CN105535321A - Sulfur-free pinellia ternata processing method - Google Patents
Sulfur-free pinellia ternata processing method Download PDFInfo
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- CN105535321A CN105535321A CN201410597584.5A CN201410597584A CN105535321A CN 105535321 A CN105535321 A CN 105535321A CN 201410597584 A CN201410597584 A CN 201410597584A CN 105535321 A CN105535321 A CN 105535321A
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- rhizoma pinelliae
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Abstract
The present invention discloses a sulfur-free pinellia ternata processing method. According to the method, fresh pinellia ternata is subjected to selection and grading, the fresh pinellia ternata having the same grade is peeled, and the peeled pinellia ternata is subjected to color protection treatment by using a special color protection agent, wherein the special color protection agent comprises any three, four or five materials selected from ascorbic acid with a mass percent concentration of 0.04-0.4%, citric acid with a mass percent concentration of 0.1-0.6%, L-cysteine with a mass percent concentration of 0.01-0.06%, sodium chloride with a mass percent concentration of 0.1-0.6%, and calcium chloride with a mass percent concentration of 0.1-0.4%; after the color protection treatment is completed, the obtained pinellia ternata is conveyed into drying equipment, and drying is performed until the water content in the pinellia ternata is less than 15%, wherein high temperature enzyme inactivation and bacterial killing are performed before the drying; and the dried pinellia ternata is cooled to a room temperature, and the cooled pinellia ternata can be directly subjected to vacuum sealed packaging or can be stored at a safe temperature and a safe humidity. According to the present invention, the method has characteristics of simple process and easy operation, the obtained pinellia ternata finished product has characteristics of white surface, good color and no sulfur residue, and the chemical components and the medicinal value of the pinellia ternata are not affected, and the advantages of economy and environmental protection are provided.
Description
Technical field
The invention belongs to technical field of Chinese medicines, relate to the processing method of the Rhizoma Pinelliae, be specifically related to a kind of processing method without the sulfur Rhizoma Pinelliae.
Background technology
The Rhizoma Pinelliae is the dry tuber of the aroid Rhizoma Pinelliae, has effect of drying dampness to eliminate phlegm, stopping nausea and vomiting by lowering the adverse flow of QI, dissolving lump and resolving mass, for various disease conditions such as abundant expectoration cough with asthma, vomiting regurgitation, breast wrist feeling of fullness, globus hystericus, carbuncle sucutaneous nodule, is Chinese tradition Chinese crude drug.
The fresh Rhizoma Pinelliae is perishable, needs to carry out dried and be beneficial to preserve after gathering.The skin of the Rhizoma Pinelliae does not have much values, needs to peel in the fresh Rhizoma Pinelliae course of processing, and fresh Rhizoma Pinelliae decortication rear surface is pure white vivid, but dry rear surface color becomes yellow, has a strong impact on its exterior quality and price.For improving the outward appearance of Rhizoma Pinelliae goods, now take stove drying method to process to ensure that its surface is pure white to it more, but, sulfur is smoked in process can produce sulfur dioxide, as easy as rolling off a logly remain in the middle of medical material, sulfur dioxide residue can damage human body, and sulfur is smoked total alkaloid content in the Rhizoma Pinelliae also can be caused obviously to reduce.Stove drying method not only affects quality of medicinal material, also has very large harm to patient health, causes outlet limited." Chinese Pharmacopoeia ", though version in 2010 prohibits the use stove drying method to process medical material, surface color is too large on the impact of price, and make Rhizoma Pinelliae producing region still take this kind of processing mode, it is imperative therefore to look for without sulfur processing method.
(patent No.: 201110147028.4), this patent of invention discloses a kind of processing method of the Rhizoma Pinelliae to Chinese invention " a kind of Rhizoma Pinelliae and processing method thereof ", and the method adopts pH to be dry behind the acid solution process Rhizoma Pinelliae surface of 1-6.Although the method can make Rhizoma Pinelliae finished surface keep pure white, there is following shortcoming in the method: need to use a large amount of acid to process, the acid pickle after process can to environment; And strongly acidic solution process can affect the medical value of the Rhizoma Pinelliae.
Summary of the invention
For solving above-mentioned prior art Problems existing, the invention provides a kind of processing method without the sulfur Rhizoma Pinelliae.The method technique is simple, and easy and simple to handle, the Rhizoma Pinelliae finished surface obtained is pure white, and good colour, remains without sulfur, does not almost affect the chemical composition of Rhizoma Pinelliae finished product and medical value, and economic environmental protection.
Realizing the technical scheme that above-mentioned purpose of the present invention takes is:
Without a processing method for the sulfur Rhizoma Pinelliae, comprise the steps:
1) the fresh Rhizoma Pinelliae is carried out sorting, peel after cleaning;
2) color fixative is carried out by the Rhizoma Pinelliae immersion colour fixative after decortication, described colour fixative be containing mass percent concentration be the ascorbic acid of 0.04%-0.4%, the citric acid of 0.1%-0.6%, the Cys of 0.01%-0.06%, the sodium chloride of 0.1%-0.6% and the calcium chloride of 0.1%-0.4% wherein any three kinds, the mixed solution of any four kinds or five kinds, wherein the mass ratio of colour fixative and the Rhizoma Pinelliae is 1: 2-10, after color fixative 0.5-5 hour, the Rhizoma Pinelliae after color fixative is washed, airing is to Rhizoma Pinelliae surface attachment water evaporates or directly remove Rhizoma Pinelliae surface attachment moisture,
3) by step 2) in the Rhizoma Pinelliae through color retention and after removing surface attachment moisture send into drying equipment, the moisture of drying at 40 DEG C-60 DEG C to the Rhizoma Pinelliae is less than 15%, takes out the Rhizoma Pinelliae, allows the Rhizoma Pinelliae be cooled to room temperature 20 DEG C-25 DEG C.
Technique scheme is improved, step 1) in the fresh Rhizoma Pinelliae is selected, pick out the Rhizoma Pinelliae of impurity and the deterioration failure that can not be used as medicine; Before cleaning, first by the size of the Rhizoma Pinelliae, stepping is carried out to the Rhizoma Pinelliae, after being peeled by the Rhizoma Pinelliae of same gear after cleaning, carry out color retention; Step 3) in the Rhizoma Pinelliae before baking first at 80 DEG C-100 DEG C high temperature enzyme denaturing carry out dried again after 9-11 minute; Step 3) in the Rhizoma Pinelliae be cooled to after under room temperature, by the Rhizoma Pinelliae temperature be 0 DEG C-30 DEG C, relative humidity be 45%-75% under storage or directly carry out vacuum sealed package.
As shown from the above technical solution, first the method is selected and stepping the fresh Rhizoma Pinelliae, special colour fixative is adopted to carry out color retention by after the fresh Rhizoma Pinelliae decortication of same gear, send into after color retention in drying equipment, first carry out enzyme denaturing at high temperature 80 DEG C-100 DEG C before the drying, eliminating bacteria, then to be dried in the Rhizoma Pinelliae a point water content and to be less than 15%, can direct vacuum sealed package or store under safe temperature and humidity after the Rhizoma Pinelliae of dried is cooled to room temperature.In the method, the Rhizoma Pinelliae is carried out stepping, the Rhizoma Pinelliae of same gear is carried out the time that color retention is conducive to controlling color fixative, save time and resource, ensure the quality of products.Special colour fixative is adopted for the Rhizoma Pinelliae in the method, this colour fixative be containing mass percent concentration be the ascorbic acid of 0.04%-0.4%, the citric acid of 0.1%-0.6%, the Cys of 0.01%-0.06%, the sodium chloride of 0.1%-0.6% and the calcium chloride of 0.1%-0.4% wherein any three kinds, the mixed solution of any four kinds or five kinds, ascorbic acid in this colour fixative, citric acid and Cys have reproducibility, can with the oxygen in air and other oxidant reactions, pigment in the protection Rhizoma Pinelliae is oxidized, wherein Cys can prevent Rhizoma Pinelliae non-enzymatic browning, ascorbic acid and citric acid have chelation to Rhizoma Pinelliae metal ion, the trace metal ion passivation of enable accelerating oxidation, thus reduce Oxidation.Calcium chloride solution has sterilization and color-protecting function, and calcium chloride as sclerosing agent, can improve the hardness of the Rhizoma Pinelliae, be conducive to the carrying out of subsequent technique.The vigor of sodium chloride solution to enzyme has certain inhibitory action, have sterilization and color-protecting function, and the dissolubility of oxygen in sodium chloride solution is smaller, avoids the oxidation of oxygen to the Rhizoma Pinelliae to a certain extent.For the feature of the Rhizoma Pinelliae self, in this colour fixative multiple colour fixative according to described concentration arbitrarily with the use of, multiple colour fixative combined effect in multiple combination colour fixative, work in coordination, make the Rhizoma Pinelliae can keep original pure white color and luster preferably, and the chemical composition of the Rhizoma Pinelliae and medical value are not almost affected, maintain the medical value of the Rhizoma Pinelliae.
Compared with prior art, its beneficial effect and advantage are in the present invention:
1, the method technique is simple, and easy to operate, the processing technique cycle is short, whole process is no more than 10 hours, and the reagent used in the course of processing is common agents, and the equipment of use is common equipment, reagent and equipment price cheap, therefore processing cost is low, is easy to suitability for industrialized production.
2, the method does not introduce sulphur-containing substance, and the Rhizoma Pinelliae finished product obtained remains without sulfur, totally has no side effect, improves the quality of Rhizoma Pinelliae finished product.
3, the method very environmental protection, does not use mineral acid, and the waste liquid that color retention obtains easily processes, and farthest can reduce environmental pollution, pollutes little.
4, the method first adopts colour fixative to carry out keeping fresh and protecting color, carry out the sterilization of high temperature enzyme denaturing again, not only make the Rhizoma Pinelliae can keep original pure white color and luster preferably, the chemical composition of the Rhizoma Pinelliae and medical value are not almost affected, maintain the medical value of the Rhizoma Pinelliae, and the sterilization of high temperature enzyme denaturing is also easy to the storage of the Rhizoma Pinelliae and guarantees the quality.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in detail.
Embodiment 1:
Without a processing method for the sulfur Rhizoma Pinelliae, the steps include:
A, the fresh Rhizoma Pinelliae to be selected, pick out the Rhizoma Pinelliae of impurity and the deterioration failure that can not be used as medicine, then the Rhizoma Pinelliae of select is carried out stepping to the Rhizoma Pinelliae by size, by gear, the Rhizoma Pinelliae is cleaned up rear employing Rhizoma Pinelliae stripping machine and peel.
B, the Rhizoma Pinelliae of the same gear of decortication immersed in colour fixative and carries out color fixative, described colour fixative be containing mass percent concentration be 0.2% ascorbic acid, 0.2% citric acid, the Cys of 0.05%, the sodium chloride of 0.2% and 0.2% the mixed solution of calcium chloride, wherein the mass ratio of colour fixative and the Rhizoma Pinelliae is 1: 5, color fixative is after 1 hour, washed by the Rhizoma Pinelliae after color fixative, airing is to Rhizoma Pinelliae surface attachment water evaporates.
C, by through color retention and Rhizoma Pinelliae dehydrator sent into by the Rhizoma Pinelliae removing surface attachment moisture, first high temperature enzyme denaturing 8 minutes at 80 DEG C, the moisture of drying at 60 DEG C again to the Rhizoma Pinelliae is 15%, take out the Rhizoma Pinelliae, allow the Rhizoma Pinelliae be cooled to room temperature 20 DEG C, finally by the Rhizoma Pinelliae finished product of cooling temperature be 30 DEG C, relative humidity be 45% time storage.
Embodiment 2:
Without a processing method for the sulfur Rhizoma Pinelliae, the steps include:
A, the fresh Rhizoma Pinelliae to be selected, pick out the Rhizoma Pinelliae of impurity and the deterioration failure that can not be used as medicine, then the Rhizoma Pinelliae of select is carried out stepping to the Rhizoma Pinelliae by size, by gear, the Rhizoma Pinelliae is cleaned up rear employing Rhizoma Pinelliae stripping machine and peel.
B, the Rhizoma Pinelliae of the same gear of decortication immersed in colour fixative and carries out color fixative, described colour fixative be containing mass percent concentration be 0.1% ascorbic acid, the citric acid of 0.5%, the Cys of 0.02% and 0.2% the mixed solution of sodium chloride, wherein the mass ratio of colour fixative and the Rhizoma Pinelliae is 1: 4, color fixative is after 0.5 hour, the Rhizoma Pinelliae after color fixative is washed, directly removes the moisture being attached to Rhizoma Pinelliae surface.
C, by through color retention and Rhizoma Pinelliae dehydrator sent into by the Rhizoma Pinelliae removing surface attachment moisture, first high temperature enzyme denaturing 10 minutes at 100 DEG C, the moisture of drying at 60 DEG C again to the Rhizoma Pinelliae is 12%, take out the Rhizoma Pinelliae, allow the Rhizoma Pinelliae be cooled to room temperature 25 DEG C, finally by the Rhizoma Pinelliae finished product of cooling temperature be 20 DEG C, relative humidity be 75% time storage.
Embodiment 3:
Without a processing method for the sulfur Rhizoma Pinelliae, the steps include:
A, the fresh Rhizoma Pinelliae to be selected, pick out the Rhizoma Pinelliae of impurity and the deterioration failure that can not be used as medicine, then the Rhizoma Pinelliae of select is carried out stepping to the Rhizoma Pinelliae by size, by gear, the Rhizoma Pinelliae is cleaned up rear employing Rhizoma Pinelliae stripping machine and peel.
B, the Rhizoma Pinelliae of the same gear of decortication immersed in colour fixative and carries out color fixative, described colour fixative be containing mass percent concentration be 0.05% ascorbic acid, 0.2% citric acid, the Cys of 0.02%, the sodium chloride of 0.1% and 0.1% the mixed solution of calcium chloride, wherein the mass ratio of colour fixative and the Rhizoma Pinelliae is 1: 6, color fixative is after 3 hours, washed by the Rhizoma Pinelliae after color fixative, airing is to Rhizoma Pinelliae surface attachment water evaporates.
C, by through color retention and drying equipment sent into by the Rhizoma Pinelliae removing surface attachment moisture, first high temperature enzyme denaturing 11 minutes at 80 DEG C, the moisture of drying at 50 DEG C again to the Rhizoma Pinelliae is 10%, take out the Rhizoma Pinelliae, allow the Rhizoma Pinelliae be cooled to room temperature 22 DEG C, finally the Rhizoma Pinelliae finished product of cooling is directly carried out vacuum sealed package.
Embodiment 4:
Without a processing method for the sulfur Rhizoma Pinelliae, the steps include:
A, the fresh Rhizoma Pinelliae to be selected, pick out the Rhizoma Pinelliae of impurity and the deterioration failure that can not be used as medicine, then the Rhizoma Pinelliae of select is carried out stepping to the Rhizoma Pinelliae by size, by gear, the Rhizoma Pinelliae is cleaned up rear employing Rhizoma Pinelliae stripping machine and peel.
B, the Rhizoma Pinelliae of the same gear of decortication immersed in colour fixative and carries out color fixative, described colour fixative be containing mass percent concentration be the ascorbic acid of 0.3%, the sodium chloride of 0.5% and 0.2% the mixed solution of calcium chloride, wherein the mass ratio of colour fixative and the Rhizoma Pinelliae is 1: 5, color fixative is after 4 hours, washed by the Rhizoma Pinelliae after color fixative, airing is to Rhizoma Pinelliae surface attachment water evaporates.
C, by through color retention and Rhizoma Pinelliae dehydrator sent into by the Rhizoma Pinelliae removing surface attachment moisture, first high temperature enzyme denaturing 9 minutes at 90 DEG C, the moisture of drying at 40 DEG C again to the Rhizoma Pinelliae is 8%, take out the Rhizoma Pinelliae, allow the Rhizoma Pinelliae be cooled to room temperature 21 DEG C, finally by the Rhizoma Pinelliae finished product of cooling temperature be 0 DEG C, relative humidity be 50% time storage.
Embodiment 5:
Without a processing method for the sulfur Rhizoma Pinelliae, the steps include:
A, the fresh Rhizoma Pinelliae to be selected, pick out the Rhizoma Pinelliae of impurity and the deterioration failure that can not be used as medicine, then the Rhizoma Pinelliae of select is carried out stepping to the Rhizoma Pinelliae by size, peel after the Rhizoma Pinelliae being cleaned up by gear.
B, the Rhizoma Pinelliae of the same gear of decortication immersed in colour fixative and carries out color fixative, described colour fixative be containing mass percent concentration be 0.2% citric acid, the Cys of 0.05%, the sodium chloride of 0.5% and 0.2% the mixed solution of calcium chloride, wherein the mass ratio of colour fixative and the Rhizoma Pinelliae is 1: 10, color fixative is after 1 hour, the Rhizoma Pinelliae after color fixative is washed, directly removes the moisture being attached to Rhizoma Pinelliae surface.
C, by through color retention and drying equipment sent into by the Rhizoma Pinelliae removing surface attachment moisture, first high temperature enzyme denaturing 10 minutes at 100 DEG C, the moisture of drying at 60 DEG C again to the Rhizoma Pinelliae is 5%, take out the Rhizoma Pinelliae, allow the Rhizoma Pinelliae be cooled to room temperature 24 DEG C, finally by the Rhizoma Pinelliae finished product of cooling temperature be 10 DEG C, relative humidity be 45% time storage.
Embodiment 6:
Without a processing method for the sulfur Rhizoma Pinelliae, the steps include:
A, the fresh Rhizoma Pinelliae to be selected, pick out the Rhizoma Pinelliae of impurity and the deterioration failure that can not be used as medicine, then the Rhizoma Pinelliae of select is carried out stepping to the Rhizoma Pinelliae by size, peel after the Rhizoma Pinelliae being cleaned up by gear.
B, the Rhizoma Pinelliae of the same gear of decortication immersed in colour fixative and carries out color fixative, described colour fixative be containing mass percent concentration be the citric acid of 0.5%, the sodium chloride of 0.2% and 0.2% the mixed solution of calcium chloride, wherein the mass ratio of colour fixative and the Rhizoma Pinelliae is 1: 6, color fixative is after 5 hours, washed by the Rhizoma Pinelliae after color fixative, airing is to Rhizoma Pinelliae surface attachment water evaporates.
C, by through color retention and drying equipment sent into by the Rhizoma Pinelliae removing surface attachment moisture, first high temperature enzyme denaturing 12 minutes at 80 DEG C, the moisture of drying at 50 DEG C again to the Rhizoma Pinelliae is 13%, take out the Rhizoma Pinelliae, allow the Rhizoma Pinelliae be cooled to room temperature 20 DEG C, finally by the Rhizoma Pinelliae finished product of cooling temperature be 25 DEG C, relative humidity be 60% time storage.
Embodiment 7:
Without a processing method for the sulfur Rhizoma Pinelliae, the steps include:
A, the fresh Rhizoma Pinelliae to be selected, pick out the Rhizoma Pinelliae of impurity and the deterioration failure that can not be used as medicine, then the Rhizoma Pinelliae of select is carried out stepping to the Rhizoma Pinelliae by size, by gear, the Rhizoma Pinelliae is cleaned up rear employing Rhizoma Pinelliae stripping machine and peel.
B, the Rhizoma Pinelliae of the same gear of decortication immersed in colour fixative and carries out color fixative, described colour fixative be containing mass percent concentration be the ascorbic acid of 0.2%, the citric acid of 0.2% and 0.05% the mixed solution of Cys, wherein the mass ratio of colour fixative and the Rhizoma Pinelliae is 1: 5, color fixative is after 3 hours, washed by the Rhizoma Pinelliae after color fixative, airing is to Rhizoma Pinelliae surface attachment water evaporates.
C, by through color retention and Rhizoma Pinelliae dehydrator sent into by the Rhizoma Pinelliae removing surface attachment moisture, first high temperature enzyme denaturing 10 minutes at 90 DEG C, the moisture of drying at 55 DEG C again to the Rhizoma Pinelliae is 9%, take out the Rhizoma Pinelliae, allow the Rhizoma Pinelliae be cooled to room temperature 25 DEG C, finally by the Rhizoma Pinelliae finished product of cooling temperature be 15 DEG C, relative humidity be 50% time storage.
Claims (5)
1., without a processing method for the sulfur Rhizoma Pinelliae, it is characterized in that comprising the steps:
1) the fresh Rhizoma Pinelliae is carried out sorting, peel after cleaning;
2) color fixative is carried out by the Rhizoma Pinelliae immersion colour fixative after decortication, described colour fixative be containing mass percent concentration be the ascorbic acid of 0.04%-0.4%, the citric acid of 0.1%-0.6%, the Cys of 0.01%-0.06%, the sodium chloride of 0.1%-0.6% and the calcium chloride of 0.1%-0.4% wherein any three kinds, the mixed solution of any four kinds or five kinds, wherein the mass ratio of colour fixative and the Rhizoma Pinelliae is 1: 2-10, after color fixative 0.5-5 hour, the Rhizoma Pinelliae after color fixative is washed, airing is to Rhizoma Pinelliae surface attachment water evaporates or directly remove Rhizoma Pinelliae surface attachment moisture,
3) by step 2) in through color retention and drying equipment sent into by the Rhizoma Pinelliae removing surface attachment moisture, the moisture of drying at 40 DEG C-60 DEG C to the Rhizoma Pinelliae is less than 15%, takes out the Rhizoma Pinelliae, allows the Rhizoma Pinelliae be cooled to room temperature 20 DEG C-25 DEG C.
2. a kind of processing method without the sulfur Rhizoma Pinelliae according to claim 1, is characterized in that: selected by the fresh Rhizoma Pinelliae in step 1), picks out the Rhizoma Pinelliae of impurity and the deterioration failure that can not be used as medicine.
3. the concocting method of Radix Paeoniae Alba decoction pieces according to claim 1, is characterized in that: before cleaning, first carry out stepping by the size of the Rhizoma Pinelliae to the Rhizoma Pinelliae, carries out color retention after being peeled by the Rhizoma Pinelliae of same gear after cleaning.
4. the concocting method of Radix Paeoniae Alba decoction pieces according to claim 1, is characterized in that: the Rhizoma Pinelliae in step 3) before baking elder generation's high temperature enzyme denaturing at 80 DEG C-100 DEG C carries out dried after 8-12 minute again.
5. the concocting method of Radix Paeoniae Alba decoction pieces according to claim 1, is characterized in that: the Rhizoma Pinelliae in step 3) is cooled to after under room temperature, by the Rhizoma Pinelliae temperature be 0 DEG C-30 DEG C, relative humidity be 45%-75% under storage or directly carry out vacuum sealed package.
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| CN110960633A (en) * | 2019-11-12 | 2020-04-07 | 珠海禾间堂本草科技有限公司 | Preparation method of dendrobium officinale dried product |
| CN113100379A (en) * | 2021-05-07 | 2021-07-13 | 江苏康润农业科技发展有限公司 | Processing method of fresh asparagus lettuce |
| CN113197956A (en) * | 2021-04-30 | 2021-08-03 | 浙江尖峰健康科技有限公司 | Processing technology of pinellia ternata |
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| CN102258653A (en) * | 2010-05-24 | 2011-11-30 | 成都中医药大学 | Pinellia ternata and processing method thereof |
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| CN101028134A (en) * | 2006-11-24 | 2007-09-05 | 康明轩 | Method for processing non-sulfur Chinese yam |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110960633A (en) * | 2019-11-12 | 2020-04-07 | 珠海禾间堂本草科技有限公司 | Preparation method of dendrobium officinale dried product |
| CN113197956A (en) * | 2021-04-30 | 2021-08-03 | 浙江尖峰健康科技有限公司 | Processing technology of pinellia ternata |
| CN113100379A (en) * | 2021-05-07 | 2021-07-13 | 江苏康润农业科技发展有限公司 | Processing method of fresh asparagus lettuce |
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