CN107312645B - Active oxygen laundry tablet and preparation method thereof - Google Patents

Active oxygen laundry tablet and preparation method thereof Download PDF

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Publication number
CN107312645B
CN107312645B CN201710474100.1A CN201710474100A CN107312645B CN 107312645 B CN107312645 B CN 107312645B CN 201710474100 A CN201710474100 A CN 201710474100A CN 107312645 B CN107312645 B CN 107312645B
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active oxygen
alcohol
washing
tablet
agent
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CN107312645A (en
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杨兴旺
李晓峰
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Kesh Chemical Industry Shenzhen Co ltd
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Kesh Chemical Industry Shenzhen Co ltd
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047—Detergents in the form of bars or tablets
    • C11D17/0065—Solid detergents containing builders
    • C11D17/0073—Tablets
    • C11D17/0086—Laundry tablets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/1266—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in liquid compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2065—Polyhydric alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/34—Organic compounds containing sulfur
    • C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3753—Polyvinylalcohol; Ethers or esters thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3757—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
    • C11D3/3765—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions in liquid compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/39—Organic or inorganic per-compounds
    • C11D3/3942—Inorganic per-compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C11D1/143—Sulfonic acid esters
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C11D1/146—Sulfuric acid esters
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C11D1/721—End blocked ethers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/90—Betaines

Abstract

A multifunctional active oxygen washing tablet with the functions of removing dirt, killing bacteria and removing odour is prepared from filming agent, non-ionic surfactant, anionic surfactant, zwitterionic surfactant, humectant, filler, saturated alkane, oxygen releasing agent, chelating agent, antiseptic, edible pigment and natural perfume through weighing, preparing pulp and tabletting. The invention adds the oxygen releasing agent as the active oxygen auxiliary agent, improves the detergency of the washing sheet, and adds the functions of sterilization and peculiar smell removal, so that the clothes can be washed more cleanly.

Description

Active oxygen laundry tablet and preparation method thereof
Technical Field
The invention relates to a daily washing product, in particular to a multifunctional active oxygen laundry tablet with functions of decontamination, sterilization and peculiar smell removal and a preparation method thereof.
Background
The laundry piece is an innovative washing product, is different from the appearance form of the traditional washing product, and is characterized by easy carrying and convenient use. At present, washing products for washing clothes mainly comprise three types of washing powder, washing soap and washing liquid.
The washing powder is strong in alkalinity, hands can be seriously injured when the washing powder is washed by hands, clothes become hard after washing, the wearing comfort is influenced, the washing powder needs to be measured when the washing powder is used, and the washing powder is inconvenient to carry when people go out; the pH value of the laundry detergent is close to neutral, and the laundry detergent belongs to a mild washing product, but the dosage is not easy to control when in use, and the laundry detergent is easy to leak to the ground and is inconvenient to transport; the laundry soap is mainly used for hand washing, hard water resistance is low, odor is seriously remained, and bacteria are easy to breed in rainy days.
Recently, a novel laundry product laundry piece appears in the market, can only be used as a common laundry product, and reports of simultaneously realizing decontamination, sterilization and peculiar smell removal on one laundry piece do not exist.
Disclosure of Invention
The invention aims to provide a functional laundry sheet for decontaminating, sterilizing and removing peculiar smell by using active oxygen and a preparation method thereof.
A multifunctional active oxygen laundry tablet with the functions of decontamination, sterilization and peculiar smell removal is characterized by comprising the following raw materials in parts by weight: (in mass percent):
Figure BDA0001325730080000011
Figure BDA0001325730080000021
the film forming agent can be one or more of polyvinyl alcohol, polyvinylpyrrolidone and cellulose.
The nonionic surfactant is preferably one or more of alkyl alcohol polyoxyethylene ether, alkyl alcohol polyoxyethylene polyoxypropylene ether and coconut oil alkanolamide.
The anionic surfactant is preferably one or more of fatty alcohol sulfate, linear alkyl benzene sulfonate, alkenyl sulfonate, fatty alcohol ether sulfate, fatty alcohol ether carboxylate and the like.
The zwitterionic surfactant is preferably one or more of carboxylic acid betaine, alkyl betaine and sulfobetaine.
The humectant is preferably one or more of polyethylene glycol, propylene glycol, glycerol and the like.
The filler can be one or more of silicon dioxide, kaolin, talcum powder, zeolite, starch and the like.
The saturated alkane can be saturated alkane with 8-16 carbon atoms.
The oxygen releasing agent can be one or more of sodium percarbonate, sodium perborate and the like.
The chelating agent can be one or more of polyacrylate, maleic acrylic acid copolymer, ethylene diamine tetraacetic acid salt and the like.
The preservative is isothiazolinone or methyl p-hydroxybenzoate or other high-temperature-resistant preservatives.
The natural perfume is water-soluble. The natural perfume is a high-temperature-resistant faint scent type natural perfume for washing.
The preparation method of the multifunctional active oxygen laundry tablet with the functions of decontamination, sterilization and deodorization comprises the following specific steps:
weighing: weighing the raw and auxiliary materials according to the formula proportion for later use.
Pulping: dissolving a film forming agent in water, heating while stirring for dissolving, then sequentially adding a nonionic surfactant, a zwitterionic surfactant, a humectant, an anionic surfactant, a filler, saturated alkane, an oxygen release agent, a chelating agent, a preservative, an edible pigment, a natural perfume and the balance of water, fully and uniformly stirring every time one raw material is added, and then adding the next raw material.
Tabletting: and drying the prepared material body by a heating drying cylinder, controlling the temperature of the drying cylinder to be 120-200 ℃ and the rotating speed to be 3-15 r/min, and forming the material body into a sheet shape. And then slicing according to the required size. The multifunctional active oxygen laundry tablet with the functions of decontamination, sterilization and peculiar smell removal is obtained.
The film-forming agent polyvinyl alcohol is compounded with humectant glycerol and filler silicon dioxide according to the proportion of the invention when the polymerization degree is 1650-1850 and the molecular weight is about 75000, and a water-soluble film with excellent humectant, ultra-fast water-soluble speed and excellent flexibility can be obtained.
The anionic surfactant provides a laundry sheet forming function and performs an effective cleaning function for various foreign matters in cooperation with the nonionic surfactant and the zwitterionic surfactant. The reasonable use of a plurality of active agents and complexing agents enables the product to form a special active system, in the active system, bacteria are not easy to breed, active oxygen is not easy to decompose, the stability of the product is well improved, and oxygen released by the active oxygen has the effects of sterilization and peculiar smell removal.
The specific implementation mode is as follows:
the functional laundry sheet embodiments of the present invention are as follows:
example 1
Figure BDA0001325730080000031
The preparation method of the laundry tablet comprises the following steps:
1. and weighing the ingredients.
2. Pulping: the preparation method comprises the steps of weighing the components of the formula for later use, adding polyvinyl alcohol, then adding deionized water, heating under stirring to completely dissolve the components, sequentially adding coconut oil alcohol amide, fatty alcohol sulfate, alkyl betaine, polyethylene glycol, starch, white wax oil, sodium percarbonate, polyacrylate, isothiazolinone, edible pigment and natural spice, stirring uniformly after adding one of the raw materials, and finally fully stirring and dispersing.
3. Tabletting: and drying the prepared material body by a heating drying cylinder, controlling the temperature of the drying cylinder to be 150 ℃ and the rotating speed to be 8 r/min, and forming the material body into a sheet shape. And slicing and cutting into pieces to obtain the multifunctional active oxygen washing tablet with the functions of decontamination, sterilization and peculiar smell removal.
4
Figure BDA0001325730080000041
Example 2
Figure BDA0001325730080000042
Figure BDA0001325730080000051
The preparation method of the laundry tablet comprises the following steps:
1. and weighing the ingredients.
2. Pulping: the preparation method comprises the steps of weighing the components of the formula for later use, adding polyvinyl alcohol, then adding deionized water, heating under stirring to completely dissolve the polyvinyl alcohol, sequentially adding alkyl alcohol polyoxyethylene ether, fatty alcohol sulfate, alkyl betaine, polyethylene glycol, starch, white wax oil, sodium percarbonate, polyacrylate, isothiazolinone, edible pigment and natural spice, uniformly stirring after adding one of the raw materials, and finally fully stirring and dispersing.
3. Tabletting: and drying the prepared material body by a heating drying cylinder, controlling the temperature of the drying cylinder to be 135 ℃ and the rotating speed to be 8 r/min, and forming the material body into a sheet shape. And slicing and cutting into pieces to obtain the multifunctional active oxygen washing tablet with the functions of decontamination, sterilization and peculiar smell removal.
Figure BDA0001325730080000052
Figure BDA0001325730080000061
Example 3
Figure BDA0001325730080000062
The preparation method of the laundry tablet comprises the following steps:
1. and weighing the ingredients.
2. Pulping: the preparation method comprises the steps of weighing the components of the formula for later use, adding polyvinyl alcohol and polyvinylpyrrolidone, then adding deionized water, heating under stirring to completely dissolve the components, sequentially adding coconut oil alcohol amide, alkenyl sulfonate, alkyl betaine, polyethylene glycol, starch, kaolin, white wax oil, sodium percarbonate, ethylene diamine tetraacetate, isothiazolinone, edible pigment and natural spice, stirring uniformly after adding one of the raw materials, and finally fully stirring and dispersing.
3. Tabletting: and drying the prepared material body by a heating drying cylinder, controlling the temperature of the drying cylinder to be 120 ℃ and the rotating speed to be 6 r/min, and forming the material body into a sheet shape. And slicing and cutting into pieces to obtain the multifunctional active oxygen washing tablet with the functions of decontamination, sterilization and peculiar smell removal.
Figure BDA0001325730080000071

Claims (3)

1. The application of the active oxygen laundry tablet in removing staphylococcus aureus and escherichia coli is characterized by comprising the following raw materials by mass:
polyvinyl alcohol 8kg
Coconut oil alcohol amide 1kg
Fatty alcohol sulfate 12kg
Alkyl betaine 1kg
Polyethylene glycol 2kg
16kg of starch
White wax oil 0.3kg
Sodium percarbonate 5kg
Polyacrylate 0.5kg
Isothiazolinone 0.2kg
0.1kg of edible pigment
Natural perfume 0.5kg
53.4kg of deionized water.
2. The application of the active oxygen laundry tablet in removing staphylococcus aureus and escherichia coli is characterized by comprising the following raw materials by mass:
6kg of polyvinyl alcohol
Alkyl alcohol polyoxyethylene ether 1kg
15kg of fatty alcohol sulfate
Alkyl betaine 1kg
Glycerol 3kg
Starch 12kg
Kaolin 4kg
White wax oil 0.5kg
Sodium percarbonate 5kg
Polyacrylate 0.5kg
Isothiazolinone 0.2kg
0.1kg of edible pigment
Natural perfume 0.5kg
51.2kg of deionized water.
3. The application of the active oxygen laundry tablet in removing staphylococcus aureus and escherichia coli is characterized by comprising the following raw materials by mass:
6kg of polyvinyl alcohol
Polyvinylpyrrolidone 1.5kg
Coconut oil alcohol amide 1kg
Alkenyl sulfonate 18kg
Alkyl betaine 1kg
Polyethylene glycol 3kg
10kg of starch
Kaolin 4kg
White wax oil 0.3kg
Sodium percarbonate 8kg
Ethylenediamine tetraacetate 0.2kg
Isothiazolinone 0.2kg
0.1kg of edible pigment
Natural perfume 0.5kg
46.2kg of deionized water.
CN201710474100.1A 2017-06-19 2017-06-19 Active oxygen laundry tablet and preparation method thereof Active CN107312645B (en)

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Publication number Priority date Publication date Assignee Title
CN109913323A (en) * 2019-04-08 2019-06-21 戴文浩 Laundry sheet and its processing procedure is concentrated
CN115651781B (en) * 2022-11-25 2023-12-12 广州洁生日化有限公司 Integrated composition washing tablet and preparation method thereof

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JP3126675B2 (en) * 1997-01-23 2001-01-22 花王株式会社 Sheet detergent
DE19806200A1 (en) * 1998-02-16 1999-08-19 Henkel Kgaa Detergent tablets with bleach
CN106635572B (en) * 2016-12-12 2020-09-22 广州立白企业集团有限公司 Detergent composition in tablet form and process for producing the same
CN106833934B (en) * 2017-01-16 2020-04-10 广州立白企业集团有限公司 Enzyme-containing sheet detergent and preparation method thereof

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