferably include:
according to the present invention, the B vitamins preferably include 0.01 to 1.5 parts by weight of folic acid; more preferably 0.05 to 1.3 parts by weight of folic acid; most preferably 0.05 to 1.0 parts by weight of folic acid.
The B vitamins preferably comprise 0.01-3.5 parts by weight of nicotinamide; more preferably 0.1 to 3.0 parts by weight of nicotinamide; most preferably from 0.2 to 2.0 parts by weight of niacinamide.
The B vitamins preferably comprise 0-2 parts by weight of vitamin B6, and more preferably comprise 0.02-1.5 parts by weight of vitamin B6; most preferably 0.02-1.3 parts by weight of vitamin B6.
The B vitamins preferably comprise 0-2 parts by weight of vitamin B12, and more preferably comprise 0.02-1.5 parts by weight of vitamin B12; most preferably 0.02-1.3 parts by weight of vitamin B12.
The amino acid soap raw material provided by the invention comprises 20-40 parts by weight of amino acid; preferably 22 to 38 parts by weight of amino acid; more preferably 25 to 35 parts by weight of an amino acid; most preferably 29 to 33 parts by weight of an amino acid.
The amino acid is selected from one or more of lauroyl glutamic acid, cocoyl glutamic acid, myristoyl glutamic acid, stearoyl glutamic acid, palmitoyl glutamic acid and cocamido propionic acid; preferably one or more of stearoyl glutamic acid, palmitoyl glutamic acid and cocamido propionic acid.
The amino acid soap raw material provided by the invention comprises 15-25 parts by weight of triethanolamine; preferably 16 to 24 parts by weight of triethanolamine; more preferably 18 to 22 parts by weight of triethanolamine; most preferably 18 to 20 parts by weight of triethanolamine. In the present invention, the source of the triethanolamine is not limited and may be commercially available.
The amino acid soap raw material provided by the invention comprises 5-15 parts by weight of amino acid salt; preferably 5 to 13 parts by weight of an amino acid salt; more preferably 5 to 10 parts by weight of an amino acid salt; most preferably 6 to 9 parts by weight of an amino acid salt.
The amino acid salt is preferably selected from one or more of potassium lauroyl glutamate, sodium cocoyl glutamate, disodium cocoyl glutamate, sodium cocoyl methyl taurate, potassium cocoyl glutamate, sodium myristoyl glutamate, potassium myristoyl glutamate, sodium stearoyl glutamate, potassium stearoyl glutamate, sodium palmitoyl glutamate, potassium palmitoyl glutamate and sodium cocoyl amido propionate; more preferably one or more selected from sodium cocoyl glutamate, disodium cocoyl glutamate, sodium cocoyl methyl taurate, potassium cocoyl glutamate, sodium stearyl glutamate, potassium stearyl glutamate, sodium palmitoyl glutamate, potassium palmitoyl glutamate and sodium cocoyl amido propionate.
The amino acid soap raw material provided by the invention comprises 10-30 parts by weight of a humectant; preferably 12 to 28 parts by weight of a humectant; more preferably 12 to 25 parts by weight of a humectant; most preferably 12 to 20 parts by weight of a humectant.
The humectant is preferably one or more selected from glycerol, sorbitol, propylene glycol and polyethylene glycol.
The sources of the glycerin, sorbitol, propylene glycol and polyethylene glycol are not limited in the present invention, and they may be commercially available.
The amino acid soap raw material provided by the invention comprises 0.2-10 parts by weight of a skin feel modifier; preferably 1-9 parts by weight of a skin feel modifier; more preferably 1 to 7 parts by weight of a skin feel modifier; most preferably 1 to 5 parts by weight of a skin feel modifier.
The skin feeling regulator is preferably one or more selected from polyglycerol-10, betaine, urea, allantoin, seaweed extract, hyaluronic acid, sodium hyaluronate, trehalose, maltitol, erythritol, mannitol and sucrose.
In the present invention, the source of the skin feel modifier is not limited and may be commercially available.
In the invention, the raw material of the amino acid soap preferably further comprises 0-5 parts by weight of an aromatic agent; more preferably 0.1 to 3 parts by weight of an aromatic agent; most preferably, the perfume composition comprises 0.2-2 parts by weight of the perfume.
In the invention, the flavoring agent is preferably selected from one or more of essence and essential oil.
In the invention, the raw material of the amino acid soap preferably further comprises 0-0.5 weight part of appearance modifier; more preferably, the appearance improver is included in an amount of 0.1 to 0.4 parts by weight.
The appearance modifier is preferably selected from one or more of pigment, dried flower, titanium dioxide and bamboo charcoal powder; more preferably one or more selected from pigment and dried flower; most preferably a pigment; the pigments include, but are not limited to, blue, caramel, and yellow pigments.
According to the invention, by selecting the content of specific creatine and B vitamins (including folic acid, nicotinamide and one or two of vitamin B6 and vitamin B12) and simultaneously proportioning reasonable amino acid, triethanolamine, amino acid salt, humectant, skin feel regulator and other auxiliary materials, the obtained amino acid soap is mild and clean, has moderate degreasing force, has fresh and smooth skin feel during cleaning, has moist and tight skin feel after cleaning, and also has the functions of removing dark skin color, fading acne marks and chloasma; black heads and acnes are reduced; enhancing moisture retention and skin elasticity; multiple effects such as after-sun repair and the like.
The invention provides a preparation method of amino acid soap, which comprises the following steps:
A) mixing amino acid, amino acid salt, a humectant and a solvent, and heating and stirring to obtain a first mixed solution;
mixing and heating triethanolamine and a solvent to obtain a second mixed solution;
B) mixing the first mixed solution and the second mixed solution, mixing with a skin feel regulator, cooling after mixing, and mixing with B vitamins and creatine to obtain a third mixed solution;
C) and filling the third mixed solution into a mold to obtain the amino acid soap.
The method comprises the steps of mixing amino acid, amino acid salt, a humectant and a solvent, and heating and stirring to obtain a first mixed solution.
The specific components and proportions of the amino acid, the amino acid salt, the humectant and the solvent are clearly described in the invention, and are not described in detail herein.
The specific manner of mixing and stirring according to the present invention is not limited and is well known to those skilled in the art; the heating temperature of the heating and stirring is preferably 80-95 ℃; more preferably 80 to 90 ℃.
The solvent added here in the present invention is preferably 40% to 60% of the total solvent mass.
Mixing and heating triethanolamine and a solvent to obtain a second mixed solution.
The specific components and proportions of the triethanolamine and the solvent are clearly described in the invention, and are not described in detail herein.
According to the present invention, the specific mode of mixing is not limited, and it is preferable to stir after mixing. The heating temperature of the mixing and heating is preferably 80-95 ℃; more preferably 80 to 90 ℃.
Mixing the first mixed solution and the second mixed solution, and mixing with the skin feeling regulator after mixing.
The specific components and proportions of the skin feel modifier are clearly described above, and are not repeated herein. According to the present invention, the specific mode of mixing is not limited, and it is preferable to stir after mixing. The heating temperature of the mixing and heating is preferably 80-95 ℃; more preferably 80 to 90 ℃.
Mixing, cooling, and mixing with vitamin B and creatine to obtain a third mixed solution;
the temperature for reducing the temperature is preferably 55-75 ℃; more preferably 65-75 ℃; the specific components and proportions of the vitamin B group and the creatine in the invention are clearly described above, and are not described in detail herein.
And after the third mixed solution is obtained, filling the third mixed solution into a mold to obtain the amino acid soap.
The third mixed solution of the present invention can be prepared by: mixing the first mixed solution and the second mixed solution, mixing with a skin feel regulator after mixing, cooling, mixing with one or more of B vitamins, creatine, appearance modifier and aroma-binding agent to obtain a third mixed solution, standing for defoaming, and filling into a mold to obtain the amino acid soap.
The temperature for reducing the temperature is preferably 55-75 ℃; more preferably 65 to 75 ℃.
The present invention is not limited to the specific manner of filling into the mold, and the filling method is well known to those skilled in the art.
The evaluation methods of the skin care composition and the amino acid soap in the examples of the present invention were mainly performed as follows:
the skin care composition and the evaluation of the effect of the skin care product comprising the composition in the examples are carried out by human trial experiments, and 4 human trial experiments are designed in each example:
(1) and selecting the crowd with dark skin color, sunburn, chloasma and acne marks to participate in the test of the whitening effect of the sample. The samples in examples and comparative examples were used for each group of 20 persons, and the average value of change in ITA and the average value of change in the number of spots before and after 4 weeks of continuous use of the samples were measured and calculated using the ITA individual type angle.
(2) And selecting the population with blackheads and acnes to participate in the test of the blackhead and acne removing effect of the sample. The samples were continuously used for 4 weeks in each of 20 persons per group, and the number of blackheads and pimples before and after use were compared with each other for 4 weeks.
(3) Selecting the people with loose and dry skin to participate in the test of the skin elasticity increasing and moisturizing effect of the sample; the samples were divided into 20 persons per group according to the number of samples, and each group of test persons used the samples in examples and comparative examples, respectively, and tested by using a CK skin tester, skin moisture content before and after continuously using the samples for 4 weeks, and an average value of skin moisture content change was calculated. The effect of the sample on increasing skin elasticity was evaluated by subject scoring. After 4 weeks of continuous use, subjects scored the perception of skin elasticity changes. The scoring criteria used a 9-point scoring method, and the scores and corresponding perceptions are shown in the table below.
Sample use experience and corresponding score value
(4) Selecting the people with red, peeled, burning and painful skin after the two arms are sunned to participate in the test of the sample after-sun repair effect; the samples in the examples and the comparative examples were used in groups of 20 persons, each group of persons tested. The corresponding sample is used for the left arm of each subject, no product is used for the right arm, and the erythema, skin inflammation and pain feeling of the sunburn part of the two arms are observed and compared after 3 days, and the sunburn repairing effect of the corresponding amino acid soap is graded according to the scoring standard shown in the table.
The invention also discovers that the amino acid soap containing the skin care product composition has the advantages that the amino acid soap has a pH value close to human skin, is good in transparency and moderate in hardness by reasonably selecting and proportioning the contents of the amino acid, the triethanolamine and the amino acid salt, is favorable for maintaining the appearance of the amino acid soap, and does not influence the efficacy of the amino acid soap. The physical and chemical property measurement of the amino acid soap comprises the following steps:
(1) hardness test of amino acid soap: the amino acid soap was placed under the probe by a puncture test method, measured by a physical property tester, and the surface hardness/g, the internal hardness/g, and the viscosity/g · s were recorded.
(2) Transparency detection of amino acid soap: the amino acid soap was cut into a flat and smooth sheet having a thickness of 6.5 ± 0.15mm on both sides, and the sheet was inserted into a light-impervious stationary cylinder, and the numerical value of the light reflection factor (R0) in the case where the sample was backed with a black back and the numerical value of the internal light reflection factor (R ∞) in the case where the sample was backed with a white board were measured on a whiteness meter, and the transparency of the amino acid soap was calculated according to the formula T (%) (1-R0/R ∞) × 100%.
(3) pH value detection of amino acid soap: and adding water into the mixed solution before injection molding of the amino acid soap to prepare amino acid soap water, and detecting the pH value of the soap water by adopting a pH meter.
In order to further illustrate the present invention, the skin care composition, the amino acid soap and the preparation method thereof provided by the present invention are described in detail below with reference to examples.
Example 1
A skin care composition.
(1) Formulation of
(2) The preparation method comprises the following steps: mixing the above components, adding distilled water to desired volume of 100ml, and mixing to obtain the skin care composition.
(3) Effect testing
Example 2
A skin care composition.
(1) Formulation of
(2) The preparation method comprises the following steps: mixing the above components, adding distilled water to desired volume of 100ml, and mixing to obtain the skin care composition.
(3) Effect testing
Example 3
A skin care composition.
(1) Formulation of
(2) The preparation method comprises the following steps: mixing the above components, adding distilled water to desired volume of 100ml, and mixing to obtain the skin care composition.
(3) Effect testing
Example 4
A skin care composition.
(1) Formulation of
(2) The preparation method comprises the following steps: mixing the above components, adding distilled water to desired volume of 100ml, and mixing to obtain the skin care composition.
(3) Effect testing
Example 5
A skin care composition.
(1) Formulation of
(2) The preparation method comprises the following steps: mixing the above components, adding distilled water to desired volume of 100ml, and mixing to obtain the skin care composition.
(3) Effect testing
Example 6
An amino acid soap.
(1) Formulation of
(2) The preparation method comprises the following steps:
1) mixing lauroyl glutamic acid, sodium lauroyl glutamate, glycerol and water, stirring at constant speed, and heating to 80 deg.C.
2) Mixing triethanolamine and water, heating to 80 ℃, slowly adding the mixed solution obtained in the step 1), uniformly stirring, and adding polyglycerol-10.
3) Cooling to 55 deg.C, adding B vitamins (including folic acid, nicotinamide, vitamin B6, and vitamin B12), creatine, blue color, and essence.
4) Filling in a mold, and quickly cooling and solidifying.
(3) Effect testing
Example 7
An amino acid soap.
(1) Formulation of
(2) The preparation method comprises the following steps:
1) mixing lauroyl glutamic acid, sodium lauroyl glutamate, glycerol and water, stirring at constant speed, and heating to 90 deg.C.
2) Mixing triethanolamine and water, heating to 90 ℃, slowly adding the mixed solution obtained in the step 1), uniformly stirring, and adding polyglycerol-10.
3) Cooling to 65 deg.C, adding B vitamins (including folic acid, nicotinamide, vitamin B12), creatine, blue color and essence.
4) Filling into a mold, and rapidly cooling.
(3) Effect testing
Example 8
An amino acid soap.
(1) Formulation of
(2) The preparation method comprises the following steps:
1) mixing lauroyl glutamic acid, sodium lauroyl glutamate, glycerol and water, stirring at constant speed, and heating to 95 deg.C.
2) Mixing triethanolamine and water, heating to 95 ℃, slowly adding into the step 1), stirring uniformly, and adding into polyglycerol-10.
3) Cooling to 75 deg.C, adding B vitamins (including folic acid, nicotinamide, vitamin B6), creatine, blue color and essence.
4) Filling in a mold, and quickly cooling and solidifying.
(3) Effect testing
Example 9
An amino acid soap.
(1) Formulation of
(2) The preparation method comprises the following steps:
1) mixing lauroyl glutamic acid, sodium lauroyl glutamate, glycerol and water, stirring at constant speed, and heating to 85 deg.C.
2) Mixing triethanolamine and water, heating to 85 ℃, slowly adding into the step 1), stirring uniformly, and adding into polyglycerol-10.
3) Cooling to 60 deg.C, and adding B vitamins (including folic acid and nicotinamide), creatine, blue and essence.
4) Standing, defoaming, and filling in a mold.
(3) Effect testing
Example 10
An amino acid soap.
(1) Formulation of
(2) The preparation method comprises the following steps:
1) mixing lauroyl glutamic acid, sodium lauroyl glutamate, glycerol and water, stirring at constant speed, and heating to 85 deg.C.
2) Mixing triethanolamine and water, heating to 85 ℃, slowly adding into the step 1), stirring uniformly, and adding into polyglycerol-10.
3) Cooling to 70 deg.C, and adding B vitamins (including folic acid and nicotinamide), creatine, blue and essence.
4) Standing, defoaming, and filling in a mold.
(3) Effect testing
Example 11
An amino acid soap.
(1) Formulation of
(2) The preparation method comprises the following steps:
1) mixing lauroyl glutamic acid, sodium lauroyl glutamate, glycerol and water, stirring at constant speed, and heating to 80 deg.C.
2) Mixing triethanolamine and water, heating to 80 ℃, slowly adding into the step 1), stirring uniformly, and adding into polyglycerol-10.
3) Cooling to 60 deg.C, and adding B vitamins (including folic acid, nicotinamide, vitamin B6), creatine, blue and essence.
4) Standing, defoaming, and filling in a mold.
(3) Effect testing
(4) Measurement of physical and chemical Properties
Example 12
A facial cream.
(1) Formulation of
(2) Preparation method
1. Adding the phase A material into a water phase pot, stirring and heating to 85 ℃, adding the phase C material into an oil phase pot, stirring and heating to 85 ℃, and stirring and dissolving.
2. Mixing phase B in a prefabricated tank, and keeping.
And 3, starting stirring the phase A, adding the phase C, the phase B and the phase D, and homogenizing for 5 minutes after stirring.
4. Cooling to 60 deg.C, adding phase E, and stirring.
5. Cool to 45 ℃, add phase F. Discharging.
(3) Effect testing
Example 13
A body lotion.
(1) And (4) preparing.
(2) Preparation method
Heating phase A and phase B to 85 deg.C respectively.
Phase A was added to phase B, stirred and homogenized for 5 minutes.
3. Cooling to 45 deg.C, and adding phase C. Discharging.
(3) Effect testing
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.
Claims (9)
1.A skin care composition comprising:
0.01-0.3 parts by weight of creatine;
0.02-6.5 parts by weight of B vitamins;
the B vitamins comprise:
2. the composition of claim 1, wherein the skin care composition comprises
0.02-0.25 parts of creatine;
0.05-5 parts of B vitamins.
3. Use of a composition according to any one of claims 1 to 2 for the preparation of a cosmetic product.
4. A cosmetic comprising the composition according to any one of claims 1 to 2.
5. The cosmetic according to claim 4, wherein the dosage form of the cosmetic is one or more of soap, cream and milk.
6. The amino acid soap is characterized in that raw materials comprise a solvent and the following components:
the B vitamins comprise:
7. the amino acid soap according to claim 6, wherein the amino acid is selected from one or more of lauroyl glutamic acid, cocoyl glutamic acid, myristoyl glutamic acid, stearoyl glutamic acid, palmitoyl glutamic acid, and cocamido propionic acid; the amino acid salt is selected from one or more of potassium lauroyl glutamate, sodium cocoyl glutamate, disodium cocoyl glutamate, sodium cocoyl methyl taurate, potassium cocoyl glutamate, sodium myristoyl glutamate, potassium myristoyl glutamate, sodium stearoyl glutamate, potassium stearoyl glutamate, sodium palmitoyl glutamate, potassium palmitoyl glutamate and sodium cocoyl amido propionate; the humectant is selected from one or more of glycerol, sorbitol, propylene glycol and polyethylene glycol; the skin feeling regulator is one or more selected from polyglycerol-10, betaine, urea, allantoin, seaweed extract, hyaluronic acid, sodium hyaluronate, trehalose, maltitol, erythritol, mannitol and sucrose.
8. The amino acid soap of claim 6, further comprising the following raw materials:
0-5 parts by weight of an aromatic agent;
0-0.5 parts by weight of an appearance modifier;
the flavoring agent is selected from one or more of essence and essential oil;
the appearance modifier is selected from one or more of pigment, dried flower, titanium dioxide and bamboo charcoal powder.
9. A method for preparing the amino acid soap of claim 6, comprising the steps of:
A) mixing amino acid, amino acid salt, a humectant and a solvent, and heating and stirring to obtain a first mixed solution;
mixing and heating triethanolamine and a solvent to obtain a second mixed solution;
B) mixing the first mixed solution and the second mixed solution, mixing with a skin feel regulator, cooling after mixing, and mixing with B vitamins and creatine to obtain a third mixed solution;
C) and filling the third mixed solution into a mold to obtain the amino acid soap.
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| CN109381357B (en) * | 2018-12-13 | 2021-09-03 | 广州宝莱生物科技有限公司 | Leech freeze-dried powder capable of removing acne and moisturizing skin |
| CN109846779A (en) * | 2019-03-06 | 2019-06-07 | 上海乐宝日化股份有限公司 | A kind of maintenance makeup remover and preparation method thereof containing vitamin B12 |
| CN113201422A (en) * | 2021-06-07 | 2021-08-03 | 深圳市垛润商业有限公司 | Preparation method of multi-sugar alcohol mineral rock facial soap |
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| JPS60166604A (en) * | 1984-02-09 | 1985-08-29 | Kobayashi Kooc:Kk | Preparation of weakly acidic w/o/w-type emulsion cosmetic |
| DE102007038413A1 (en) * | 2007-08-09 | 2009-02-12 | Beiersdorf Ag | Cosmetic emulsifier combination |
| WO2009053163A1 (en) * | 2007-10-25 | 2009-04-30 | Unilever Plc | Hair care composition |
| CN103301051B (en) * | 2012-03-07 | 2015-01-21 | 南京华狮化工有限公司 | Transparent beauty treatment soap composition |
| CN102978048B (en) * | 2012-11-16 | 2014-11-05 | 广州伊凡生物科技有限公司 | Weakly acidic transparent soap and preparation method thereof |
| CN103520081B (en) * | 2013-09-27 | 2015-10-28 | 无限极（中国）有限公司 | The external use skin care of a kind of regulation of skin immunity, delay skin aging |
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