CN107354000B - Peony seed shell rotting spray liquid and using method thereof - Google Patents

Peony seed shell rotting spray liquid and using method thereof Download PDF

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CN107354000B
CN107354000B CN201710657642.2A CN201710657642A CN107354000B CN 107354000 B CN107354000 B CN 107354000B CN 201710657642 A CN201710657642 A CN 201710657642A CN 107354000 B CN107354000 B CN 107354000B
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parts
rotting
spray liquid
peony seed
peony
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CN107354000A (en
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雷金云
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JINZHAI YINONG AGRICULTURAL TECHNOLOGY DEVELOPMENT Co.,Ltd.
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01GHORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G18/00Cultivation of mushrooms
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F5/00Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
    • C05F5/006Waste from chemical processing of material, e.g. diestillation, roasting, cooking
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P21/00Preparation of peptides or proteins
    • C12P21/06Preparation of peptides or proteins produced by the hydrolysis of a peptide bond, e.g. hydrolysate products
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/10Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
    • Y02A40/20Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Mycology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Zoology (AREA)
  • Biochemistry (AREA)
  • Botany (AREA)
  • General Chemical & Material Sciences (AREA)
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  • Bioinformatics & Cheminformatics (AREA)
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  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Microbiology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Molecular Biology (AREA)
  • Environmental Sciences (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Pretreatment Of Seeds And Plants (AREA)

Abstract

A peony seed-shell rotting spray liquid and a using method thereof are disclosed, wherein the spray liquid is composed of the following raw materials in parts by weight: 2-3 parts of serine protease, 3-5 parts of Bordeaux mixture, 5-10 parts of alkyl naphthalene sulfonate, 8-12 parts of acetic acid, 5-10 parts of acid-resistant cellulase, 5-10 parts of acrylic emulsion, 1-2 parts of salicylic acid, 2-4 parts of potassium borate and 1-2 parts of tea polyphenol. The spraying liquid has simple formula, does not contain harmful ingredients, is convenient to use, has large treatment capacity, and is particularly suitable for planters with large peony seed planting area or peony seed oil production enterprises.

Description

Peony seed shell rotting spray liquid and using method thereof
Technical Field
The invention relates to the field of preparation of peony seed oil, and particularly relates to a peony seed shell rotting spray liquid and a using method thereof.
Background
The peony seeds are the essential crystals of peony plants, have unique medical and nutritional ingredients besides all the characteristics of the peony, are nuts protected by shells and shells, and have natural longevity genes. The origin is located in the Shandong lotus, the first peony seed oil in the world is released in 2009, and provincial achievement identification in the Shandong province is obtained. Tests of multiple professional institutions such as Jiangnan university and Chinese grain and oil quality supervision and inspection center of oil and fat authority department show that the content of unsaturated fatty acid in the peony seed oil reaches over 90 percent, and particularly, the content of the polyunsaturated fatty acid, namely linolenic acid (belonging to omega-3 series), is over 40 percent and is 140 times of that of olive oil, which is difficult and expensive. The vegetable oil extracted from peony seeds is unique woody nut oil in China, has medical health care function due to rich nutrition, is called as ' the best oil in the world ' by related experts, is a treasure in vegetable oil, and obtains new resource food approval in 2011, 3, and 22 days (bulletin about approval of acer truncatum seed oil and peony seed oil as new resource food (2011, No. 9) the Council of the national health and family planning of the people's republic of China).
The processing of shelling needs to be carried out to the in-process is prepared to tree peony seed oil, and the tradition mode of shelling utilizes machinery to shell after drying in the sun, and this kind of mode of shelling needs to dry tree peony seed in advance, and the sunning needs to occupy the place on the one hand, and on the other hand can take away partial nourishment at the moisture of sunning in-process evaporation, and mechanical shelling is with high costs, consumes the manpower, is unsuitable for tree peony seed oil to prepare.
Disclosure of Invention
The invention aims to overcome the defects in the prior art for removing fresh peony seed shells, and provides a peony seed shell rotting spray liquid and a using method thereof.
The peony seed-shell rotting spray liquid is prepared from the following raw materials in parts by weight:
2-3 parts of serine protease, 3-5 parts of Bordeaux mixture, 5-10 parts of alkyl naphthalene sulfonate, 8-12 parts of acetic acid, 5-10 parts of acid-resistant cellulase, 5-10 parts of acrylic emulsion, 1-2 parts of salicylic acid, 2-4 parts of potassium borate and 1-2 parts of tea polyphenol.
Preferably, the spraying liquid consists of the following raw materials in parts by weight:
2 parts of serine protease, 4 parts of Bordeaux mixture, 8 parts of alkyl naphthalene sulfonate, 10 parts of acetic acid, 8 parts of acid-resistant cellulase, 7 parts of acrylic emulsion, 2 parts of salicylic acid, 3 parts of potassium borate and 2 parts of tea polyphenol.
Preferably, the boldo solution is formulated from 5 grams of copper sulfate, 4.5 grams of hydrated lime, and 0.5 kilograms of water.
Preferably, the alkyl naphthalene sulfonate is sodium alkyl naphthalene sulfonate.
Preferably, the acid-resistant cellulase consists of exo-beta-glucanase, endo-beta-glucanase and beta-glucosidase in a weight ratio of 1:2: 1.
The spraying liquid is in a weakly acidic environment, and the pH is preferably 6.2-6.5.
The pH value of the spraying liquid is adjusted by the content of acetic acid or salicylic acid.
A use method of the peony seed-shell rotting spraying liquid comprises the following steps: spraying a corrupting agent on the collected fresh peony seeds, uniformly stirring, filling the peony seeds into a bamboo basket, and then putting the peony seeds into a corrupting chamber to gradually soften the shell; 30kg of peony seeds are contained in one basket, every 4-6 baskets form a stack, and gaps are reserved between the stacks; the temperature of the decomposition chamber is controlled to be 20-25 ℃, the air humidity is 70-75%, the time is 24-36 hours, and after the decomposition treatment is finished, the peony seed shells are softened and separated from the fruits.
Preferably, 0.5-1 kg of the spraying liquid is sprayed on every basket of peony seeds.
The action mechanism of the invention is as follows: the peptide bond of macromolecular protein in the peony seed hulls is broken by serine protease in the spraying liquid to enable the macromolecular protein to become micromolecular protein, meanwhile, a large amount of cellulose contained in the peony seed hulls is converted into polysaccharide by cellulase, full utilization of the peony seed hulls is achieved, Bordeaux liquid enables the whole decomposition treatment process not to be infected by bacteria, the probability of mildew generation of the processed peony seed hulls can be reduced by potassium borate, and the tea polyphenol is combined with anthocyanin in the peony seed hulls to keep the activity of the anthocyanin.
Compared with the prior art, the invention has the following beneficial effects:
(1) the peony seed shells contain rich anthocyanin which is a water-soluble pigment and can be used as a raw material of a health-care product, the anthocyanin is evaporated along with water and lost by mechanical shelling and airing, and the anthocyanin component and the activity thereof in the seed shells can be effectively retained by using the spraying liquid for shelling;
(2) spraying the spraying liquid on the peony seeds to obtain softened peony seed shells, which can be directly used as fungus sticks for planting precious peony mushrooms;
(3) manual airing and shelling are not needed, the problem of an airing field is solved, a large amount of labor cost is saved for enterprises, and the method is suitable for large-batch processing of peony seeds;
(4) the spraying liquid has simple formula, convenient use and large treatment capacity, and is particularly suitable for planters with large planting area of the peony seeds or peony seed oil production enterprises;
(5) contains no harmful components and causes no pollution to peony seeds.
Detailed Description
In order to make the technical means, the creation features, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the embodiment.
Example 1
The peony seed-shell rotting spray liquid is prepared from the following raw materials in parts by weight:
2 parts of serine protease, 3 parts of Bordeaux mixture, 5 parts of alkyl naphthalene sulfonate, 8 parts of acetic acid, 5 parts of acid-resistant cellulase, 5 parts of acrylic emulsion, 1 part of salicylic acid, 2 parts of potassium borate and 1 part of tea polyphenol.
The boldo solution is prepared from 5 grams of copper sulfate, 4.5 grams of hydrated lime and 0.5 kilogram of water.
The alkyl naphthalene sulfonate is sodium alkyl naphthalene sulfonate.
The acid-resistant cellulase consists of exo-beta-glucanase, endo-beta-glucanase and beta-glucosidase in a weight ratio of 1:2: 1.
The spraying liquid is in a weakly acidic environment, and the pH value is 6.2.
The pH value of the spraying liquid is adjusted by the content of acetic acid or salicylic acid.
A use method of the peony seed-shell rotting spraying liquid comprises the following steps: spraying a corrupting agent on the collected fresh peony seeds, uniformly stirring, filling the peony seeds into a bamboo basket, and then putting the peony seeds into a corrupting chamber to gradually soften the shell; 30kg of peony seeds are contained in one basket, every 4-6 baskets form a stack, and gaps are reserved between the stacks; the temperature of the decomposition chamber is controlled to be 20-25 ℃, the air humidity is 70-75%, the time is 24-36 hours, and after the decomposition treatment is finished, the peony seed shells are softened and separated from the fruits.
Spraying 0.5kg of spraying liquid to every basket of peony seeds.
Example 2
The peony seed-shell rotting spray liquid is prepared from the following raw materials in parts by weight:
2 parts of serine protease, 4 parts of Bordeaux mixture, 8 parts of alkyl naphthalene sulfonate, 10 parts of acetic acid, 8 parts of acid-resistant cellulase, 7 parts of acrylic emulsion, 2 parts of salicylic acid, 3 parts of potassium borate and 2 parts of tea polyphenol.
The boldo solution is prepared from 5 grams of copper sulfate, 4.5 grams of hydrated lime and 0.5 kilogram of water.
The alkyl naphthalene sulfonate is sodium alkyl naphthalene sulfonate.
The acid-resistant cellulase consists of exo-beta-glucanase, endo-beta-glucanase and beta-glucosidase in a weight ratio of 1:2: 1.
The spraying liquid is in a weakly acidic environment, and the pH value is 6.4.
The pH value of the spraying liquid is adjusted by the content of acetic acid or salicylic acid.
A use method of the peony seed-shell rotting spraying liquid comprises the following steps: spraying a corrupting agent on the collected fresh peony seeds, uniformly stirring, filling the peony seeds into a bamboo basket, and then putting the peony seeds into a corrupting chamber to gradually soften the shell; 30kg of peony seeds are contained in one basket, every 4-6 baskets form a stack, and gaps are reserved between the stacks; the temperature of the decomposition chamber is controlled to be 20-25 ℃, the air humidity is 70-75%, the time is 24-36 hours, and after the decomposition treatment is finished, the peony seed shells are softened and separated from the fruits.
Preferably, 0.8kg of spraying liquid is sprayed on every basket of peony seeds.
Example 3
The peony seed-shell rotting spray liquid is prepared from the following raw materials in parts by weight:
3 parts of serine protease, 5 parts of Bordeaux mixture, 10 parts of alkyl naphthalene sulfonate, 12 parts of acetic acid, 10 parts of acid-resistant cellulase, 10 parts of acrylic emulsion, 2 parts of salicylic acid, 4 parts of potassium borate and 2 parts of tea polyphenol.
The boldo solution is prepared from 5 grams of copper sulfate, 4.5 grams of hydrated lime and 0.5 kilogram of water.
The alkyl naphthalene sulfonate is sodium alkyl naphthalene sulfonate.
The acid-resistant cellulase consists of exo-beta-glucanase, endo-beta-glucanase and beta-glucosidase in a weight ratio of 1:2: 1.
The spraying liquid is in a weakly acidic environment, and the pH value is 6.5.
The pH value of the spraying liquid is adjusted by the content of acetic acid or salicylic acid.
A use method of the peony seed-shell rotting spraying liquid comprises the following steps: spraying a corrupting agent on the collected fresh peony seeds, uniformly stirring, filling the peony seeds into a bamboo basket, and then putting the peony seeds into a corrupting chamber to gradually soften the shell; 30kg of peony seeds are contained in one basket, every 4-6 baskets form a stack, and gaps are reserved between the stacks; the temperature of the decomposition chamber is controlled to be 20-25 ℃, the air humidity is 70-75%, the time is 24-36 hours, and after the decomposition treatment is finished, the peony seed shells are softened and separated from the fruits.
Spraying 1kg of spraying liquid on each basket of peony seeds.
Experimental data: the spray solutions prepared in examples 1-3 were sprayed on peony seed husks and compared to the effect of using a common mechanical shelling machine (comparative example 1):
Figure BDA0001369722420000051
the foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and the preferred embodiments of the present invention are described in the above embodiments and the description, and are not intended to limit the present invention. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (5)

1. The peony seed-shell rotting spray liquid is characterized by comprising the following raw materials in parts by weight:
2-3 parts of serine protease, 3-5 parts of Bordeaux mixture, 5-10 parts of alkyl naphthalene sulfonate, 8-12 parts of acetic acid, 5-10 parts of acid-resistant cellulase, 5-10 parts of acrylic emulsion, 1-2 parts of salicylic acid, 2-4 parts of potassium borate and 1-2 parts of tea polyphenol;
the Bordeaux mixture is prepared from 5 g of copper sulfate, 4.5 g of hydrated lime and 0.5kg of water;
the alkyl naphthalene sulfonate is sodium alkyl naphthalene sulfonate;
the acid-resistant cellulase consists of exo-beta-glucanase, endo-beta-glucanase and beta-glucosidase in a weight ratio of 1:2: 1;
the spraying liquid is in a weakly acidic environment.
2. The peony seed hull rotting spray liquid as claimed in claim 1, wherein the spray liquid is composed of the following raw materials in parts by weight:
2 parts of serine protease, 4 parts of Bordeaux mixture, 8 parts of alkyl naphthalene sulfonate, 10 parts of acetic acid, 8 parts of acid-resistant cellulase, 7 parts of acrylic emulsion, 2 parts of salicylic acid, 3 parts of potassium borate and 2 parts of tea polyphenol.
3. The peony seed hull rotting spray liquid as claimed in claim 1, wherein the pH of the spray liquid is 6.2-6.5.
4. The use method of the peony seed husk rotting spray liquid as claimed in any one of claims 1 to 3, characterized in that the rotting agent is sprayed on the harvested fresh peony seeds and stirred uniformly, and the seeds are put into a rotting chamber after being filled into a bamboo basket to gradually soften the shell; 30kg of peony seeds are contained in one basket, every 4-6 baskets form a stack, and gaps are reserved between the stacks; the temperature of the decomposition chamber is controlled to be 20-25 ℃, the air humidity is 70-75%, the time is 24-36 hours, and after the decomposition treatment is finished, the peony seed shells are softened and separated from the fruits.
5. The use method of the peony seed-husk rotting spray liquid as claimed in claim 4, wherein 0.5-1 kg of the spray liquid is sprayed to every basket of peony seeds.
CN201710657642.2A 2017-08-03 2017-08-03 Peony seed shell rotting spray liquid and using method thereof Active CN107354000B (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR970061049A (en) * 1996-02-16 1997-09-12 이희철 Roller for a microwave machine and method of manufacturing the same
CN102731486A (en) * 2011-12-25 2012-10-17 大兴安岭林格贝有机食品有限责任公司 New method for purifying silymarin
CN105394589A (en) * 2015-12-15 2016-03-16 安徽省砀山兴达罐业食品有限公司 Preparation method for instant green soya bean can

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR970061049A (en) * 1996-02-16 1997-09-12 이희철 Roller for a microwave machine and method of manufacturing the same
CN102731486A (en) * 2011-12-25 2012-10-17 大兴安岭林格贝有机食品有限责任公司 New method for purifying silymarin
CN105394589A (en) * 2015-12-15 2016-03-16 安徽省砀山兴达罐业食品有限公司 Preparation method for instant green soya bean can

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