CN107275103A - 一种MnCO3/Ni(OH)2/NF多级网状复合电极材料及其制备方法 - Google Patents
一种MnCO3/Ni(OH)2/NF多级网状复合电极材料及其制备方法 Download PDFInfo
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- CN107275103A CN107275103A CN201710436775.7A CN201710436775A CN107275103A CN 107275103 A CN107275103 A CN 107275103A CN 201710436775 A CN201710436775 A CN 201710436775A CN 107275103 A CN107275103 A CN 107275103A
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- Prior art keywords
- foam
- nickel
- mnco
- deionized water
- taken out
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000007772 electrode material Substances 0.000 title claims abstract description 32
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000011656 manganese carbonate Substances 0.000 title claims abstract description 11
- 229910000016 manganese(II) carbonate Inorganic materials 0.000 title claims abstract description 11
- 229910018661 Ni(OH) Inorganic materials 0.000 title description 2
- 235000006748 manganese carbonate Nutrition 0.000 title description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 147
- 239000006260 foam Substances 0.000 claims abstract description 67
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 66
- 239000002131 composite material Substances 0.000 claims abstract description 24
- 239000008367 deionised water Substances 0.000 claims abstract description 23
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 23
- 229910021508 nickel(II) hydroxide Inorganic materials 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000004202 carbamide Substances 0.000 claims abstract description 22
- 101100513612 Microdochium nivale MnCO gene Proteins 0.000 claims abstract description 18
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims abstract description 16
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000007788 liquid Substances 0.000 claims abstract description 15
- 238000001291 vacuum drying Methods 0.000 claims abstract description 14
- 238000011065 in-situ storage Methods 0.000 claims abstract description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000005406 washing Methods 0.000 claims abstract description 8
- 239000000463 material Substances 0.000 claims description 16
- 238000010276 construction Methods 0.000 claims description 7
- 239000011521 glass Substances 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 abstract description 2
- 230000014759 maintenance of location Effects 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 10
- 238000000634 powder X-ray diffraction Methods 0.000 description 4
- 239000003990 capacitor Substances 0.000 description 3
- 230000005611 electricity Effects 0.000 description 3
- BFDHFSHZJLFAMC-UHFFFAOYSA-L nickel(ii) hydroxide Chemical compound [OH-].[OH-].[Ni+2] BFDHFSHZJLFAMC-UHFFFAOYSA-L 0.000 description 3
- QHASIAZYSXZCGO-UHFFFAOYSA-N selanylidenenickel Chemical compound [Se]=[Ni] QHASIAZYSXZCGO-UHFFFAOYSA-N 0.000 description 3
- 239000003792 electrolyte Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 2
- 238000013112 stability test Methods 0.000 description 2
- 235000009262 Dracaena angustifolia Nutrition 0.000 description 1
- 240000007833 Dracaena angustifolia Species 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- DHPNXAFERMWNAB-UHFFFAOYSA-L [Ni](O)O.[O-2].[O-2].[Mn+4] Chemical compound [Ni](O)O.[O-2].[O-2].[Mn+4] DHPNXAFERMWNAB-UHFFFAOYSA-L 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000010405 anode material Substances 0.000 description 1
- 230000006399 behavior Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000005253 cladding Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000012983 electrochemical energy storage Methods 0.000 description 1
- 238000003487 electrochemical reaction Methods 0.000 description 1
- 230000005518 electrochemistry Effects 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002070 nanowire Substances 0.000 description 1
- 230000033116 oxidation-reduction process Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 238000007039 two-step reaction Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/26—Electrodes characterised by their structure, e.g. multi-layered, porosity or surface features
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/84—Processes for the manufacture of hybrid or EDL capacitors, or components thereof
- H01G11/86—Processes for the manufacture of hybrid or EDL capacitors, or components thereof specially adapted for electrodes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/13—Energy storage using capacitors
Abstract
Description
Claims (1)
Priority Applications (1)
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CN201710436775.7A CN107275103B (zh) | 2017-06-12 | 2017-06-12 | 一种MnCO3/Ni(OH)2/泡沫镍多级网状复合电极材料的制备方法 |
Applications Claiming Priority (1)
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CN201710436775.7A CN107275103B (zh) | 2017-06-12 | 2017-06-12 | 一种MnCO3/Ni(OH)2/泡沫镍多级网状复合电极材料的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN107275103A true CN107275103A (zh) | 2017-10-20 |
CN107275103B CN107275103B (zh) | 2018-09-04 |
Family
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Family Applications (1)
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CN201710436775.7A Active CN107275103B (zh) | 2017-06-12 | 2017-06-12 | 一种MnCO3/Ni(OH)2/泡沫镍多级网状复合电极材料的制备方法 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108806996A (zh) * | 2018-06-08 | 2018-11-13 | 上海应用技术大学 | 一种以泡沫镍为基体的NixMn1-xCo2O4纳米花的制备方法 |
CN111841567A (zh) * | 2020-08-04 | 2020-10-30 | 南通大学 | 一种具有图灵结构的镍锰羟基氧化物薄膜的制备方法及应用 |
CN113394030A (zh) * | 2021-06-26 | 2021-09-14 | 南昌师范学院 | 一种镍基电极材料及其制备方法和应用 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2003034538A (ja) * | 2001-05-17 | 2003-02-07 | Mitsubishi Chemicals Corp | リチウムニッケルマンガン複合酸化物の製造方法 |
CN105304352A (zh) * | 2015-10-12 | 2016-02-03 | 哈尔滨工业大学深圳研究生院 | 泡沫镍自反应制备二氧化锰/氢氧化镍复合纳米片的方法及其超级电容器应用 |
CN105355468A (zh) * | 2015-11-27 | 2016-02-24 | 渤海大学 | 一种三氧化二锰多孔微米片/泡沫镍复合电极材料的制备方法 |
CN106158394A (zh) * | 2016-06-29 | 2016-11-23 | 西北师范大学 | 一种泡沫镍基超级电容器电极材料的制备方法 |
-
2017
- 2017-06-12 CN CN201710436775.7A patent/CN107275103B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2003034538A (ja) * | 2001-05-17 | 2003-02-07 | Mitsubishi Chemicals Corp | リチウムニッケルマンガン複合酸化物の製造方法 |
CN105304352A (zh) * | 2015-10-12 | 2016-02-03 | 哈尔滨工业大学深圳研究生院 | 泡沫镍自反应制备二氧化锰/氢氧化镍复合纳米片的方法及其超级电容器应用 |
CN105355468A (zh) * | 2015-11-27 | 2016-02-24 | 渤海大学 | 一种三氧化二锰多孔微米片/泡沫镍复合电极材料的制备方法 |
CN106158394A (zh) * | 2016-06-29 | 2016-11-23 | 西北师范大学 | 一种泡沫镍基超级电容器电极材料的制备方法 |
Non-Patent Citations (3)
Title |
---|
FANGPING WANG ETC: "Microwave preparation of 3D flower-like MnO2/Ni(OH)2/nickel foam composite for high-performance supercapacitors", 《JOURNAL OF ALLOYS AND COMPOUNDS》 * |
WEI SONG ETC: "Enhanced electrochemical performance of nano-MnO2 modified by Ni(OH)2 as electrode material for supercapacitor", 《J SOLID STATE ELECTROCHEM》 * |
XIAO LONG GUO ETC: "Nickel-Manganese Layered Double Hydroxide Nanosheets Supported on Nickel Foam for High-performance Supercapacitor Electrode Materials", 《ELECTROCHIMICA ACTA》 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108806996A (zh) * | 2018-06-08 | 2018-11-13 | 上海应用技术大学 | 一种以泡沫镍为基体的NixMn1-xCo2O4纳米花的制备方法 |
CN111841567A (zh) * | 2020-08-04 | 2020-10-30 | 南通大学 | 一种具有图灵结构的镍锰羟基氧化物薄膜的制备方法及应用 |
CN113394030A (zh) * | 2021-06-26 | 2021-09-14 | 南昌师范学院 | 一种镍基电极材料及其制备方法和应用 |
CN113394030B (zh) * | 2021-06-26 | 2022-09-09 | 南昌师范学院 | 一种镍基电极材料及其制备方法和应用 |
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Address after: 266000 Shandong Province, Qingdao city Laoshan District Songling Road No. 99 Patentee after: QINGDAO University OF SCIENCE AND TECHNOLOGY Address before: 266000 Shandong province Qingdao City, Zhengzhou Road No. 53, Qingdao University of Science & Technology Patentee before: QINGDAO University OF SCIENCE AND TECHNOLOGY |
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Effective date of registration: 20221108 Address after: No. 19, Gangcheng Road, Dongying Port Economic Development Zone, Dongying City, Shandong Province 257237 Patentee after: Dongying Ruigang Pipeline Engineering Co.,Ltd. Address before: 266000 Songling Road, Laoshan District, Qingdao, Shandong Province, No. 99 Patentee before: QINGDAO University OF SCIENCE AND TECHNOLOGY |
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